CN112274451A - Moisturizing transparent nutritional shampoo and preparation method thereof - Google Patents
Moisturizing transparent nutritional shampoo and preparation method thereof Download PDFInfo
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- CN112274451A CN112274451A CN202011213906.3A CN202011213906A CN112274451A CN 112274451 A CN112274451 A CN 112274451A CN 202011213906 A CN202011213906 A CN 202011213906A CN 112274451 A CN112274451 A CN 112274451A
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- mixture
- transparent
- moisturizing
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- shampoo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
Abstract
The invention discloses moisturizing transparent nourishing shampoo and a preparation method thereof, wherein the shampoo comprises 0.5-2 parts of thickening agent, 0.5-2 parts of hair conditioner, 3-5 parts of vegetable oil, 1-3 parts of cationic polymer, 0.1-1 part of pH regulator, 0.2-1.0 part of preservative, 20-30 parts of surfactant, 0.2-0.8 part of aromatizing agent, 0.5-3 parts of humectant and 50-80 parts of deionized water in parts by weight. By adding various cationic polymers and vegetable oil into the components of the shampoo, the vegetable oil, panthenol and the cationic polymers can provide multiple care for the hair; the hair is glossy and smooth after shampooing, is easy to comb, does not contain silicone oil, avoids the problems of scalp itching and the like caused by long-term use, and meanwhile, the moisturizing transparent nutritional shampoo and the preparation method thereof provided by the invention have simple steps and are easy to manufacture.
Description
Technical Field
The invention relates to a shampoo, in particular to a moisturizing transparent nutritional shampoo and a preparation method thereof.
Background
With the improvement of the living standard of consumers, the quality requirement of the shampoo is higher and higher, the smoothness of hair can be improved by adding the silicone oil in the shampoo containing the silicone oil in the market, but the silicone oil can be deposited on the hair after long-term use, so that the phenomena of scalp itching and even hair loss are caused, and the silicone oil is difficult to degrade, so that the potential environmental protection problem is caused. With the improvement of living standard, people pay more and more attention to the concept of scalp care, and consumers want to have a shampoo similar to skin care to wash hair and care scalp. Most of transparent shampoo is surfactant composition, and the problems that the scalp is dry and the secretion of oil is unbalanced because hair is dry and difficult to comb after cleaning and decontamination, and the oil of the scalp is seriously removed are always difficult to solve. There is a need in the market for a conditioner composition that will care the scalp and moisturize the hair and provide good combing properties.
Disclosure of Invention
One of the purposes of the invention is to provide a moisturizing transparent nourishing shampoo and a preparation method thereof aiming at the defects, so as to hopefully solve the technical problems that the similar shampoo in the prior art adds silicone oil for smoothing hair, the scalp is easy to itch, the potential environmental protection problem is brought, and the like.
In order to solve the technical problems, the invention adopts the following technical scheme:
the invention provides a moisturizing transparent nourishing shampoo, which comprises, by weight, 0.5-2 parts of a thickening agent, 0.5-2 parts of a hair conditioner, 3-5 parts of vegetable oil, 0.5-3 parts of a cationic polymer, 0.1-1 part of a pH regulator, 0.2-1.0 part of a preservative, 20-30 parts of a surfactant, 0.2-0.8 part of an aromatizing agent, 0.2-3 parts of a humectant and 50-80 parts of deionized water.
Preferably, the further technical proposal is as follows: the thickener is one or more of cocamide MEA, polyoxyethylene-55 propylene glycol oleate, and sodium chloride.
The further technical scheme is as follows: the hair conditioner is one or more of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, panthenol and allantoin.
The further technical scheme is as follows: the vegetable oil is a composition prepared by mixing camellia seed oil, palm oil, almond oil, avocado oil, wheat germ oil, hydrogenated castor oil and sesame oil according to the proportion of 1: 1: 0.5: 0.5: 1: 2: 0.1.
The further technical scheme is as follows: the cationic polymer is one or a mixture of polyquaternium-10 and hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride; one or a mixture of two of the pH regulator sodium hydroxide and citric acid.
The further technical scheme is as follows: the preservative is one or a mixture of phenoxyethanol, methyl paraben and DMDM-H; the aromatizer is a daily chemical essence.
The further technical scheme is as follows: the surfactant is one or more of laureth phosphate MIPA salt, coco betaine, sodium laureth sulfate, cocamidopropyl betaine and PEG-60 hydrogenated castor oil; the humectant is one or a mixture of two of polyethylene glycol-8 and sodium hyaluronate.
