CN112245487A - Mould detoxifying additive for animals and preparation method thereof - Google Patents
Mould detoxifying additive for animals and preparation method thereof Download PDFInfo
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- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/287—Chrysanthemum, e.g. daisy
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- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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Abstract
The invention discloses a mould detoxification additive for animals and a preparation method thereof, belonging to the field of feed additives. The adhesive comprises the following substances in parts by weight: 30-50 parts of gardenia, 30-50 parts of liquorice, 15-30 parts of chrysanthemum and 1-5 parts of esterified glucomannan. The additive of the invention fully mixes the esterified glucomannan with adsorption and anti-mildew effects with the Chinese herbal medicines of gardenia, liquorice and chrysanthemum with detoxification functions, the esterified glucomannan has adsorption effect and can be used as a carrier of the traditional Chinese medicine components, the traditional Chinese medicine components can perform detoxification while being adsorbed in the animal body, viruses and mildew in the animal body can be effectively killed, animal vomiting and a series of gastrointestinal diseases can be effectively prevented, and the detoxification effect is good and quick. The product can be mixed with water for drinking, and has effects of accelerating gastrointestinal absorption of medicinal components, and shortening detoxification time.
Description
Technical Field
The invention relates to the field of feed additives, in particular to a mould detoxification additive for animals and a preparation method thereof.
Background
The animal needs to be fed with a large amount of industrially produced feed in the feeding process, the feed is produced from a large amount of grains and byproducts thereof, the feed can generate mildew in the processes of raw material storage and storage of stored products due to various reasons, the mildew is caused by various moulds, and the harmful moulds can cause mould poisoning after the animal takes the feed for a long time.
To solve these problems, various methods are disclosed in the prior art. For example, adsorption type mold removal agents (CN102836694A, CN106578416A) are adopted to reduce the harm of mold in feed to animal bodies through physical adsorption, but the method cannot completely adsorb mycotoxin. For example, vitamin (CN101181008B), licorice powder (CN103918895A), mung bean water and the like are used as antidotes, but the method has the advantages of large dosage of single effective components, long use time and slow action. In addition, publication No. CN107660643A discloses a mold poisoning detoxification additive for animals, which mainly adopts 30-50% of glucose; 10-30% of licorice extract; 10-30% of vitamin C; 10-30% of mung bean extract. And is added into the feed, and the method is to kill the mould in the feed in advance outside the animal body. Sometimes, animals can eat other molds by mistake besides the molds in the feed or enter the animal bodies by other accidents, poisoning still can be caused, and the mold detoxification additive of the dry powder is absorbed slowly and has slow detoxification effect, so that the health of the animals is influenced.
Disclosure of Invention
In order to solve the problems, the invention provides the additive which takes water as a carrier, has quick response and quick absorption and detoxifies mycotoxin in animal bodies.
Furthermore, the invention also provides a preparation method of the mould detoxification additive for animals.
In order to achieve the purpose, the invention is realized by the following technical scheme:
the mould detoxification additive for the animals comprises the following substances in parts by weight: 30-50 parts of gardenia, 30-50 parts of liquorice, 15-30 parts of chrysanthemum and 1-5 parts of esterified glucomannan.
Further, the mould detoxification additive for animals comprises the following substances in parts by weight: 35-45 parts of gardenia, 35-45 parts of liquorice, 15-25 parts of chrysanthemum and 2-4 parts of esterified glucomannan.
Further, the mould detoxification additive for animals comprises the following substances in parts by weight: 40-45 parts of gardenia, 40-45 parts of liquorice, 20-25 parts of chrysanthemum and 3-5 parts of esterified glucomannan.
Further, the mould detoxification additive for animals comprises the following substances in parts by weight: 40 parts of gardenia, 40 parts of liquorice, 20 parts of chrysanthemum and 3 parts of esterified glucomannan.
