CN112471513A - Preparation method of rhizoma polygonati honeyed pills - Google Patents
Preparation method of rhizoma polygonati honeyed pills Download PDFInfo
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- CN112471513A CN112471513A CN202011526660.5A CN202011526660A CN112471513A CN 112471513 A CN112471513 A CN 112471513A CN 202011526660 A CN202011526660 A CN 202011526660A CN 112471513 A CN112471513 A CN 112471513A
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- rhizoma polygonati
- sealwort
- sesame
- honey
- mixing
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- 239000006187 pill Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims description 15
- 235000012907 honey Nutrition 0.000 claims abstract description 25
- 238000002156 mixing Methods 0.000 claims abstract description 23
- 238000004880 explosion Methods 0.000 claims abstract description 22
- 238000007670 refining Methods 0.000 claims abstract description 8
- 241000207961 Sesamum Species 0.000 claims description 30
- 235000003434 Sesamum indicum Nutrition 0.000 claims description 30
- 239000000463 material Substances 0.000 claims description 25
- 239000000706 filtrate Substances 0.000 claims description 20
- 238000003756 stirring Methods 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 17
- 239000002245 particle Substances 0.000 claims description 15
- 241000756042 Polygonatum Species 0.000 claims description 13
- 239000011812 mixed powder Substances 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000008187 granular material Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 10
- 238000004140 cleaning Methods 0.000 claims description 8
- 241000037831 Polygonatum sibiricum Species 0.000 claims description 7
- 239000011363 dried mixture Substances 0.000 claims description 7
- 238000009835 boiling Methods 0.000 claims description 6
- 238000003825 pressing Methods 0.000 claims description 6
- 239000002352 surface water Substances 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 5
- 230000006837 decompression Effects 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 238000004898 kneading Methods 0.000 claims description 5
- 238000004321 preservation Methods 0.000 claims description 5
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- 238000009210 therapy by ultrasound Methods 0.000 claims description 5
- 235000007215 black sesame Nutrition 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 7
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- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract description 3
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- 239000011888 foil Substances 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract description 2
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- 241000238631 Hexapoda Species 0.000 description 2
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- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
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- 208000018522 Gastrointestinal disease Diseases 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 241000257303 Hymenoptera Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
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- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
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- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 208000007502 anemia Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
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- 229910052804 chromium Inorganic materials 0.000 description 1
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- 229930003944 flavone Natural products 0.000 description 1
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- 235000011949 flavones Nutrition 0.000 description 1
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- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
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- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229960003284 iron Drugs 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 229920005610 lignin Polymers 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
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- 239000000047 product Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
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- 239000007787 solid Substances 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
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- 229940045997 vitamin a Drugs 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
- A23L21/25—Honey; Honey substitutes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L25/00—Food consisting mainly of nutmeat or seeds; Preparation or treatment thereof
- A23L25/30—Mashed or comminuted products, e.g. pulp, pastes, meal, powders; Products made therefrom, e.g. blocks, flakes, snacks; Liquid or semi-liquid products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
- A23L5/32—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using phonon wave energy, e.g. sound or ultrasonic waves
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/63—Arthropods
- A61K35/64—Insects, e.g. bees, wasps or fleas
- A61K35/644—Beeswax; Propolis; Royal jelly; Honey
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8969—Polygonatum (Solomon's seal)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- A61K9/2004—Excipients; Inactive ingredients
- A61K9/2068—Compounds of unknown constitution, e.g. material from plants or animals
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P39/00—General protective or antinoxious agents
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
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Abstract
A rhizoma Polygonati honeyed pill is prepared from rhizoma Polygonati, semen Sesami Niger, and Mel by steam explosion, squeezing, decocting, vacuum concentrating, pulverizing, refining Mel, mixing, and molding. The rhizoma polygonati honeyed pills prepared by the method can be wrapped by aluminum foil paper or vacuum bagged; can be used after being unsealed, is sweet and delicious, and has the nutrition and health preserving effects of rhizoma polygonati, black sesame and honey.
Description
Technical Field
The invention belongs to the technical field of food processing, and relates to a preparation method of polygonatum sibiricum honeyed pills.
Background
The honeyed pill is a spherical solid preparation for oral administration prepared by mixing one or more kinds of medicine powder with refined honey, and is a pill prepared by using honey as a binder. Honey, black sesame and sealwort, which are the same as medicine and food.
The honey is a natural sweet substance which is obtained by sufficiently brewing the nectar collected from the flowers of the flowering plants by bees in a honeycomb; is a natural incubation product obtained by enriching various natural vitamins, minerals and amino acids to a certain value and simultaneously converting polysaccharides in the nectar into glucose, fructose and the like which can be directly absorbed by human bodies. The honey has fragrant and rich smell and pure, sweet and delicious taste, can prevent and treat anemia, heart disease, gastrointestinal diseases and the like, and can improve the immunity of a human body.
The semen Sesami Niger is black seed of semen Sesami Niger of Pedaliaceae. The black sesame contains a large amount of fat and protein, and also contains nutrient components such as sugar, vitamin A, vitamin E, lecithin, calcium, iron, chromium and the like, and has the effects of invigorating stomach, protecting liver, promoting erythrocyte growth, blackening hair, beautifying face and the like.
Rhizoma polygonati is a perennial herb plant of the genus polygonatum of the family liliaceae and is an important traditional Chinese medicinal material in China. Rhizoma Polygonati has the same shape as rhizoma Dioscoreae, can be eaten raw or stewed, and has effects of allaying hunger and promoting health. The rhizome of sealwort contains polysaccharide, glycan, flavone, lignin, alkaloid, amino acid and other substances, and modern pharmacological research shows that the sealwort has the effects of tonifying kidney and replenishing vital essence, nourishing yin and moistening dryness, resisting oxidation and aging, regulating human immunity, reducing blood fat, reducing blood sugar, inhibiting cholesterol, preventing atheromatosis, improving learning and memory capacity, resisting inflammation, resisting virus and the like, and is very beneficial to human bodies.
Disclosure of Invention
The invention aims to provide a preparation method of polygonatum sibiricum honeyed pills.
In order to achieve the above objects and other related objects, the present invention provides the following technical solutions: a preparation method of rhizoma polygonati honeyed pills comprises the following steps:
step 1: cleaning collected rhizoma Polygonati, removing surface silt, draining surface water, and crushing into rhizoma Polygonati granule with particle size of 0.5-1.5 cm;
step 2: putting rhizoma Polygonati granules into steam explosion equipment, and performing steam explosion treatment by using parameters of water-material ratio of 1:5-10, pressure maintaining time of 10-15min, and steam pressure of 2.0-2.5 MPa; collecting rhizoma Polygonati granules subjected to steam explosion, and naturally cooling to 40-60 deg.C;
and step 3: carrying out filter pressing on the polygonatum particles subjected to steam explosion treatment to obtain polygonatum filtrate and polygonatum filter residues for later use;
and 4, step 4: mixing rhizoma Polygonati filter residue with purified water at a mass ratio of 1:2.5-5.0, heating the mixture to boil and maintaining the temperature, and starting ultrasonic treatment for 1 time at intervals of 8-10min during the heat preservation period; decocting and extracting for 60-120min under the assistance of ultrasonic waves, filtering the mixed materials by adopting a filter screen of 150 meshes and 300 meshes, and respectively collecting filtrate and filter residues for later use;
and 5: combining the filtrate obtained in the step (3) and the filtrate obtained in the step (4), placing the mixture into vacuum decompression concentration equipment, and carrying out boiling concentration to 5-10% of the original volume under the condition of vacuum gauge pressure of-0.08 to-0.10 MPa to obtain sealwort concentrated solution;
step 6: mixing the cleaned sesame and the filter residue obtained in the step (4) according to a mass ratio of 100:50-250, and stir-frying and drying at a temperature of 50-60 ℃ and a stirring speed of 15-60r/min until the water content of the material is less than or equal to 8% to obtain a dried mixture of sesame and sealwort;
and 7: crushing the dried mixture of the sesame and the sealwort to the fineness of more than or equal to 100 meshes to obtain mixed powder of the sesame and the sealwort for later use;
and 8: heating fresh honey to 110-115 ℃ under stirring or turning over, and preserving heat for 10-20min to obtain refined honey; then mixing the sesame and sealwort mixed powder, the sealwort concentrated solution and the honey after honey refining according to the mass ratio of 100: 20-45: 125-150, stirring and mixing uniformly; then dividing the mixed materials into small blocks with the weight of 8-15g, and kneading into round pills respectively to obtain the polygonatum sibiricum honeyed pills.
The preferable technical scheme is as follows: in the step 2, the filter pressing pressure is 0.30-0.40MPa, and the aperture of the filter screen is 60-100 meshes.
The preferable technical scheme is as follows: in step 4, the ultrasonic frequency is 25-35 KHz, and the power density is 0.3-0.5W/cm2And the treatment time is 1.5-3.0 min.
Due to the application of the technical scheme, compared with the prior art, the invention has the advantages that:
1. the invention adopts squeezing to prepare fresh sealwort juice, adopts ultrasonic-assisted boiling to extract sealwort filter residue, and then fries the extracted filter residue and black sesame together to be fragrant and crushed for utilization, thereby fully extracting the nutrient substances and functional components of sealwort and improving the taste of sealwort.
2. The sealwort of the invention is extracted by juicing, decocting and ultrafine grinding, so that the nutrition and natural active ingredients of the sealwort are easier to absorb.
3. The rhizoma polygonati honeyed pills prepared by the invention can be wrapped by aluminum foil paper or vacuum bagged; can be used after being unsealed, is sweet and delicious, and has the nutrition and health preserving effects of rhizoma polygonati, black sesame and honey.
Detailed Description
The following description of the embodiments of the present invention is provided for illustrative purposes, and other advantages and effects of the present invention will become apparent to those skilled in the art from the present disclosure.
Example 1: preparation method of rhizoma polygonati honeyed pills
A preparation method of rhizoma polygonati honeyed pills is characterized by comprising the following technical steps.
(1) Pretreatment of rhizoma polygonati
The rhizoma Polygonati is obtained from fresh harvested mature rhizoma Polygonati rhizome without mildew, insect pest and mechanical injury.
And (5) cleaning. Cleaning rhizoma Polygonati completely, removing surface silt, and draining surface water.
And (4) crushing. Crushing rhizoma Polygonati uniformly into granules with particle diameter of 0.5-1.5 cm.
(2) Steam explosion treatment of sealwort
Putting the mesohuangjing particles in the step (1) into steam explosion equipment, and performing steam explosion treatment by adopting parameters of a water-material ratio of 1:8, a pressure maintaining time of 12min and a steam pressure of 2.3 MPa; collecting the rhizoma Polygonati granules after steam explosion, and naturally cooling to 50 deg.C for use.
(3) Squeezing of rhizoma Polygonati
Carrying out pressure filtration treatment on the sealwort particles subjected to steam explosion in the step (2) by using a food-grade pressure filter to obtain sealwort filtrate and sealwort filter residues for later use; wherein the pressure filtration pressure is 0.35MPa, and the aperture of the filter screen is 80 meshes.
(4) Decocting and extracting rhizoma Polygonati filter residue
Mixing the sealwort filter residue in the step (3) with food-grade purified water according to the mass ratio of 1:3.5, putting the mixed material into a heat extraction device with an ultrasonic generating device and a distilled water condensation recovery device, heating to boil and preserving heat; during the heat preservation period, ultrasonic treatment is started for 1 time at intervals of 9min, the ultrasonic frequency is 30KHz, and the power density is 0.4W/cm2The treatment time is 2.2 min; decocting and extracting for 100min under the assistance of ultrasonic wave, filtering the mixed materials by adopting a 200-mesh filter screen, and respectively collecting filtrate and filter residue for later use.
(5) Preparing sealwort concentrated solution
And (4) combining the filtrate in the step (3) and the filtrate in the step (4), placing the mixture into vacuum decompression concentration equipment, and boiling and concentrating the mixture to 8 percent of the original volume under the condition of vacuum gauge pressure of-0.09 MPa to obtain sealwort concentrated solution for later use.
(6) Pretreatment of sesame
The sesame raw material is black sesame seeds with good maturity, no mildew and no insect pest.
And (5) winnowing. Placing sesame into food sanitation grade air separation equipment, performing air separation at air speed of 4-5m/s, and collecting un-blown materials.
And (5) cleaning. Fully cleaning the air-separated sesame, and draining off surface water for later use.
(7) Vacuum parching semen Sesami and distilled rhizoma Polygonati residue at low temperature
Mixing the sesame cleaned in the step (6) and the filter residue in the step (4) according to the mass ratio of 100:150), putting the mixture into a vacuum drying device with stirring, and stir-frying and drying the mixture at a low temperature in vacuum under the conditions of vacuum gauge pressure of-0.095 MPa, temperature of 55 ℃ and stirring speed of 40r/min until the water content of the material is lower than 8% to obtain a dry mixture of the sesame and the sealwort for later use.
(8) Pulverizing
And (3) fully crushing the dried mixture of the sesame and the sealwort in the step (7) until the fineness is higher than 100 meshes to obtain the mixed powder of the sesame and the sealwort for later use. Preferably, the crushing equipment adopts airflow crushing, and the air source is nitrogen.
(9) Making honeyed pills
And (5) refining honey. Heating fresh Mel under stirring or stirring to 112 deg.C, and keeping the temperature for 15min until the Mel becomes light red and the viscosity is remarkably increased.
And (5) stirring the materials. Mixing the sesame and sealwort mixed powder, the sealwort concentrated solution and the honey after honey refining in the step (8) according to a mass ratio of 100: 35: 130, fully stirring and uniformly mixing. Preferably, the sesame and sealwort mixed powder, the sealwort concentrated solution and the honey after honey refining are fully stirred in a flour mixer and are mixed and kneaded into uniform bulk materials.
And (5) molding. Uniformly dividing the material after mixing into small blocks with the weight of 8-15g, and kneading into round pills respectively to obtain the polygonatum sibiricum honeyed pills.
The rhizoma polygonati honeyed pills prepared by the method can be wrapped by aluminum foil paper or vacuum bagged; can be used after being unsealed, is sweet and delicious, and has the nutrition and health preserving effects of rhizoma polygonati, black sesame and honey.
Example 2: preparation method of rhizoma polygonati honeyed pills
A preparation method of rhizoma polygonati honeyed pills comprises the following steps:
step 1: cleaning collected rhizoma Polygonati, removing surface silt, draining surface water, and crushing into rhizoma Polygonati granule with particle size of 0.5 cm;
step 2: putting the rhizoma polygonati particles into steam explosion equipment, and performing steam explosion treatment by adopting parameters of a water-material ratio of 1:5, a pressure maintaining time of 10min and a steam pressure of 2.0 MPa; collecting the rhizoma polygonati particles subjected to steam explosion, and naturally cooling to 40 ℃;
and step 3: carrying out filter pressing on the polygonatum particles subjected to steam explosion treatment to obtain polygonatum filtrate and polygonatum filter residues for later use;
and 4, step 4: mixing rhizoma Polygonati filter residue with purified water at a mass ratio of 1:2.5, heating the mixture to boil and maintaining the temperature, wherein ultrasonic treatment is started for 1 time every 8min during the heat preservation period; decocting and extracting for 60min under the assistance of ultrasonic wave, filtering the mixed materials by adopting a 150-mesh filter screen, and respectively collecting filtrate and filter residue for later use;
and 5: combining the filtrate obtained in the step (3) and the filtrate obtained in the step (4), placing the mixture into vacuum decompression concentration equipment, and boiling and concentrating the mixture to 5% of the original volume under the condition of vacuum gauge pressure of-0.08 MPa to obtain sealwort concentrated solution;
step 6: mixing the cleaned sesame and the filter residue obtained in the step (4) according to the mass ratio of 100:50, and stir-frying and drying at the temperature of 50 ℃ and the stirring speed of 15r/min until the water content of the material is 7.52% to obtain a dry sesame and sealwort mixture;
and 7: crushing the dried mixture of the sesame and the sealwort to the fineness of more than or equal to 100 meshes to obtain mixed powder of the sesame and the sealwort for later use;
and 8: heating fresh Mel to 110 deg.C under stirring or turning over, and keeping the temperature for 10min to obtain refined Mel; then mixing the sesame and sealwort mixed powder, the sealwort concentrated solution and the honey after honey refining according to the mass ratio of 100: 20: 125, and stirring and mixing uniformly; then dividing the mixed materials into small blocks with the weight of 8g, and kneading the small blocks into round pills respectively to obtain the polygonatum sibiricum honeyed pills.
The preferred embodiment is: in the step 2, the pressure filtration pressure is 0.30MPa, and the mesh diameter of the filter screen is 60 meshes.
The preferred embodiment is: in step 4, the ultrasonic frequency is 25KHz, and the power density is 0.3W/cm2And the treatment time is 1.5 min.
Example 3: preparation method of rhizoma polygonati honeyed pills
A preparation method of rhizoma polygonati honeyed pills comprises the following steps:
step 1: cleaning collected rhizoma Polygonati, removing surface silt, draining surface water, and crushing into rhizoma Polygonati granule with particle size of 1.5 cm;
step 2: putting the rhizoma polygonati particles into steam explosion equipment, and performing steam explosion treatment by adopting parameters of a water-material ratio of 1:10, a pressure maintaining time of 15min and a steam pressure of 2.5 MPa; collecting the rhizoma polygonati particles subjected to steam explosion, and naturally cooling to 60 ℃;
and step 3: carrying out filter pressing on the polygonatum particles subjected to steam explosion treatment to obtain polygonatum filtrate and polygonatum filter residues for later use;
and 4, step 4: mixing rhizoma Polygonati filter residue with purified water at a mass ratio of 1:5.0, heating the mixture to boil and maintaining the temperature, and starting ultrasonic treatment for 1 time every 10min during the heat preservation period; decocting and extracting for 120min under the assistance of ultrasonic waves, filtering the mixed materials by adopting a 300-mesh filter screen, and respectively collecting filtrate and filter residues for later use;
and 5: combining the filtrate obtained in the step (3) and the filtrate obtained in the step (4), placing the mixture into vacuum decompression concentration equipment, and boiling and concentrating the mixture to 10 percent of the original volume under the condition of vacuum gauge pressure of-0.10 MPa to obtain sealwort concentrated solution;
step 6: mixing the cleaned sesame and the filter residue obtained in the step (4) according to the mass ratio of 100:250, and stir-frying and drying at the temperature of 60 ℃, the stirring speed and the speed of 60r/min until the water content of the material is less than or equal to 8% to obtain a dry sesame and sealwort mixture;
and 7: crushing the dried mixture of the sesame and the sealwort to the fineness of more than or equal to 100 meshes to obtain mixed powder of the sesame and the sealwort for later use;
and 8: heating fresh Mel under stirring or turning over to 115 deg.C, and keeping the temperature for 20min to obtain refined Mel; then mixing the sesame and sealwort mixed powder, the sealwort concentrated solution and the honey after honey refining according to the mass ratio of 10045150, and stirring and mixing uniformly; then dividing the mixed materials into small blocks with the weight of 15g, and kneading the small blocks into round pills respectively to obtain the polygonatum sibiricum honeyed pills.
The preferred embodiment is: in the step 2, the pressure filtration pressure is 0.40MPa, and the mesh diameter of the filter screen is 100 meshes.
The preferred embodiment is: in step 4, the ultrasonic frequency is 35 KHz, and the power density is 0.5W/cm2And the treatment time is 3.0 min.
The foregoing is illustrative of the preferred embodiment of the present invention and is not to be construed as limiting thereof in any way, and any modifications or variations thereof that fall within the spirit of the invention are intended to be included within the scope thereof.
Claims (3)
1. A preparation method of rhizoma polygonati honeyed pills is characterized by comprising the following steps: comprises the following steps:
step 1: cleaning collected rhizoma Polygonati, removing surface silt, draining surface water, and crushing into rhizoma Polygonati granule with particle size of 0.5-1.5 cm;
step 2: putting rhizoma Polygonati granules into steam explosion equipment, and performing steam explosion treatment by using parameters of water-material ratio of 1:5-10, pressure maintaining time of 10-15min, and steam pressure of 2.0-2.5 MPa; collecting rhizoma Polygonati granules subjected to steam explosion, and naturally cooling to 40-60 deg.C;
and step 3: carrying out filter pressing on the polygonatum particles subjected to steam explosion treatment to obtain polygonatum filtrate and polygonatum filter residues for later use;
and 4, step 4: mixing rhizoma Polygonati filter residue with purified water at a mass ratio of 1:2.5-5.0, heating the mixture to boil and maintaining the temperature, and starting ultrasonic treatment for 1 time at intervals of 8-10min during the heat preservation period; decocting and extracting for 60-120min under the assistance of ultrasonic waves, filtering the mixed materials by adopting a filter screen of 150 meshes and 300 meshes, and respectively collecting filtrate and filter residues for later use;
and 5: combining the filtrate obtained in the step (3) and the filtrate obtained in the step (4), placing the mixture into vacuum decompression concentration equipment, and carrying out boiling concentration to 5-10% of the original volume under the condition of vacuum gauge pressure of-0.08 to-0.10 MPa to obtain sealwort concentrated solution;
step 6: mixing the cleaned sesame and the filter residue obtained in the step (4) according to a mass ratio of 100:50-250, and stir-frying and drying at a temperature of 50-60 ℃ and a stirring speed of 15-60r/min until the water content of the material is less than or equal to 8% to obtain a dried mixture of sesame and sealwort;
and 7: crushing the dried mixture of the sesame and the sealwort to the fineness of more than or equal to 100 meshes to obtain mixed powder of the sesame and the sealwort for later use;
and 8: heating fresh honey to 110-115 ℃ under stirring or turning over, and preserving heat for 10-20min to obtain refined honey; then mixing the sesame and sealwort mixed powder, the sealwort concentrated solution and the honey after honey refining according to the mass ratio of 100: 20-45: 125-150, stirring and mixing uniformly; then dividing the mixed materials into small blocks with the weight of 8-15g, and kneading into round pills respectively to obtain the polygonatum sibiricum honeyed pills.
2. The preparation method of the rhizoma polygonati honeyed pill according to claim 1, which is characterized by comprising the following steps: in the step 2, the filter pressing pressure is 0.30-0.40MPa, and the aperture of the filter screen is 60-100 meshes.
3. The preparation method of the rhizoma polygonati honeyed pill according to claim 1, which is characterized by comprising the following steps: in step 4, the ultrasonic frequency is 25-35 KHz, and the power density is 0.3-0.5W/cm2And the treatment time is 1.5-3.0 min.
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