The invention also provides a preparation method of the moisturizing transparent nutritional shampoo, the method comprises the following steps of weighing the thickening agent, the hair conditioner, the vegetable oil, the cationic polymer, the pH regulator, the preservative, the surfactant, the aromatizing agent, the humectant and the deionized water:
step A, vegetable oil pretreatment; heating the surfactant and the vegetable oil to 50 ℃, uniformly stirring, keeping the temperature and homogenizing for a first unit time, and cooling for later use to obtain a first mixture;
step B, adding deionized water into a dispersion machine, setting the stirring speed to be 1200-1800 r/min, adding the cationic polymer into the water in the stirring process, and fully stirring to completely and uniformly disperse the cationic polymer in the deionized water to obtain a second mixture;
step C, transferring the second mixture to a reaction kettle, adding a humectant and a hair conditioner, stirring and heating to 80-85 ℃; then adding a surfactant, and continuously stirring for a second unit time until the mixture is uniform and transparent; adding antiseptic and perfuming agent, stirring, and cooling to below 25 deg.C;
and D, adding the first mixture into the cooled second mixture in batches, repeatedly stirring until the mixture is transparent, then adding a pH regulator, stirring, and controlling the pH value of the materials to be 5.5-6.0 to obtain a finished product of the shampoo.
Preferably, the further technical scheme is as follows: the first unit time is 10min, and the second unit time is 30 min.
The further technical scheme is as follows: and D, adding the first mixture into the second mixture in five times in the step D, and adding the mixture into the second mixture once after stirring until the mixture is transparent.
Compared with the prior art, the invention has the following beneficial effects: by adding various cationic polymers and vegetable oil into the components of the shampoo, the vegetable oil, panthenol and the cationic polymers can provide multiple care for the hair; the hair is glossy and smooth after shampooing, is easy to comb, does not contain silicone oil, avoids the problems of scalp itching and the like caused by long-term use, and meanwhile, the moisturizing transparent nutritional shampoo and the preparation method thereof provided by the invention have simple steps and are easy to manufacture.
Detailed Description
The invention is further illustrated by the following specific examples.
Example one
In this example, a moisturizing transparent nourishing shampoo is prepared, and the total amount of the prepared examples is g, firstly, the raw materials, specifically, 1.9g of thickener, 0.8g of conditioner for hair, 3g of vegetable oil, 0.5g of cationic polymer, 0.35g of pH regulator, 0.8g of preservative, 28g of surfactant, 0.5g of fragrance, 0.5g of humectant, and 63.65g of deionized water are weighed according to the following standards.
Wherein the thickener is a mixture of 0.8g of polyoxyethylene-55 propylene glycol oleate and 1.1g of sodium chloride, the hair conditioner is a mixture of 0.5g of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 0.2g of panthenol and 0.1g of allantoin, the cationic polymer is polyquaternium-10, the pH regulator is a mixture of 0.05g of sodium hydroxide and 0.3g of citric acid, the preservative is phenoxyethanol, the flavoring agent is daily chemical essence, and the humectant is polyoxyethylene-8.
In addition, the vegetable oil and fat is mixture of camellia seed oil, palm oil, almond oil, avocado oil, wheat germ oil, hydrogenated castor oil and sesame oil according to the proportion of 1: 1: 0.5: 0.5: 1: 2: 0.1. The surfactant is a mixture of 12g of lauryl alcohol ether phosphate MIPA salt, 2g of PEG-60 hydrogenated castor oil, 6g of cocobetaine and 8g of sodium laureth sulfate.
After the preparation of the raw materials is finished, the moisturizing transparent nutritional shampoo is prepared according to the following steps:
step 1, pretreating vegetable oil; heating surfactant and vegetable oil at 50 deg.C, stirring, homogenizing for 8-15min, and cooling to obtain a first mixture;
step 2, adding deionized water into a dispersion machine, setting the stirring speed to be 1200-1800 r/min, adding the cationic polymer into the water in the stirring process, and fully stirring to completely and uniformly disperse the cationic polymer in the deionized water to obtain a second mixture;
step 3, transferring the second mixture to a reaction kettle, adding a humectant and a hair conditioner, stirring and heating to 80-85 ℃; then adding a surfactant, and continuously stirring for 30-45min to achieve uniformity and transparency; adding antiseptic and perfuming agent, stirring for more than 30min, and cooling to below 25 deg.C;
and 4, adding the first mixture into the cooled second mixture in batches, repeatedly stirring until the mixture is transparent, then adding a pH regulator, stirring, and controlling the pH value of the materials to be 5.5-6.0 to obtain a finished product of the shampoo.
Example two
In this example, a moisturizing transparent nourishing shampoo is prepared, and the total amount of the prepared example is 300g, firstly, raw materials, specifically, 5.1g of thickener, 2.4g of conditioner for hair, 12g of vegetable oil, 2.4g of cationic polymer, 0.9g of pH regulator, 2.4g of preservative, 85.5g of surfactant, 1.5g of fragrance, 3.3g of humectant, and 183.6g of deionized water are weighed according to the following standard.