The preparation method of the mould detoxification additive for animals comprises the following steps:
(1) preparing a gardenia extract: pulverizing fructus Gardeniae into coarse powder, soaking in 70-80% ethanol for 24 hr, percolating at flow rate of 5mL/min, recovering ethanol from percolate under reduced pressure, and concentrating the extractive solution to 1/3-1/2; obtaining gardenia extract;
(2) preparation of a licorice extract: pulverizing Glycyrrhrizae radix into coarse powder, adding deionized water and diastase, boiling for 2-5min, and filtering to obtain filtrate; adding deionized water, and extracting for 1-2 times; comprehensively extracting the filtrate, and concentrating to 1/3 of the original volume to obtain Glycyrrhrizae radix extractive solution;
(3) preparing a chrysanthemum extract: pulverizing flos Chrysanthemi into coarse powder, adding 80% ethanol, ultrasonic extracting for 10-20min, and recovering ethanol under reduced pressure to obtain flos Chrysanthemi extract;
(4) vacuum drying the obtained fructus Gardeniae extract, Glycyrrhrizae radix extract and flos Chrysanthemi extract to obtain powder, and mixing with esterified glucomannan.
Further, the proportion of the gardenia coarse powder and the ethanol in the step (1) is 1 (0.8-1).
Further, the solid-to-liquid ratio of the licorice coarse powder and the deionized water in the step (2) is 1: 2; the adding amount of the saccharifying enzyme is 0.2-0.5% of the licorice coarse powder.
Further, the ratio of the chrysanthemum coarse powder to 80% ethanol in the step (3) is 1: 20.
Further, the ethanol concentration of the gardenia coarse powder soaked in the step (1) is 75%.
The use method of the mould detoxification additive for animals comprises the following steps: the additive obtained by the preparation method is added into drinking water to prepare a solution with the concentration of 0.015-0.02 percent, and the solution is used as drinking water for animals.
Or adding the mould detoxification additive for animals obtained by the preparation method into feed, wherein the addition amount is 1 kg/ton feed.
Gardenia jasminoides is dry fruit of Gardenia jasminoides Ellis of Rubiaceae, and has effects of clearing heat and purging fire, cooling blood and removing toxic substance, and can be used for treating diseases such as heat, vexation, jaundice due to damp-heat, stranguria with blood, pain, hematemesis, epistaxis, conjunctival congestion, swelling and pain, and pyocutaneous disease due to fire toxin. The fructus Gardeniae contains chemical components such as geniposide, genistein, and deshydroxy geniposide. Fructus Gardeniae has inhibitory effect on Staphylococcus aureus, Diplococcus meningitidis, and Catalpa. And the gardenia water has an inhibiting effect on fungi and mold.
Licorice root: has the effects of tonifying qi and strengthening the middle warmer, moistening lung for arresting cough, clearing away heat and toxic materials, relieving spasm and pain, and harmonizing drug properties. It can be used for treating spleen deficiency, asthenia, palpitation, cough, asthma, carbuncle, cellulitis, pharyngitis, abdominal distention, spasm of limbs, and pain. The Glycyrrhrizae radix contains licoflavone, isolicoflavonol, glycyrrhizin, etc. Has effects in resisting pathogenic microorganism, and inhibiting Staphylococcus aureus, Mycobacterium tuberculosis, and Escherichia coli. And the glycyrrhiza polysaccharide has obvious inhibition effect on vesicular stomatitis virus, adenovirus type III, herpes simplex virus type I and vaccinia virus. The licorice has certain detoxifying effect on drug poisoning, food poisoning, in-vivo metabolite poisoning and bacterial toxin poisoning.
Chrysanthemum: has the effects of dispelling wind and heat, suppressing liver yang, removing liver heat, improving eyesight, and clearing away heat and toxic materials. It can be used for treating wind-heat type common cold, early stage of epidemic febrile disease, vertigo due to liver-yang, excessive liver-wind, conjunctival congestion, blurred vision, sore, carbuncle, and toxic swelling. The flos Chrysanthemi contains volatile oil, such as Borneolum, Camphora, and chrysanthenone, and in addition, contains stevioside, adenine, choline, flavone, stachydrine, vitamin A, vitamin B1, vitamin E, amino acids, and Robinia Pseudoacacia. Has antibacterial effect on Staphylococcus aureus, various pathogenic bacilli and dermatophytes. The product also has inhibitory effect on influenza virus PR3 and leptospira.
