CN112972313A - Preparation method of modified humus extract and shampoo composition containing modified humus extract - Google Patents
Preparation method of modified humus extract and shampoo composition containing modified humus extract Download PDFInfo
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- CN112972313A CN112972313A CN202110248857.5A CN202110248857A CN112972313A CN 112972313 A CN112972313 A CN 112972313A CN 202110248857 A CN202110248857 A CN 202110248857A CN 112972313 A CN112972313 A CN 112972313A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/14—Drugs for dermatological disorders for baldness or alopecia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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Abstract
The invention relates to the field of daily chemicals, in particular to a preparation method of a modified humus extract and a shampoo composition containing the extract. The preparation method of the modified humus extract comprises weighing humus extract, ohm flower fragrance essence and pure water, mixing, homogenizing, standing, mixing with shampoo base material, homogenizing, and packaging to obtain the shampoo composition containing the modified humus extract. The invention provides a novel application approach of the humus extract, and the modified humus extract can promote blood circulation, is beneficial to preventing alopecia, is beneficial to hair growth and the like.
Description
Technical Field
The invention relates to the field of daily chemicals, in particular to a preparation method of a modified humus extract and a shampoo composition containing the extract.
Background
The humus is a high molecular compound without a specific structure, contains various active functional groups, has very wide application, and comprises the functions of promoting crop stress resistance, improving soil environment and the like, and is even used for food (such as beverage and the like), but the application for hair care is not found, and the application for hair care (preventing alopecia, promoting hair growth and the like) is worthy of intensive study.
Disclosure of Invention
One of the objects of the present invention is: provides a modified humus extract suitable for hair care and a preparation method thereof.
In order to realize the purpose, the technical scheme adopted by the invention is as follows:
a preparation method of a modified humus extract comprises the following steps:
weighing humus extract, ohmic flower fragrance essence and pure water for later use;
adding the humus extract and pure water into a homogenizer, and homogenizing to form a humus extract solution;
thirdly, adding the ohm flower fragrance essence into the humus extract solution, and homogenizing;
fourthly, keeping the sealing state and standing to obtain the modified humus extract.
Preferably, the weight ratio of the raw materials in the step (i) is humus extract: ohm flower fragrance essence: pure water (20-55): (10-27.5): (17.5-70).
Preferably, the mass ratio of the humus extract to the ohm flower fragrance in the step (i) is 2: 1.
preferably, the temperature in the homogenizing step II is 35-55 ℃, and the homogenizing time is 1-3 h.
Preferably, the temperature during homogenization in the third step is 50-65 ℃, and the homogenization time is 1-3 h.
Preferably, the standing time in the step (iv) is 0.5-1 h.
The modified humus extract is prepared by the method.
The second purpose of the invention is that: provides a shampoo composition using the modified humus extract.
In order to realize the purpose, the technical scheme adopted by the invention is as follows:
a shampoo composition containing modified humus extract is prepared according to the following weight ratio: 5-15% of modified humus extract and 85-95% of shampoo base stock, wherein the sum of the modified humus extract and the shampoo base stock is 100%.
The invention has the beneficial effects that:
1. in the homogenizing process of the ohm flower fragrance essence, the ohm flower fragrance essence is combined with humus to excite and activate various complex active functional groups of the humus, and the prepared modified humus extract can promote blood circulation, is beneficial to preventing alopecia and is beneficial to hair growth due to modification of the essence.
2. The prepared shampoo composition containing the modified humus extract has obvious effect, and focuses on preventing alopecia and promoting hair growth.
3. Develops a brand new application way of the humus extract and develops a brand new solution for preventing alopecia and promoting hair growth.
Detailed Description
The invention will be further illustrated by reference to the following examples, wherein the various raw materials are commercially available or prepared according to the prior art, the humus extract is available and reliable, and the ohm flower fragrance is a professionally formulated fragrance.
