CN112587464A - Baby mica talcum powder and preparation method thereof - Google Patents
Baby mica talcum powder and preparation method thereof Download PDFInfo
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- CN112587464A CN112587464A CN202011500054.6A CN202011500054A CN112587464A CN 112587464 A CN112587464 A CN 112587464A CN 202011500054 A CN202011500054 A CN 202011500054A CN 112587464 A CN112587464 A CN 112587464A
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- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 title claims abstract description 53
- 239000010445 mica Substances 0.000 title claims abstract description 50
- 229910052618 mica group Inorganic materials 0.000 title claims abstract description 50
- 238000002360 preparation method Methods 0.000 title abstract description 11
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000011787 zinc oxide Substances 0.000 claims abstract description 32
- 235000014692 zinc oxide Nutrition 0.000 claims abstract description 31
- 229920000881 Modified starch Polymers 0.000 claims abstract description 24
- 102000008186 Collagen Human genes 0.000 claims abstract description 22
- 108010035532 Collagen Proteins 0.000 claims abstract description 22
- 229920001436 collagen Polymers 0.000 claims abstract description 22
- 235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 21
- 239000008158 vegetable oil Substances 0.000 claims abstract description 21
- 239000001140 aloe barbadensis leaf extract Substances 0.000 claims abstract description 16
- 239000000945 filler Substances 0.000 claims abstract description 9
- 239000003906 humectant Substances 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims description 32
- 239000002994 raw material Substances 0.000 claims description 30
- 239000000843 powder Substances 0.000 claims description 29
- 238000005507 spraying Methods 0.000 claims description 26
- 238000005303 weighing Methods 0.000 claims description 18
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 claims description 16
- 239000003921 oil Substances 0.000 claims description 12
- 235000019198 oils Nutrition 0.000 claims description 12
- 238000007873 sieving Methods 0.000 claims description 12
- 229940105847 calamine Drugs 0.000 claims description 11
- 239000000284 extract Substances 0.000 claims description 11
- 229910052864 hemimorphite Inorganic materials 0.000 claims description 11
- CPYIZQLXMGRKSW-UHFFFAOYSA-N zinc;iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Fe+3].[Fe+3].[Zn+2] CPYIZQLXMGRKSW-UHFFFAOYSA-N 0.000 claims description 11
- 229940105902 mint extract Drugs 0.000 claims description 10
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 9
- 229960005323 phenoxyethanol Drugs 0.000 claims description 9
- 230000001954 sterilising effect Effects 0.000 claims description 7
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- 229940069521 aloe extract Drugs 0.000 claims description 6
- 239000011812 mixed powder Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 238000004806 packaging method and process Methods 0.000 claims description 6
- 238000005070 sampling Methods 0.000 claims description 6
- UREZNYTWGJKWBI-UHFFFAOYSA-M benzethonium chloride Chemical compound [Cl-].C1=CC(C(C)(C)CC(C)(C)C)=CC=C1OCCOCC[N+](C)(C)CC1=CC=CC=C1 UREZNYTWGJKWBI-UHFFFAOYSA-M 0.000 claims description 5
- 229960001950 benzethonium chloride Drugs 0.000 claims description 5
- 229940069445 licorice extract Drugs 0.000 claims description 5
- 239000003755 preservative agent Substances 0.000 claims description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- 244000303040 Glycyrrhiza glabra Species 0.000 claims description 4
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 claims description 4
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 claims description 4
- 235000011477 liquorice Nutrition 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 230000002335 preservative effect Effects 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 3
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- 229940105990 diglycerin Drugs 0.000 claims description 2
- GPLRAVKSCUXZTP-UHFFFAOYSA-N diglycerol Chemical compound OCC(O)COCC(O)CO GPLRAVKSCUXZTP-UHFFFAOYSA-N 0.000 claims description 2
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims description 2
- 235000011187 glycerol Nutrition 0.000 claims description 2
- UWJJYHHHVWZFEP-UHFFFAOYSA-N pentane-1,1-diol Chemical compound CCCCC(O)O UWJJYHHHVWZFEP-UHFFFAOYSA-N 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- 241000894006 Bacteria Species 0.000 abstract description 9
- 230000006378 damage Effects 0.000 abstract description 7
- 206010061218 Inflammation Diseases 0.000 abstract description 5
- 230000004054 inflammatory process Effects 0.000 abstract description 5
- 230000001681 protective effect Effects 0.000 abstract description 5
- 239000010425 asbestos Substances 0.000 abstract description 4
- 230000004888 barrier function Effects 0.000 abstract description 4
- 229910001385 heavy metal Inorganic materials 0.000 abstract description 4
- 229910052895 riebeckite Inorganic materials 0.000 abstract description 4
- 208000010201 Exanthema Diseases 0.000 abstract description 3
