CN112522723A - Water-soluble precision cleaning solution and preparation method thereof - Google Patents
Water-soluble precision cleaning solution and preparation method thereof Download PDFInfo
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- CN112522723A CN112522723A CN202011306142.2A CN202011306142A CN112522723A CN 112522723 A CN112522723 A CN 112522723A CN 202011306142 A CN202011306142 A CN 202011306142A CN 112522723 A CN112522723 A CN 112522723A
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/24—Cleaning or pickling metallic material with solutions or molten salts with neutral solutions
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Abstract
The invention provides a water-soluble precise cleaning solution and a preparation method thereof, wherein the preparation method comprises the steps of preparing raw materials, cleaning a reaction kettle, adding water into the reaction kettle after cleaning, and starting the reaction kettle for stirring; sequentially adding sodium gluconate, sodium metasilicate pentahydrate, sodium citrate and sodium dodecyl benzene sulfonate into a reaction kettle, stirring, and stirring until the sodium gluconate, the sodium metasilicate pentahydrate, the sodium citrate and the sodium dodecyl benzene sulfonate are completely dissolved; dissolving in a reaction kettle, sequentially adding TX-10, RQ-139CE and AEO-9 into the reaction kettle, uniformly stirring, sequentially adding ethylene oxide propylene oxide copolymerized polyoxyethylene ether and fatty alcohol polyoxyethylene ether sodium sulfate into the reaction kettle, and uniformly stirring until all raw materials are uniformly mixed; after the raw materials are completely mixed, sampling and detecting the stirred raw materials; and barreling the uniformly stirred raw materials. The invention effectively improves the cleaning effect of the cleaning solution, and has water solubility, thereby reducing the pollution of the waste cleaning solution to the environment.
Description
Technical Field
The invention belongs to the technical field of cleaning solutions, and particularly relates to a water-soluble precision cleaning solution and a preparation method thereof.
Background
The metal material needs to be cleaned before being processed, and the consumption of common mechanical parts and precision components used in other fields prepared by processing the metal material is quite large, so the workload for cleaning the metal parts is correspondingly large, and the consumption of cleaning solution required in the cleaning process is quite large.
With the strictness of the environmental protection requirement standards, the emission control of industrial wastewater is more and more strict, so that the emission of a large amount of waste cleaning agents becomes an important subject to be researched by the industry. The cleaning effect of the existing cleaning solution is not ideal, the cleaned metal parts are easy to have black surface layers, which brings troubles to subsequent processing, particularly causes confusion to the processing of precise components, and the cleaning time is long.
Therefore, there is a need for a water-soluble precision cleaning solution and a preparation method thereof, which can reduce the pollution of the waste cleaning solution to the environment and effectively improve the cleaning effect.
Disclosure of Invention
In order to solve the technical problems, the invention provides a water-soluble precision cleaning solution and a preparation method thereof, the formula of the water-soluble precision cleaning solution comprises water, sodium gluconate, sodium metasilicate pentahydrate, sodium citrate, sodium dodecyl benzene sulfonate, TX-10, RQ-139CE, AEO-9, ethylene oxide propylene oxide copolymerized polyoxyethylene ether and fatty alcohol polyoxyethylene ether sodium sulfate, and the preparation method of the precision cleaning solution comprises the following steps:
the method comprises the following steps: pretreatment: preparing raw materials, cleaning a reaction kettle, adding water into the reaction kettle after cleaning, and starting the reaction kettle for stirring;
step two: sequentially adding sodium gluconate, sodium metasilicate pentahydrate, sodium citrate and sodium dodecyl benzene sulfonate into a reaction kettle, stirring, and stirring until the sodium gluconate, the sodium metasilicate pentahydrate, the sodium citrate and the sodium dodecyl benzene sulfonate are completely dissolved;
step three: after the sodium gluconate, sodium metasilicate pentahydrate, sodium citrate and sodium dodecyl benzene sulfonate are completely dissolved in the reaction kettle, sequentially adding TX-10, RQ-139CE and AEO-9 into the reaction kettle, uniformly stirring, then sequentially adding ethylene oxide propylene oxide copolymerized polyoxyethylene ether and fatty alcohol polyoxyethylene ether sodium sulfate into the reaction kettle, and uniformly stirring until all the raw materials are uniformly mixed;
step four: after the raw materials are completely mixed, sampling and detecting the stirred raw materials;
step five: and barreling the uniformly stirred raw materials.
