CN112656698A

CN112656698A - Preparation process of anti-fading lipstick

Info

Publication number: CN112656698A
Application number: CN202011401665.5A
Authority: CN
Inventors: 罗亚文
Original assignee: Individual
Current assignee: Individual
Priority date: 2021-03-15
Filing date: 2021-03-15
Publication date: 2021-04-16

Abstract

The invention discloses a preparation process of a fading-preventing lipstick, which comprises the following steps: adding carnauba wax, cocoa butter, beeswax, castor oil, white vaseline, anhydrous lanolin, monoglyceride, grape seed oil and polyurethane resin into a melting pot, heating to about 90 ℃, melting, and stirring uniformly to obtain a mixture; filtering the mixture, and continuously stirring; grinding the rest raw materials, and heating and stirring with the mixture for 40-60 min. The method has the beneficial effects that: the addition of the carnauba wax can be beneficial to keeping the lipstick cream body to have a higher melting point without influencing the thixotropic property, the beeswax can well ensure the compatibility of the lipstick, and in addition, the anhydrous lanolin is also added in the preparation of the lipstick, so that the lipstick can have good compatibility with other grease and wax, is cold-resistant and hot-resistant, and can reduce the phenomenon of 'sweating' of the lipstick, thereby further preventing the erosion of fading.

Description

Preparation process of anti-fading lipstick

Technical Field

The invention relates to the field of anti-fading lipstick, in particular to a preparation process of anti-fading lipstick.

Background

Lipstick is a generic term for all lip color cosmetics. The lipstick comprises lipstick, lip stick, lip gloss, lip glaze and the like, can make the lips ruddy and glossy, achieves the effects of moistening and protecting the lips, increasing the aesthetic feeling of the face and correcting the contour of the lips, is a product with a backing effect, is one of necessary beauty cosmetics for women, according to Chinese patent document with publication number CN108618999A, a method for preparing lipstick with moisture-keeping effect is provided, the materials used in the invention are edible materials, the content of chemical components in the lipstick is greatly reduced, the use is superior to the lipstick sold on the world, and the lipstick can play a role in moisturizing the lips and the mouth for a long time, but the conventional lipstick also has the moisturizing effect, in addition, the lip balm is used for moistening in advance when a lipstick is generally used, but the effect of preventing the lipstick from fading cannot be realized, the phenomenon of sweating of lipstick products cannot be reduced, and the phenomenon of fading or accelerated fading is easily caused.

An effective solution to the problems in the related art has not been proposed yet.

Disclosure of Invention

Aiming at the problems in the related art, the invention provides a preparation process of a lipstick for preventing fading, which aims to overcome the technical problems in the prior related art.

Therefore, the invention adopts the following specific technical scheme:

according to one aspect of the present invention, there is provided a lipstick preventing fading.

The anti-fading lipstick consists of the following raw materials in percentage by mass:

7-10% of carnauba wax, 7-10% of cocoa butter, 7-10% of beeswax, 7-10% of castor oil, 7-10% of white vaseline, 5-8% of bromohydrin, 5-8% of anhydrous lanolin, 5-8% of glyceryl monostearate, 7-10% of monoglyceride, 3-5% of organic silicon, 3-5% of mint powder, 3-5% of mica powder, 78-8% of vitamin E5, 5-8% of essence, 2-3% of grape seed oil, 5-8% of octyldodecanol, 1-2% of polyurethane resin and 10-15% of polyvinylidene fluoride emulsion.

According to another aspect of the present invention, there is provided a process for preparing a lipstick for preventing discoloration

The preparation process of the anti-fading lipstick comprises the following steps:

the method comprises the following steps: adding carnauba wax, cocoa butter, beeswax, castor oil, white vaseline, anhydrous lanolin, monoglyceride, grape seed oil and polyurethane resin into a melting pot, heating to about 90 ℃, melting, and stirring uniformly to obtain a mixture;

step two: filtering the mixture, and continuously stirring;

step three: grinding the rest raw materials, and heating and stirring the ground raw materials and the mixture for 40-60 minutes again;

step four: stirring, filtering, placing into a vacuum defoaming pot, and mixing and stirring again;

step five: pouring the mixture into a pouring mold, and standing for cooling;

step six: and (5) demolding to finish the lipstick manufacturing.

