CN112516035A

CN112516035A - Cherry blossom nourishing and repairing hair conditioner and preparation method thereof

Info

Publication number: CN112516035A
Application number: CN202011533541.2A
Authority: CN
Inventors: 陈出新
Original assignee: Hubei Yanzhuang Industrial Co ltd
Current assignee: Hubei Yanzhuang Industrial Co ltd
Priority date: 2020-12-23
Filing date: 2020-12-23
Publication date: 2021-03-19

Abstract

The invention relates to a cherry blossom nourishing and repairing hair conditioner and a preparation method thereof, wherein the hair conditioner comprises, by weight, 0.1-1.0 part of polyquaternium-67, 0.05-1.0 part of cherry blossom extract, 0.1-2.0 parts of film forming agent, 0.01-0.3 part of chelating agent, 1.01-10.8 parts of humectant, 0.5-5.0 parts of cetearyl alcohol, 1-8 parts of emulsifier, 0.7-10.0 parts of fat-increasing agent, 0.001-1.0 part of citric acid, 60-90 parts of water and 0.75-17.4 parts of additive. The cherry blossom extract, the quaternary ammonium salt-67 and the specific film-forming agent are combined in a specific ratio to generate the hair conditioner with the function of repairing and nourishing damaged ends, and the hair conditioner has good effects of repairing, nourishing and damaged hair and preventing excessive dryness of hair; the shampoo has the effects of relieving scalp allergy caused by substances such as surfactant, antiseptic and the like in the hair washing process, effectively removing dandruff, relieving itching and preventing alopecia, and simultaneously all the components cooperate with each other, so that the oil-water phase can effectively ensure the stability of the whole hair conditioner system.

Description

Cherry blossom nourishing and repairing hair conditioner and preparation method thereof

Technical Field

The invention relates to the technical field of daily chemicals, and particularly relates to a cherry blossom nourishing and repairing hair conditioner and a preparation method thereof.

Background

With the improvement of the living standard of residents, the increasing popularity of hair perming and hair dyeing and the factors of environment, pressure and the like cause the common malnutrition of hair roots and hair of people, and then the hair becomes thinner, dry and even becomes crisp and falls off. And as the length of the hair is increased, the hair scale cells are partially shed, the hair is poor in flexibility and easy to twist, so that the hair is easy to knot and break in the combing and washing processes. Therefore, the hair care product becomes one of the necessities of modern families.

The hair conditioner has the effects that after the head is washed by products such as shampoo and the like, the residual detergent on the head is neutralized and taken away, the scalp stimulated by the surfactant is relieved, the scalp is nourished, a certain film effect is formed to carry out moisture preservation and nursing on the scalp and the hair, the tangled hair is smooth and easy to comb, a certain sun-screening effect is provided, hair fiber damage is prevented, and certain brightness and elasticity are endowed. With the development of technology, people are demanding hair care products which, in addition to the above, also have the functions of repairing hair damage to some extent, as well as dressing and fixing hair style.

Hair care compositions having a variety of characteristics are attractive to consumers because they require less composition to be applied to the hair to achieve the desired effect. However, in order to formulate such hair care compositions, multiple components are often necessary. The long-term stability of such compositions may be compromised by incompatibility between the various components. Furthermore, because of the large number of components in many hair care compositions, formulators are faced with the challenge of not only finding suitable components to provide desired cosmetic properties, but also of manufacturing these complex compositions.

Disclosure of Invention

The invention aims to provide a cherry blossom nourishing and repairing hair conditioner and a preparation method thereof, and the hair conditioner has good effects of repairing, nourishing and damaging damaged hair and preventing excessive dryness of hair by optimizing a product formula. The hair conditioner prepared by the invention has stable physical and chemical properties.

In order to realize the purpose, the invention is realized by the following technical scheme:

the first purpose of the invention is to provide a cherry blossom nourishing and repairing hair conditioner, which comprises 0.1-1.0 part of polyquaternium-67, 0.05-1.0 part of cherry blossom extract, 0.1-2.0 parts of film forming agent, 0.01-0.3 part of chelating agent, 1.01-10.8 parts of humectant, 0.5-5.0 parts of cetostearyl alcohol, 1-8 parts of emulsifier, 0.7-10.0 parts of fat-increasing agent, 0.001-1.0 part of citric acid, 60-90 parts of water and 0.75-17.4 parts of additive in parts by weight.

Further, the hair conditioner also comprises 0.05-1.0 part of olive leaf extract.