Preferably, the TX-10 is alkylphenol polyoxyethylene ether, is an emulsifier and is easily soluble in water.
Preferably, the RQ-139CE is a nonionic surfactant.
Preferably, AEO-9 is fatty alcohol-polyoxyethylene ether, is a nonionic surfactant and has excellent water solubility.
Preferably, the raw materials are uniformly stirred in the third step until the raw materials are completely and uniformly mixed, and the uniformly mixed raw materials are transparent.
Preferably, the volume of the barrel in the barrel filling process is 200L.
Compared with the prior art, the invention has the beneficial effects that: according to the invention, TX-10 is added into the formula, the TX-10 has excellent emulsifying and cleaning capabilities and is one of important components of a synthetic detergent, the added RQ-139CE is phosphorus-free, has excellent water-washing performance and matching performance, is electrolyte-resistant and concentrated alkali-resistant, the added AEO-9 has excellent emulsifying, dirt-removing and cleaning performances and the like, the cleaning effect of the cleaning solution is effectively improved, and the water solubility can reduce the pollution to the environment caused by the treatment and discharge of the waste cleaning solution.
Drawings
FIG. 1 is a diagram of the preparation steps of the present invention.
Detailed Description
The invention is further described below with reference to the accompanying drawings:
example 1:
a water-soluble precision cleaning solution and its preparation method, its formulation includes water, sodium gluconate, sodium metasilicate pentahydrate, sodium citrate, sodium dodecylbenzene sulfonate, TX-10, RQ-139CE, AEO-9, ethylene oxide propylene oxide copolymerized polyoxyethylene ether, sodium fatty alcohol polyoxyethylene ether sulfate, said TX-10 is alkylphenol polyoxyethylene ether, it is an emulsifier, it is easy to dissolve in water; said RQ-139CE is a nonionic surfactant; the AEO-9 is fatty alcohol-polyoxyethylene ether, is a nonionic surfactant, has excellent water solubility, effectively improves the cleaning effect of the cleaning solution, and can reduce the pollution to the environment caused by the treatment and discharge of the waste cleaning solution due to the water solubility.
As shown in the attached figure 1, the preparation method of the precision cleaning solution comprises the following steps:
(1) pretreatment: preparing water, sodium gluconate, sodium metasilicate pentahydrate, sodium citrate, sodium dodecyl benzene sulfonate, TX-10, RQ-139CE, AEO-9, ethylene oxide propylene oxide copolymerized polyoxyethylene ether and fatty alcohol polyoxyethylene ether sodium sulfate, cleaning a reaction kettle after preparation, firstly adding water into the reaction kettle after cleaning, and starting the reaction kettle for stirring;
(2) sequentially adding sodium gluconate, sodium metasilicate pentahydrate, sodium citrate and sodium dodecyl benzene sulfonate into a reaction kettle, stirring until the sodium gluconate, the sodium metasilicate pentahydrate, the sodium citrate and the sodium dodecyl benzene sulfonate are completely dissolved in water;
(3) after the sodium gluconate, sodium metasilicate pentahydrate, sodium citrate and sodium dodecyl benzene sulfonate are completely dissolved in the reaction kettle, sequentially adding TX-10, RQ-139CE and AEO-9 into the reaction kettle, uniformly stirring, then sequentially adding ethylene oxide propylene oxide copolymerized polyoxyethylene ether and fatty alcohol polyoxyethylene ether sodium sulfate into the reaction kettle, uniformly stirring until all the raw materials are uniformly mixed until the raw materials are uniformly mixed into transparent liquid;
(4) after the raw materials are completely mixed, sampling and detecting the stirred transparent liquid;
(5) after sampling is qualified, the stirred transparent liquid, namely the cleaning solution, is barreled, wherein the volume of the barrel is 220L.
The technical solutions of the present invention or similar technical solutions designed by those skilled in the art based on the teachings of the technical solutions of the present invention are all within the scope of the present invention.