Esterified glucomannan: the functional carbohydrate with pores can be used as an adsorbent of mycotoxin, and can adsorb different types of mycotoxin simultaneously, so that the transfer amount of the toxin to feed or in vivo is reduced; it also has effects in protecting animal intestine and stomach, and reducing incidence of enteritis and peritonitis.
The mould detoxification additive for animals and the preparation method thereof have the beneficial effects that:
(1) the esterified glucomannan with the adsorption and anti-mildew effects is fully mixed with the Chinese herbal medicines of gardenia, liquorice and chrysanthemum with the detoxification function, the esterified glucomannan has the adsorption effect and can be used as a carrier of the traditional Chinese medicine components, the traditional Chinese medicine components can perform the detoxification effect while being adsorbed in the animal body, the viruses and the mildew in the animal body can be effectively killed, the animal vomiting and a series of gastrointestinal diseases can be effectively prevented, the detoxification effect is good, and the detoxification is quick.
(2) The product can be mixed with water for drinking, and has effects of accelerating gastrointestinal absorption of medicinal components, and shortening detoxification time.
(3) The product can solve the problem that mould-removing component medicine or adsorbent cannot be mixed after production of feed industrial granules, and can be directly fed into gastrointestinal tract by drinking water. Has effects of protecting intestinal health and relieving damage to liver and kidney.
Detailed Description
The present invention will be described in further detail with reference to the following examples.
Example 1
The mould detoxification additive for the animals comprises the following substances in parts by weight: 50g of cape jasmine fruit, 30g of liquorice, 15g of chrysanthemum and 5g of esterified glucomannan.
In this embodiment, the preparation method of the mold detoxification additive for animals comprises the following steps:
(1) preparing a gardenia extract: pulverizing fructus Gardeniae into coarse powder, adding 70% ethanol at a solid-to-liquid ratio of 1:1, soaking for 24 hr, percolating at a flow rate of 5mL/min, recovering ethanol from the percolate under reduced pressure, and concentrating the extractive solution to 1/3; obtaining gardenia extract;
(2) preparation of a licorice extract: pulverizing Glycyrrhrizae radix into coarse powder, adding deionized water and diastase, boiling for 5min, and filtering to obtain filtrate, wherein the solid-to-liquid ratio of Glycyrrhrizae radix coarse powder and deionized water is 1: 2; the adding amount of saccharifying enzyme is 0.2% of Glycyrrhrizae radix coarse powder. Adding deionized water into the filter residue, and extracting for 1 time; combining the filtrates obtained in the two extractions, and concentrating to 1/3 of the original volume to obtain a licorice extract;
(3) preparing a chrysanthemum extract: pulverizing flos Chrysanthemi into coarse powder, adding 80% ethanol, wherein the ratio of flos Chrysanthemi coarse powder to 80% ethanol is 1: 20; ultrasonic extracting for 10min, and recovering ethanol under reduced pressure to obtain flos Chrysanthemi extract;
(4) vacuum drying the obtained fructus Gardeniae extract, Glycyrrhrizae radix extract and flos Chrysanthemi extract at 80 deg.C to obtain powder, and mixing with esterified glucomannan.
Mould detoxification additive for animals: the additive obtained above was added to drinking water and mixed, and the concentration of the additive in water was 0.015%.
Example 2
The mould detoxification additive for the animals comprises the following substances in parts by weight: 30 parts of gardenia, 50 parts of liquorice, 30 parts of chrysanthemum and 1 part of esterified glucomannan.