Further, for the stirring in the first step, the stirring speed is 125-150 rpm, the reaction time is 45 minutes, and the reaction temperature is 60-90 ℃.

Further, as for the cooling condition in the fifth step, the cooling is carried out to room temperature under an inert gas atmosphere.

Further, the inert gas is carbon dioxide.

Further, for the stirring in the fourth step, the stirring speed is 125-150 rpm, the vacuum material temperature is controlled to be 30-55 ℃, and the vacuum degree is 100-5 Pa.

Further, the filter cloth is used for filtering in the third step, and the filter cloth is filtered through 120 meshes to remove slag.

Further, the stirring speed is 300-800r/min, and the stirring time is 20-30 mi.

Further, in the third step, the stirring state is maintained after stirring and mixing, and the temperature is maintained between 75 and 80 ℃ by heating.

The raw material components adopted by the invention are explained as follows:

carnauba wax: the resin is obtained from Brazilian palm leaves, has a melting point of 66-82 ℃, a relative density of 0.996-0.998 (25 ℃), a saponification value of 78-88 and an iodine value of 7-14, and is a light yellow solid. The carnauba wax has good intersolubility with castor oil, and mainly comprises wax ester, higher alcohol, hydrocarbon and resin-like substances.

Cocoa butter: is a natural edible oil extracted from cocoa beans during the process of making chocolate and cocoa powder. It has only slight chocolate taste and fragrance, and is one of the materials for making real chocolate. A candy sheet, commonly known as white chocolate, is made from it. Cocoa butter has a melting point of about 34-38 degrees celsius (93-100 degrees fahrenheit), so chocolate is solid at room temperature and melts quickly in the mouth.

Beeswax: is wax secreted by Apis cerana or Apis mellifera of Apidae. Has the effects of detoxifying, healing sore, promoting granulation and relieving pain. It is commonly used for unhealing ulcer, ecthyma erosion, traumatic ulceration and burn and scald.

Castor oil: is a composite triglyceride which exists in the seeds of castor, the content of the triglyceride is 35 percent to 57 percent, and the castor oil is prepared by generally using a squeezing or solvent extraction method. The castor oil comprises the following components: 80% to 85% ricinoleic acid, 7% oleic acid, 3% linoleic acid, 2% palmitic acid, 1% stearic acid, flammable but not flammable, soluble in ethanol, slightly soluble in aliphatic hydrocarbons, practically insoluble in water and slightly volatile.

White vaseline: petrolatum is a semi-liquid mixture of alkanes or saturated hydrocarbons, also called petrolatum, which is obtained by fractionation of petroleum. The state of the product is between solid and liquid at normal temperature, and the product has three colors of brown, yellow and white due to different purposes. The white petrolatum is white vaseline.

Glyceryl monostearate: is an organic compound with the molecular formula of C21H42O4, and has two configurations, namely 1-MG and 2-MG. Monoglyceride can be classified into glyceryl monostearate, glyceryl monolaurate, glyceryl monooleate, and the like according to the names of main constituent fatty acids, with glyceryl monostearate being the most widely used yield.

Monoglyceride: generally oily, greasy or waxy, yellowish or ivory in color, greasy or odorless, depending on the size and degree of saturation of the fatty groups, with excellent organoleptic properties. Monoglycerides are insoluble in water and glycerol, but form stable aqueous dispersions in water. In addition, monoglyceride is a polyol type nonionic surfactant, has good surface activity due to the structure of the monoglyceride which has a lipophilic long-chain alkyl group and two hydrophilic hydroxyl groups, can play roles in emulsification, foaming, dispersion, defoaming, starch aging resistance and the like, and is an emulsifier which is most widely applied to foods and cosmetics.

