CN112553884B - Preparation method of crease-resistant wear-resistant fabric special for outdoor sportswear - Google Patents

Preparation method of crease-resistant wear-resistant fabric special for outdoor sportswear Download PDF

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CN112553884B
CN112553884B CN202011422802.3A CN202011422802A CN112553884B CN 112553884 B CN112553884 B CN 112553884B CN 202011422802 A CN202011422802 A CN 202011422802A CN 112553884 B CN112553884 B CN 112553884B
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fiber
wear
reaction
resistant
wrinkle
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CN112553884A (en
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邱婷
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Zhejiang Lantu Outdoor Products Co ltd
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Zhejiang Lantu Outdoor Products Co ltd
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/38Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
    • AHUMAN NECESSITIES
    • A41WEARING APPAREL
    • A41DOUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
    • A41D31/00Materials specially adapted for outerwear
    • A41D31/04Materials specially adapted for outerwear characterised by special function or use
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    • D03WEAVING
    • D03DWOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
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    • D06M11/68Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
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    • D06M11/76Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
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    • D06M11/77Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144Alcohols; Metal alcoholates
    • D06M13/148Polyalcohols, e.g. glycerol or glucose
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    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/188Monocarboxylic acids; Anhydrides, halides or salts thereof
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    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224Esters of carboxylic acids; Esters of carbonic acid
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    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
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    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/20Treatment influencing the crease behaviour, the wrinkle resistance, the crease recovery or the ironing ease
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    • D06M2200/35Abrasion, pilling or fibrillation resistance
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  • Textile Engineering (AREA)
  • Health & Medical Sciences (AREA)
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Abstract

The invention relates to the technical field of fabric, in particular to a crease-resistant wear-resistant fabric special for outdoor sportswear and a preparation method thereof. The invention firstly takes nano silicon dioxide as a raw material, the nano silicon dioxide is mixed with polyvinylpyrrolidone for reaction, then sodium hydroxide solution is used for etching the surface of the nano silicon dioxide, the nano silicon dioxide with rough surface and porous structure is obtained by sintering and removing the polyvinylpyrrolidone template, then mulberry bark fiber with excellent crease resistance is taken as the raw material, the mulberry bark fiber, sodium polyphosphate, nickel nitrate and alkali liquor are mixed and boiled at high temperature to obtain pretreated mulberry bark fiber, simultaneously, the invention also prepares oily sucrose polyester, finally, the invention mixes the silicon dioxide with rough surface and porous surface with the oily sucrose polyester to prepare impregnation liquid, the pretreated mulberry bark fiber and the impregnation liquid are mixed for high temperature reaction, and finally, the anti-crease wear-resistant fabric is prepared by blending with spandex fiber and polyester fiber.

Description

Preparation method of crease-resistant wear-resistant fabric special for outdoor sportswear
Technical Field
The invention relates to the technical field of fabric fabrics, in particular to a preparation method of a special anti-wrinkle wear-resistant fabric for outdoor sportswear.
Background
With the progress of science and technology and the development of society, the textile technology in China is rapidly developed, and a great deal of novel textile fabrics emerge therewith.
The fabric is used for making clothes, is various in variety, and most of the fabric for making clothes has the characteristics of comfort in wearing, sweat absorption, breathability and the like. With the increasing importance of people on health and sports, the daily wear of clothes is gradually increased; particularly, for some consumers who love fitness and outdoor sports, the requirements on the wear resistance of the fabric of the clothes are higher. However, the existing wear-resistant fabric comprises a base fabric formed by interweaving warp yarns and weft yarns, and the fabric with the structure is poor in air permeability, free of elasticity and easy to damage. Particularly, the fabric of the trousers has the defects of unsatisfactory wear resistance, easy abrasion, unsatisfactory durability, easy wrinkle and use influence. Therefore, the existing clothes fabrics have the problems of unsatisfactory wear resistance, unsatisfactory durability and easy wrinkling.
