CN112724115A - Firecracker spark cream and preparation method thereof - Google Patents
Firecracker spark cream and preparation method thereof Download PDFInfo
- Publication number
- CN112724115A CN112724115A CN202011556219.1A CN202011556219A CN112724115A CN 112724115 A CN112724115 A CN 112724115A CN 202011556219 A CN202011556219 A CN 202011556219A CN 112724115 A CN112724115 A CN 112724115A
- Authority
- CN
- China
- Prior art keywords
- flower
- paste
- firecracker
- spark
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000006071 cream Substances 0.000 title claims abstract description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 73
- 235000010208 anthocyanin Nutrition 0.000 claims abstract description 21
- 229930002877 anthocyanin Natural products 0.000 claims abstract description 21
- 239000004410 anthocyanin Substances 0.000 claims abstract description 21
- 150000004636 anthocyanins Chemical class 0.000 claims abstract description 21
- 241000764065 Persicaria capitata Species 0.000 claims abstract description 15
- 238000000034 method Methods 0.000 claims abstract description 10
- 238000002791 soaking Methods 0.000 claims abstract description 9
- 239000003814 drug Substances 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 8
- 241000046193 Dichelostemma ida-maia Species 0.000 claims description 4
- 238000007598 dipping method Methods 0.000 claims description 4
- 238000005325 percolation Methods 0.000 claims description 2
- 241001377830 Polygonum ramosissimum Species 0.000 claims 1
- 238000000605 extraction Methods 0.000 abstract description 21
- 239000003513 alkali Substances 0.000 abstract description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 8
- 238000003809 water extraction Methods 0.000 abstract description 6
- 238000002386 leaching Methods 0.000 description 4
- 241000205407 Polygonum Species 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 241001090347 Bignoniaceae Species 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 241001648835 Polygonum cuspidatum Species 0.000 description 1
- 235000018167 Reynoutria japonica Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000000675 anti-caries Effects 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 208000027866 inflammatory disease Diseases 0.000 description 1
- 208000030159 metabolic disease Diseases 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
- C07D311/60—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with aryl radicals attached in position 2
- C07D311/62—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with aryl radicals attached in position 2 with oxygen atoms directly attached in position 3, e.g. anthocyanidins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a firecracker spark cream and a preparation method thereof, and the preparation method of the firecracker spark cream comprises the following steps: soaking, percolating and concentrating the polygonum capitatum flower sequentially by adopting NaOH solution with solute mass fraction of 0.05-0.07% to obtain the polygonum capitatum flower paste. The technical scheme of the invention adopts a cold extraction mode, and uses low-concentration alkali liquor to extract anthocyanin in the polygonum capitatum flower to the maximum extent, so that the content of anthocyanin in the polygonum capitatum flower paste reaches 20-30 mg/g, and the anthocyanin contained in the polygonum capitatum flower is fully utilized. Compared with the traditional water extraction method and the traditional alcohol extraction method, the preparation method has the advantages of simple extraction conditions, low cost and high extraction efficiency.
Description
Technical Field
The invention relates to the technical field of food processing, in particular to a firecracker spark paste and a preparation method thereof.
Background
Rhizoma Polygoni Cuspidati flower is also called as caulis Fibraureae, and is a vine of Bignoniaceae, rhizoma Polygoni Cuspidati. Researches show that the phenolic substances in the polygonum capitatum extract have antibacterial, anti-caries and antioxidant activities, are used as conventional supplements for treating any inflammatory diseases in the traditional Brazilian medicine, and also have the effects of resisting tumors and regulating metabolic disorders. Therefore, the development of the firecracker flower food has good market prospect.
The main antibacterial component in the fire tier flower is anthocyanin, and at present, the known methods for extracting the anthocyanin comprise the following steps: water extraction, water extraction and alcohol precipitation, dilute alcohol extraction, acid alcohol extraction, degreasing alcohol extraction and ultrasonic extraction. The water extraction method has the advantages of low solvent cost, short extraction time and high extract extraction rate, and has the defects of more extraction impurities, more times for extracting the anthocyanin to an extreme value, and high environmental temperature during extraction easily causes anthocyanin oxidation. The alcohol extraction method has the disadvantages of higher solvent cost, increased fat-soluble components in the extract, less extraction impurities, high anthocyanin extraction rate, mild extraction temperature and difficult anthocyanin oxidation, especially in an acidic environment.
Disclosure of Invention
Based on the above, the invention aims to overcome the defects of the prior art and provide the polygonum capitatum cream and the preparation method thereof, so that the problems of higher temperature of the water extraction method and higher solvent cost of the alcohol extraction method in the extraction process of the polygonum capitatum are solved.
