CN112587449A

CN112587449A - Natural plant aromatic coating balm and preparation method and application thereof

Info

Publication number: CN112587449A
Application number: CN202011327600.0A
Authority: CN
Inventors: 李莉; 张益丽; 华翠
Original assignee: Individual
Current assignee: Individual
Priority date: 2020-11-24
Filing date: 2020-11-24
Publication date: 2021-04-02

Abstract

The invention discloses a natural plant aromatic coating balm and a preparation method and application thereof, belonging to the technical field of fine chemical engineering. The preparation method comprises the following steps: melting shea butter, spreading and cooling; picking fresh flowers of the half-opened flowers with dew, and spreading the fresh flowers until the flowers with dew are two thirds of the flowers; taking out pistils, inserting the pistils into the shea butter, spreading petals on the shea butter, placing the shea butter in a closed environment, keeping the temperature constant for 7-9 hours, taking out the pistils and the petals, repeatedly replacing the pistils and the petals to obtain the shea butter with saturated aromatic oil, melting, filtering, cooling, adding ambergris, musk tincture, frankincense, myrrh original essence, agilawood and sandalwood original essence, and sealing and storing. The natural plant aromatic coating paste takes fresh flowers and shea butter as main raw materials, and ambergris, musk, frankincense, myrrh, agilawood and sandalwood are added, so that the effects of clearing and activating the channels and collaterals, promoting blood circulation and supporting yang, inducing resuscitation and refreshing mind, and promoting blood circulation and removing stasis of the aromatic coating paste are effectively assisted.

Description

Natural plant aromatic coating balm and preparation method and application thereof

Technical Field

The invention relates to the technical field of fine chemical engineering, in particular to a natural plant essence-coated balm and a preparation method and application thereof.

Background

The fragrance can bring various pleasant experiences to the sense of smell of people and subtly control the emotion of human beings. For example, the perfume is used as the main component, and the fragrance emitted by the perfume can affect the functions of human viscera and regulate qi, blood and body fluids of human, thereby achieving the purposes of disease prevention, health care, body soothing and spirit soothing. Many fragrances also have sedative and antibacterial effects. Therefore, the fragrance products are produced and used in large quantities.

At present, most balm products are prepared by blending artificial spices and synthetic spices. The balm products have various degrees of injuries to human bodies after long-term smelling no matter how good the fragrance is. Therefore, the development of non-toxic and non-irritant fragrance products from natural plant flowers is a trend of modern technological development. The existing method for extracting volatile oil from natural plants comprises steam distillation method and supercritical CO₂The extraction method, the Soxhlet extraction method, the chemical organic solvent extraction method and the like are long in time consumption and low in extraction rate, and various chemical toxic solvents are not easy to remove completely. For example, the steam distillation method is to distill flowers with steam for 3-6 hours, the distillate needs a large amount of diethyl ether to extract for several times, the extract is dried with chemicals, and then the solvent is distilled off.

Disclosure of Invention

In view of the above, the invention aims to provide a natural plant essence-coated balm, and a preparation method and application thereof.

Through research, the invention provides the following technical scheme:

1. a preparation method of natural plant aromatic coating balm comprises the following steps:

1) after the shea butter is melted, spreading the shea butter, naturally cooling and solidifying the shea butter;

2) selecting high-fragrance fresh flowers with homology of medicine and food, picking half-opened flower bones with dew between 3-4 points in the morning, and then spreading and ventilating until the flower bones with dew naturally bloom to two thirds, and no dew exists;

3) taking out the pistils, inserting the pistils into shea butter, flatly laying the petals on the shea butter with the pistils, then placing the pistils and the petals in a closed environment, keeping the temperature for 7-9 hours, taking out the pistils and the petals, and repeatedly replacing the pistils and the petals 80-100 times to obtain shea butter saturated with aromatic oil;

4) melting shea butter saturated with aromatic oil, filtering, cooling to 40-45 deg.C, adding ambergris, Moschus tincture, Olibanum and Myrrha original essence, lignum Aquilariae Resinatum and lignum Santali albi original essence, and sealing for storage.