The hair conditioner is a mixture of 1.5g of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 0.6g of panthenol and 0.3g of allantoin, the cationic polymer is a mixture of 2.4g of polyquaternium-10 and 0.9g of hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride, the pH regulator is a mixture of 0.15g of sodium hydroxide and 0.75g of citric acid, the preservative is phenoxyethanol, the flavoring agent is a daily chemical essence, and the humectant is sodium hyaluronate.
In addition, the vegetable oil and fat is mixture of camellia seed oil, palm oil, almond oil, avocado oil, wheat germ oil, hydrogenated castor oil and sesame oil according to the proportion of 1: 1: 0.5: 0.5: 1: 2: 0.1. The surfactant is a mixture of 45g of lauryl alcohol ether phosphate MIPA salt, 6g of PEG-60 hydrogenated castor oil, 18g of cocobetaine and 16.5g of sodium laureth sulfate.
After the preparation of the raw materials is finished, the moisturizing transparent nutritious shampoo is prepared according to the method of the embodiment 1, and the homogenizing and stirring time can be slightly adjusted according to the preparation amount.
EXAMPLE III
In this example, a moisturizing transparent nourishing shampoo is prepared, and the total amount of the prepared example is 500g, firstly, the raw materials, specifically, 10g of thickener, 4g of hair conditioner, 25g of vegetable oil, 5g of cationic polymer, 1.75g of pH regulator, 2.5g of preservative, 135g of surfactant, 2g of fragrance, 1g of humectant, and 313.75g of deionized water are weighed according to the following standard.
The hair conditioner is a mixture of 2.5g of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 1g of panthenol and 0.5g of allantoin, the cationic polymer is a mixture of 1.5g of polyquaternium-10 and 3.5g of hydroxypropyl guar hydroxypropyl trimonium chloride, the pH regulator is a mixture of 0.25g of sodium hydroxide and 1.5g of citric acid, the preservative is phenoxyethanol, the fragrance giving agent is a daily chemical essence, and the humectant is sodium hyaluronate.
In addition, the vegetable oil and fat is mixture of camellia seed oil, palm oil, almond oil, avocado oil, wheat germ oil, hydrogenated castor oil and sesame oil according to the proportion of 1: 1: 0.5: 0.5: 1: 2: 0.1. The surfactant is a mixture of 60g of lauryl alcohol ether phosphate MIPA salt, 7.5g of PEG-60 hydrogenated castor oil, 30g of cocobetaine and 37.5g of sodium laureth sulfate.
After the preparation of the raw materials is finished, the moisturizing transparent nutritious shampoo is prepared according to the method of the embodiment 1, and the homogenizing and stirring time can be slightly adjusted according to the preparation amount.
Example four
The present example is a test example of the moisturizing transparent nourishing shampoo prepared based on the above three examples, and specifically includes a cold and hot test and a room temperature standing test. The cold and hot test comprises placing the product into a transparent sealed glass bottle, refrigerating in a refrigerator at-10 deg.C for 3 months, and observing for no deterioration; no layering phenomenon in a thermostat at 48 ℃ for three months. The room temperature placing test is that the sealed container is placed for 1 year at room temperature, and the physical and chemical indexes are unchanged, and the phenomena of oil-water separation and deterioration are avoided. In addition, the prepared moistening transparent nutritional shampoo has good softness, moistening degree and combing property of hair through trial tests of consumers, and reduces the phenomena of scalp itching and dry peeling of the consumers.
In addition to the foregoing, it should be noted that reference throughout this specification to "one embodiment," "another embodiment," "an embodiment," or the like, means that a particular feature, structure, or characteristic described in connection with the embodiment is included in at least one embodiment described generally in this application. The appearances of the same phrase in various places in the specification are not necessarily all referring to the same embodiment. Further, when a particular feature, structure, or characteristic is described in connection with any embodiment, it is submitted that it is within the scope of the invention to effect such feature, structure, or characteristic in connection with other embodiments.
Although the invention has been described herein with reference to a number of illustrative embodiments thereof, it should be understood that numerous other modifications and embodiments can be devised by those skilled in the art that will fall within the spirit and scope of the principles of this disclosure. More specifically, various variations and modifications are possible in the component parts and/or arrangements of the subject combination arrangement within the scope of the disclosure and claims of this specification. In addition to variations and modifications in the component parts and/or arrangements, other uses will also be apparent to those skilled in the art.
Claims (10)
1. The moisturizing transparent nutritious shampoo is characterized by comprising, by weight, 0.5-2 parts of a thickening agent, 0.5-2 parts of a hair conditioner, 3-5 parts of vegetable oil, 0.5-3 parts of a cationic polymer, 0.1-1 part of a pH regulator, 0.2-1.0 part of a preservative, 20-30 parts of a surfactant, 0.2-0.8 part of an aromatizing agent, 0.2-3 parts of a humectant and 50-80 parts of deionized water.
2. The moisturizing transparent nourishing shampoo of claim 1, characterized by: the thickener is one or more of cocamide MEA, polyoxyethylene-55 propylene glycol oleate, and sodium chloride.
3. The moisturizing transparent nourishing shampoo of claim 1, characterized by: the hair conditioner is one or more of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, panthenol and allantoin.
4. The moisturizing transparent nourishing shampoo of claim 1, characterized by: the vegetable oil is a composition prepared by mixing camellia seed oil, palm oil, almond oil, avocado oil, wheat germ oil, hydrogenated castor oil and sesame oil according to the proportion of 1: 1: 0.5: 0.5: 1: 2: 0.1.
5. The moisturizing transparent nourishing shampoo of claim 1, characterized by: the cationic polymer is one or a mixture of polyquaternium-10 and hydroxypropyl guar hydroxypropyl trimethyl ammonium chloride; one or a mixture of two of the pH regulator sodium hydroxide and citric acid.
6. The moisturizing transparent nourishing shampoo of claim 1, characterized by: the preservative is one or a mixture of phenoxyethanol, methyl paraben and DMDM-H; the aromatizer is a daily chemical essence.
7. The moisturizing transparent nourishing shampoo of claim 1, characterized by: the surfactant is one or more of laureth phosphate MIPA salt, coco betaine, sodium laureth sulfate, cocamidopropyl betaine and PEG-60 hydrogenated castor oil; the humectant is one or a mixture of two of polyethylene glycol-8 and sodium hyaluronate.
8. A method for preparing moisturizing transparent nourishing shampoo, characterized in that the method is that the thickening agent, hair conditioner, vegetable oil, cationic polymer, pH regulator, antiseptic, surfactant, aromatizing agent, humectant and deionized water are weighed according to the claims 1 to 7, and the following steps are carried out:
step A, vegetable oil pretreatment; heating the surfactant and the vegetable oil to 50 ℃, uniformly stirring, keeping the temperature and homogenizing for a first unit time, and cooling for later use to obtain a first mixture;
step B, adding deionized water into a dispersion machine, setting the stirring speed to be 1200-1800 r/min, adding the cationic polymer into the water in the stirring process, and fully stirring to completely and uniformly disperse the cationic polymer in the deionized water to obtain a second mixture;
step C, transferring the second mixture to a reaction kettle, adding a humectant and a hair conditioner, stirring and heating to 80-85 ℃; then adding a surfactant, and continuously stirring for a second unit time until the mixture is uniform and transparent; adding antiseptic and perfuming agent, stirring, and cooling to below 25 deg.C;
and D, adding the first mixture into the cooled second mixture in batches, repeatedly stirring until the mixture is transparent, then adding a pH regulator, stirring, and controlling the pH value of the materials to be 5.5-6.0 to obtain a finished product of the shampoo.
9. The method of making a moisturizing transparent nourishing shampoo according to claim 1, characterized in that: the first unit time is 10min, and the second unit time is 30 min.
10. The method of making a moisturizing transparent nourishing shampoo according to claim 1, characterized in that: and D, adding the first mixture into the second mixture in five times in the step D, and adding the mixture into the second mixture once after stirring until the mixture is transparent.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106265169A (en) * | 2016-10-12 | 2017-01-04 | 广州丹奇日用化工厂有限公司 | A kind of without silicone oil shampoo |
CN107375053A (en) * | 2017-06-16 | 2017-11-24 | 曾万祥 | A kind of ginseng and Chinese angelica root is without silicone oil shampoo and preparation method thereof |
CN111529466A (en) * | 2020-05-20 | 2020-08-14 | 南京夏悦贸易有限公司 | Washing-free protein nourishing hair-moistening cream and preparation method thereof |
-
2020
- 2020-11-04 CN CN202011213906.3A patent/CN112274451A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106265169A (en) * | 2016-10-12 | 2017-01-04 | 广州丹奇日用化工厂有限公司 | A kind of without silicone oil shampoo |
CN107375053A (en) * | 2017-06-16 | 2017-11-24 | 曾万祥 | A kind of ginseng and Chinese angelica root is without silicone oil shampoo and preparation method thereof |
CN111529466A (en) * | 2020-05-20 | 2020-08-14 | 南京夏悦贸易有限公司 | Washing-free protein nourishing hair-moistening cream and preparation method thereof |
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Application publication date: 20210129 |