In order to realize the purpose, the invention provides a preparation method of a firecracker spark paste, which comprises the following steps: soaking, percolating and concentrating the polygonum capitatum flower sequentially by adopting NaOH solution with solute mass fraction of 0.05-0.07% to obtain the polygonum capitatum flower paste.
As a preferred embodiment of the preparation method of the thick stick flower cream, the amount of the NaOH solution is 10-16 times of the mass of the thick stick flower, and the NaOH solution submerges the thick stick flower and is 30cm higher than the thick stick flower during dipping.
As a preferred embodiment of the preparation method of the firecracker spark paste, the dipping time is 20-25 h.
As a preferred embodiment of the preparation method of the polygonum cuspidatum cream, the percolation time is 70-75 h.
In a preferred embodiment of the method for preparing the polygonum branch cream, the mixture is concentrated under reduced pressure until the relative density of the liquid medicine is 1.17-1.20.
In order to achieve the purpose, the invention also provides a firecracker spark paste, which is prepared by any one of the preparation methods.
As a preferred embodiment of the preparation method of the polygonum branch cream, the anthocyanin content in the polygonum branch cream is 20 mg-30 mg/g.
Compared with the prior art, the invention has the beneficial effects that:
the technical scheme of the invention adopts a cold extraction mode, and uses low-concentration alkali liquor to extract anthocyanin in the polygonum capitatum flower to the maximum extent, so that the content of anthocyanin in the polygonum capitatum flower paste reaches 20-30 mg/g, and the anthocyanin contained in the polygonum capitatum flower is fully utilized. Compared with the traditional water extraction method and the traditional alcohol extraction method, the preparation method has the advantages of simple extraction conditions, low cost and high extraction efficiency.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.
Example 1
Taking NaOH lye with solute mass fraction of 0.04%, according to m (NaOH lye): m (firecracker) is 16: 1, soaking for 24 hours until the alkali liquor is used up, collecting the alkali liquor, concentrating under reduced pressure until the relative density of the final liquid medicine is 1.20, and determining the content of anthocyanin.
Example 2
Taking NaOH alkaline leaching solution with solute mass fraction of 0.05%, and mixing the solution according to m (NaOH alkaline leaching solution): m (firecracker) is 16: 1, soaking for 24 hours until the alkali liquor is used up, collecting the alkali liquor, concentrating under reduced pressure until the relative density of the final liquid medicine is 1.20, and determining the content of anthocyanin.
Example 3
Taking NaOH lye with solute mass fraction of 0.06%, according to m (NaOH lye): m (firecracker) is 16: 1, soaking for 24 hours until the alkali liquor is used up, collecting the alkali liquor, concentrating under reduced pressure until the relative density of the final liquid medicine is 1.20, and determining the content of anthocyanin.
Example 4
Taking NaOH lye with solute mass fraction of 0.07%, according to m (NaOH lye): m (firecracker) is 16: 1, soaking for 24 hours until the alkali liquor is used up, collecting the alkali liquor, concentrating under reduced pressure until the relative density of the final liquid medicine is 1.20, and determining the content of anthocyanin.
Example 5
Taking NaOH alkaline leaching solution with solute mass fraction of 0.05%, and mixing the solution according to m (NaOH alkaline leaching solution): m (firecracker) is 12: 1, soaking for 24 hours until the alkali liquor is used up, collecting the alkali liquor, concentrating under reduced pressure until the relative density of the final liquid medicine is 1.18, and determining the content of anthocyanin.
Example 6
Taking NaOH lye with solute mass fraction of 0.06%, according to m (NaOH lye): m (firecracker) is 12: 1, soaking for 24 hours until the alkali liquor is used up, collecting the alkali liquor, concentrating under reduced pressure until the relative density of the final liquid medicine is 1.18, and determining the content of anthocyanin.
TABLE 1. anthocyanin content results of the cream of firecracker flowers prepared in examples 1-6
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (7)
1. The preparation method of the firecracker spark paste is characterized by comprising the following steps: soaking, percolating and concentrating the polygonum capitatum flower sequentially by adopting NaOH solution with solute mass fraction of 0.05-0.07% to obtain the polygonum capitatum flower paste.
2. The method for preparing paste of fire crackers of claim 1, wherein the amount of the NaOH solution is 10-16 times of the weight of fire crackers, and the NaOH solution submerges the fire crackers and is 30cm higher than the fire crackers during dipping.