- 239000013566 allergen Substances 0.000 abstract description 3
- 230000003467 diminishing effect Effects 0.000 abstract description 3
- 201000005884 exanthem Diseases 0.000 abstract description 3
- 206010037844 rash Diseases 0.000 abstract description 3
- 208000015181 infectious disease Diseases 0.000 abstract description 2
- 231100000046 skin rash Toxicity 0.000 abstract description 2
- 210000003491 skin Anatomy 0.000 description 26
- 239000004368 Modified starch Substances 0.000 description 10
- 240000008042 Zea mays Species 0.000 description 10
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 10
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 10
- 235000005822 corn Nutrition 0.000 description 10
- 235000019426 modified starch Nutrition 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- 238000001514 detection method Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000002537 cosmetic Substances 0.000 description 3
- 239000000454 talc Substances 0.000 description 3
- 229910052623 talc Inorganic materials 0.000 description 3
- 235000012222 talc Nutrition 0.000 description 3
- 208000035143 Bacterial infection Diseases 0.000 description 2
- 241000202807 Glycyrrhiza Species 0.000 description 2
- 241000607715 Serratia marcescens Species 0.000 description 2
- 208000022362 bacterial infectious disease Diseases 0.000 description 2
- 210000004207 dermis Anatomy 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 2
- LTINPJMVDKPJJI-UHFFFAOYSA-N iodinated glycerol Chemical compound CC(I)C1OCC(CO)O1 LTINPJMVDKPJJI-UHFFFAOYSA-N 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000012046 mixed solvent Substances 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 206010034133 Pathogen resistance Diseases 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012620 biological material Substances 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000007705 chemical test Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 210000002249 digestive system Anatomy 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000001848 glycyrrhiza glabra l. root extract powder Substances 0.000 description 1
- 210000000777 hematopoietic system Anatomy 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 238000012009 microbiological test Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 239000006916 nutrient agar Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 210000000434 stratum corneum Anatomy 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Inorganic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a mica baby talcum powder and a preparation method thereof, wherein the mica baby talcum powder comprises the following components in parts by weight: (1)60-99 parts of filler, (2)0.02-0.5 part of humectant, and (3)1.301-27.5 parts of skin conditioner, wherein the filler is mica, and the skin conditioner comprises 0.10-15 parts of modified corn starch, 1-5 parts of hydrolyzed collagen, 0.1-0.5 part of vegetable oil, 0.001-2 parts of aloe leaf extract and 0.1-5 parts of zinc oxide. On the premise of taking mica and modified corn starch as fillers and adding hydrolyzed collagen, vegetable oil, zinc oxide, aloe leaf extract and other skin conditioners, the developed baby talcum powder has the functions of resisting inflammation and moistening the skin, can form a natural biological protective film barrier on the surface of the skin, resists the damage of external bacteria and allergens, prevents infection, indirectly generates the functions of resisting bacteria and diminishing inflammation, and obviously reduces the skin rash and redness. Meanwhile, the invention also avoids the damage of asbestos and heavy metal lead in the talcum powder to the body function of the infant.
Description
Technical Field
The invention relates to the technical field of daily necessities, in particular to a mica baby talcum powder and a preparation method thereof.
Background
The infant immune system is not perfect, the resistance is weak, the skin of the infant is only one tenth as thick as that of an adult, the epidermis is a monolayer of cells, and the collagen fibers in the dermis are few, so the infant lacks elasticity and is easily penetrated and rubbed by foreign objects to be damaged. Meanwhile, the stratum corneum is immature, the dermis and fibrous tissue are thin, the skin is delicate and sensitive, and the capability of resisting a dry environment is weak. The skin has poor acid-base controlling capability, and infants only rely on a layer of natural acidic protective film on the surface of the skin to protect the skin, so as to prevent bacterial infection and maintain the skin moist and smooth.
The primary function of conventional baby powders is to absorb residual moisture from the skin, dry the skin, and provide a moderate level of lubrication, reducing possible abrasions and discomfort when cleaning the skin. Meanwhile, the baby talcum powder is also used for diminishing inflammation, relieving itching and sterilizing, is often smeared on the skin fold parts of babies, and prevents the babies from reddening and even being damaged because the skin fold parts are airtight.