Organosilicon: that is, the organosilicon compound means a compound having an Si-C bond in which at least one organic group is directly bonded to a silicon atom, and conventionally, a compound in which an organic group is bonded to a silicon atom via oxygen, sulfur, nitrogen or the like is also commonly used as the organosilicon compound. Among them, the polysiloxane having a siloxane bond (-Si-O-Si-) as a skeleton is the most abundant, most studied and most widely used class of organosilicon compounds, and accounts for about 90% or more of the total amount.

Mica powder: the mineral is a non-metallic mineral and contains a plurality of components, wherein SiO2 is mainly contained, the content is about 49 percent generally, and the content of Al2O3 is about 30 percent. The mica powder has good elasticity and toughness. The additive has the characteristics of insulativity, high temperature resistance, acid and alkali resistance, corrosion resistance, strong adhesive force and the like, and is an excellent additive. It is widely used in the industries of electric appliances, welding electrodes, rubber, plastics, paper making, paint, coating, pigment, ceramics, cosmetics, novel building materials and the like, and has extremely wide application.

Octyl dodecanol: a lubricant, an emulsifier, a solvent and a thickener are used in cosmetics and external preparations, and have the functions of an emulsifier and a lubricant. Octyl dodecanol has transdermal promoting effect, and can promote transdermal absorption of naproxen. For the medicine with poor transdermal performance, the microemulsion taking the octyl dodecanol as the auxiliary material can improve the transdermal speed.

The invention has the beneficial effects that: the addition of the carnauba wax can be beneficial to keeping the lipstick cream body to have a higher melting point without influencing the thixotropic property, the beeswax can well ensure the compatibility of the lipstick, and can help various components to be dissolved and uniform during the preparation of the lipstick, in addition, the anhydrous lanolin is also added in the preparation of the lipstick, the lipstick can be well compatible with other grease and wax, is cold-resistant, hot-hot, and can reduce the phenomenon of 'sweating' of the lipstick, thereby increasing the lubricity of the lipstick and preventing the fading.

Drawings

In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings needed in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without creative efforts.

Fig. 1 is a schematic flow chart of a process for preparing a lipstick for preventing fading according to an embodiment of the present invention.

Detailed Description

For further explanation of the various embodiments, the drawings which form a part of the disclosure and which are incorporated in and constitute a part of this specification, illustrate embodiments and, together with the description, serve to explain the principles of operation of the embodiments, and to enable others of ordinary skill in the art to understand the various embodiments and advantages of the invention, and, by reference to these figures, reference is made to the accompanying drawings, which are not to scale and wherein like reference numerals generally refer to like elements.

According to an embodiment of the present invention, there is provided a process for preparing a lipstick preventing fading.

The fading-prevented lipstick according to the embodiment of the invention is composed of the following raw materials in percentage by weight:

In order to clearly understand the technical scheme of the invention, the technical scheme of the invention is described in detail through specific examples.

The first embodiment is as follows:

7% of carnauba wax, 7% of cocoa butter, 7% of beeswax, 7% of castor oil, 7% of white vaseline, 5% of bromohydrin, 5% of anhydrous lanolin, 5% of glyceryl monostearate, 7% of monoglyceride, 3-5% of organic silicon, 3% of mint powder, 3% of mica powder, 5% of vitamin E, 5% of essence, 2% of grape seed oil, 5% of octyldodecanol, 1% of polyurethane resin and 10% of polyvinylidene fluoride emulsion.

Example two:

8% of carnauba wax, 8% of cocoa butter, 8% of beeswax, 8% of castor oil, 8% of white vaseline, 7% of bromohydrin, 7% of anhydrous lanolin, 7% of glyceryl monostearate, 8% of monoglyceride, 4% of organosilicon, 4% of mint powder, 4% of mica powder, 7% of vitamin E, 7% of essence, 2.5% of grape seed oil, 6.5% of octyldodecanol, 1.5% of polyurethane resin and 12.5% of polyvinylidene fluoride emulsion.

