CN113041186A - Whitening and anti-wrinkle hemerocallis fulva tea extract and preparation method thereof - Google Patents
Whitening and anti-wrinkle hemerocallis fulva tea extract and preparation method thereof Download PDFInfo
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- CN113041186A CN113041186A CN202110290113.XA CN202110290113A CN113041186A CN 113041186 A CN113041186 A CN 113041186A CN 202110290113 A CN202110290113 A CN 202110290113A CN 113041186 A CN113041186 A CN 113041186A
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- day lily
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention discloses a preparation method of a golden day lily tea extract for whitening skin and resisting wrinkles, which comprises the following steps: s1: picking fresh leaves of the hemerocallis fulva tea trees as raw materials, ventilating and air-drying the fresh leaves indoors until the water content of the leaves is 35-40%, crushing the leaves by using a crusher, and selecting 95-100 parts by weight of components for later use; s2: selecting and cleaning mushroom, ventilating and air-drying the mushroom indoors until the water content is 40-45%, crushing the mushroom by using a crusher, and selecting 25-30 parts by weight of components for later use; s3: adding 95-100 parts by weight of S1 crushed golden day lily tea leaves and 25-30 parts by weight of crushed mushroom obtained from S2 into a fermentation tank, uniformly mixing and shaking, sealing and fermenting, wherein the fermentation temperature is controlled to be 25-30 ℃, the relative humidity of the environment is 55-60%, and the fermentation time is 42-48 h; s4: and (3) adding 200-210 parts by weight of sterile water into S3, extracting the fermented product by adopting a flash extraction method, and then filtering and evaporating to obtain the hemerocallis fulva tea extract.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a Jinxuan tea extract for whitening skin and resisting wrinkles and a preparation method thereof.
Background
Skin aging is a very complex process and is influenced by a number of factors, of which melanin production and free radical induced degeneration of the elastic fibers of the skin are two major factors. Tyrosine is an essential amino acid for the human body, and the content of tyrosine is controlled by the human body. When an external environment such as ultraviolet light is stimulated, the pigmentation of melanin is intensified, and thus the pigmentation of melanin is controlled by controlling the number of melanocytes, the activity of tyrosinase, and the content of oxygen radicals. The external environment influence can also cause the reduction of the anti-free radical capability of the human body, the free radical is an important factor causing skin aging, the air pollution, the pressure, the medicine and the like can cause the body to generate the free radical, and the ultraviolet ray is a main induction factor of the free radical of the skin. Most free radicals are very reactive and have a high degree of chemical activity. Under normal conditions, free radicals in the human body are in a dynamic equilibrium with constant production and elimination. However, the free radicals are excessively generated or slowly eliminated, and can cause various damages to the body by attacking vital macromolecular substances and various cells, accelerate the aging process of the body, and show gradual aging changes, such as senile pigmentation, skin wrinkling and the like. It is very important to enhance the oxidation resistance.
At present, a large number of whitening anti-wrinkle products appear in the market, and the anti-oxidation ingredients contained in the whitening anti-wrinkle products can slow down skin aging. The antioxidant component is extracted from other substances, but the existing extraction method has expensive raw materials and low extraction rate, so that the cost of the skin care product is high.
Disclosure of Invention
The invention aims to provide a preparation method of a golden day lily tea extract for whitening and resisting wrinkles, which adopts mushroom and golden day lily tea with lower cost as raw materials to be fermented together, so that the content of an antioxidant substance in the golden day lily tea is increased, and the component can be used as a whitening and anti-wrinkle component in a skin care product, so as to solve the technical problems in the background technology.