The traditional baby talcum powder mainly has the following two problems: (1) the talcum powder is used as a main component, the preservative is added, the talcum powder contains carcinogenic asbestos, the talcum powder contains inseparable heavy metal lead, the lead cannot be excreted quickly after entering the body of the infant, and when the lead is accumulated in the human body for a long time, the lead can harm the nerve, hematopoietic system and digestive system, thus seriously affecting the intelligence and physical development of the infant. (2) The efficacy of traditional talcum powder is very limited under the condition of ensuring safety because of thin skin and weak resistance of infants.
Disclosure of Invention
Aiming at the technical problem of poor effect of the baby talcum powder in the prior art, the invention provides the baby mica talcum powder and the preparation method thereof, a layer of biological film is formed on the surface of skin of a product by optimizing the formula of the product, and the safety and the effectiveness of the baby talcum powder are obviously improved.
In order to realize the purpose, the invention is realized by the following technical scheme:
the invention provides a mica baby talcum powder, which is characterized by comprising the following components in parts by weight:
(a)60-99 parts of a filler;
(b)0.02-0.5 parts of humectant; and
(c)1.301-27.5 parts of a skin conditioner;
the filler is mica; the skin conditioner comprises 0.10-15 parts of modified corn starch, 1-5 parts of hydrolyzed collagen, 0.1-0.5 part of vegetable oil, 0.001-2 parts of aloe leaf extract and 0.1-5 parts of zinc oxide.
Further, the talcum powder also comprises 0.001-2 parts by weight of liquorice extract.
Further, the talcum powder also comprises 0.001-2 parts by weight of mint extract.
Further, the talcum powder also comprises 0.1-8 parts of calamine by weight.
Further, the humectant is one or more selected from caprylyl glycol, propylene glycol, pentanediol, polyethylene glycol, glycerin, diglycerin and dipropylene glycol.
Further, the talcum powder also comprises 0.052-0.8 parts by weight of a preservative, and the preservative is selected from one or two of phenoxyethanol or benzethonium chloride.
Further, the talcum powder also comprises 0.001-0.5 part of essence according to the parts by weight.
The second purpose of the invention is to provide a preparation method of the baby mica talcum powder, which is characterized by comprising the following steps:
(1) respectively weighing the filler, the modified corn starch and the zinc oxide, adding the mixture into a high-speed powder stirring machine, starting homogenizing for 0.5-3 minutes, and uniformly mixing to form a phase A mixed raw material;
(2) respectively weighing humectant, hydrolyzed collagen and vegetable oil, dissolving at 30-40 deg.C, and adding into oil-spraying pot to form B phase raw material; starting the high-speed powder stirring machine, and slowly spraying the B-phase raw material while stirring;
(3) weighing folium Aloe extract, and spraying to oil pan to form C phase raw material; starting the high-speed powder stirring machine, and slowly spraying the C-phase raw material while stirring;
(4) and transferring the mixed powder into a vibrating sieving machine for sieving, sterilizing, sampling, inspecting, and filling and packaging.
Further, calamine is added into the high-speed powder stirring machine in the step (1) according to a proportion.
Further, the oil spraying pot in the step (3) is also added with a liquorice extract and a mint extract according to a proportion.
Compared with the prior art, the invention has the following beneficial technical effects:
(1) experiments prove that the baby talcum powder developed by the invention has the functions of resisting inflammation and moistening skin, can form a natural biological protective film barrier on the surface of the skin, resists the damage of external bacteria and allergen, prevents infection, indirectly generates the functions of resisting bacteria and diminishing inflammation, and obviously reduces the conditions of skin rash and redness on the premise of taking mica and modified corn starch as fillers and adding hydrolyzed collagen, vegetable oil, zinc oxide, aloe leaf extract and other skin conditioners.
(2) The invention replaces the talcum powder in the traditional talcum powder with the mixture of the mica and the modified corn starch, thereby avoiding the damage of asbestos and heavy metal lead in the talcum powder to the body function of the baby.
Detailed Description
The following examples are presented to illustrate certain embodiments of the invention in particular and should not be construed as limiting the scope of the invention. The present disclosure may be modified from materials, methods, and reaction conditions at the same time, and all such modifications are intended to be within the spirit and scope of the present invention. Unless otherwise specified, the technical means used in the examples are conventional means well known to those skilled in the art. The reagents and biomaterials, if not specifically indicated, are commercially available.