Claims (6)
1. The water-soluble precision cleaning solution is characterized by comprising water, sodium gluconate, sodium metasilicate pentahydrate, sodium citrate, sodium dodecyl benzene sulfonate, TX-10, RQ-139CE, AEO-9, ethylene oxide propylene oxide copolymerized polyoxyethylene ether and fatty alcohol polyoxyethylene ether sodium sulfate, and the preparation method comprises the following steps:
the method comprises the following steps: pretreatment: preparing raw materials, cleaning a reaction kettle, adding water into the reaction kettle after cleaning, and starting the reaction kettle for stirring;
step two: sequentially adding sodium gluconate, sodium metasilicate pentahydrate, sodium citrate and sodium dodecyl benzene sulfonate into a reaction kettle, stirring, and stirring until the sodium gluconate, the sodium metasilicate pentahydrate, the sodium citrate and the sodium dodecyl benzene sulfonate are completely dissolved;
step three: after the sodium gluconate, sodium metasilicate pentahydrate, sodium citrate and sodium dodecyl benzene sulfonate are completely dissolved in the reaction kettle, sequentially adding TX-10, RQ-139CE and AEO-9 into the reaction kettle, uniformly stirring, then sequentially adding ethylene oxide propylene oxide copolymerized polyoxyethylene ether and fatty alcohol polyoxyethylene ether sodium sulfate into the reaction kettle, and uniformly stirring until all the raw materials are uniformly mixed;
step four: after the raw materials are completely mixed, sampling and detecting the stirred raw materials;
step five: and barreling the uniformly stirred raw materials.
2. The precise water-soluble detergent according to claim 1, wherein said TX-10 is alkylphenol ethoxylate, which is an emulsifier, and is easily soluble in water.
3. The precision water-soluble cleaning solution according to claim 1 wherein said RQ-139CE is a nonionic surfactant.
4. The water-soluble precision cleaning solution as claimed in claim 1, wherein said AEO-9 is fatty alcohol polyoxyethylene ether, is a nonionic surfactant, and has excellent water solubility.
5. The water-soluble precision cleaning solution as claimed in claim 1, wherein the above-mentioned step three is carried out by stirring until the raw materials are completely mixed, and the mixed raw materials are transparent.
6. The water-soluble precision cleaning solution according to claim 1 wherein the volume of said barrel in said barrel-filling treatment is 200L.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN202011306142.2A CN112522723A (en) | 2020-11-20 | 2020-11-20 | Water-soluble precision cleaning solution and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202011306142.2A CN112522723A (en) | 2020-11-20 | 2020-11-20 | Water-soluble precision cleaning solution and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113789234A (en) * | 2021-10-13 | 2021-12-14 | 常州智高化学科技有限公司 | Water-based water-soluble precision cleaning solution and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5734029A (en) * | 1991-10-10 | 1998-03-31 | Henkel Corporation | Preparation of improved alkypolygloycoside surfactant mixtures |
| CN104562059A (en) * | 2014-11-27 | 2015-04-29 | 镇江润德节能科技有限公司 | Preparation method of industrial water-base detergent for metals |
| CN105331995A (en) * | 2015-10-19 | 2016-02-17 | 江南工业集团有限公司 | Environment-friendly industrial cleaning agent |
| CN109338384A (en) * | 2018-12-10 | 2019-02-15 | 徐州特普勒金属科技有限公司 | A kind of water base metal cleaning agent and preparation method thereof |
-
2020
- 2020-11-20 CN CN202011306142.2A patent/CN112522723A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5734029A (en) * | 1991-10-10 | 1998-03-31 | Henkel Corporation | Preparation of improved alkypolygloycoside surfactant mixtures |
| CN104562059A (en) * | 2014-11-27 | 2015-04-29 | 镇江润德节能科技有限公司 | Preparation method of industrial water-base detergent for metals |
| CN105331995A (en) * | 2015-10-19 | 2016-02-17 | 江南工业集团有限公司 | Environment-friendly industrial cleaning agent |
| CN109338384A (en) * | 2018-12-10 | 2019-02-15 | 徐州特普勒金属科技有限公司 | A kind of water base metal cleaning agent and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113789234A (en) * | 2021-10-13 | 2021-12-14 | 常州智高化学科技有限公司 | Water-based water-soluble precision cleaning solution and preparation method thereof |
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