Further, the film forming agent is formed by fully mixing polyquaternium-37, C13-16 isoparaffin, tridecyl alcohol polyether-6 and water, wherein the mass ratio of the polyquaternium-37 to the C13-16 isoparaffin to the tridecyl alcohol polyether-6 to the water is 1: 2: 1: 10.

further, the humectant is selected from one or two of glycerin and ethylhexyl glycerin.

Further, the humectant comprises 1-10 parts of glycerin and 0.01-0.8 part of ethylhexyl glycerin.

Further, the fat-increasing agent comprises one or two of cyclopentadimethylsiloxane, polydimethylsiloxane and bis-aminopropylpolydimethylsiloxane.

Furthermore, the sum of the cyclopentadimethylsiloxane and the polydimethylsiloxane in the fat-increasing agent is 0.5-5.0 parts, and the bis-aminopropyl polydimethylsiloxane is 0.2-5.0 parts.

Further, the additive comprises 0.05-5.0 parts of panthenol, 0.05-3.0 parts of vitamin E and 0.1-2.0 parts of hydroxyethyl cellulose.

The second purpose of the invention is to provide a preparation method of the cherry blossom nourishing and repairing hair conditioner, which comprises the following steps:

(1) weighing the humectant, the polyquaternium-67, the film forming agent, the chelating agent and the citric acid according to the weight, dissolving in a proper amount of water, adding the solution into an emulsifying pot, homogenizing, stirring and dissolving, and heating to 80-85 ℃ for later use;

(2) weighing emulsifier and cetostearyl alcohol according to the amount, adding the emulsifier and the cetostearyl alcohol into an oil pan, stirring and heating to 80-85 ℃ for later use;

(3) when the temperature of the oil pan and the emulsifying pan reaches 80 ℃, starting vacuum to pump the mixture in the oil pan into the emulsifying pan, rapidly stirring and homogenizing for 1-3 minutes;

(4) opening to cool, and adding the fat increasing agent under the vacuum condition after cooling to 60 ℃;

(5) continuously cooling in the emulsifying pot, adding oriental cherry extract and antiseptic after cooling to 45 deg.C, stirring for 8-15 min, sampling, inspecting, and discharging.

Further, the method comprises the following steps:

(1) weighing the humectant, the polyquaternium-67, the film forming agent, the chelating agent, the citric acid and the panthenol according to the weight, dissolving in a proper amount of water, adding the solution into an emulsifying pot, homogenizing, stirring and dissolving, and heating to 80-85 ℃ for later use;

(4) dissolving colorant and hydroxyethyl cellulose with appropriate amount of water respectively, sequentially adding into emulsifying pot, vacuum stirring for homogenizing for 2-4 min, and stirring for 15-25 min; then opening to cool, after cooling to 60 ℃, adding a fat-increasing agent and vitamin E under the condition of vacuum pumping;

(5) continuously cooling in the emulsifying pot, adding the oriental cherry extract, the olive leaf extract, the essence and the preservative after cooling to 45 ℃, uniformly stirring for 8-15 minutes, sampling, inspecting, and discharging after the materials are qualified.

Compared with the prior art, the invention has the following beneficial technical effects:

(1) the cherry blossom extract, the quaternary ammonium salt-67 and the specific film forming agent are combined in a specific ratio to generate the hair conditioner for repairing the damaged forked tail ends, the positive charge of the quaternary ammonium salt-67 is attracted to the total negative charge of hair fibers, so that the quaternary ammonium salt with the positive charge has affinity to the hair, the quaternary ammonium salt cannot neutralize anionic surfactants remained on the surface of the hair of shampoo, the cherry blossom extract can better act on the hair to repair the damaged hair quality and promote the hair growth, and under the action of the film forming agent, the nutrient components, the humectant and other nutrient components of the cherry blossom extract are locked on the hair in a mode of forming a monomolecular film by being adsorbed on the hair, so that the effect of long-acting repair of the damaged hair quality is achieved; meanwhile, the film can also give softness and luster to the hair, enable the hair to be rich in elasticity, prevent static electricity from being generated, and enable the hair to be soft, smooth and easy to comb.

(2) Experiments prove that the cherry blossom extract, the olive leaf extract and the vitamin E which are added in the optimized proportion have the effect of relieving scalp allergy caused by substances such as a surfactant, an antiseptic and the like in a hair washing process, and can effectively remove dandruff, relieve itching and prevent alopecia.

(3) In the hair conditioner formula, the components cooperate with each other, so that the oil-water phase can effectively ensure the stability of the whole hair conditioner system.