Aloe leaf extract: glycyrrhiza extract was purchased as a yellowish powder from chenguang biotechnology group, inc.
And (3) mint extract: the mint extract is purchased from Baoji Cheng biology, and is dissolved in a mixed solvent of water and phenoxyethanol. The mass ratio of the mint extract powder to the water to the phenoxyethanol is 1: 30: 10.
and (3) liquorice extract: glycyrrhiza extract yellowish powder was purchased from Chenguang Biotechnology group, Inc. and dissolved in a mixed solvent of water and phenoxyethanol. The mass ratio of the licorice extract powder to water to phenoxyethanol is 1: 30: 10.
example 1:
an infant mica talcum powder comprises the following components: 60.0g mica, 0.1g corn modified starch, 1.0g hydrolyzed collagen, 0.1g vegetable oil, 0.5g aloe leaf extract, 0.1g zinc oxide, 0.02g caprylyl glycol.
(1) Respectively weighing mica, modified corn starch and zinc oxide, adding into a high-speed powder stirring machine, opening for homogenizing for 0.5-3 minutes, and uniformly mixing to form a phase A mixed raw material;
(2) respectively weighing the caprylyl glycol, the hydrolyzed collagen and the vegetable oil, dissolving uniformly at 30-40 ℃, and adding into an oil spraying pot to form a B-phase raw material; starting the high-speed powder stirring machine, and slowly spraying the B-phase raw material while stirring;
(3) weighing folium Aloe extract, and spraying to oil pan to form C phase raw material; starting the high-speed powder stirring machine, and slowly spraying the C-phase raw material while stirring;
(4) and transferring the mixed powder into a vibrating sieving machine for sieving, sterilizing, sampling, inspecting, and filling and packaging.
Example 2:
an infant mica talcum powder comprises the following components: 75.0g mica, 15.0g corn modified starch, 3.0g hydrolyzed collagen, 0.5g vegetable oil, 2.0g aloe leaf extract, 5.0g zinc oxide, 0.20g caprylyl glycol.
The preparation method is the same as example 1.
Example 3:
an infant mica talcum powder comprises the following components: 99.0g of mica, 8.0g of corn modified starch, 5.0g of hydrolyzed collagen, 0.3g of vegetable oil, 0.001g of aloe leaf extract, 2.5g of zinc oxide and 0.50g of caprylyl glycol.
The preparation method is the same as example 1.
Example 4:
an infant mica talcum powder comprises the following components: 60.0g mica, 0.1g corn modified starch, 1.0g hydrolyzed collagen, 0.1g vegetable oil, 0.5 aloe leaf extract, 0.1g zinc oxide, 0.02g caprylyl glycol, 0.1g calamine, 0.001g licorice extract.
(1) Respectively weighing mica, modified corn starch, zinc oxide and calamine, adding into a high-speed powder stirring machine, opening and homogenizing for 2 minutes, and uniformly mixing to form a phase A mixed raw material;
(2) respectively weighing the caprylyl glycol, the hydrolyzed collagen and the vegetable oil, dissolving uniformly at 40 ℃, and adding into an oil spraying pot to form a B-phase raw material; starting the high-speed powder stirring machine, and slowly spraying the B-phase raw material while stirring;
(3) respectively weighing Glycyrrhrizae radix extract and folium Aloe extract, and spraying into oil pan to form C phase raw material; starting the high-speed powder stirring machine, and slowly spraying the C-phase raw material while stirring;
(4) and transferring the mixed powder into a vibrating sieving machine for sieving, sterilizing, sampling, inspecting, and filling and packaging.
Example 5:
an infant mica talcum powder comprises the following components: 75.0g mica, 15.0g corn modified starch, 3.0g hydrolyzed collagen, 0.5g vegetable oil, 2.0g aloe leaf extract, 5.0g zinc oxide, 0.2g caprylyl glycol, 5.0g calamine, 2.0g licorice extract, 1.0g mint extract.
(1) Respectively weighing mica, modified corn starch, zinc oxide and calamine, adding into a high-speed powder stirring machine, opening and homogenizing for 2 minutes, and uniformly mixing to form a phase A mixed raw material;
(2) respectively weighing the caprylyl glycol, the hydrolyzed collagen and the vegetable oil, dissolving uniformly at 40 ℃, and adding into an oil spraying pot to form a B-phase raw material; starting the high-speed powder stirring machine, and slowly spraying the B-phase raw material while stirring;
(3) respectively weighing Glycyrrhrizae radix extract, folium Aloe extract, and herba Menthae extract, and making into C phase raw material in oil spraying pan; starting the high-speed powder stirring machine, and slowly spraying the C-phase raw material while stirring;
(4) and transferring the mixed powder into a vibrating sieving machine for sieving, sterilizing, sampling, inspecting, and filling and packaging.