At present, a common textile fabric can meet the functions of keeping warm and covering skin, and is generally poor in wear resistance. For some special workers, the field environment is severe, and the general textile fabric is difficult to meet the requirements of the environment. And some fabrics appear obvious fold easily when taking out the use after folding and storing, influence the whole effect of surface fabric, are unfavorable for promoting the grade sense of surface fabric.
Therefore, the fabric with the anti-wrinkle and wear-resistant properties specially used for the outdoor sportswear has positive significance in the technical field of textiles.
Disclosure of Invention
The invention aims to provide a crease-resistant wear-resistant fabric special for outdoor sportswear and a preparation method thereof, and aims to solve the problems of unsatisfactory wear resistance, unsatisfactory durability and easiness in wrinkling of the conventional fabric for clothes in the prior art.
In order to achieve the purpose, the invention provides the following technical scheme:
the utility model provides a special crease-resistant wear-resistant surface fabric of outdoor exercises dress, special crease-resistant wear-resistant surface fabric of outdoor exercises dress includes: polyester fiber, self-made wear-resistant crease-resistant fiber and spandex fiber.
The special anti-wrinkle wear-resistant fabric for the outdoor sportswear comprises the following components in parts by weight: 30-40 parts of polyester fiber, 50-60 parts of self-made wear-resistant crease-resistant fiber and 6-8 parts of spandex fiber.
A preparation method of a special anti-wrinkle wear-resistant fabric for outdoor sportswear comprises the following specific preparation steps:
(1) preparing porous nano silicon dioxide;
(2) preparing an upper oily substance;
(3) preparing pretreated mulberry bark fibers;
(4) preparing self-made wear-resistant anti-wrinkle fibers;
(5) the preparation of the special anti-wrinkle wear-resistant fabric for the outdoor sportswear.
A preparation method of a special anti-wrinkle wear-resistant fabric for outdoor sportswear comprises the following specific preparation steps:
(1) preparing porous nano silicon dioxide:
mixing nano silicon dioxide and polyvinylpyrrolidone, putting the mixture into an oil bath pot, raising the temperature of the oil bath pot, and stirring the mixture by using a stirrer for reaction for 3-5 hours to obtain a reaction solution;
mixing a sodium hydroxide solution with the mass concentration of 0.1g/L and the reaction solution, then putting the mixture into an ultrasonic oscillator, carrying out ultrasonic oscillation reaction, filtering and separating after the reaction is finished to obtain reaction filter residue, putting the reaction filter residue into a sintering furnace, sintering for 40-50 min, and discharging to obtain porous nano silicon dioxide;
(2) preparation of the upper oil:
mixing sucrose, potassium oleate, potassium carbonate and methyl oleate, placing the mixture into a three-neck flask, heating, keeping the temperature, reacting, taking out the reactant, standing and layering for 15-20 h, and separating to obtain an upper-layer oily substance;
(3) preparation of pretreated mulberry bark fiber:
mixing the mulberry bark fiber with a sodium hydroxide solution with the mass fraction of 10%, a sodium polyphosphate solution with the mass fraction of 5% and nickel nitrate, transferring the mixture into a high-temperature reaction kettle, carrying out heat preservation and cooking treatment for 2-3 h, filtering and separating after the heat preservation and cooking treatment is finished to obtain cooking filter residue, and drying the cooking filter residue in an oven to obtain pretreated mulberry bark fiber;
(4) preparing self-made wear-resistant anti-wrinkle fiber:
stirring and mixing the porous nano silicon dioxide and the upper-layer oily matter for 10-15 min to obtain a mixed solution, completely immersing the pretreated mulberry bark fiber into the mixed solution, heating, stirring and reacting for 1-2 h, discharging, and naturally drying to obtain the self-made wear-resistant anti-wrinkle fiber;
(5) the preparation of the special anti-wrinkle wear-resistant fabric for the outdoor sportswear comprises the following steps:
weighing polyester fibers, self-made wear-resistant anti-wrinkle fibers and spandex fibers, and weaving the alternate-arrangement wefts of one-way blended spinning of the self-made wear-resistant anti-wrinkle fibers and the spandex fibers and one-way blended spinning of the polyester fibers and the spandex fibers to obtain the anti-wrinkle wear-resistant fabric special for outdoor sportswear.