In this embodiment, the preparation method of the mold detoxification additive for animals comprises the following steps:
(1) preparing a gardenia extract: pulverizing fructus Gardeniae into coarse powder, adding 80% ethanol according to the solid-to-liquid ratio of 1:0.9, soaking for 24 hr, percolating at the flow rate of 5mL/min, recovering ethanol from percolate under reduced pressure, and concentrating the extractive solution to 1/3 of original volume; obtaining gardenia extract;
(2) preparation of a licorice extract: pulverizing Glycyrrhrizae radix into coarse powder, adding deionized water and diastase, boiling for 2min, and filtering to obtain filtrate, wherein the solid-to-liquid ratio of Glycyrrhrizae radix coarse powder and deionized water is 1: 2; the adding amount of saccharifying enzyme is 0.2% of Glycyrrhrizae radix coarse powder. Adding deionized water into the filter residue, and extracting for 2 times; combining the filtrates obtained in the two extractions, and concentrating to 1/3 of the original volume to obtain a licorice extract;
(3) preparing a chrysanthemum extract: pulverizing flos Chrysanthemi into coarse powder, adding 80% ethanol, wherein the ratio of flos Chrysanthemi coarse powder to 80% ethanol is 1: 20; ultrasonic extracting for 15min, and recovering ethanol under reduced pressure to obtain flos Chrysanthemi extract;
(4) vacuum drying the obtained fructus Gardeniae extract, Glycyrrhrizae radix extract and flos Chrysanthemi extract at 60 deg.C to obtain powder, and mixing with esterified glucomannan.
Mould detoxification additive for animals: the additive obtained above is added into drinking water and mixed, and the concentration of the additive in the water is 0.02%.
Example 3
The mould detoxification additive for the animals comprises the following substances in parts by weight: 45 parts of gardenia, 45 parts of liquorice, 25 parts of chrysanthemum and 4 parts of esterified glucomannan.
In this embodiment, the preparation method of the mold detoxification additive for animals comprises the following steps:
(1) preparing a gardenia extract: pulverizing fructus Gardeniae into coarse powder, adding 75% ethanol according to the solid-to-liquid ratio of 1:0.8, soaking for 24 hr, percolating at the flow rate of 5mL/min, recovering ethanol from percolate under reduced pressure, and concentrating the extractive solution to 1/3 of original volume; obtaining gardenia extract;
(2) preparation of a licorice extract: pulverizing Glycyrrhrizae radix into coarse powder, adding deionized water and diastase, boiling for 2min, and filtering to obtain filtrate, wherein the solid-to-liquid ratio of Glycyrrhrizae radix coarse powder and deionized water is 1: 2; the adding amount of saccharifying enzyme is 0.4% of Glycyrrhrizae radix coarse powder. Adding deionized water into the filter residue, and extracting for 1 time; combining the filtrates obtained in the two extractions, and concentrating to 1/3 of the original volume to obtain a licorice extract;
(3) preparing a chrysanthemum extract: pulverizing flos Chrysanthemi into coarse powder, adding 80% ethanol, wherein the ratio of flos Chrysanthemi coarse powder to 80% ethanol is 1: 20; ultrasonic extracting for 15min, and recovering ethanol under reduced pressure to obtain flos Chrysanthemi extract;
(4) vacuum drying the obtained fructus Gardeniae extract, Glycyrrhrizae radix extract and flos Chrysanthemi extract at 60 deg.C to obtain powder, and mixing with esterified glucomannan.
Mould detoxification additive for animals: the additive obtained above is added into drinking water and mixed, and the concentration of the additive in the water is 0.018%.
Example 4
The mould detoxification additive for the animals comprises the following substances in parts by weight: 35 parts of gardenia, 35 parts of liquorice, 15 parts of chrysanthemum and 2 parts of esterified glucomannan.
In this embodiment, the preparation method of the mold detoxification additive for animals comprises the following steps:
(1) preparing a gardenia extract: pulverizing fructus Gardeniae into coarse powder, adding 75% ethanol according to the solid-to-liquid ratio of 1:0.8, soaking for 24 hr, percolating at the flow rate of 5mL/min, recovering ethanol from percolate under reduced pressure, and concentrating the extractive solution to 1/3 of original volume; obtaining gardenia extract;
(2) preparation of a licorice extract: pulverizing Glycyrrhrizae radix into coarse powder, adding deionized water and diastase, boiling for 2min, and filtering to obtain filtrate, wherein the solid-to-liquid ratio of Glycyrrhrizae radix coarse powder and deionized water is 1: 2; the adding amount of saccharifying enzyme is 0.5% of Glycyrrhrizae radix coarse powder. Adding deionized water into the filter residue, and extracting for 1 time; combining the filtrates obtained in the two extractions, and concentrating to 1/3 of the original volume to obtain a licorice extract;
(3) preparing a chrysanthemum extract: pulverizing flos Chrysanthemi into coarse powder, adding 80% ethanol, wherein the ratio of flos Chrysanthemi coarse powder to 80% ethanol is 1: 20; ultrasonic extracting for 15min, and recovering ethanol under reduced pressure to obtain flos Chrysanthemi extract;
(4) vacuum drying the obtained fructus Gardeniae extract, Glycyrrhrizae radix extract and flos Chrysanthemi extract at 60 deg.C to obtain powder, and mixing with esterified glucomannan.
Mould detoxification additive for animals: the additive obtained above is added into drinking water and mixed, and the concentration of the additive in the water is 0.018%.
Example 5
The mould detoxification additive for the animals comprises the following substances in parts by weight: 40 parts of gardenia, 40 parts of liquorice, 20 parts of chrysanthemum and 5 parts of esterified glucomannan.
In this embodiment, the preparation method of the mold detoxification additive for animals comprises the following steps:
(1) preparing a gardenia extract: pulverizing fructus Gardeniae into coarse powder, adding 75% ethanol according to the solid-to-liquid ratio of 1:0.8, soaking for 24 hr, percolating at the flow rate of 5mL/min, recovering ethanol from percolate under reduced pressure, and concentrating the extractive solution to 1/3 of original volume; obtaining gardenia extract;
(2) preparation of a licorice extract: pulverizing Glycyrrhrizae radix into coarse powder, adding deionized water and diastase, boiling for 2min, and filtering to obtain filtrate, wherein the solid-to-liquid ratio of Glycyrrhrizae radix coarse powder and deionized water is 1: 2; the adding amount of saccharifying enzyme is 0.3% of Glycyrrhrizae radix coarse powder. Adding deionized water into the filter residue, and extracting for 1 time; combining the filtrates obtained in the two extractions, and concentrating to 1/3 of the original volume to obtain a licorice extract;
(3) preparing a chrysanthemum extract: pulverizing flos Chrysanthemi into coarse powder, adding 80% ethanol, wherein the ratio of flos Chrysanthemi coarse powder to 80% ethanol is 1: 20; ultrasonic extracting for 15min, and recovering ethanol under reduced pressure to obtain flos Chrysanthemi extract;
(4) vacuum drying the obtained fructus Gardeniae extract, Glycyrrhrizae radix extract and flos Chrysanthemi extract at 60 deg.C to obtain powder, and mixing with esterified glucomannan.
Mould detoxification additive for animals: the additive obtained above is added into drinking water and mixed, and the concentration of the additive in the water is 0.018%.
Example 6
The mould detoxification additive for the animals comprises the following substances in parts by weight: 40 parts of gardenia, 40 parts of liquorice, 20 parts of chrysanthemum and 3 parts of esterified glucomannan.
In this embodiment, the preparation method of the mold detoxification additive for animals comprises the following steps:
(1) preparing a gardenia extract: pulverizing fructus Gardeniae into coarse powder, adding 75% ethanol according to the solid-to-liquid ratio of 1:0.8, soaking for 24 hr, percolating at the flow rate of 5mL/min, recovering ethanol from percolate under reduced pressure, and concentrating the extractive solution to 1/3 of original volume; obtaining gardenia extract;
(2) preparation of a licorice extract: pulverizing Glycyrrhrizae radix into coarse powder, adding deionized water and diastase, boiling for 2min, and filtering to obtain filtrate, wherein the solid-to-liquid ratio of Glycyrrhrizae radix coarse powder and deionized water is 1: 2; the adding amount of saccharifying enzyme is 0.5% of Glycyrrhrizae radix coarse powder. Adding deionized water into the filter residue, and extracting for 1 time; combining the filtrates obtained in the two extractions, and concentrating to 1/3 of the original volume to obtain a licorice extract;
(3) preparing a chrysanthemum extract: pulverizing flos Chrysanthemi into coarse powder, adding 80% ethanol, wherein the ratio of flos Chrysanthemi coarse powder to 80% ethanol is 1: 20; ultrasonic extracting for 15min, and recovering ethanol under reduced pressure to obtain flos Chrysanthemi extract;
(4) vacuum drying the obtained fructus Gardeniae extract, Glycyrrhrizae radix extract and flos Chrysanthemi extract at 60 deg.C to obtain powder, and mixing with esterified glucomannan.