Example three:

10% of carnauba wax, 10% of cocoa butter, 10% of beeswax, 10% of castor oil, 7-10% of white vaseline, 8% of bromohydrin, 8% of anhydrous lanolin, 8% of glyceryl monostearate, 10% of monoglyceride, 5% of silicone, 5% of mint powder, 5% of mica powder, 8% of vitamin E, 8% of essence, 3% of grape seed oil, 8% of octyldodecanol, 2% of polyurethane resin and 115% of polyvinylidene fluoride emulsion. .

For the convenience of understanding the technical solutions of the present invention, the following detailed description will be made on the working principle or the operation mode of the present invention in the practical process.

As shown in fig. 1, the preparation process of the anti-fading lipstick in the actual production process comprises the following steps:

step S101: adding carnauba wax, cocoa butter, beeswax, castor oil, white vaseline, anhydrous lanolin, monoglyceride, grape seed oil and polyurethane resin into a melting pot, heating to about 90 ℃, melting, and stirring uniformly to obtain a mixture;

step S103: filtering the mixture, and continuously stirring;

step S105: grinding the rest raw materials, and heating and stirring the ground raw materials and the mixture for 40-60 minutes again;

step S107: stirring, filtering, placing into a vacuum defoaming pot, and mixing and stirring again;

step S109: pouring the mixture into a pouring mold, and standing for cooling;

step S111: and (5) demolding to finish the lipstick manufacturing.

In one embodiment, for the stirring in the step S101, the stirring speed is 125-150 rpm, the reaction time is 45 minutes, and the reaction temperature is 60-90 ℃.

In one embodiment, for the cooling condition in step S109 described above, the cooling is performed to room temperature under an inert gas atmosphere.

In one embodiment, the inert gas is carbon dioxide.

In one embodiment, for the stirring in step S107, the stirring speed is 125-150 rpm, the vacuum material temperature is controlled to be 30-55 ℃, and the vacuum degree is controlled to be 100-5 Pa.

In one embodiment, the residue is removed by passing through 120-mesh gauze for the filtering in step S105.

In one embodiment, the stirring speed is 300-800r/min and the stirring time is 20-30mi for the stirring in step S103.

In one embodiment, for the above step S105, the stirring state is maintained after stirring and mixing, and the temperature is maintained by heating and is between 75 and 80 degrees.

In conclusion, by means of the technical scheme, the carnauba wax is added, so that the lipstick paste can be kept to have a higher melting point without influencing the thixotropic property, the beeswax can well ensure the compatibility of the lipstick, and can help to dissolve and homogenize various components during the preparation of the lipstick.

The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims

1. The fading-prevented lipstick is characterized by comprising the following raw materials in percentage by weight:

2. A preparation process of a fading-prevented lipstick is characterized by comprising the following steps:

step two: filtering the mixture, and continuously stirring;

step five: pouring the mixture into a pouring mold, and standing for cooling;

step six: and (5) demolding to finish the lipstick manufacturing.

3. The process for preparing lipstick capable of preventing fading as claimed in claim 2, wherein for the stirring in the first step, the stirring speed is 125-150 rpm, the reaction time is 45 minutes, and the reaction temperature is 60-90 °.

4. The process for preparing a lipstick against fading as described in claim 2, wherein the cooling condition in said step five is that the lipstick is cooled to room temperature under an inert gas atmosphere.

5. A process for preparing a lipstick against fading as claimed in claim 4, wherein said inert gas is carbon dioxide.

6. The process for preparing lipstick capable of preventing fading as claimed in claim 2, wherein the stirring speed in the fourth step is 125-150 rpm, the vacuum temperature is controlled from 30 ℃ to 55 ℃, and the vacuum degree is 100Pa to 5 Pa.

7. The process for preparing a lipstick capable of preventing fading as claimed in claim 2, wherein the filtering in the third step is carried out by passing through 120 mesh gauze to remove the residue.

8. The process for preparing lipstick capable of preventing fading as defined in claim 2, wherein the stirring speed used in said step two is 300-800r/min, and the stirring time is 20-30 min.

9. A process for preparing a lipstick against fading as claimed in claim 2, wherein in the third step, the mixture is stirred and heated to a temperature of 75-80 °.