A preparation method of a special anti-wrinkle wear-resistant fabric for outdoor sportswear comprises the following specific preparation steps:
(1) preparing porous nano silicon dioxide:
mixing nano silicon dioxide and polyvinylpyrrolidone, putting the mixture into an oil bath pot, raising the temperature of the oil bath pot to 100-105 ℃, and stirring and reacting for 3-5 hours by using a stirrer at a rotating speed of 50-60 r/min to obtain a reaction solution;
mixing a sodium hydroxide solution with the mass concentration of 0.1g/L and the reaction liquid according to the volume ratio of 1:4, putting the mixture into an ultrasonic oscillator, carrying out ultrasonic oscillation reaction for 3-4 h at the frequency of 30-40 kHz, filtering and separating after the reaction is finished to obtain reaction filter residue, putting the reaction filter residue into a sintering furnace, sintering for 40-50 min at the temperature of 300-400 ℃, and discharging to obtain porous nano silicon dioxide;
(2) preparation of the upper oil:
mixing sucrose, potassium oleate, potassium carbonate and methyl oleate, placing the mixture into a three-neck flask, heating the mixture to 145-150 ℃, keeping the temperature for reaction for 4-5 hours, taking out the reactant, standing and layering the mixture for 15-20 hours, and separating the mixture to obtain an upper-layer oily substance;
(3) preparation of pretreated mulberry bark fiber:
mixing the mulberry bark fiber with a sodium hydroxide solution with the mass fraction of 10%, a sodium polyphosphate solution with the mass fraction of 5% and nickel nitrate according to the mass ratio of 10:80:10:3, then moving the mixture into a high-temperature reaction kettle, carrying out heat preservation cooking treatment for 2-3 h, after the heat preservation cooking treatment is finished, filtering and separating to obtain cooking filter residue, and drying the cooking filter residue in an oven to obtain the pretreated mulberry bark fiber;
(4) preparing self-made wear-resistant anti-wrinkle fiber:
stirring and mixing the porous nano silicon dioxide and the upper-layer oily matter for 10-15 min according to the mass ratio of 1:15 to obtain a mixed solution, completely soaking the pretreated mulberry bark fiber into the mixed solution, heating, stirring and reacting for 1-2 h, discharging, and naturally drying to obtain the self-made wear-resistant anti-wrinkle fiber;
(5) the preparation of the special anti-wrinkle wear-resistant fabric for the outdoor sportswear comprises the following steps:
weighing 30-40 parts of polyester fiber, 50-60 parts of the self-made wear-resistant anti-wrinkle fiber and 6-8 parts of spandex fiber, and weaving weft yarns which are alternately arranged by one-path blending of the self-made wear-resistant anti-wrinkle fiber and the spandex fiber and one-path blending of the polyester fiber and the spandex fiber to obtain the anti-wrinkle wear-resistant fabric special for the outdoor sportswear.
In the preparation step of the porous nano-silica, the molar ratio of the nano-silica to the polyvinylpyrrolidone is 1: 10.
In the preparation step of the upper-layer oil, the mass ratio of sucrose to potassium oleate to potassium carbonate to methyl oleate is 6:1:1: 47.
In the preparation step of the pretreated mulberry bark fiber in the preferred scheme, the temperature of the heat-preservation steaming treatment is 160-180 ℃.
In the preparation step of the self-made wear-resistant anti-wrinkle fiber in the preferred scheme, the temperature for heating, raising the temperature and stirring the reaction is 160-180 ℃.