Wherein, in the step 3), when the petals are in a rapid withering state, the stamens and the petals are taken out and replaced by new stamens and petals. In the step 3), in a closed environment, the aromatic oil component and the medicinal component in the pistils and the petals can permeate into the shea butter.

Because the aromatic oil components in the pistil and the petals are different, the pistil and the petals need to be separated, then the pistil is inserted on the shea butter, and then the petals are flatly laid on the pistil and the petals, so that the aromatic oil components in the pistil and the petals are adsorbed on the shea butter. In practical experiments, the petals are only flatly laid on the shea butter, the stamen part is discarded, other conditions are the same as those of the petals, and after the petals are sealed for a period of time at constant temperature, the shea butter is found not to be adsorbed to any aromatic oil component. Thus, it is also demonstrated that the fragrance of the aromatic oil in the petals cannot be directly adsorbed onto shea butter, but rather, the aromatic oil in the pistil and petals needs to be adsorbed onto shea butter under the synergistic effect with the pistil.

The frequency of replacing pistils and petals depends on the color of the shea butter, and when the color of the shea butter is changed from white to red, the shea butter can be judged to reach a saturated state.

Preferably, the high-fragrance fresh flower comprises one or more of edible rose, gardenia, jasmine, magnolia, orchid, sweet osmanthus and wintersweet flower.

Preferably, in the step 4), the aromatic oil saturated shea butter, ambergris, musk tincture, frankincense and myrrh original essence, and the agilawood and sandalwood original essence are 1000:1:5:5:5 in parts by weight.

Preferably, the preparation method of ambroxol comprises the following steps: melting ambergris with 95-degree double dealdehyding alcohol solution, and extracting with ice drops to obtain ambergris, wherein the 95-degree double dealdehyding alcohol and water are mixed in the 95-degree double dealdehyding alcohol solution according to the volume ratio of 1: 50.

Preferably, the preparation method of the musk tincture comprises the following steps: soaking musk in 95-degree double dealdehyding alcohol solution in which 95-degree double dealdehyding alcohol and water are mixed in a volume ratio of 1:59 for 1 month to obtain the musk tincture.

Preferably, the preparation method of the frankincense and myrrh original essence comprises the following steps: soaking Olibanum and Myrrha in 95% (v/v) dideal alcohol at a ratio of 3:3:1 for 3 months, distilling at constant temperature, and removing the dideal alcohol.

Preferably, the preparation method of the agilawood and sandalwood original essence comprises the following steps: soaking agilawood and sandalwood in 95-degree dialdehyde alcohol for 3 months, distilling at constant temperature, and removing the dialdehyde alcohol to obtain the agilawood, the sandalwood and the 95-degree dialdehyde alcohol in a weight ratio of 10:5: 100.

Preferably, the melting temperature of the shea butter in the step 1) and the step 4) is 55-65 ℃.

Preferably, the melting temperature of the shea butter in the step 1) and the step 4) is 60 ℃.

Preferably, in the step 3), the constant temperature is 35-40 ℃.

Preferably, in the step 3), the constant temperature is 39 ℃. In tests, the temperature is too low to be beneficial to adsorbing the aromatic oil components in the pistil and the petals by the shea butter, and the pistil and the petals are easy to ripen due to too high temperature, so that oil cells secreting the aromatic oil die quickly, and the aromatic oil in the pistil and the petals cannot be volatilized.

2. The natural plant essence-coated balm prepared by the preparation method.

3. The natural plant aromatic coating balm prepared by the preparation method is applied to the medicines for preventing viruses.

Musk: pungent in flavor, warm in nature, non-toxic, entering twelve meridians. Mainly aversion to qi and ghost evil, poisonous snake poisonous snake poisonous carbuncle deep-rooted carbuncle, middle aversion to heart and abdomen sudden pain and fullness, nebula membrane, tear in eye, wind poisonous wind warm malaria epilepsy, recovery from epilepsy, resuscitation of custom. Musk is the most fragrant, and its qi permeates through bone marrow, so it is not absorbed by meridians.