Example 1
1. Preparation of modified humus extract
Weighing 20g of humus extract, 10g of ohm flower fragrance essence and 70g of pure water for later use;
② adding the humus extract and pure water into a homogenizer, homogenizing at 35 ℃ for 3 h;
thirdly, adding the ohm flower fragrance essence into the humus extract solution, and homogenizing at 65 ℃ for 1 h;
fourthly, keeping the sealing state, and standing for 1 hour to obtain the modified humus extract.
2. Preparation method of shampoo composition containing modified humus extract
Weighing the following components in proportion (in 100 g): 5g of modified humus extract and 95g of shampoo base stock.
Secondly, according to the production process of the common shampoo, the modified humus extract and the shampoo base material are homogenized to be uniform and then filled into a bottle, and the shampoo composition containing the modified humus extract is obtained.
Example 2
1. Preparation of modified humus extract
Weighing 30g of humus extract, 15g of ohm flower fragrance essence and 55g of pure water for later use;
② adding the humus extract and pure water into a homogenizer, homogenizing at 40 ℃ for 2 h;
thirdly, adding the ohm flower fragrance essence into the humus extract solution, and homogenizing at the temperature of 60 ℃ for 2 hours;
fourthly, keeping the sealing state, and standing for 0.5h to obtain the modified humus extract.
2. Preparation method of shampoo composition containing modified humus extract
Weighing the following components in proportion (in 100 g): 10g of modified humus extract and 90g of shampoo base stock.
Secondly, according to the production process of the common shampoo, the modified humus extract and the shampoo base material are homogenized to be uniform and then filled into a bottle, and the shampoo composition containing the modified humus extract is obtained.
Example 3
1. Preparation of modified humus extract
Weighing 40g of humus extract, 20g of ohm flower fragrance essence and 40g of pure water for later use;
② adding the humus extract and pure water into a homogenizer, homogenizing at 45 ℃ for 1 h;
thirdly, adding the ohm flower fragrance essence into the humus extract solution, and homogenizing at the temperature of 55 ℃ for 1 h;
fourthly, keeping the sealing state, and standing for 1 hour to obtain the modified humus extract.
2. Preparation method of shampoo composition containing modified humus extract
Weighing the following components in proportion (in 100 g): 15g of modified humus extract and 85g of shampoo base stock.
Secondly, according to the production process of the common shampoo, the modified humus extract and the shampoo base material are homogenized to be uniform and then filled into a bottle, and the shampoo composition containing the modified humus extract is obtained.
Example 4
1. Preparation of modified humus extract
45g of humus extract, 22.5g of ohm flower fragrance essence and 32.5g of pure water are weighed for later use;
② adding the humus extract and pure water into a homogenizer, homogenizing at 50 ℃ for 2 h;
thirdly, adding the ohm flower fragrance essence into the humus extract solution, and homogenizing at the temperature of 50 ℃ for 2 hours;
fourthly, keeping the sealing state, and standing for 0.5h to obtain the modified humus extract.
2. Preparation method of shampoo composition containing modified humus extract
Weighing the following components in proportion (in 100 g): 10g of modified humus extract and 90g of shampoo base stock.
Secondly, according to the production process of the common shampoo, the modified humus extract and the shampoo base material are homogenized to be uniform and then filled into a bottle, and the shampoo composition containing the modified humus extract is obtained.
Example 5
1. Preparation of modified humus extract
Weighing 50g of humus extract, 25g of ohm flower fragrance essence and 25g of pure water for later use;
② adding the humus extract and pure water into a homogenizer, homogenizing at 55 ℃ for 3 h;
thirdly, adding the ohm flower fragrance essence into the humus extract solution, and homogenizing at the temperature of 55 ℃ for 3 hours;
fourthly, keeping the sealing state, and standing for 1 hour to obtain the modified humus extract.