Example 6:
an infant mica talcum powder comprises the following components: 99.0g of mica, 8.0g of corn modified starch, 5.0g of hydrolyzed collagen, 0.3g of vegetable oil, 0.001g of aloe leaf extract, 2.5g of zinc oxide, 0.5g of caprylyl glycol, 8.0g of calamine, 1.0g of licorice extract, 2.0g of mint extract, 0.05g of phenoxyethanol, 0.002g of benzethonium chloride and 0.001g of essence.
(1) Respectively weighing mica, modified corn starch, zinc oxide and calamine, adding into a high-speed powder stirring machine, opening and homogenizing for 2 minutes, and uniformly mixing to form a phase A mixed raw material;
(2) respectively weighing the caprylyl glycol, the hydrolyzed collagen, the vegetable oil, the phenoxyethanol, the benzethonium chloride and the essence, uniformly dissolving at 40 ℃, and adding into an oil spraying pot to form a B-phase raw material; starting the high-speed powder stirring machine, and slowly spraying the B-phase raw material while stirring;
(3) respectively weighing Glycyrrhrizae radix extract, folium Aloe extract, and herba Menthae extract, and making into C phase raw material in oil spraying pan; starting the high-speed powder stirring machine, and slowly spraying the C-phase raw material while stirring;
(4) and transferring the mixed powder into a vibrating sieving machine for sieving, sterilizing, sampling, inspecting, and filling and packaging.
Example 7:
an infant mica talcum powder comprises the following components: 99.0g of mica, 8.0g of corn modified starch, 5.0g of hydrolyzed collagen, 0.3g of vegetable oil, 0.001g of aloe leaf extract, 2.5g of zinc oxide, 0.5g of caprylyl glycol, 8.0g of calamine, 1.0g of licorice extract, 2.0g of mint extract, 0.6g of phenoxyethanol, 0.2g of benzethonium chloride and 0.5g of essence.
Comparative example 1:
an infant mica talcum powder comprises the following components: 75.0g mica, 15.0g corn modified starch, 3.0g hydrolyzed collagen, 2.0g aloe leaf extract, 5.0g zinc oxide, 0.20g caprylyl glycol.
The preparation method is the same as example 6.
Comparative example 2:
an infant mica talcum powder comprises the following components: 75.0g mica, 15.0g corn modified starch, 0.5g vegetable oil, 2.0g aloe leaf extract, 5.0g zinc oxide, 0.20g caprylyl glycol.
The preparation method is the same as example 1.
Comparative example 3:
an infant mica talcum powder comprises the following components: 75.0g mica, 15.0g corn modified starch, 3.0g hydrolyzed collagen, 0.5g vegetable oil, 2.0g aloe leaf extract, 0.20g caprylyl glycol.
The preparation method is the same as example 1.
Analysis of results
1. The talcum powders of examples 1 to 7 were tested according to the following: the results of the tests in technical standards for cosmetic safety (Ministry of health, 2015) are shown in Table 1 below.
TABLE 1
Examples 4-7 further adjusted the skin conditioning agents and added preservatives, and the tests showed that both chemical and microbiological tests met the standards.
And (4) evaluating the results: according to the requirements of the cosmetic hygiene code, the indexes of the microorganism detection in examples 1 to 7 meet the requirements, and the indexes of the hygienic chemical detection meet the requirements. Therefore, the mixture of the mica and the modified corn starch is used for replacing the talcum powder in the traditional talcum powder, so that the damage of asbestos and heavy metal lead in the talcum powder to the body function of the infant can be avoided.
2. Measurement of skin moisturizing effect
In a space where there was no air movement and direct light and constant temperature and humidity conditions were maintained (222 ℃, 505%), 120 (20 subjects per experimental group) waited for a minimum of 15 minutes or more, the toilet powders of examples 1 to 3 and comparative examples 1 to 3 were applied to the skin surface of the subjects, respectively, and the moisture amount was measured. The moisture content was measured using a skin moisture tester before the start of application, 30 minutes after application, and 8 hours after application, respectively.