Detailed Description

The following examples are presented to illustrate certain embodiments of the invention in particular and should not be construed as limiting the scope of the invention. The present disclosure may be modified from materials, methods, and reaction conditions at the same time, and all such modifications are intended to be within the spirit and scope of the present invention. Unless otherwise specified, the technical means used in the examples are conventional means well known to those skilled in the art. The reagents and biomaterials, if not specifically indicated, are commercially available.

The film forming agent is formed by fully mixing polyquaternium-37, C13-16 isoparaffin, tridecyl alcohol polyether-6 and water, wherein the mass ratio of the polyquaternium-37 to the C13-16 isoparaffin to the tridecyl alcohol polyether-6 to the water is 1: 2: 1: 10.

cherry extract: a fine brown yellow powder of cherry blossom extract is purchased from a Murray organism and dissolved in a mixed solvent of water, butylene glycol and phenoxyethanol. The mol ratio of oriental cherry extract powder, water, butanediol and phenoxyethanol is 1: 30: 10: 10.

olive leaf extract: olive leaf extract fine powder is purchased from a garter organism and dissolved in a mixed solvent of water, butylene glycol, phenoxyethanol. The mol ratio of oriental cherry extract powder, water, butanediol and phenoxyethanol is 1: 30: 10: 10.

example 1:

a cherry blossom nourishing and repairing hair conditioner comprises, by weight, 0.1 part of polyquaternium-67, 0.5 part of cherry blossom extract, 0.1 part of film forming agent, 0.01 part of EDTA disodium, 5.0 parts of glycerol, 0.5 part of cetostearyl alcohol, 1.0 part of emulsifier (behenyl trimethyl ammonium chloride), 0.3 part of cyclopentadimethylsiloxane, 0.2 part of polydimethylsiloxane, 0.2 part of bis-aminopropyl polydimethylsiloxane, 0.001 part of citric acid, 70 parts of water and 0.5 part of preservative.

The preparation method of the cherry blossom nourishing and repairing hair conditioner comprises the following steps:

(1) weighing glycerol, polyquaternium-67, a film forming agent, EDTA disodium and citric acid according to the weight, dissolving in a proper amount of water, adding the solution into an emulsifying pot, homogenizing, stirring and dissolving, and heating to 80-85 ℃ for later use;

(4) opening and cooling, and adding cyclopentadimethylsiloxane, polydimethylsiloxane and bis-aminopropyl polydimethylsiloxane under the condition of vacuumizing after the temperature is reduced to 60 ℃;

Example 2:

a cherry blossom nourishing and repairing hair conditioner comprises, by weight, 5.0 parts of polyquaternium-67, 0.05 part of a cherry blossom extract, 2.0 parts of a film forming agent, 0.2 part of EDTA disodium, 10.0 parts of glycerol, 2.5 parts of cetostearyl alcohol, 8.0 parts of an emulsifier (behenyl trimethyl ammonium chloride), 3.0 parts of cyclopentadimethylsiloxane, 2.0 parts of polydimethylsiloxane, 5.0 parts of bis-aminopropyl polydimethylsiloxane, 1.0 part of citric acid, 60 parts of water and 0.03 part of a preservative.

The preparation method is the same as example 1.

Example 3:

a cherry blossom nourishing and repairing hair conditioner comprises, by weight, 1.0 part of polyquaternium-67, 1.0 part of cherry blossom extract, 1.0 part of film forming agent, 0.3 part of EDTA disodium, 1.0 part of glycerol, 5.0 parts of cetostearyl alcohol, 4.0 parts of emulsifier (behenyl trimethyl ammonium chloride), 1.3 parts of cyclopentadimethylsiloxane, 1.2 parts of polydimethylsiloxane, 2.5 parts of bis-aminopropyl polydimethylsiloxane, 0.5 part of citric acid, 90 parts of water and 0.8 part of preservative.

The preparation method is the same as example 1.

Example 4:

a cherry blossom nourishing and repairing hair conditioner comprises, by weight, 0.1 part of polyquaternium-67, 0.5 part of cherry blossom extract, 0.5 part of olive leaf extract, 0.1 part of a film forming agent, 0.01 part of EDTA disodium, 5.0 parts of glycerol, 0.01 part of ethylhexyl glycerol, 0.5 part of cetostearyl alcohol, 1.0 part of an emulsifier (behenyltrimethyl ammonium chloride), 0.3 part of cyclopentadimethylsiloxane, 0.2 part of polydimethylsiloxane, 0.2 part of bis-aminopropylpolydimethylsiloxane, 0.001 part of citric acid, 70 parts of water, 0.05 part of panthenol, 0.05 part of vitamin E, 0.1 part of hydroxyethyl cellulose, 0.6 part of essence, 0.00001 part of CI 16255 and 0.5 part of a preservative.