2. Preparation method of shampoo composition containing modified humus extract
Weighing the following components in proportion (in 100 g): 5g of modified humus extract and 95g of shampoo base stock.
Secondly, according to the production process of the common shampoo, the modified humus extract and the shampoo base material are homogenized to be uniform and then filled into a bottle, and the shampoo composition containing the modified humus extract is obtained.
Example 6
1. Preparation of modified humus extract
Weighing 55g of humus extract, 27.5g of ohm flower fragrance essence and 17.5g of pure water for later use;
② adding the humus extract and pure water into a homogenizer, homogenizing at 55 ℃ for 1 h;
thirdly, adding the ohm flower fragrance essence into the humus extract solution, and homogenizing at 65 ℃ for 1 h;
fourthly, keeping the sealing state, and standing for 0.5h to obtain the modified humus extract.
2. Preparation method of shampoo composition containing modified humus extract
Weighing the following components in proportion (in 100 g): 15g of modified humus extract and 85g of shampoo base stock.
Secondly, according to the production process of the common shampoo, the modified humus extract and the shampoo base material are homogenized to be uniform and then filled into a bottle, and the shampoo composition containing the modified humus extract is obtained.
The ohmic flower fragrance essence in the embodiments 1-6 comprises the following components in parts by weight (1-9): (44-56.6) mixing the extract B with the essence C;
the extract B is prepared from (1-6) by weight: (11-16): (2-9): (11-16): (1-9): (1-9): (21-26) extracting fructus crataegi, Lyme, fig, dream halo rose flower, soapberry peel, water and dipropylene glycol;
the weight ratio of the essence base C is (2.3-2.8): (2-2.6): (13-18): (11-16): (4.6-5.1): (5.4-5.9): (5.7-6.2) benzyl salicylate, lignum Santali albi, galaxolide, ambergris, lilial, methyl dihydrojasmonate, and limonene.
The shampoo base material in the embodiments 1-6 comprises, by weight, 11-16% of sodium laureth sulfate, 3-8% of cocamidopropyl betaine, 1-6% of decyl glucoside, 0.1-0.6% of dipotassium glycyrrhizinate, 0.1-1% of PPG-3 octyl ether, 0.1-1.5% of piroctone olamine, 0.1-1.1% of cetyl alcohol, 0.1-0.6% of guar hydroxypropyltrimonium chloride, 0.1-0.3% of disodium EDTA, 0.01-3.9% of silicone emulsion, and purified water added to 100%.
Comparative example 1
The only difference from example 1 is that only the humus extract before modification was added to prepare a shampoo composition, and the other components and contents were the same as in example 1 (less than 100g was made up with pure water).
Comparative example 2
Preparation of shampoo composition
Weighing the following components in proportion (in 100 g): 5g of ohm flower fragrance essence and 95g of shampoo base stock.
Secondly, the ohm flower fragrance essence and the shampoo base material are homogenized to be uniform according to the production process of the common shampoo, and then the mixture is filled into a bottle, so that the shampoo composition containing the modified humus extract is obtained.
Clinical trial effect
The test method comprises the following steps: 150 subjects with hair loss are selected for the test, half of the male and the female are tested, the age is 25-50 years, and the average age is 30-40 years. The hair shampoo compositions prepared in example 1 were randomly divided into 3 groups (50 persons/group), the hair shampoo compositions prepared in comparative example 1 were used in the experimental group, only the humus extract before modification was added to the comparative example 1, and the hair shampoo compositions prepared in comparative example 2 were used in the comparative example 2 to wash the hair once a day in the evening.
Before the test, the hair loss condition of the testee is uniformly tested and recorded.
After the 21 st day of the test, the test subjects were examined and recorded for the effects of preventing hair loss and promoting hair growth (hair loss was used as the basis for the judgment).
And (3) judging standard: after 21 days of the test, the subjects are effective in reducing or eliminating hair loss, and on the contrary, the subjects with no change or hair loss and heavy hair are considered to be ineffective.