The preparation method of the hemerocallis fulva tea extract for whitening skin and resisting wrinkles is characterized by comprising the following steps of:
s1: picking fresh leaves of the hemerocallis fulva tea trees as raw materials, ventilating and air-drying the fresh leaves indoors until the water content of the leaves is 35-40%, crushing the leaves by using a crusher, and selecting 95-100 parts by weight of components for later use;
s2: selecting and cleaning mushroom, ventilating and air-drying the mushroom indoors until the water content is 40-45%, crushing the mushroom by using a crusher, and selecting 25-30 parts by weight of components for later use;
s3: adding 95-100 parts by weight of S1 crushed golden day lily tea leaves and 25-30 parts by weight of crushed mushroom obtained from S2 into a fermentation tank, uniformly mixing and shaking, sealing and fermenting, wherein the fermentation temperature is controlled to be 25-30 ℃, the relative humidity of the environment is 55-60%, and the fermentation time is 42-48 h;
s4: and (3) adding 200-210 parts by weight of sterile water into S3, extracting the fermented product by adopting a flash extraction method, and then filtering and evaporating to obtain the hemerocallis fulva tea extract.
In a preferred embodiment, the pulverizing process of the golden day lily tea leaves in S1 is as follows: putting the golden day lily tea leaves into a grinder, grinding for 1-2 min, and enabling the grain diameter to be 2-4 mm after grinding; the crushing process of the mushroom in the S2 is as follows: and (3) putting the mushroom into a grinder, grinding for 2-3 min, wherein the grain diameter is 1-2 mm after grinding.
In a preferred embodiment, the mushroom is one of hericium erinaceus, flammulina velutipes and shiitake mushrooms.
In a preferred embodiment, the flash extraction conditions in S4 are: extracting at normal temperature for 40-50 s, wherein the extraction voltage is 110-120V.
In a preferred embodiment, S4 is filtered by ceramic membrane and evaporated by rotary evaporator.
In a preferred embodiment, the preparation method of the hemerocallis fulva tea extract comprises the following steps of: 9-11% of flavonols, 5-8% of vitamin C and 3-4% of vitamin E.
The technical scheme of the invention has the beneficial effects that:
1. the preparation method comprises the steps of mixing mushroom and golden day lily tea, fermenting and converting substances in the golden day lily tea by using fungi carried by mushrooms, and extracting the fermented substance to obtain a composition with oxidation resistance, wherein the composition has the functions of whitening and resisting wrinkles when used in cosmetics; meanwhile, the extraction cost is low, the operation steps are simple, and the large-scale production is facilitated.
2. Air-dry processing and smashing are done to bright leaf of golden day lily tea and fungus mushroom, avoid the interior more influence that causes the fermentation of water content of fermenter through air-dry processing, and shredding guarantees that bright leaf of golden day lily tea and fungus mushroom fully contact and mix, promotes fermentation rate and fermentation effect.
3. The flavonols, vitamins and vitamins contained in the hemerocallis fulva tea extract have oxidation resistance, and the content of the extract is greatly increased compared with the content of the extract without the mushroom.
Detailed Description
The present invention will be described in further detail with reference to specific embodiments. The embodiments of the present invention have been presented for purposes of illustration and description, and are not intended to be exhaustive or limited to the invention in the form disclosed. Many modifications and variations will be apparent to those of ordinary skill in the art. The embodiment was chosen and described in order to best explain the principles of the invention and the practical application, and to enable others of ordinary skill in the art to understand the invention for various embodiments with various modifications as are suited to the particular use contemplated.
Example 1
The preparation method of the hemerocallis fulva tea extract for whitening skin and resisting wrinkles is characterized by comprising the following steps of:
s1: picking fresh leaves of the hemerocallis fulva tea trees as raw materials, ventilating and air-drying the fresh leaves indoors until the water content of the leaves is 35-40%, crushing the leaves by using a crusher, and selecting 95 parts by weight of components for later use;
s2: selecting hericium erinaceus, cleaning, ventilating and air-drying indoors until the water content is 40-45%, crushing by using a crusher, and selecting 25 parts by weight of components for later use;
s3: adding 95 parts of crushed golden day lily tea leaves S1 and 25 parts of crushed mushroom obtained from S2 into a fermentation tank, mixing, shaking uniformly, sealing and fermenting, wherein the fermentation temperature is controlled to be 25-30 ℃, the environmental relative humidity is 55-60%, and the fermentation time is 42-48 h;
s4: and (3) adding 200-210 parts by weight of sterile water into S3, extracting the fermented product by adopting a flash extraction method, and then filtering and evaporating to obtain the hemerocallis fulva tea extract.