(1) weighing glycerol, polyquaternium-67, a film forming agent, a chelating agent, citric acid and panthenol according to the weight, dissolving in a proper amount of water, adding the solution into an emulsifying pot, homogenizing, stirring and dissolving, and heating to 80-85 ℃ for later use;

(4) dissolving CI 16255 and hydroxyethyl cellulose with appropriate amount of water respectively, sequentially adding into an emulsifying pot, stirring under vacuum for homogenizing for 2-4 min, and stirring under heat preservation for 15-25 min; then opening and cooling, and adding cyclopentadimethylsiloxane, polydimethylsiloxane, bis-aminopropyl polydimethylsiloxane and vitamin E under the condition of vacuumizing after cooling to 60 ℃;

Example 5:

a cherry blossom nourishing and repairing hair conditioner comprises, by weight, 1.0 part of polyquaternium-67, 0.05 part of cherry blossom extract, 0.05 part of olive leaf extract, 0.1 part of a film forming agent, 0.01 part of EDTA disodium, 5.0 parts of glycerol, 0.01 part of ethylhexyl glycerol, 0.5 part of cetostearyl alcohol, 1.0 part of an emulsifier (behenyl trimethyl ammonium chloride), 0.3 part of cyclopentadimethylsiloxane, 0.2 part of polydimethylsiloxane, 0.2 part of bis-aminopropylpolydimethylsiloxane, 0.001 part of citric acid, 70 parts of water, 5.0 part of panthenol, 3.0 part of vitamin E, 1.0 part of hydroxyethyl cellulose, 0.02 part of essence, 1.0 part of CI 16255 and 0.03 part of a preservative.

The preparation method is the same as example 4.

Example 6:

a cherry blossom nourishing and repairing hair conditioner comprises, by weight, 5.0 parts of polyquaternium-67, 1.0 part of cherry blossom extract, 1.0 part of olive leaf extract, 0.1 part of a film forming agent, 0.01 part of EDTA disodium, 5.0 parts of glycerol, 0.4 part of ethylhexyl glycerol, 0.5 part of cetostearyl alcohol, 1.0 part of an emulsifier (behenyltrimethyl ammonium chloride), 0.3 part of cyclopentadimethylsiloxane, 0.2 part of polydimethylsiloxane, 0.2 part of bis-aminopropylpolydimethylsiloxane, 0.001 part of citric acid, 70 parts of water, 2.5 parts of panthenol, 1.5 parts of vitamin E, 2.0 parts of hydroxyethyl cellulose, 0.3 part of essence, 0.5 part of CI 16255 and 0.8 part of a preservative.

The preparation method is the same as example 4.

Comparative example 1:

the comparative example examines the effects of polyquaternium, cherry blossom extract and film forming agent on the effects of the hair conditioner in repairing damaged hair and nourishing hair. Comparative example 1 experiments were carried out on the basis of example 1 with the proportions of the components being varied as indicated in table 1. The preparation method is the same as example 1.

Table 1 formulation of comparative example 1

Comparative example 2:

the comparative example examines the influences of the cherry blossom extract, the olive leaf extract and the vitamin E on the aspects of scalp soothing, dandruff removing, itching relieving and efficacy of the hair conditioner. Comparative example 2 experiments were carried out on the basis of example 5 with the proportions of the components being varied according to table 2. The preparation method is the same as example 4.

Table 2 formulation of comparative example 2

Analysis of results

Test 1 Hair conditioner stability test

The hair conditioners prepared in examples 1 to 6 were subjected to a cooling and heating cycle test, and the results are shown in Table 3.

Table 3 examples 1-6 conditioner cold and hot cycling results

As can be seen from Table 3, the cold and hot cycles of the conditioner prepared by the method of the present invention can smoothly pass, which indicates that the components in the conditioner formula cooperate with each other, such that the oil-water phase can effectively ensure the stability of the whole conditioner system.

Test 2, efficacy test for damaged Hair repair

The hair conditioner of the present invention was applied to 180 damaged hairs (20 hair for each of examples 1 to 6, comparative examples 1 to 1, 1 to 2, and 1 to 3) at 3-day intervals, and the recording was observed, and the results are shown in Table 4.