3. The method for preparing firecracker spark paste according to claim 1, wherein the dipping time is 20-25 h.
4. The method for preparing paste of bushy knotweed of claim 1, wherein the percolation time is 70-75 h.
5. The method for preparing paste of fire fighting stick according to claim 1, wherein the paste is concentrated under reduced pressure until the relative density of the liquid medicine is 1.17-1.20.
6. A firecracker spark cream, characterized in that the firecracker spark cream is prepared by the preparation method of any one of claims 1-5.
7. The fire cracker flower paste of claim 6, wherein the content of anthocyanin in the fire cracker flower paste is 20 mg-30 mg/g.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011556219.1A CN112724115A (en) | 2020-12-24 | 2020-12-24 | Firecracker spark cream and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011556219.1A CN112724115A (en) | 2020-12-24 | 2020-12-24 | Firecracker spark cream and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112724115A true CN112724115A (en) | 2021-04-30 |
Family
ID=75615684
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011556219.1A Pending CN112724115A (en) | 2020-12-24 | 2020-12-24 | Firecracker spark cream and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112724115A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112675205A (en) * | 2020-12-29 | 2021-04-20 | 广州城市职业学院 | Processing method of firecracker flower |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101023974A (en) * | 2006-02-22 | 2007-08-29 | 北京源生素源生物科技有限公司 | Preparing method for honeysuckle paste |
| CN109796431A (en) * | 2019-01-31 | 2019-05-24 | 河北三狮生物科技有限公司 | A method of extracting anthocyanidin |
-
2020
- 2020-12-24 CN CN202011556219.1A patent/CN112724115A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101023974A (en) * | 2006-02-22 | 2007-08-29 | 北京源生素源生物科技有限公司 | Preparing method for honeysuckle paste |
| CN109796431A (en) * | 2019-01-31 | 2019-05-24 | 河北三狮生物科技有限公司 | A method of extracting anthocyanidin |
Non-Patent Citations (3)
| Title |
|---|
| 刘晶晶 等: "翅碱蓬花青素提取方法研究", 《新疆农业化学》 * |
| 林泽森 等: "炮仗花花青素的纯化及应用前景", 《广东化工》 * |
| 罗琴 等: "pH值及食品添加剂对炮仗花色素吸收光谱的影响", 《楚雄师范学院学报》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112675205A (en) * | 2020-12-29 | 2021-04-20 | 广州城市职业学院 | Processing method of firecracker flower |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102318477B (en) | Production method of selenium-rich tea | |
| CN110526804B (en) | Method for extracting hydroxytyrosol by using eutectic solvent | |
| CN101348529A (en) | Extraction and separation method of medlar polysaccharide | |
| WO2020155726A1 (en) | Application of polysaccharide composite nano-selenium in production of selenium-enriched tea | |
| CN105146162A (en) | Chick feed additive prepared by comprehensively using coconut shell and capable of improving intestinal health | |
| CN112724115A (en) | Firecracker spark cream and preparation method thereof | |
| CN103054131B (en) | Preparation method of high-purity Caulerpa racemesa polyphenol and application thereof to fresh-keeping of shrimp | |
| CN115463063B (en) | Preparation method of orange extract and cosmetic | |
| CN104628798A (en) | Method for preparing anthocyanin and polysaccharide from raw material purple dendrobe | |
| CN104232310B (en) | A kind of preparation method of dragon fruit pulp quintessence oil | |
| CN113164428A (en) | Preparation method of red perilla leaf extract | |
| CN107337589B (en) | Method for efficiently extracting phenols extract from pyroligneous liquor | |
| CN112877133B (en) | Tea oil extraction method | |
| CN106720801B (en) | Burdock tea rich in inulin | |
| CN111171111B (en) | Method for continuously extracting crude protein, polysaccharide and cellulose from fresh xanthoceras sorbifolia shells | |
| CN112717009B (en) | Preparation method of gardenia extract | |
| CN111544460A (en) | Method for extracting selenium-containing antioxidant active ingredients from selenium-rich moringa oleifera tea | |
| CN104287032B (en) | Ulva juice product containing ulva oligosaccharide and preparation method thereof | |
| CN112481014A (en) | Enzymatic extraction process for oil in camellia seed kernels | |
| CN104921122B (en) | Resveratrol grape concentration essence and preparation method thereof | |
| CN105567415A (en) | Method for preparing peony seed oil | |
| CN109381614A (en) | A kind of preparation method of Rhizoma Gastrodiae instant powder | |
| CN103805487A (en) | Preparation method of seaweed wine | |
| CN104839523A (en) | Perilla oil meal-containing red bayberry jam and preparation method thereof | |
| CN108432869A (en) | A kind of vegetables and fruits preservative specially and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210430 |