TABLE 2
The results show that the moisture content of the skin coated with the talcum powder of examples 1-3 is obviously increased compared with that of comparative examples 1-3, and the baby talcum powder developed by using the mica and the modified corn starch as fillers and adding hydrolyzed collagen, vegetable oil and zinc oxide can form a natural biological protective film barrier on the skin surface and has obvious moisturizing effect.
3. Resistance to bacteria test
A120-mesh sieve was cut into 30 pieces of 33 square cm round structures, and the toilet powders of examples 1 to 7 and comparative examples 1 to 3 were sufficiently applied to the round structures to prepare detection materials.
Reference is made to YY/T0471.5-2007 for the detection of bacterial resistance. The test method comprises the following steps: culturing Serratia marcescens with 20-25 nutrient broth for 24 hr to obtain a culture with a bacteria content of about 109One sterile sample is aseptically transferred to a petri dish containing a sterile nutrient agar medium; dripping 5 drops of culture bacteria liquid on the sample by using a sterile pipette, and placing the sample in a culture tank for 20-25 to culture for 24 hours; after the culture is finished, the culture bacteria liquid is sucked from the sample by using a sterile pipette, the sample is placed under 20-25 to be cultured for 24 hours, whether the serratia marcescens grows in the surface area covered by the sample or not is observed, each sample is parallelly measured for 3 times, no detection is found out for 3 times, the detection is not detected for 1 time, the test result is unqualified, and the test result is shown in the table below.
And (4) evaluating the results: the talcum powders of examples 1-6 have antibacterial property after film forming, can effectively prevent bacterial infection and maintain skin moist and smooth.
4. Acute skin irritation test
The talcum powders of examples 1-3 and comparative examples 1-3 were tested according to the following: the results of the tests in the "standards for cosmetics hygiene" (Ministry of health, 2015) are shown in Table 4:
TABLE 4
And (4) evaluating the results: the baby talcum powder can form a natural biological protective film barrier on the surface of skin, resist the damage of external bacteria and allergens and obviously reduce the conditions of rash and red swelling.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (10)
1. The baby mica talcum powder is characterized by comprising the following components in parts by weight:
(a)60-99 parts of mica;
(b)0.02-0.5 parts of humectant; and
(c)1.301-27.5 parts of a skin conditioner;
the skin conditioner comprises 0.1-15 parts of modified corn starch, 1-5 parts of hydrolyzed collagen, 0.1-0.5 part of vegetable oil, 0.001-2 parts of aloe leaf extract and 0.1-5 parts of zinc oxide.
2. An infant mica talcum powder according to claim 1, which further comprises 0.001-2 parts by weight of licorice extract.
3. An infant mica talcum powder according to claim 1, which further comprises 0.001-2 parts by weight of mint extract.
4. An infant mica talcum powder according to claim 1, which further comprises 0.1-8 parts by weight of calamine.
5. An infant mica talcum powder according to claim 1, wherein said humectant is selected from one or more of caprylyl glycol, propylene glycol, pentanediol, polyethylene glycol, glycerin, diglycerin, and dipropylene glycol.
6. An infant mica talcum powder according to claim 1, which further comprises 0.052-0.8 parts of a preservative selected from one or both of phenoxyethanol and benzethonium chloride.
7. An infant mica talcum powder according to claim 1, which further comprises 0.001-0.5 parts by weight of essence.
8. A process for preparing an infant mica talcum powder as claimed in claims 1-7, which comprises the following steps:
(1) respectively weighing the filler, the modified corn starch and the zinc oxide, adding the mixture into a high-speed powder stirring machine, starting homogenizing for 0.5-3 minutes, and uniformly mixing to form a phase A mixed raw material;
(2) respectively weighing humectant, hydrolyzed collagen and vegetable oil, dissolving at 30-40 deg.C, and adding into oil-spraying pot to form B phase raw material; starting the high-speed powder stirring machine, and slowly spraying the B-phase raw material while stirring;
(3) weighing folium Aloe extract, and spraying to oil pan to form C phase raw material; starting the high-speed powder stirring machine, and slowly spraying the C-phase raw material while stirring;
(4) and transferring the mixed powder into a vibrating sieving machine for sieving, sterilizing, sampling, inspecting, and filling and packaging.
9. The method for preparing an infant mica talcum powder according to claim 8, wherein calamine is further added into the high-speed powder stirring machine in the step (1) in proportion.
10. The method for preparing an infant mica talcum powder according to claim 8, wherein in the step (3), the oil spraying pot is further added with a liquorice extract and a mint extract in proportion.
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