In the preparation steps of the crease-resistant wear-resistant fabric special for outdoor sportswear, the feeding length of each yarn during the manufacture is as follows: the high-tenacity fibers are 280-320 mm/100N, the terylene is 270-310 mm/100N, and the spandex is 110-130 mm/100N. Compared with the prior art, the invention has the beneficial effects that:
(1) the invention firstly takes nano silicon dioxide as a raw material, the nano silicon dioxide is mixed with polyvinylpyrrolidone for reaction, the polyvinylpyrrolidone is condensed and attached to the surface of nano silicon dioxide particles, the polyvinylpyrrolidone is taken as a template protection layer, then the surface of the nano silicon dioxide is etched by using a sodium hydroxide solution, the polyvinylpyrrolidone template is removed by sintering, the nano silicon dioxide with rough surface and porous structure is obtained, then the mulberry bark fiber with excellent crease resistance is taken as the raw material, the mulberry bark fiber, sodium polyphosphate, nickel nitrate and alkali liquor are mixed and are subjected to high-temperature alkali boiling, during the alkali boiling process, the sodium polyphosphate solution can integrate metal nickel ions of the solution around the mulberry bark cellulose and can be combined with hydroxyl in the mulberry bark cellulose, the gap of the rough part of the cotton and hemp fiber is filled, and the rough feeling of the cotton and hemp fiber is improved, the production of short fibers is reduced, the smoothness of the fabric is improved, wrinkling is avoided, the mechanical strength of the mulberry bark fiber filled with metal ions is improved, the wear resistance is obviously improved, meanwhile, the oily sucrose polyester is prepared, finally, the silica with rough and porous surfaces and the oily sucrose polyester are mixed to prepare impregnation liquid, the pretreated mulberry bark fiber and the impregnation liquid are mixed and then are subjected to high-temperature reaction, the silicon hydroxyl on the surface of the nano silica and the hydroxyl on the surface of the pretreated mulberry bark fiber are subjected to dehydration condensation or other chemical bonding force through high temperature, so that the nano silica is attached to the surface of the fiber, and finally, the nano silica is blended with spandex fiber and polyester fiber to prepare the anti-wrinkle wear-resistant fabric;
(2) in addition, the nano silicon dioxide attached to the surface of the mulberry bark fiber in the fabric has high mechanical strength, the wear resistance of the fabric fiber can be improved preliminarily, the silicon dioxide can be used as soft particles, when the fabric fiber and other interfaces move relatively, the nano silicon dioxide on the surface of the fabric moves microscopically such as extrusion, deformation, sliding and rolling, the friction coefficient among fibers is reduced, the internal energy loss of the fabric is prevented, and the wear resistance of the fabric is improved again.
Detailed Description
Preparing porous nano silicon dioxide:
(1) mixing nano silicon dioxide and polyvinylpyrrolidone according to a molar ratio of 1:10, putting the mixture into an oil bath pot, raising the temperature of the oil bath pot to 100-105 ℃, and stirring and reacting for 3-5 hours by using a stirrer at a rotating speed of 50-60 r/min to obtain a reaction solution;
(2) mixing a sodium hydroxide solution with the mass concentration of 0.1g/L and the reaction liquid according to the volume ratio of 1:4, putting the mixture into an ultrasonic oscillator, carrying out ultrasonic oscillation reaction for 3-4 h at the frequency of 30-40 kHz, filtering and separating after the reaction is finished to obtain reaction filter residue, putting the reaction filter residue into a sintering furnace, sintering for 40-50 min at the temperature of 300-400 ℃, and discharging to obtain porous nano silicon dioxide for later use;
preparation of the upper oil:
mixing sucrose, potassium oleate, potassium carbonate and methyl oleate according to the mass ratio of 6:1:1:47, placing the mixture into a three-neck flask, heating to 145-150 ℃, keeping the temperature for reaction for 4-5 hours, taking out the reactant, standing for layering for 15-20 hours, and separating to obtain an upper-layer oily substance;
preparation of pretreated mulberry bark fiber:
mixing the mulberry bark fiber with a sodium hydroxide solution with the mass fraction of 10%, a sodium polyphosphate solution with the mass fraction of 5% and nickel nitrate according to the mass ratio of 10:80:10:3, then transferring the mixture into a high-temperature reaction kettle, carrying out heat preservation and cooking treatment for 2-3 h at 160-180 ℃, after the heat preservation and cooking treatment is finished, filtering and separating to obtain a cooking filter residue, and drying the cooking filter residue in an oven to obtain the pretreated mulberry bark fiber;
preparing self-made wear-resistant anti-wrinkle fiber:
stirring and mixing the porous nano silicon dioxide and the upper-layer oily matter for 10-15 min according to the mass ratio of 1:15 to obtain a mixed solution, completely soaking the pretreated mulberry bark fiber into the mixed solution, heating to 160-180 ℃, stirring for reaction for 1-2 h, discharging, and naturally drying to obtain the self-made wear-resistant anti-wrinkle fiber;
the preparation of the special anti-wrinkle wear-resistant fabric for the outdoor sportswear comprises the following steps:
weighing 30-40 parts of polyester fiber, 50-60 parts of the self-made wear-resistant anti-wrinkle fiber and 6-8 parts of spandex fiber, and alternately arranging weft yarns of one-path blending of the self-made wear-resistant anti-wrinkle fiber and the spandex fiber and one-path blending of the polyester fiber and the spandex fiber, wherein the feeding length of each yarn is as follows: the high-tenacity fibers are 280-320 mm/100N, the terylene is 270-310 mm/100N, the spandex is 110-130 mm/100N, and the special crease-resistant wear-resistant fabric for the outdoor sportswear is woven.
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
Preparing porous nano silicon dioxide:
(1) mixing nano silicon dioxide and polyvinylpyrrolidone according to a molar ratio of 1:10, putting the mixture into an oil bath pot, raising the temperature of the oil bath pot to 100 ℃, and stirring the mixture by using a stirrer at a rotating speed of 50r/min for reaction for 3 hours to obtain a reaction solution;
(2) mixing a sodium hydroxide solution with the mass concentration of 0.1g/L and the reaction liquid according to the volume ratio of 1:4, putting the mixture into an ultrasonic oscillator, carrying out ultrasonic oscillation reaction for 3 hours at the frequency of 30kHz, filtering and separating after the reaction is finished to obtain reaction filter residue, putting the reaction filter residue into a sintering furnace, sintering for 40 minutes at the temperature of 300 ℃, and discharging to obtain porous nano silicon dioxide for later use;
preparation of the upper oil:
mixing sucrose, potassium oleate, potassium carbonate and methyl oleate according to the mass ratio of 6:1:1:47, placing the mixture into a three-neck flask, heating to 145 ℃, keeping the temperature for reaction for 4 hours, taking out the reactant, standing for layering for 15 hours, and separating to obtain an upper-layer oily substance;
preparation of pretreated mulberry bark fiber:
mixing the mulberry bark fiber with a sodium hydroxide solution with the mass fraction of 10%, a sodium polyphosphate solution with the mass fraction of 5% and nickel nitrate according to the mass ratio of 10:80:10:3, then moving the mixture into a high-temperature reaction kettle, carrying out heat preservation and cooking treatment for 2 hours at 160 ℃, filtering and separating to obtain cooking filter residue after the heat preservation and cooking treatment is finished, and drying the filter residue in an oven to obtain the pretreated mulberry bark fiber;
preparing self-made wear-resistant anti-wrinkle fiber:
stirring and mixing the porous nano silicon dioxide and the upper-layer oily matter for 10min according to the mass ratio of 1:15 to obtain a mixed solution, completely soaking the pretreated mulberry bark fiber into the mixed solution, heating to 160 ℃, stirring for reaction for 1h, discharging, and naturally drying to obtain the self-made wear-resistant anti-wrinkle fiber;
the preparation of the special anti-wrinkle wear-resistant fabric for the outdoor sportswear comprises the following steps:
weighing 30 parts of polyester fiber, 50 parts of the self-made wear-resistant anti-wrinkle fiber and 6 parts of spandex fiber, and alternately arranging all weft yarns of one-path blended spinning of the self-made wear-resistant anti-wrinkle fiber and the spandex fiber and one-path blended spinning of the polyester fiber and the spandex fiber, wherein the feeding length of each weft yarn is as follows: the rich fiber is 280mm/100N, the polyester is 270mm/100N, and the spandex is 110mm/100N, so that the special anti-wrinkle wear-resistant fabric for the outdoor sportswear is woven.