Sandalwood: [ PROPERTIES, WEI GUIJING ] is pungent and warm. It enters spleen, stomach and lung meridians. [ EFFECT ] the actions of regulating qi, regulating middle energizer, dispersing cold and alleviating pain. [ APPLICATION ] can be used for treating chest and abdomen pain, stomach cold pain, emesis and clear water due to cold accumulation and qi stagnation. It is warm in nature and dispelling cold, pungent in property and capable of dispersing and dispersing, good at promoting diaphragma and relieving chest stuffiness, moving qi and alleviating pain, and fragrant in qi and activating spleen, so it has the actions of regulating middle energizer and harmonizing stomach. It is often combined with Sha ren, Bai Dou kou and Wu Yao, etc. In addition, in recent years, the Chinese medicinal composition is frequently used for treating patients with coronary heart disease with qi stagnation and blood stasis, and is combined with long pepper, rhizoma corydalis, asarum and the like to obtain the broad chest pill, which has a certain effect of relieving angina.

Agilawood: [ PROPERTIES AND FLAVOUR GUIDING CHANNEL ] is pungent, bitter and warm. It is ascribed to the spleen, stomach and kidney meridians. [ EFFECT ] moving qi and relieving pain, lowering adverse qi and regulating middle warmer, warming kidney and receiving qi. [ APPLICATION ] 1) is used for treating cold accumulation, qi stagnation, chest and abdomen distention and stuffiness with pain. The agilawood is spicy and fragrant, can dispel cold in chest and abdomen, and has good effects of promoting qi circulation and relieving pain. It is often combined with Wu Yao, mu Xiang and Bing Lang to obtain Chen Xiang Si Mo Tang. 2) It is indicated for vomiting due to stomach cold and hiccup. It has the actions of lowering temperature and regulating middle energizer. It is combined with herbs such as Ding Xiang, Bai Dou kou and Shi Di. 3) It is indicated for deficiency-cold in the lower-jiao, dyspnea due to deficiency caused by failure of kidney to receive qi, cough and dyspnea due to phlegm-fluid retention, and upper-preponderance and lower-deficiency. For the former, it can be combined with Fu Zi, Rou Gui and Bu Gu Zhi; for the latter, it is often combined with phlegm-resolving and cough-relieving herbs and qi-descending and dyspnea-relieving herbs, such as Su Zi, Qian Hu, Hou Po, Chen Pi and ban Xia. All can take the action of warming kidney and receiving qi.

And (3) rose: [ PROPERTIES AND WESTERN CHANNELS ] is sweet, slightly bitter and warm. It enters liver and spleen meridians. [ EFFECT ] the actions of moving qi and resolving stagnation, regulating blood and dissipating blood stasis. [ APPLICATION ] 1) can be used for treating hypochondriac pain, abdominal distention and pain due to incoordination between liver and stomach. It can move qi and relieve depression, soothe liver and harmonize stomach. It is combined with finger citron, cyperus tuber, curcuma root, etc. 2) Can be used for treating menoxenia, premenstrual breast distending pain, and injury pain due to blood stasis. It can soothe liver and regulate qi, and has the actions of harmonizing blood and dissipating stasis. For regulating menstruation, it can be combined with Angelicae Gigantis radix, rhizoma Ligustici Chuanxiong, radix Paeoniae alba, and herba Lycopi; for blood stasis and pain due to injury, it is combined with spatholobus stem, corydalis tuber and red peony root.