Table 4 repair efficacy test results

The results show that the combination of the cherry blossom extract, the quaternary ammonium salt-67 and the specific film forming agent in a specific ratio produces the hair conditioner for repairing the damaged forked tail ends, and the hair becomes soft, smooth and glossy by using the hair conditioner. After long-term use, the damaged hair recovers elasticity, the hair tip is not forked and is easy to comb through, and the hair is neat and smooth.

Experiment 3 scalp soothing effect experiment

The population selection standard is as follows: sensitive people who suffer from phenomena of scalp itching, dandruff increasing, red and swollen scalp, pimple, pain and the like when using the shampoo.

280 subjects were selected according to the above population inclusion criteria. 140 men and 140 women; the age was 18-50 years, and the groups were divided into 7 groups of 40 persons.

The sample using method comprises the following steps:

the conditioners prepared in examples 4 to 6 and comparative examples 2 to 1, 2 to 2, 2 to 3 and 2 to 4 were applied to the hair every 3 days, and statistics were counted after 9 days. The test results are shown in table 6.

TABLE 5 Hair conditioner population trial test results

	Example 4	Example 5	Example 6	Comparative example 2-1	Comparative examples 2 to 2	Comparative examples 2 to 3	Comparative examples 2 to 4
								Number of effective persons	39	40	38	1	3	0	2

The experimental results show that: the hair conditioner of the embodiment 4-6 has a remarkable scalp soothing effect on allergy prone people, while the hair conditioner of the comparative example 2 has no remarkable scalp soothing effect on allergy prone scalp, which shows that the hair conditioner of the invention has the scalp soothing effect on scalp allergy caused by substances such as surfactants, preservatives and the like in a hair washing process by adding the cherry blossom extract, the olive leaf extract and the vitamin E in an optimized ratio, and can effectively remove dandruff, relieve itching and prevent alopecia.

The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims

1. The cherry blossom nourishing and repairing hair conditioner is characterized by comprising, by weight, 0.1-1.0 part of polyquaternium-67, 0.05-1.0 part of cherry blossom extract, 0.1-2.0 parts of a film forming agent, 0.01-0.3 part of a chelating agent, 1.01-10.8 parts of a humectant, 0.5-5.0 parts of cetearyl alcohol, 1-8 parts of an emulsifier, 0.7-10.0 parts of a fat-increasing agent, 0.001-1.0 part of citric acid, 60-90 parts of water and 0.75-17.4 parts of an additive.

2. The cherry blossom nourishing and repairing hair conditioner according to claim 1, wherein the hair conditioner further comprises 0.05-1.0 parts of olive leaf extract.

3. The nourishing and repairing cherry blossom hair conditioner as claimed in claim 1, wherein the film forming agent is prepared by thoroughly mixing polyquaternium-37, C13-16 isoparaffin, tridecyl alcohol polyether-6 and water, wherein the mass ratio of polyquaternium-37, C13-16 isoparaffin, tridecyl alcohol polyether-6 and water is 1: 2: 1: 10.

4. the cherry blossom nourishing and repairing hair conditioner according to claim 1, wherein the humectant is one or two selected from glycerin and ethylhexyl glycerin.

5. The cherry blossom nourishing and repairing hair conditioner according to claim 4, wherein the moisturizer comprises 1-10 parts of glycerin and 0.01-0.8 part of ethylhexyl glycerin.

6. The cherry blossom nourishing and repairing hair conditioner according to claim 1, wherein the lipid-increasing agent comprises one or two of cyclopentadimethylsiloxane, polydimethylsiloxane and bis-aminopropylpolydimethylsiloxane.

7. The nourishing and repairing cherry blossom hair conditioner of claim 6, wherein the sum of cyclopentadimethylsiloxane and polydimethylsiloxane in the lipid-increasing agent is 0.5-5.0 parts, and the bis-aminopropyl polydimethylsiloxane is 0.2-5.0 parts.

8. The nourishing and repairing cherry blossom hair conditioner of claim 1, wherein the additive comprises 0.05-5.0 parts of panthenol, 0.05-3.0 parts of vitamin E, and 0.1-2.0 parts of hydroxyethyl cellulose.

9. The method of preparing the cherry blossom nourishing and repairing hair conditioner of claims 1 to 8, characterized by comprising the following steps:

10. The method for preparing the oriental cherry nourishing and repairing hair conditioner according to claim 9, wherein the method comprises the following steps: