CN112436818B - Graphene resonator and phonon maser and method based on graphene resonator - Google Patents
Graphene resonator and phonon maser and method based on graphene resonator Download PDFInfo
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Abstract
Description
技术领域Technical field
本发明涉及到二维材料谐振子制备、腔光力学、声子信息器件、精密测量等技术领域,特别涉及一种利用石墨烯谐振子实现声子激射器的方法及装置。The invention relates to the technical fields of two-dimensional material resonator preparation, cavity optomechanics, phonon information devices, precision measurement and other technical fields, and particularly relates to a method and device for realizing a phonon maser using graphene resonators.
背景技术Background technique
近些年来,快速发展的激光技术在光量子信息领域方面做出了巨大贡献,极大推动了人们对量子物理学的认知。同光子相比,声子(晶格振动能量量子)具有几个独特的优势:一是声子在相同频率下具有更短的波长,即声子更加局域化,相对微波和光子而言,在芯片上传递速度比较慢,因此更易于操控,可以在成像和精密加工等应用中实现更高的分辨率;二是声子的相干时间比较长,对于经典的相干信息传递和处理以及量子信息处理都有重要意义;三是在固态体系中,声子和许多物理体系(如电子)的耦合都比较强,可用于复合量子体系的扩展和操控等领域。因此,人们对声子激射器在经典和量子信息处理领域的应用都非常感兴趣。然而,基于激光原理的声子激射现象,一直以来很难有效地推动声子激光器的实际应用。随着近年来微纳机电系统的快速发展,机械振子和激光构成的光机电系统成为探索声子激光器的有效手段。而基于石墨烯制备的机械振子具有质量小、频率高、品质因子大等优点,这些优点有利于我们利用它进行声子激射的基础和应用研究。石墨烯机械振子与芯片上的微孔组成了光学谐振腔腔体,在激光入射到该光学谐振腔时,蓝失谐激光在石墨烯上产生的光辐射压力会随着激光功率的的增大,对谐振子的声子耗散产生影响,使得声子耗散的程度逐渐减小,直至为零。此后石墨烯机械振子中的声子会出现类似于激光中光子的受激辐射过程,声子数随泵浦激光功率增加表现出明显的阈值效应,即出现了声子激射现象。随着石墨烯机械谐子的振动,光学谐振腔反射的激光光强在高频状态下被同步调制,通过光电探测器转换为电信号再经频谱分析仪处理,即可提取出机械振子的谐振模式,对声子激射这一现象进行探究。In recent years, the rapidly developing laser technology has made great contributions to the field of optical quantum information and greatly promoted people's understanding of quantum physics. Compared with photons, phonons (lattice vibration energy quanta) have several unique advantages: First, phonons have a shorter wavelength at the same frequency, that is, phonons are more localized. Compared with microwaves and photons, The transmission speed on the chip is relatively slow, so it is easier to control and can achieve higher resolution in applications such as imaging and precision processing. Second, the coherence time of phonons is relatively long, which is difficult for classical coherent information transmission and processing as well as quantum information. The third is that in solid-state systems, the coupling between phonons and many physical systems (such as electrons) is relatively strong, and can be used in fields such as the expansion and manipulation of composite quantum systems. Therefore, there is great interest in the application of phonon masers in both classical and quantum information processing. However, the phonon lasing phenomenon based on the laser principle has been difficult to effectively promote the practical application of phonon lasers. With the rapid development of micro-nano electromechanical systems in recent years, optomechanical systems composed of mechanical oscillators and lasers have become an effective means to explore phonon lasers. The mechanical oscillator prepared based on graphene has the advantages of small mass, high frequency, and large quality factor. These advantages are conducive to our use of it for basic and applied research on phonon lasing. The graphene mechanical oscillator and the microholes on the chip form an optical resonant cavity. When the laser is incident on the optical resonant cavity, the optical radiation pressure generated by the blue detuned laser on the graphene will increase with the increase of laser power. , which affects the phonon dissipation of the resonator, causing the degree of phonon dissipation to gradually decrease until it reaches zero. After that, the phonons in the graphene mechanical oscillator will undergo a stimulated emission process similar to that of photons in lasers. The number of phonons will show an obvious threshold effect as the pump laser power increases, that is, the phonon lasing phenomenon will occur. As the graphene mechanical resonator vibrates, the laser light intensity reflected by the optical resonant cavity is synchronously modulated in a high-frequency state. It is converted into an electrical signal through a photodetector and then processed by a spectrum analyzer to extract the resonance of the mechanical oscillator. mode to explore the phenomenon of phonon lasing.
发明内容Contents of the invention
鉴于以上所述现有技术的缺点,本发明的目的在于提供一种石墨烯谐振子,以及基于石墨烯谐振子的声子激射器和工作方法In view of the above-mentioned shortcomings of the prior art, the object of the present invention is to provide a graphene resonator, as well as a phonon maser and working method based on the graphene resonator.
为实现上述发明目的,本发明技术方案如下:In order to achieve the above-mentioned object of the invention, the technical solutions of the present invention are as follows:
一种石墨烯谐振子,包括衬底芯片,所述的衬底芯片通过刻蚀硅晶片来制备,衬底芯片包括底部的硅层,硅层上表面左右两端有二氧化硅层,二氧化硅层中间设有凹槽,凹槽正上方覆盖石墨烯薄膜,石墨烯薄膜通过机械剥离块状石墨得到,石墨烯薄膜的两端覆盖部分二氧化硅层,衬底芯片和石墨烯薄膜之间构成一个光学谐振腔。A graphene resonator includes a substrate chip. The substrate chip is prepared by etching a silicon wafer. The substrate chip includes a silicon layer at the bottom. There are silicon dioxide layers on the left and right ends of the upper surface of the silicon layer. The silicon dioxide layer is There is a groove in the middle of the silicon layer, and a graphene film is covered directly above the groove. The graphene film is obtained by mechanically peeling off block graphite. Both ends of the graphene film cover part of the silicon dioxide layer, and there is a gap between the substrate chip and the graphene film. constitute an optical resonant cavity.
作为优选方式,在激光入射到该光学谐振腔时,蓝失谐激光在石墨烯上产生的光辐射压力会随着激光功率的增大,导致石墨烯谐振子中的声子耗散减小,直至为零;此后石墨烯谐振子中的声子会表现出类似激光中光子受激辐射过程,声子数随泵浦激光功率增加表现出明显的阈值效应,即出现了声子激射现象,得到声子激射器。As a preferred way, when the laser is incident on the optical resonant cavity, the optical radiation pressure generated by the blue detuned laser on the graphene will increase with the increase of the laser power, resulting in the reduction of phonon dissipation in the graphene resonator. until it reaches zero; after that, the phonons in the graphene resonator will show a process similar to the photon stimulated radiation in the laser. The number of phonons will show an obvious threshold effect as the pump laser power increases, that is, the phenomenon of phonon lasing will occur. Get the phonon maser.
为实现上述发明目的,本发明还提供一种基于石墨烯谐振子的声子激射器,包括上述石墨烯谐振子8,其为:沿光路方向,依次包括驱动激光源1、和驱动激光源1中心对准的第一光纤耦合器21、和第一光纤耦合器21通过光纤连接的第二光纤耦合器22、和第二光纤耦合器22中心对准的第一半波片31、和第一半波片31中心对准且和第一半波片31夹角呈45度的第一高反镜41、和第一高反镜41的出射光对准的第一偏振分束棱镜51、和第一偏振分束棱镜51的出射光对准的第二半波片32、和第二半波片32的出射光对准的第二偏振分束棱镜52、和第二偏振分束棱镜52的出射光对准的四分之一波片6、和四分之一波片6中心对准的物镜7、和物镜7中心对准的石墨烯谐振子8、石墨烯谐振子8固定在纳米电动位移台9上,和第二偏振分束棱镜52的出射光对准的分束器10、分束器10的一部分出射光和CCD相机11中心对齐、另一部分出射光和第二高反镜42中心对齐,和第二高反镜42的出射光对准的滤波片12、和滤波片12中心对准的光电探测器13、和光电探测器13电性连接的频谱分析仪14,第一偏振分束棱镜51远离第二半波片32的一侧设有照明光源15,照明光源15和所述第一偏振分束棱镜51的出射光对准。In order to achieve the above-mentioned object of the invention, the present invention also provides a phonon maser based on graphene resonators, including the above-mentioned graphene resonators 8, which include: a driving laser source 1 and a driving laser source along the optical path direction. 1. A first optical fiber coupler 21 that is centrally aligned, a second optical fiber coupler 22 that is connected to the first optical fiber coupler 21 through an optical fiber, and a first half-wave plate 31 that is centrally aligned with the second optical fiber coupler 22. The first high-reflection mirror 41 is aligned with the center of the half-wave plate 31 and forms an angle of 45 degrees with the first half-wave plate 31, and the first polarizing beam splitting prism 51 is aligned with the outgoing light of the first high-reflection mirror 41. The second half-wave plate 32 is aligned with the outgoing light of the first polarizing beam splitting prism 51, and the second polarizing beam splitting prism 52 is aligned with the outgoing light of the second half-wave plate 32, and the second polarizing beam splitting prism 52 The quarter-wave plate 6 is aligned with the output light, the objective lens 7 is aligned with the center of the quarter-wave plate 6, the graphene resonator 8 is aligned with the center of the objective lens 7, and the graphene resonator 8 is fixed on the nanometer On the electric displacement stage 9, the beam splitter 10 is aligned with the outgoing light of the second polarizing beam splitting prism 52. A part of the outgoing light of the beam splitter 10 is aligned with the center of the CCD camera 11, and the other part of the outgoing light is aligned with the second high reflection mirror. 42 is centered and aligned with the filter 12 aligned with the emitted light of the second high reflection mirror 42, the photodetector 13 aligned with the center of the filter 12, and the spectrum analyzer 14 electrically connected to the photodetector 13, the first An illumination light source 15 is provided on the side of the polarizing beam splitting prism 51 away from the second half-wave plate 32 , and the illuminating light source 15 is aligned with the outgoing light of the first polarizing beam splitting prism 51 .
作为优选方式,驱动激光源1的泵浦激光同时用于激光干涉测量谐振子振动模式,激光以自由空间光的形式通过物镜聚焦照射在石墨烯谐振子8表面,石墨烯谐振子8与硅衬底芯片之间形成光学谐振腔,随着石墨烯谐振子8的振动,光学谐振腔反射的激光光强被同步调制,通过光电探测器转换为电信号再经频谱分析仪即可提取出石墨烯谐振子的谐振模式。As a preferred way, the pump laser that drives the laser source 1 is also used for laser interference measurement of the vibration mode of the resonator. The laser is focused and irradiated on the surface of the graphene resonator 8 through the objective lens in the form of free space light. The graphene resonator 8 is in contact with the silicon liner. An optical resonant cavity is formed between the bottom chips. As the graphene resonator 8 vibrates, the laser light intensity reflected by the optical resonant cavity is synchronously modulated, and is converted into an electrical signal through a photodetector and then through a spectrum analyzer to extract graphene. The resonant mode of the oscillator.
作为优选方式,所述分束器10为10:90分束器。As a preferred way, the beam splitter 10 is a 10:90 beam splitter.
作为优选方式,纳米电动位移台9是个三轴位移台,沿空间三维方向移动,初始时通过位移台的移动使物镜7中心和石墨烯谐振器8中心对准。As a preferred method, the nanoelectric displacement stage 9 is a three-axis displacement stage that moves along the three-dimensional direction of space. Initially, the center of the objective lens 7 and the center of the graphene resonator 8 are aligned through the movement of the displacement stage.
作为优选方式,驱动激光源采用633nm单模连续光激光器。As a preferred method, the driving laser source uses a 633nm single-mode continuous light laser.
作为优选方式,白色LED作为CCD成像的照明光源;As a preferred way, white LED is used as the illumination source for CCD imaging;
为实现上述发明目的,本发明还提供一种上述基于石墨烯谐振子的声子激射器的工作方法,其为:驱动激光源1发出激光,经过第一光纤耦合器21准直收集、第二光纤耦合器22再准直后,平行进入第一半波片31,第一半波片31的出射光被该半波片改变偏振后,经第一高反镜41改变光路方向,使激光垂直入射到第一偏振分束棱镜51,第一偏振分束棱镜51将具有竖直偏振方向的激光反射,使第一偏振分束棱镜51的出射光垂直经第二半波片32中心,被第二半波片32改变偏振态的激光,进入第二偏振分束棱镜52,此时激光透过第二偏振分束棱镜52,并经四分之一波片6改变偏振态,四分之一波片6的出射光经过物镜7聚焦后,照射纳米电动位移台9上垂直固定的石墨烯谐振子8,石墨烯谐振子8反射的激光经物镜7收集、被四分之一波片6再次改变偏振态后,第二次经过第二偏振分束棱镜52,第二偏振分束棱镜52反射此偏振的激光,使该激光进入分束器10,分束器10对激光光束进行分束,一束进入CCD相机用于成像,另一束经第二高反镜42改变光路方向,激光经过滤波片12过滤后,保证与驱动激光源1同波长的激光进入光电探测器13,光电探测器13将接受的光信号转换为电信号,该电信号经频谱分析仪14提取石墨烯谐振子8的谐振模式,所有的半波片和四分之一波片也用于调节光路中各部分激光的功率;纳米电动位移台9用于调节石墨烯谐振子的位置,使得激光光斑能够准确聚焦到石墨烯谐振子的目标位置。In order to achieve the above-mentioned object of the invention, the present invention also provides a working method of the above-mentioned graphene resonator-based phonon maser, which is: driving the laser source 1 to emit laser, collimating and collecting it through the first optical fiber coupler 21, and After the two optical fiber couplers 22 are collimated again, they enter the first half-wave plate 31 in parallel. After the outgoing light from the first half-wave plate 31 is polarized by the half-wave plate, it changes the direction of the optical path through the first high-reflection mirror 41, so that the laser Vertically incident on the first polarizing beam splitting prism 51, the first polarizing beam splitting prism 51 will reflect the laser with the vertical polarization direction, so that the emitted light of the first polarizing beam splitting prism 51 passes vertically through the center of the second half-wave plate 32 and is The laser light whose polarization state is changed by the second half-wave plate 32 enters the second polarization beam splitter prism 52. At this time, the laser light passes through the second polarization beam splitter prism 52 and changes its polarization state through the quarter-wave plate 6. After being focused by the objective lens 7 , the emitted light from the wave plate 6 irradiates the vertically fixed graphene resonator 8 on the nanoelectric displacement stage 9 . The laser light reflected by the graphene resonator 8 is collected by the objective lens 7 and is collected by the quarter-wave plate 6 After changing the polarization state again, it passes through the second polarization beam splitting prism 52 for the second time. The second polarization beam splitting prism 52 reflects this polarized laser, causing the laser to enter the beam splitter 10, and the beam splitter 10 splits the laser beam. , one beam enters the CCD camera for imaging, and the other beam changes the direction of the optical path through the second high-reflection mirror 42. After the laser is filtered by the filter 12, it is ensured that the laser with the same wavelength as the driving laser source 1 enters the photodetector 13. Photoelectric detection The receiver 13 converts the received optical signal into an electrical signal, and the electrical signal is extracted by the spectrum analyzer 14 to extract the resonance mode of the graphene resonator 8. All half-wave plates and quarter-wave plates are also used to adjust various parts of the optical path. The power of the laser; the nanoelectric displacement stage 9 is used to adjust the position of the graphene resonator so that the laser spot can accurately focus on the target position of the graphene resonator.
作为优选方式,所述工作方法进一步:将波长为633nm的驱动连续光激光源聚焦到光学谐振腔上,再利用90:10分束器,将石墨烯谐振子8反射的激光光束分为两束,其中一束用于成像,另一束则被光电探测器转换为电信号,通过频谱分析后经频谱分析仪提取石墨烯机械振子的谐振模式,获得谐振子振动的频域信息;随着激光功率增加,声子出现了明显的阈值效应,声子发生激射,成为一个声子激射器;保证装置正常运行,能观测到石墨烯谐振子8的机械振动模式后,旋转光路中的半波片和四分之一波片,来改变聚焦在石墨烯薄膜上的激光功率;在不损坏石墨烯薄膜的前提下,增加入射激光的光功率,根据频谱信息中振动模式的幅值变化判断声子激射器的实现情况。这个幅值变化是以图4为基础,如果出现类似图4中幅值变化,则可以判断声子激射器实现。As a preferred way, the working method further: focus the driving continuous light laser source with a wavelength of 633 nm onto the optical resonant cavity, and then use a 90:10 beam splitter to divide the laser beam reflected by the graphene resonator 8 into two beams , one beam is used for imaging, and the other beam is converted into an electrical signal by a photodetector. After spectrum analysis, the resonance mode of the graphene mechanical oscillator is extracted by a spectrum analyzer to obtain the frequency domain information of the resonator vibration; with the laser As the power increases, the phonons have an obvious threshold effect, and the phonons maser and become a phonon maser. After ensuring the normal operation of the device and observing the mechanical vibration mode of the graphene resonator 8, half of the rotating optical path is Wave plates and quarter-wave plates are used to change the laser power focused on the graphene film; without damaging the graphene film, increase the optical power of the incident laser and judge based on the amplitude changes of the vibration modes in the spectrum information. Realization of phonon masers. This amplitude change is based on Figure 4. If there is an amplitude change similar to Figure 4, it can be judged that the phonon maser has been implemented.
本发明的有益效果为:相比于已知的声子激射器装置,本发明所述声子激射器具有制备工艺简单、技术难度低、易于芯片集成和批量化制备等优点。稳定可控的声子激射器在发展声学量子信息器件、实现不同量子信息系统间的信息交互以及精密测量等领域,具有重要的基础研究意义和广泛的应用前景。The beneficial effects of the present invention are: compared with known phonon maser devices, the phonon maser of the present invention has the advantages of simple preparation process, low technical difficulty, easy chip integration and batch preparation. Stable and controllable phonon masers have important basic research significance and broad application prospects in the fields of developing acoustic quantum information devices, realizing information interaction between different quantum information systems, and precision measurement.
附图说明Description of the drawings
图1为本发明的基于石墨烯谐振子的声子激射器的装置示意图。Figure 1 is a schematic diagram of the device of the graphene resonator-based phonon maser of the present invention.
图2为本发明石墨烯谐振子激光泵浦驱动测量原理示意图。Figure 2 is a schematic diagram of the graphene resonator laser pump driving measurement principle of the present invention.
图3为本发明石墨烯谐振子光镜、电镜图像,以及谐振模式的频域显示。其中(a).悬浮石墨烯谐振子光镜图。(b).悬浮石墨烯谐振子电镜图。(c).悬浮石墨烯谐振子测量频谱图。Figure 3 shows the optical microscope and electron microscope images of the graphene resonator of the present invention, as well as the frequency domain display of the resonance mode. Among them (a). Optical microscope image of suspended graphene resonator. (b). Electron microscope image of suspended graphene resonator. (c). Measurement spectrum of suspended graphene resonator.
图4为本发明不同入射光功率下谐振模式信息的变化趋势图。其中(a)图为不同入射光功率下某一振动模式变化瀑布图;图(b)为不同入射光功率下某一振动模式峰值变化曲线。Figure 4 is a change trend diagram of the resonance mode information under different incident light powers of the present invention. The picture (a) is a waterfall chart of the change of a certain vibration mode under different incident light powers; the picture (b) is the peak change curve of a certain vibration mode under different incident light powers.
其中,1为驱动激光源,21为第一光纤耦合器,22为第二光纤耦合器,31为第一半波片,32为第二半波片,41为第一高反镜,42为第二高反镜,51为第一偏振分束棱镜,52为第二偏振分束棱镜,6为四分之一波片,7为物镜,8为石墨烯谐振子,9为纳米电动位移台,10为分束器,11为CCD相机,12为滤波片,13光电探测器,14为频谱分析仪,15为照明光源。Among them, 1 is the driving laser source, 21 is the first fiber coupler, 22 is the second fiber coupler, 31 is the first half-wave plate, 32 is the second half-wave plate, 41 is the first high reflection mirror, and 42 is The second high reflection mirror, 51 is the first polarizing beam splitting prism, 52 is the second polarizing beam splitting prism, 6 is a quarter wave plate, 7 is the objective lens, 8 is the graphene resonator, and 9 is the nano electric displacement stage. , 10 is a beam splitter, 11 is a CCD camera, 12 is a filter, 13 is a photodetector, 14 is a spectrum analyzer, and 15 is an illumination source.
具体实施方式Detailed ways
以下通过特定的具体实例说明本发明的实施方式,本领域技术人员可由本说明书所揭露的内容轻易地了解本发明的其他优点与功效。本发明还可以通过另外不同的具体实施方式加以实施或应用,本说明书中的各项细节也可以基于不同观点与应用,在没有背离本发明的精神下进行各种修饰或改变。The following describes the embodiments of the present invention through specific examples. Those skilled in the art can easily understand other advantages and effects of the present invention from the content disclosed in this specification. The present invention can also be implemented or applied through other different specific embodiments. Various details in this specification can also be modified or changed in various ways based on different viewpoints and applications without departing from the spirit of the present invention.
本实施例提供一种石墨烯谐振子,包括衬底芯片,所述的衬底芯片通过刻蚀硅晶片来制备,衬底芯片包括底部的硅层,硅层上表面左右两端有二氧化硅层,二氧化硅层中间设有凹槽,凹槽正上方覆盖石墨烯薄膜,石墨烯薄膜通过机械剥离块状石墨得到,石墨烯薄膜的两端覆盖部分二氧化硅层,衬底芯片和石墨烯薄膜之间构成一个光学谐振腔。This embodiment provides a graphene resonator, including a substrate chip. The substrate chip is prepared by etching a silicon wafer. The substrate chip includes a silicon layer at the bottom. There are silicon dioxide on the left and right ends of the upper surface of the silicon layer. layer, there is a groove in the middle of the silicon dioxide layer, and the graphene film is covered directly above the groove. The graphene film is obtained by mechanically peeling off block graphite. Both ends of the graphene film cover part of the silicon dioxide layer, the substrate chip and the graphite An optical resonant cavity is formed between the ene films.
在激光入射到该光学谐振腔时,蓝失谐激光在石墨烯上产生的光辐射压力会随着激光功率的增大,导致石墨烯谐振子中的声子耗散减小,直至为零;此后石墨烯谐振子中的声子会表现出类似激光中光子受激辐射过程,声子数随泵浦激光功率增加表现出明显的阈值效应,即出现了声子激射现象,得到声子激射器。When the laser is incident on the optical resonator, the optical radiation pressure generated by the blue detuned laser on the graphene will increase as the laser power increases, causing the phonon dissipation in the graphene resonator to decrease until it reaches zero; After that, the phonons in the graphene resonator will show a process similar to the photon stimulated radiation in the laser. The number of phonons will show an obvious threshold effect as the pump laser power increases, that is, the phenomenon of phonon lasing will occur, and the phonon lasing phenomenon will be obtained. launcher.
如图1所示,本实施例还提供一种基于石墨烯谐振子的声子激射器,包括上述石墨烯谐振子8,其为:沿光路方向,依次包括驱动激光源1、和驱动激光源1中心对准的第一光纤耦合器21、和第一光纤耦合器21通过光纤连接的第二光纤耦合器22、和第二光纤耦合器22中心对准的第一半波片31、和第一半波片31中心对准且和第一半波片31夹角呈45度的第一高反镜41、和第一高反镜41的出射光对准的第一偏振分束棱镜51、和第一偏振分束棱镜51的出射光对准的第二半波片32、和第二半波片32的出射光对准的第二偏振分束棱镜52、和第二偏振分束棱镜52的出射光对准的四分之一波片6、和四分之一波片6中心对准的物镜7、和物镜7中心对准的石墨烯谐振子8、石墨烯谐振子8固定在纳米电动位移台9上,和第二偏振分束棱镜52的出射光对准的分束器10、分束器10的一部分出射光和CCD相机11中心对齐、另一部分出射光和第二高反镜42中心对齐,和第二高反镜42的出射光对准的滤波片12、和滤波片12中心对准的光电探测器13、和光电探测器13电性连接的频谱分析仪14,第一偏振分束棱镜51远离第二半波片32的一侧设有照明光源15,照明光源15和所述第一偏振分束棱镜51的出射光对准。As shown in Figure 1, this embodiment also provides a phonon maser based on graphene resonators, including the above-mentioned graphene resonators 8, which include: a driving laser source 1 and a driving laser along the optical path direction. The first optical fiber coupler 21 in which the source 1 is centrally aligned, the second optical fiber coupler 22 connected to the first optical fiber coupler 21 through optical fibers, and the first half-wave plate 31 in which the second optical fiber coupler 22 is centrally aligned, and The first high-reflection mirror 41 is aligned with the center of the first half-wave plate 31 and forms an angle of 45 degrees with the first half-wave plate 31 , and the first polarizing beam splitting prism 51 is aligned with the outgoing light of the first high-reflection mirror 41 , the second half-wave plate 32 aligned with the outgoing light of the first polarizing beam splitting prism 51, the second polarizing beam splitting prism 52 aligned with the outgoing light of the second half-wave plate 32, and the second polarizing beam splitting prism. The quarter-wave plate 6 aligned with the exit light of 52, the objective lens 7 aligned with the center of the quarter-wave plate 6, the graphene resonator 8 aligned with the center of the objective lens 7, the graphene resonator 8 is fixed on On the nano electric displacement stage 9, the beam splitter 10 is aligned with the outgoing light of the second polarizing beam splitting prism 52. A part of the outgoing light of the beam splitter 10 is aligned with the center of the CCD camera 11, and the other part of the outgoing light is aligned with the second high reflectance The center of the mirror 42 is aligned, the filter 12 is aligned with the emitted light of the second high-reflection mirror 42, the photodetector 13 is aligned with the center of the filter 12, and the spectrum analyzer 14 is electrically connected to the photodetector 13. An illumination light source 15 is disposed on a side of a polarizing beam splitting prism 51 away from the second half-wave plate 32 , and the illuminating light source 15 is aligned with the outgoing light of the first polarizing beam splitting prism 51 .
具体的,本实施例中,所述分束器10为10:90分束器。纳米电动位移台9是个三轴位移台,沿空间三维方向移动,现有技术中出现了很多三维位移台,均可用于本发明;初始时通过位移台的移动使物镜7中心和石墨烯谐振器8中心对准。驱动激光源采用633nm单模连续光激光器。633nm的单模光纤和光纤准直器,把激光耦合进自由空间光路之中。激光器的激光功率为35mW。白色LED作为CCD成像的照明光源;Specifically, in this embodiment, the beam splitter 10 is a 10:90 beam splitter. The nano electric displacement stage 9 is a three-axis displacement stage that moves along the three-dimensional direction of space. There are many three-dimensional displacement stages in the prior art, all of which can be used in the present invention; initially, the center of the objective lens 7 and the graphene resonator are moved by the movement of the displacement stage. 8 Center alignment. The driving laser source uses a 633nm single-mode continuous light laser. 633nm single-mode fiber and fiber collimator couple the laser into the free space optical path. The laser power of the laser is 35mW. White LED is used as the lighting source for CCD imaging;
光路中的半波片固定在旋转安装座上,转动波片,利用激光的偏振特性,可以便捷调节波片后续光路的激光强度。The half-wave plate in the optical path is fixed on the rotating mounting base. By rotating the wave plate, the laser intensity of the subsequent optical path of the wave plate can be easily adjusted by using the polarization characteristics of the laser.
高反镜可以方便改变光路方向,以减小整个系统的占用面积。Highly reflective mirrors can easily change the direction of the optical path to reduce the area occupied by the entire system.
第一偏振分束棱镜51利用其偏振分束的特性改变光路方向,并且使白色辅助照明光源轻松的耦合入光路之中。The first polarizing beam splitting prism 51 uses its polarizing beam splitting characteristics to change the direction of the light path, and allows the white auxiliary illumination light source to be easily coupled into the light path.
第二偏振分束棱镜52和四分之一波片6构成光学隔离器,保证带有偏振特性的激光不会沿着入射光路返回,以便于进行成像与光电探测提取石墨烯谐振子的谐振模式。The second polarization beam splitting prism 52 and the quarter-wave plate 6 form an optical isolator to ensure that the laser with polarization characteristics will not return along the incident light path, so as to facilitate imaging and photoelectric detection to extract the resonance mode of the graphene resonator. .
激光通过物镜聚焦在石墨烯谐振子8上,形成1um大小的光斑,此处我们选择放大倍数为100倍,工作距离为0.9mm,数值孔径(NA)为0.8的物镜。The laser is focused on the graphene resonator 8 through the objective lens, forming a spot of 1um size. Here we choose an objective lens with a magnification of 100 times, a working distance of 0.9mm, and a numerical aperture (NA) of 0.8.
石墨烯谐振子8垂直固定在电动纳米位移台上,如图1所示。石墨烯谐振子8为石墨烯薄膜悬浮于5um硅衬底芯片圆孔所构成。The graphene resonator 8 is vertically fixed on the electric nanodisplacement stage, as shown in Figure 1. The graphene resonator 8 is composed of a graphene film suspended in a 5um silicon substrate chip circular hole.
电动纳米位移台用于负载样品精确运动,步距为100nm,可移动范围为5mm,来保证激光光斑准确聚焦到石墨烯机械振子上的目标位置。The electric nanodisplacement stage is used to carry the sample for precise movement, with a step size of 100nm and a movable range of 5mm to ensure that the laser spot is accurately focused on the target position on the graphene mechanical oscillator.
光束首次通过物镜后,石墨烯谐振子表面反射的光束和石墨烯下方硅衬底芯片表面反射的光束,发生了干涉,聚焦的激光对石墨烯产生了辐射压力,如图2所示。该干涉光束再次经过物镜后,被偏振分束棱镜改变光路方向,照射在90:10的光学分束器上。After the light beam passes through the objective lens for the first time, interference occurs between the light beam reflected on the surface of the graphene resonator and the light beam reflected on the surface of the silicon substrate chip below the graphene. The focused laser generates radiation pressure on the graphene, as shown in Figure 2. After the interference beam passes through the objective lens again, the direction of the optical path is changed by the polarizing beam splitter prism, and is illuminated on the 90:10 optical beam splitter.
90:10的光学分束器,将光学谐振腔反射的激光光束分为两束,一束用于成像;另一束则用于光电探测器,光电探测器会把光学信号转换为电学信号。此处选择响应率为0.3A/W,覆盖633nm的自由空间光光电探测器。The 90:10 optical beam splitter divides the laser beam reflected by the optical resonator into two beams, one beam is used for imaging; the other beam is used for the photodetector, which converts the optical signal into an electrical signal. Here, a free-space light photodetector with a response rate of 0.3A/W and covering 633nm is selected.
频谱分析仪将电学信号处理,得到石墨烯谐振子各个模式的振动信息,如图3,(a)图、(b)图为测试样品光镜和电镜示意图,(c)图为悬浮石墨烯谐振子测量频谱图。此处图3(c)因频谱范围的选择会显示不同范围的振动信息,仅为示例,因根据具体实验要求选择合适的频谱范围。如果得不到类似的振动信息,则应当检查:1.石墨烯谐振子的制备是否成功;2.激光光斑是否打在石墨烯谐振子上的正确位置;3.系统噪声是否将谐振模式信息淹没。The spectrum analyzer processes the electrical signals to obtain the vibration information of each mode of the graphene resonator, as shown in Figure 3. (a) and (b) are schematic diagrams of the light microscope and electron microscope of the test sample, and (c) shows the resonance of suspended graphene. Sub-measurement spectrogram. Figure 3(c) here will display different ranges of vibration information due to the selection of the spectrum range. This is only an example, because the appropriate spectrum range is selected according to specific experimental requirements. If similar vibration information cannot be obtained, you should check: 1. Whether the preparation of the graphene resonator is successful; 2. Whether the laser spot hits the correct position on the graphene resonator; 3. Whether the system noise drowns out the resonance mode information .
调节光路中半波片和四分之一波片,使聚焦在悬浮石墨烯上的激光功率从300uW平稳变化到6.3mW,在功率变化的这一过程中,以合适的功率间隔划分,重复记录各功率情况下频谱的数据以及图像信息,将多组类似图3的结果数据整合绘图,观测频谱中谐振模式的的变化。如图4所示,在增大入射光功率的情况下,石墨烯谐振子的谐振模式出现了变化:出现明显的谐振峰,谐振峰线宽逐渐减小,峰值逐渐增大。这一过程声子耗散逐渐减小至零,声子表现出明显的阈值效应,即声子出现激射现象。Adjust the half-wave plate and quarter-wave plate in the optical path so that the laser power focused on the suspended graphene changes smoothly from 300uW to 6.3mW. During the process of power change, divide it into appropriate power intervals and record repeatedly. The spectrum data and image information under each power condition are integrated into drawings from multiple sets of result data similar to Figure 3, and the changes in the resonance mode in the spectrum are observed. As shown in Figure 4, when the incident light power is increased, the resonance mode of the graphene resonator changes: an obvious resonance peak appears, the line width of the resonance peak gradually decreases, and the peak value gradually increases. In this process, the phonon dissipation gradually decreases to zero, and the phonons show an obvious threshold effect, that is, the phonons lasing.
驱动激光源1的泵浦激光同时用于激光干涉测量谐振子振动模式,激光以自由空间光的形式通过物镜聚焦照射在石墨烯谐振子8表面,石墨烯谐振子8与硅衬底芯片之间形成光学谐振腔,随着石墨烯谐振子8的振动,光学谐振腔反射的激光光强被同步调制,通过光电探测器转换为电信号再经频谱分析仪即可提取出石墨烯谐振子的谐振模式。The pump laser driving the laser source 1 is also used for laser interference measurement of the vibration mode of the resonator. The laser is focused and irradiated on the surface of the graphene resonator 8 through the objective lens in the form of free space light, between the graphene resonator 8 and the silicon substrate chip. An optical resonant cavity is formed. As the graphene resonator 8 vibrates, the laser light intensity reflected by the optical resonant cavity is synchronously modulated. It is converted into an electrical signal through a photodetector and then passed through a spectrum analyzer to extract the resonance of the graphene resonator. model.
本实施例还提供一种上述基于石墨烯谐振子的声子激射器的工作方法,其为:驱动激光源1发出激光,经过第一光纤耦合器21准直收集、第二光纤耦合器22再准直后,平行进入第一半波片31,第一半波片31的出射光被该半波片改变偏振后,经第一高反镜41改变光路方向,使激光垂直入射到第一偏振分束棱镜51,第一偏振分束棱镜51将具有偏振方向的激光反射,使第一偏振分束棱镜51的出射光垂直经第二半波片32中心,被第二半波片32改变偏振态的激光,进入第二偏振分束棱镜52,此时激光透过第二偏振分束棱镜52,并经四分之一波片6改变偏振态,四分之一波片6的出射光经过物镜7聚焦为1μm光斑后,照射纳米电动位移台9上垂直固定的石墨烯谐振子8,石墨烯谐振子8反射的激光经物镜7收集、被四分之一波片6再次改变偏振态后,第二次经过第二偏振分束棱镜52,第二偏振分束棱镜52反射此偏振的激光,使该激光进入分束器10,分束器10对激光光束进行分束,一束进入CCD相机用于成像,另一束经第二高反镜42改变光路方向,激光经过滤波片12过滤后,保证与驱动激光源1同波长的激光进入光电探测器13,光电探测器13将接受的光信号转换为电信号,该电信号经频谱分析仪14提取石墨烯谐振子8的谐振模式,所有的半波片和四分之一波片也用于调节光路中各部分激光的功率;纳米电动位移台9用于调节石墨烯谐振子的位置,使得激光光斑能够准确聚焦到石墨烯谐振子的目标位置。This embodiment also provides a working method of the above-mentioned graphene resonator-based phonon maser, which is: driving the laser source 1 to emit laser, collimating and collecting it through the first fiber coupler 21, the second fiber coupler 22 After re-collimation, it enters the first half-wave plate 31 in parallel. After the emitted light from the first half-wave plate 31 is polarized by the half-wave plate, the light path direction is changed by the first high-reflective mirror 41, so that the laser is vertically incident on the first half-wave plate. Polarizing beam splitting prism 51, the first polarizing beam splitting prism 51 reflects the laser with the polarization direction, so that the emitted light of the first polarizing beam splitting prism 51 passes vertically through the center of the second half-wave plate 32 and is changed by the second half-wave plate 32 The polarized laser enters the second polarization beam splitting prism 52. At this time, the laser passes through the second polarization beam splitting prism 52 and changes the polarization state through the quarter-wave plate 6. The exit light of the quarter-wave plate 6 After being focused by the objective lens 7 into a 1 μm spot, the vertically fixed graphene resonator 8 on the nanoelectric displacement stage 9 is irradiated. The laser reflected by the graphene resonator 8 is collected by the objective lens 7 and the polarization state is changed again by the quarter-wave plate 6 After that, it passes through the second polarization beam splitting prism 52 for the second time. The second polarization beam splitting prism 52 reflects the polarized laser light, causing the laser light to enter the beam splitter 10. The beam splitter 10 splits the laser beam, and one beam enters The CCD camera is used for imaging, and the other beam changes the direction of the optical path through the second high-reflection mirror 42. After the laser is filtered by the filter 12, it is ensured that the laser with the same wavelength as the driving laser source 1 enters the photodetector 13, and the photodetector 13 will accept The optical signal is converted into an electrical signal, and the electrical signal is extracted by the spectrum analyzer 14 to extract the resonance mode of the graphene resonator 8. All half-wave plates and quarter-wave plates are also used to adjust the power of each part of the laser in the optical path; The nanoelectric displacement stage 9 is used to adjust the position of the graphene resonator so that the laser spot can be accurately focused on the target position of the graphene resonator.
进一步的,将波长为633nm的驱动连续光激光源聚焦到光学谐振腔上,再利用90:10分束器,将石墨烯谐振子8反射的激光光束分为两束,其中一束用于成像,另一束则被光电探测器转换为电信号,通过频谱分析后经频谱分析仪提取石墨烯机械振子的谐振模式,获得谐振子振动的频域信息;随着激光功率增加,声子出现了明显的阈值效应,声子发生激射,成为一个声子激射器;保证装置正常运行,能观测到石墨烯谐振子8的机械振动模式后,旋转光路中的半波片和四分之一波片,来改变聚焦在石墨烯薄膜上的激光功率;在不损坏石墨烯薄膜的前提下,增加入射激光的光功率,根据频谱信息中振动模式的幅值变化判断声子激射器的实现情况。Further, a driven continuous light laser source with a wavelength of 633 nm is focused on the optical resonant cavity, and a 90:10 beam splitter is used to divide the laser beam reflected by the graphene resonator 8 into two beams, one of which is used for imaging. , the other beam is converted into an electrical signal by a photodetector. After spectrum analysis, the resonance mode of the graphene mechanical oscillator is extracted by a spectrum analyzer to obtain the frequency domain information of the resonator vibration. As the laser power increases, phonons appear. Obvious threshold effect, phonons maser and become a phonon maser; to ensure normal operation of the device, after observing the mechanical vibration mode of graphene resonator 8, rotate the half-wave plate and quarter-wave plate in the optical path Wave plate is used to change the laser power focused on the graphene film; without damaging the graphene film, the optical power of the incident laser is increased, and the realization of the phonon maser is judged based on the amplitude change of the vibration mode in the spectrum information. Condition.
其他不同二维材料的谐振子实施例均可实现声子激射。Other resonator embodiments of different two-dimensional materials can achieve phonon lasing.
石墨烯谐振子,具有材料制备简单、质量小、物理性能稳定、以及品质因子高的特性。涉及到的石墨烯材料,是通过机械剥离块状石墨得到的层状石墨烯样品。再利用二维材料转移平台,将机械剥离获得的少层石墨烯样品转移到具有微结构的硅衬底芯片上悬浮,得到所需石墨烯谐振子。此外,转移其他二维材料,例如MoS2、WSe2制备的谐振子,也可与激光、微电路耦合制备成光机械、微机电系统,具有广泛的研究和应用前景。Graphene resonators have the characteristics of simple material preparation, small mass, stable physical properties, and high quality factor. The graphene material involved is a layered graphene sample obtained by mechanically peeling off bulk graphite. Then, using a two-dimensional material transfer platform, the few-layer graphene sample obtained by mechanical exfoliation is transferred to a silicon substrate chip with a microstructure and suspended to obtain the required graphene resonator. In addition, resonators prepared by transferring other two-dimensional materials, such as MoS 2 and WSe 2 , can also be coupled with lasers and microcircuits to prepare opto-mechanical and micro-electromechanical systems, which has broad research and application prospects.
上述实施例仅例示性说明本发明的原理及其功效,而非用于限制本发明。任何熟悉此技术的人士皆可在不违背本发明的精神及范畴下,对上述实施例进行修饰或改变。因此,凡所属技术领域中具有通常知识者在未脱离本发明所揭示的精神与技术思想下所完成的一切等效修饰或改变,仍应由本发明的权利要求所涵盖。The above embodiments only illustrate the principles and effects of the present invention, but are not intended to limit the present invention. Anyone familiar with this technology can modify or change the above embodiments without departing from the spirit and scope of the invention. Therefore, all equivalent modifications or changes made by those with ordinary knowledge in the technical field without departing from the spirit and technical ideas disclosed in the present invention shall still be covered by the claims of the present invention.
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