Example 2
Preparing porous nano silicon dioxide:
(1) mixing nano silicon dioxide and polyvinylpyrrolidone according to a molar ratio of 1:10, putting the mixture into an oil bath pot, raising the temperature of the oil bath pot to 103 ℃, and stirring and reacting for 4 hours by using a stirrer at a rotating speed of 55r/min to obtain a reaction solution;
(2) mixing a sodium hydroxide solution with the mass concentration of 0.1g/L and the reaction liquid according to the volume ratio of 1:4, putting the mixture into an ultrasonic oscillator, carrying out ultrasonic oscillation reaction for 3 hours at the frequency of 35kHz, filtering and separating after the reaction is finished to obtain reaction filter residue, putting the reaction filter residue into a sintering furnace, sintering for 45 minutes at the temperature of 350 ℃, and discharging to obtain porous nano silicon dioxide for later use;
preparation of the upper oil:
mixing sucrose, potassium oleate, potassium carbonate and methyl oleate according to the mass ratio of 6:1:1:47, placing the mixture into a three-neck flask, heating the mixture to 148 ℃, keeping the temperature for reaction for 4 hours, taking out the reactant, standing and layering the mixture for 18 hours, and separating the mixture to obtain an upper-layer oily substance;
preparation of pretreated mulberry bark fiber:
mixing the mulberry bark fiber with a sodium hydroxide solution with the mass fraction of 10%, a sodium polyphosphate solution with the mass fraction of 5% and nickel nitrate according to the mass ratio of 10:80:10:3, then moving the mixture into a high-temperature reaction kettle, carrying out heat preservation and cooking treatment for 2 hours at 170 ℃, filtering and separating to obtain cooking filter residue after the heat preservation and cooking treatment is finished, and drying the filter residue in an oven to obtain the pretreated mulberry bark fiber;
preparing self-made wear-resistant anti-wrinkle fiber:
stirring and mixing the porous nano silicon dioxide and the upper-layer oily matter for 13min according to the mass ratio of 1:15 to obtain a mixed solution, completely immersing the pretreated mulberry bark fiber into the mixed solution, heating to 170 ℃, stirring for reaction for 2h, discharging, and naturally drying to obtain the self-made wear-resistant anti-wrinkle fiber;
the preparation of the special anti-wrinkle wear-resistant fabric for the outdoor sportswear comprises the following steps:
weighing 35 parts of polyester fiber, 55 parts of the self-made wear-resistant anti-wrinkle fiber and 7 parts of spandex fiber, and alternately arranging all weft yarns of one-path blended spinning of the self-made wear-resistant anti-wrinkle fiber and the spandex fiber and one-path blended spinning of the polyester fiber and the spandex fiber, wherein the feeding length of each weft yarn is as follows: the rich-strong fiber is 300mm/100N, the terylene is 285mm/100N, and the spandex is 120mm/100N, so that the special anti-wrinkle wear-resistant fabric for the outdoor sportswear is woven.
Example 3
Preparing porous nano silicon dioxide:
(1) mixing nano silicon dioxide and polyvinylpyrrolidone according to a molar ratio of 1:10, putting the mixture into an oil bath pot, raising the temperature of the oil bath pot to 105 ℃, and stirring and reacting for 5 hours by using a stirrer at a rotating speed of 60r/min to obtain a reaction solution;
(2) mixing a sodium hydroxide solution with the mass concentration of 0.1g/L and the reaction solution according to the volume ratio of 1:4, putting the mixture into an ultrasonic oscillator, carrying out ultrasonic oscillation reaction for 4 hours at the frequency of 40kHz, filtering and separating after the reaction is finished to obtain reaction filter residue, putting the reaction filter residue into a sintering furnace, sintering for 50 minutes at the temperature of 400 ℃, and discharging to obtain porous nano silicon dioxide for later use;
preparation of the upper oil:
mixing sucrose, potassium oleate, potassium carbonate and methyl oleate according to the mass ratio of 6:1:1:47, placing the mixture into a three-neck flask, heating to 150 ℃, keeping the temperature for 5 hours for reaction, taking out the reactant, standing for layering for 20 hours, and separating to obtain an upper-layer oily substance;
preparation of pretreated mulberry bark fiber:
mixing the mulberry bark fiber with a sodium hydroxide solution with the mass fraction of 10%, a sodium polyphosphate solution with the mass fraction of 5% and nickel nitrate according to the mass ratio of 10:80:10:3, then transferring the mixture into a high-temperature reaction kettle, carrying out heat preservation and cooking treatment for 3 hours at 180 ℃, filtering and separating to obtain cooking filter residue after the heat preservation and cooking treatment is finished, and drying the filter residue in an oven to obtain the pretreated mulberry bark fiber;
preparing self-made wear-resistant anti-wrinkle fiber:
stirring and mixing the porous nano silicon dioxide and the upper-layer oily matter for 15min according to the mass ratio of 1:15 to obtain a mixed solution, completely soaking the pretreated mulberry bark fiber into the mixed solution, heating to 180 ℃, stirring for reaction for 2h, discharging, and naturally drying to obtain the self-made wear-resistant anti-wrinkle fiber;
the preparation of the special anti-wrinkle wear-resistant fabric for the outdoor sportswear comprises the following steps:
weighing 40 parts of polyester fiber, 60 parts of the self-made wear-resistant anti-wrinkle fiber and 8 parts of spandex fiber, and alternately arranging all weft yarns of one-path blended spinning of the self-made wear-resistant anti-wrinkle fiber and the spandex fiber and one-path blended spinning of the polyester fiber and the spandex fiber, wherein the feeding length of each weft yarn is as follows: the rich-strength fiber is 320mm/100N, the terylene is 310mm/100N, and the spandex is 130mm/100N, so that the special anti-wrinkle wear-resistant fabric for outdoor sportswear is woven.
Comparative example 1: the preparation method is basically the same as that of the embodiment 1 of the invention, the only difference is that the impregnation reaction is carried out on the pretreated mulberry bark fiber without preparing the mixed solution of the porous nano silicon dioxide prepared by the invention and the last oily matter, and other steps are the same;
comparative example 2: the preparation method is basically the same as that of the example 1 of the invention, and the only difference is that the ordinary plant fiber is used for replacing the self-made wear-resistant anti-wrinkle fiber prepared by the invention, and the other preparation steps are the same as those in the example 1;
the performance of the crease-resistant wear-resistant fabric special for outdoor sportswear and the performance of the fabric prepared in the comparative example are respectively detected, and the detection results are shown in table 1:
the detection method comprises the following steps:
and (3) wear resistance test:
reference is made to GB/T21196.2-2007 determination of abrasion resistance of fabrics by the Martindall method part 2: determination of sample breakage and GB/T21196.4-2007 determination of abrasion resistance of fabrics by the Martindall method part 4: evaluation of appearance Change A model YG401 flat grinder with a weight 250g, 240 pieces/cm 2 sandpaper at 300 revolutions was used under a standard three-stage atmospheric pressure. And (4) weighing the mass and thickness difference between the ground material and the ground material by adopting a TG328A analytical balance, and calculating the mass and thickness loss rate.
And (3) wrinkle resistance detection:
the detection is carried out according to GB/T3819-1997 method for measuring the recovery angle of crease recovery of textile fabrics.
Table 1 results of performance testing:
Figure DEST_PATH_IMAGE001
as can be seen from the detection data in the table above, in comparative example 1 of the present invention, since the fabric is not impregnated with the mixed solution of the porous nano-silica prepared by the present invention and the upper oily substance, the wear quality loss rate becomes large, and the recovery angle becomes small, in comparative example 2, since the home-made wear-resistant anti-wrinkle fiber prepared by the present invention is replaced with the common plant fiber, the final wear quality loss becomes large, and the recovery angle decreases, so that it can be seen that the use of the porous nano-silica prepared by the present invention and the home-made wear-resistant anti-wrinkle fiber indeed improves the wear resistance and anti-wrinkle property of the wear-resistant fabric special for outdoor sportswear of the present invention, and has a wide application prospect.

Claims (1)

1. A preparation method of a special anti-wrinkle wear-resistant fabric for outdoor sportswear is characterized by comprising the following steps: the preparation method comprises the following specific steps:
(1) preparing porous nano silicon dioxide:
mixing nano silicon dioxide and polyvinylpyrrolidone according to a molar ratio of 1:10, putting the mixture into an oil bath pot, raising the temperature of the oil bath pot to 103 ℃, and stirring and reacting for 4 hours by using a stirrer at a rotating speed of 55r/min to obtain a reaction solution;
mixing a sodium hydroxide solution with the mass concentration of 0.1g/L and the reaction liquid according to the volume ratio of 1:4, putting the mixture into an ultrasonic oscillator, carrying out ultrasonic oscillation reaction for 3 hours at the frequency of 35kHz, filtering and separating after the reaction is finished to obtain reaction filter residue, putting the reaction filter residue into a sintering furnace, sintering for 45 minutes at the temperature of 350 ℃, and discharging to obtain porous nano silicon dioxide for later use;
(2) preparation of the upper oil:
mixing sucrose, potassium oleate, potassium carbonate and methyl oleate according to the mass ratio of 6:1:1:47, placing the mixture into a three-neck flask, heating the mixture to 148 ℃, keeping the temperature for reaction for 4 hours, taking out the reactant, standing and layering the mixture for 18 hours, and separating the mixture to obtain an upper-layer oily substance;
(3) preparation of pretreated mulberry bark fiber:
mixing the mulberry bark fiber with a sodium hydroxide solution with the mass fraction of 10%, a sodium polyphosphate solution with the mass fraction of 5% and nickel nitrate according to the mass ratio of 10:80:10:3, then moving the mixture into a high-temperature reaction kettle, carrying out heat preservation and cooking treatment for 2 hours at 170 ℃, filtering and separating to obtain cooking filter residue after the heat preservation and cooking treatment is finished, and drying the filter residue in an oven to obtain the pretreated mulberry bark fiber;
(4) preparing self-made wear-resistant anti-wrinkle fiber:
stirring and mixing the porous nano silicon dioxide and the upper-layer oily matter for 13min according to the mass ratio of 1:15 to obtain a mixed solution, completely immersing the pretreated mulberry bark fiber into the mixed solution, heating to 170 ℃, stirring for reaction for 2h, discharging, and naturally drying to obtain the self-made wear-resistant anti-wrinkle fiber;
(5) the preparation of the special anti-wrinkle wear-resistant fabric for the outdoor sportswear comprises the following steps:
weighing 35 parts of polyester fiber, 55 parts of the self-made wear-resistant anti-wrinkle fiber and 7 parts of spandex fiber, and alternately arranging all weft yarns of one-path blended spinning of the self-made wear-resistant anti-wrinkle fiber and the spandex fiber and one-path blended spinning of the polyester fiber and the spandex fiber, wherein the feeding length of each weft yarn is as follows: the rich-strong fiber is 300mm/100N, the terylene is 285mm/100N, and the spandex is 120mm/100N, so that the special anti-wrinkle wear-resistant fabric for the outdoor sportswear is woven.
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