The crushing process of the golden day lily tea leaves in the S1 is as follows: putting the golden day lily tea leaves into a grinder, grinding for 1-2 min, and enabling the grain diameter to be 2-4 mm after grinding; the crushing process of the mushroom in the S2 is as follows: and (3) putting the mushroom into a grinder, grinding for 2-3 min, wherein the grain diameter is 1-2 mm after grinding.
The flash extraction conditions in S4 are as follows: extracting at normal temperature for 40-50 s, wherein the extraction voltage is 110-120V. And S4, filtering by adopting a ceramic membrane, and evaporating by adopting a rotary evaporator.
The preparation method of the golden day lily tea extract comprises the following antioxidant components: 9% of flavonol, 5% of vitamin C and 3% of vitamin E.
Example 2
The preparation method of the hemerocallis fulva tea extract for whitening skin and resisting wrinkles is characterized by comprising the following steps of:
s1: picking fresh leaves of the hemerocallis fulva tea trees as raw materials, ventilating and air-drying the fresh leaves indoors until the water content of the leaves is 35-40%, crushing the leaves by using a crusher, and selecting 95 parts by weight of components for later use;
s2: selecting needle mushrooms, cleaning, ventilating and air-drying indoors until the water content is 40-45%, crushing by using a crusher, and selecting 25 parts by weight of components for later use;
s3: adding 95 parts of crushed golden day lily tea leaves S1 and 25 parts of crushed mushroom obtained from S2 into a fermentation tank, mixing, shaking uniformly, sealing and fermenting, wherein the fermentation temperature is controlled to be 25-30 ℃, the environmental relative humidity is 55-60%, and the fermentation time is 42-48 h;
s4: and (3) adding 200-210 parts by weight of sterile water into S3, extracting the fermented product by adopting a flash extraction method, and then filtering and evaporating to obtain the hemerocallis fulva tea extract.
The crushing process of the golden day lily tea leaves in the S1 is as follows: putting the golden day lily tea leaves into a grinder, grinding for 1-2 min, and enabling the grain diameter to be 2-4 mm after grinding; the crushing process of the mushroom in the S2 is as follows: and (3) putting the mushroom into a grinder, grinding for 2-3 min, wherein the grain diameter is 1-2 mm after grinding.
The flash extraction conditions in S4 are as follows: extracting at normal temperature for 40-50 s, wherein the extraction voltage is 110-120V. And S4, filtering by adopting a ceramic membrane, and evaporating by adopting a rotary evaporator.
The preparation method of the golden day lily tea extract comprises the following antioxidant components: 9.5 percent of flavonol, 7.2 percent of vitamin C and 3.42 percent of vitamin E.
Example 3
The preparation method of the hemerocallis fulva tea extract for whitening skin and resisting wrinkles is characterized by comprising the following steps of:
s1: picking fresh leaves of the hemerocallis fulva tea trees as raw materials, ventilating and air-drying the fresh leaves indoors until the water content of the leaves is 35-40%, crushing the leaves by using a crusher, and selecting 100 parts by weight of components for later use;
s2: selecting hericium erinaceus, cleaning, ventilating and air-drying indoors until the water content is 40-45%, crushing by using a crusher, and selecting 30 parts by weight of components for later use;
s3: adding 100 parts of crushed golden day lily tea leaves S1 and 30 parts of crushed mushroom obtained from S2 into a fermentation tank, mixing, shaking uniformly, sealing and fermenting, wherein the fermentation temperature is controlled to be 25-30 ℃, the environmental relative humidity is 55-60%, and the fermentation time is 42-48 h;
s4: and (3) adding 200-210 parts by weight of sterile water into S3, extracting the fermented product by adopting a flash extraction method, and then filtering and evaporating to obtain the hemerocallis fulva tea extract.