The results, tested by the subjects after 21 days of use, were as follows:
according to the test results of the testee, the effective rate of the modified humus extract and the shampoo composition containing the extract on preventing alopecia is 88%, and is obviously superior to 10% of the control group 1 and 8% of the control group 2. Therefore, the preparation method of the modified humus extract and the shampoo composition containing the extract have good removal effects on preventing alopecia and promoting hair growth.
The foregoing is merely exemplary and illustrative of the present inventive concept and various modifications, additions and substitutions of similar embodiments may be made to the specific embodiments described by those skilled in the art without departing from the inventive concept or exceeding the scope of the claims as defined in the accompanying claims.
Claims (8)
1. A preparation method of a modified humus extract is characterized by comprising the following steps: the method comprises the following steps:
weighing humus extract, ohmic flower fragrance essence and pure water for later use;
adding the humus extract and pure water into a homogenizer, and homogenizing to form a humus extract solution;
thirdly, adding the ohm flower fragrance essence into the humus extract solution, and homogenizing;
fourthly, keeping the sealing state and standing to obtain the modified humus extract.
2. The method for preparing a modified humic substance extract according to claim 1 wherein: the weight ratio of the raw materials in the step (i) is humus extract: ohm flower fragrance essence: pure water (20-55): (10-27.5): (17.5-70).
3. The method for preparing a modified humic substance extract according to claim 1 wherein: in the step I, the mass ratio of the humus extract to the ohm flower fragrance essence is 2: 1.
4. the method for preparing a modified humic substance extract according to claim 1 wherein: and in the step II, the temperature is 35-55 ℃ during homogenization, and the homogenization time is 1-3 h.
5. The method for preparing a modified humic substance extract according to claim 1 wherein: and in the step III, the temperature is 50-65 ℃ during homogenization, and the homogenization time is 1-3 h.
6. The method for preparing a modified humic substance extract according to claim 1 wherein: and standing for 0.5-1 h in the step IV.
7. A modified humic substance extract prepared by the process as claimed in any one of claims 1 to 6.
8. A shampoo composition containing modified humus extract is characterized in that: prepared according to the following weight proportion: 5-15% of modified humus extract and 85-95% of shampoo base stock, wherein the sum of the modified humus extract and the shampoo base stock is 100%.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110248857.5A CN112972313A (en) | 2021-03-08 | 2021-03-08 | Preparation method of modified humus extract and shampoo composition containing modified humus extract |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202110248857.5A CN112972313A (en) | 2021-03-08 | 2021-03-08 | Preparation method of modified humus extract and shampoo composition containing modified humus extract |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006327978A (en) * | 2005-05-25 | 2006-12-07 | Myubio Co Ltd | Hair grower |
| WO2018128104A1 (en) * | 2017-01-05 | 2018-07-12 | 株式会社スタイルアンドバリュージャパン | Hair growth promoter |
| CN110055134A (en) * | 2019-05-10 | 2019-07-26 | 德利宝(广州)香料有限公司 | The preparation method of a kind of ohm of floral perfume and washing containing the essence wash one's hair composition |
-
2021
- 2021-03-08 CN CN202110248857.5A patent/CN112972313A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006327978A (en) * | 2005-05-25 | 2006-12-07 | Myubio Co Ltd | Hair grower |
| WO2018128104A1 (en) * | 2017-01-05 | 2018-07-12 | 株式会社スタイルアンドバリュージャパン | Hair growth promoter |
| CN110055134A (en) * | 2019-05-10 | 2019-07-26 | 德利宝(广州)香料有限公司 | The preparation method of a kind of ohm of floral perfume and washing containing the essence wash one's hair composition |
Non-Patent Citations (1)
| Title |
|---|
| 卞兆祥等: "《百病食疗》", 30 April 2019, 中国中医药出版社 * |
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Application publication date: 20210618 |