Myrrh: [ PROPERTIES, WESTERN AND CHANNEL FENCH ] is bitter and neutral. It enters heart, liver and spleen meridians. [ EFFECT ] can promote blood circulation, alleviate pain, resolve swelling and promote granulation. [ APPLICATION ] can be used for treating amenorrhea, dysmenorrhea, stomach and abdominal pain, traumatic injury, carbuncle, cellulitis, swelling and pain, and intestinal abscess. It is similar to Ru Xiang in action, so it is often combined with Ru Xiang for the above-mentioned blood stasis and pain syndrome to reinforce the action of activating blood and alleviating pain. Ruxiang excels at activating blood and relaxing tendons, and Mo Yao is good at dissipating blood and resolving stasis. Therefore, frankincense is selected in the juanbi decoction for treating arthralgia syndrome without myrrh; for stomachache due to blood stasis and qi stagnation, myrrh is used instead of frankincense, such as Nippon cantoniensis powder, which is combined with trogopterus dung, corydalis tuber and cyperus tuber. In addition, it is combined with Ru Xiang for its external use and has the action of dispersing swelling and promoting tissue regeneration.

Frankincense: [ PROPERTIES AND WESTERN CHANNELS ] is pungent, bitter, warm in nature and nontoxic. It enters heart, liver and spleen meridians. [ EFFECT ] can promote blood circulation, alleviate pain, resolve swelling and promote granulation. [ APPLICATION ] 1) can be used for treating dysmenorrhea, amenorrhea, gastralgia, rheumatalgia, traumatic injury, carbuncle, cellulitis, swelling and pain, and intestinal abscess. Boswellia carteri, pungent in flavor and warm in nature, can activate blood and resolve stasis, and also can activate qi to dissipate stagnation. It is used for promoting blood circulation and alleviating pain for patients with pain due to stasis in internal, female, external and traumatic clinical departments, and has good effect. For dysmenorrhea and amenorrhea, it is combined with Dang Gui, Chuan Xiong, Xiang Fu, etc.; for epigastric pain, it can be combined with Chuan Meliae, rhizoma corydalis and other products; for arthralgia due to wind-cold-dampness, it is combined with Qiang Huo, Qin jiao, Dang Gui and Hai Feng Teng, as Juan Bi Tang; for blood stasis and pain due to injury, it is combined with Mo Yao, Xue Jie, hong Hua and she Xiang, such as Qili san; for abscess, deep-rooted carbuncle, swelling, toxin, hardness and pain, it is combined with Mo Yao, Xiong Huang and she Xiang, i.e. xing Xiao Wan; for intestinal abscess, it is combined with hong Teng, Zi Hua Di Ding, Lian Qiao and Yin Hua, for instance, hong Teng is decocted. 2) It is indicated for ulcer without recovery after long-term ulceration. It is ground into fine powder together with myrrh, so Haishushan powder, which is applied externally to the affected part, has the effects of relieving swelling and pain, removing necrotic tissue and promoting granulation; it can also be combined with other astringing and tissue regeneration promoting herbs. In addition, it is often used in clinic to be combined with blood-activating and stasis-dissipating or wind-dispelling and pain-relieving herbs to make plaster for application, or applied in lotion, for external use to treat traumatic injuries.

The invention has the beneficial effects that:

1) the natural plant aromatic coating paste takes fresh flowers and shea butter as main raw materials, fragrance components and medicinal components in the flowers are locked by adding ambergris, and musk is added to improve the penetrability of the fragrance and the medicinal components;

2) the preparation method of the natural plant aromatic coating balm is simple to operate, safe and environment-friendly; can also be used as solid perfume or lip gloss and has popularization and application values.

Detailed Description

The technical solutions in the embodiments of the present invention are clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Example 1

1) melting shea butter at a constant temperature of 60 ℃, spreading the shea butter on a glass sheet of a wood frame, and naturally cooling and solidifying the shea butter;

2) selecting medicinal and edible gardenia and jasmine, picking half-blossoming flower bones with dew between 3-4 points in the morning, spreading out, ventilating and paving, wherein 7-9 points in the morning, the half-blossoming flower bones with dew naturally bloom to two thirds, and no dew exists;

3) taking out pistils of the roses, inserting the pistils into shea butter, peeling the petals for standby use, then flatly laying the petals on the shea butter with the pistils until the pistils are completely inserted until the roses are airtight, covering a second glass frame, placing the glass frame in a closed environment, keeping the temperature at 39 ℃ for 8 hours, taking out the pistils and the petals when the petals on the glass are in a quick withering state, and repeatedly replacing the pistils and the petals for 90 times to ensure that the shea butter is completely saturated and adsorbs aromatic oil components and medicinal components in the flowers;

4) melting shea butter saturated with aromatic oil at 60 deg.C, filtering, cooling to 45 deg.C, adding ambergris to lock aroma components, adding Moschus tincture to improve aroma and drug penetration, adding Olibanum and Myrrha, soaking in 95 ° dialdehyde ethanol for 3 months, distilling to obtain Olibanum and Myrrha original extract, adding lignum Aquilariae Resinatum and lignum Santali albi, soaking in 95 ° dialdehyde ethanol for 3 months, distilling to obtain lignum Aquilariae Resinatum and lignum Santali albi original extract, packaging in leak-proof and odor-proof glass bottle, and naturally cooling, sealing and storing.

Experiments prove that the shea butter adsorbing the aromatic oil in the pistil also has the functions of promoting blood circulation, removing blood stasis and dissipating stagnation.

The use method of the natural plant aromatic coating balm comprises the following steps: wiping shea butter on liver and gallbladder channels before sleeping at night; can also be used as solid perfume to be applied to carotid artery and wrist artery; can also be used in place of lip balm.

The above-mentioned embodiments are merely preferred embodiments for fully illustrating the present invention, and the scope of the present invention is not limited thereto. The equivalent substitution or change made by the technical personnel in the technical field on the basis of the invention is all within the protection scope of the invention. The protection scope of the invention is subject to the claims.

Claims

1. A preparation method of natural plant aromatic coating balm is characterized by comprising the following steps:

2. The method of claim 1, wherein the high-scent fresh flowers include one or more of edible rose flowers, gardenia flowers, jasmine flowers, magnolia flowers, orchid flowers, sweet osmanthus flowers and wintersweet flowers.

3. The method for preparing the natural plant essence-coated balm according to claim 1, wherein in the step 4), the aromatic oil-saturated shea butter, ambergris, musk tincture, frankincense and myrrh original essence, and agilawood and sandalwood original essence are 1000:1:5:5:5 in parts by weight.

4. The method for preparing the natural plant essence-coated balm according to claim 3, wherein the method for preparing ambergris comprises the following steps: melting ambergris with 95-degree double dealdehyding alcohol solution, and extracting with ice drops to obtain ambergris, wherein the 95-degree double dealdehyding alcohol and water are mixed in the 95-degree double dealdehyding alcohol solution according to the volume ratio of 1: 50.

5. The preparation method of the natural plant aromatic coating balm according to claim 3, wherein the preparation method of the musk tincture is as follows: soaking musk in 95-degree double dealdehyding alcohol solution in which 95-degree double dealdehyding alcohol and water are mixed in a volume ratio of 1:59 for 1 month to obtain the musk tincture.

6. The method for preparing the natural plant essence-coated balsam according to claim 3, wherein the preparation method of the frankincense and myrrh essence comprises the following steps: soaking Olibanum and Myrrha in 95% (v/v) dideal alcohol at a ratio of 3:3:1 for 3 months, distilling at constant temperature, and removing the dideal alcohol.

7. The method for preparing natural plant essence according to claim 3, wherein the method for preparing the agilawood and sandalwood essence comprises the following steps: soaking agilawood and sandalwood in 95-degree dialdehyde alcohol for 3 months, distilling at constant temperature, and removing the dialdehyde alcohol to obtain the agilawood, the sandalwood and the 95-degree dialdehyde alcohol in a weight ratio of 10:5: 100.

8. The preparation method of the natural plant essence-coated balm according to claim 1, wherein the melting temperature of the shea butter in the steps 1) and 4) is 55-65 ℃.

9. A natural plant essence-coating balm obtained by the production method according to any one of claims 1 to 8.

10. The use of a natural plant balsam obtained by the process according to any one of claims 1 to 8 in the manufacture of a medicament for the prevention of viruses.