The crushing process of the golden day lily tea leaves in the S1 is as follows: putting the golden day lily tea leaves into a grinder, grinding for 1-2 min, and enabling the grain diameter to be 2-4 mm after grinding; the crushing process of the mushroom in the S2 is as follows: and (3) putting the mushroom into a grinder, grinding for 2-3 min, wherein the grain diameter is 1-2 mm after grinding.
The flash extraction conditions in S4 are as follows: extracting at normal temperature for 40-50 s, wherein the extraction voltage is 110-120V. And S4, filtering by adopting a ceramic membrane, and evaporating by adopting a rotary evaporator.
The preparation method of the golden day lily tea extract comprises the following antioxidant components: 11% of flavonol, 8ppm of vitamin C and 4% of vitamin E.
Comparative example
Directly fermenting the golden day lily tea without adding mushrooms, comprising the following steps: b1: picking fresh leaves of the hemerocallis fulva tea trees as raw materials, ventilating and air-drying the fresh leaves indoors until the water content of the leaves is 35-40%, crushing the leaves by using a crusher, and selecting 95 parts by weight of components for later use;
b2: adding 95 parts of crushed hemerocallis fulva tea leaves of B1 weight components into a fermentation tank, sealing and fermenting, wherein the fermentation temperature is controlled to be 25-30 ℃, the relative humidity of the environment is 55-60%, and the fermentation time is 42-48 h;
b3: adding 200-210 parts by weight of sterile water into B2, extracting the fermentation product by adopting a flash extraction method, and then filtering and evaporating to obtain the hemerocallis fulva tea extract.
B1 the crushing process of the golden day lily tea is as follows: and (3) putting the golden day lily tea leaves into a grinder, and grinding for 1-2 min to obtain particles with the particle size of 2-4 mm.
The flash extraction conditions in B3 are as follows: extracting at normal temperature for 40-50 s, wherein the extraction voltage is 110-120V. B3 is filtered by ceramic membrane and evaporated by rotary evaporator.
The hemerocallis fulva tea extract prepared by the method comprises the following components in content: 2.1 percent of flavonol, 1.2ppm of vitamin C and 0.6 percent of vitamin E.
By providing examples 1, 2, 3 and comparative examples, the difference between examples 1, 2, 3 and comparative examples is that no mushroom substance is added in the comparative examples, and it can be seen from the component content of the golden day lily tea extract that the contents of flavonols, vitamin C and vitamin E having oxidation resistance are significantly reduced compared to the examples, and thus it can be demonstrated that the mixed fermentation of golden day lily tea and mushrooms contributes to the generation of the antioxidant substance in golden day lily tea.
The preparation method comprises the steps of mixing mushroom and golden day lily tea, fermenting and converting substances in the golden day lily tea by using fungi carried by mushrooms, and extracting the fermented substance to obtain a composition with oxidation resistance, wherein the composition has the functions of whitening and resisting wrinkles when used in cosmetics; meanwhile, the extraction cost is low, the operation steps are simple, and the large-scale production is facilitated.
It is to be understood that the described embodiments are merely a few embodiments of the invention, and not all embodiments. All other embodiments, which can be derived by one of ordinary skill in the art and related arts based on the embodiments of the present invention without any creative effort, shall fall within the protection scope of the present invention. Structures, devices, and methods of operation not specifically described or illustrated herein are generally practiced in the art without specific recitation or limitation.
Claims (6)
1. The preparation method of the golden day lily tea extract for whitening skin and resisting wrinkles is characterized by comprising the following steps of:
s1: picking fresh leaves of the hemerocallis fulva tea trees as raw materials, ventilating and air-drying the fresh leaves indoors until the water content of the leaves is 35-40%, crushing the leaves by using a crusher, and selecting 95-100 parts by weight of components for later use;
s2: selecting and cleaning mushroom, ventilating and air-drying the mushroom indoors until the water content is 40-45%, crushing the mushroom by using a crusher, and selecting 25-30 parts by weight of components for later use;
s3: adding 95-100 parts by weight of S1 crushed golden day lily tea leaves and 25-30 parts by weight of crushed mushroom obtained from S2 into a fermentation tank, uniformly mixing and shaking, sealing and fermenting, wherein the fermentation temperature is controlled to be 25-30 ℃, the relative humidity of the environment is 55-60%, and the fermentation time is 42-48 h;
s4: and (3) adding 200-210 parts by weight of sterile water into S3, extracting the fermented product by adopting a flash extraction method, and then filtering and evaporating to obtain the hemerocallis fulva tea extract.
2. The method for preparing the golden day lily tea extract for whitening skin and resisting wrinkles according to claim 1, wherein the grinding process of the golden day lily tea leaves in S1 is as follows: putting the golden day lily tea leaves into a grinder, grinding for 1-2 min, and enabling the grain diameter to be 2-4 mm after grinding; the crushing process of the mushroom in the S2 is as follows: and (3) putting the mushroom into a grinder, grinding for 2-3 min, wherein the grain diameter is 1-2 mm after grinding.
3. The method for preparing the golden day lily tea extract for whitening skin and resisting wrinkles as claimed in claim 1, wherein the mushroom is one of hericium erinaceus, flammulina velutipes and lentinus edodes.
4. The method for preparing the golden day lily tea extract for whitening skin and resisting wrinkles according to claim 1, wherein flash extraction conditions in the step S4 are as follows: extracting at normal temperature for 40-50 s, wherein the extraction voltage is 110-120V.
5. The method for preparing the golden day lily tea extract for whitening skin and resisting wrinkles according to claim 1, wherein the step of S4 is performed by filtering with a ceramic membrane and evaporating with a rotary evaporator.
6. The method for producing a golden day lily tea extract according to any one of claims 1 to 6, wherein the antioxidant component of the golden day lily tea extract comprises the following components: 9-11% of flavonols, 5-8% of vitamin C and 3-4% of vitamin E.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202110290113.XA CN113041186A (en) | 2021-03-18 | 2021-03-18 | Whitening and anti-wrinkle hemerocallis fulva tea extract and preparation method thereof |
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| CN202110290113.XA CN113041186A (en) | 2021-03-18 | 2021-03-18 | Whitening and anti-wrinkle hemerocallis fulva tea extract and preparation method thereof |
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| CN102488037A (en) * | 2011-12-23 | 2012-06-13 | 王乐观 | Yeast and method for fermenting Pu'er tea by utilizing yeast |
| US20160081363A1 (en) * | 2013-04-16 | 2016-03-24 | Nongfu Spring Co., Ltd. | Tea Beverage and Preparation Method Therefor |
| CN107019070A (en) * | 2017-04-01 | 2017-08-08 | 山东众达医药科技有限公司 | A kind of tea for reducing dermal melanin and preparation method thereof |
| CN109549899A (en) * | 2017-09-25 | 2019-04-02 | 陆文奎 | A kind of facial cleanser suitable for spring and autumn |
| CN110973587A (en) * | 2019-12-25 | 2020-04-10 | 成都大学 | Mushroom red yeast rice sauce functional food prepared by co-fermentation and preparation method thereof |
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2021
- 2021-03-18 CN CN202110290113.XA patent/CN113041186A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2008064573A1 (en) * | 2006-11-29 | 2008-06-05 | Sanman Li | A fermented tea and method of manufacturing therefor |
| CN101028021A (en) * | 2007-04-06 | 2007-09-05 | 任炼 | Raw theoflavin instant tea and its production |
| CN102488037A (en) * | 2011-12-23 | 2012-06-13 | 王乐观 | Yeast and method for fermenting Pu'er tea by utilizing yeast |
| US20160081363A1 (en) * | 2013-04-16 | 2016-03-24 | Nongfu Spring Co., Ltd. | Tea Beverage and Preparation Method Therefor |
| CN107019070A (en) * | 2017-04-01 | 2017-08-08 | 山东众达医药科技有限公司 | A kind of tea for reducing dermal melanin and preparation method thereof |
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| CN110973587A (en) * | 2019-12-25 | 2020-04-10 | 成都大学 | Mushroom red yeast rice sauce functional food prepared by co-fermentation and preparation method thereof |
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Application publication date: 20210629 |