Mould detoxification additive for animals: the additive obtained above is added into drinking water and mixed, and the concentration of the additive in the water is 0.018%.
Test method
Test live pigs were divided into 4 groups, control and experimental groups, with 5 pigs each. After mould is introduced into the pig feed and cultured to be mature, the pig feed is eaten by experimental pigs, and live pigs all have symptoms such as vomit, diarrhea, dehydration and the like;
experimental group 1: adding only esterified glucomannan for detoxification;
experiment group 2; adding esterified glucomannan and Glycyrrhrizae radix extract for removing toxic substances;
experimental group 3: detoxification was carried out by adding the additive of example 6;
the data obtained are shown in the following table:
type (B) | Control group | Experimental group 1 | Experimental group 2 | Experimental group 3 |
Time to effect | -- | 1.5d | 1d | 0.5d |
Complete healing time | -- | 7d | 7d | 3d |
Cure rate | -- | 80% | 100% | 100% |
The results are shown in the table: the preparation takes the criteria of shortening vomiting time, reducing diarrhea frequency, drying feces and the like as the effect criteria.
As can be seen from the above table, only when the esterified glucomannan is mixed with the licorice extract, gardenia and chrysanthemum, the effect of mold detoxification is fast, and the cure time is greatly shortened.
The technical solutions provided by the embodiments of the present invention are described in detail above, and the principles and embodiments of the present invention are explained herein by using specific examples, and the descriptions of the embodiments are only used to help understanding the principles of the embodiments of the present invention; meanwhile, for a person skilled in the art, according to the embodiments of the present invention, there may be variations in the specific implementation manners and application ranges, and in summary, the content of the present description should not be construed as a limitation to the present invention.
Claims (9)
1. A mold detoxification additive for animals, which is characterized in that: the adhesive comprises the following substances in parts by weight: 30-50 parts of gardenia, 30-50 parts of liquorice, 15-30 parts of chrysanthemum and 1-5 parts of esterified glucomannan.
2. The mold detoxification additive for animals according to claim 1, wherein: the adhesive comprises the following substances in parts by weight: 35-45 parts of gardenia, 35-45 parts of liquorice, 15-25 parts of chrysanthemum and 2-4 parts of esterified glucomannan.
3. The mold detoxification additive for animals according to claim 1, wherein: the adhesive comprises the following substances in parts by weight: 40-45 parts of gardenia, 40-45 parts of liquorice, 20-25 parts of chrysanthemum and 3-5 parts of esterified glucomannan.
4. The mold detoxification additive for animals according to claim 1, wherein: the adhesive comprises the following substances in parts by weight: 40 parts of gardenia, 40 parts of liquorice, 20 parts of chrysanthemum and 3 parts of esterified glucomannan.
5. A process for preparing a mould detoxification additive for animals according to any of claims 1 to 4, wherein: the method comprises the following steps:
(1) preparing a gardenia extract: pulverizing fructus Gardeniae into coarse powder, soaking in 70-80% ethanol for 24 hr, percolating at flow rate of 5mL/min, recovering ethanol from percolate under reduced pressure, and concentrating the extractive solution to 1/3-1/2; obtaining gardenia extract;
(2) preparation of a licorice extract: pulverizing Glycyrrhrizae radix into coarse powder, adding deionized water and diastase, boiling for 2-5min, and filtering to obtain filtrate; adding deionized water, and extracting for 1-2 times; comprehensively extracting the filtrate, and concentrating to 1/3 of the original volume to obtain Glycyrrhrizae radix extractive solution;
(3) preparing a chrysanthemum extract: pulverizing flos Chrysanthemi into coarse powder, adding 80% ethanol, ultrasonic extracting for 10-20min, and recovering ethanol under reduced pressure to obtain flos Chrysanthemi extract;
(4) vacuum drying the obtained fructus Gardeniae extract, Glycyrrhrizae radix extract and flos Chrysanthemi extract to obtain powder, and mixing with esterified glucomannan.
6. A method for preparing a mold detoxification additive for animals according to claim 5, wherein: the proportion of the gardenia coarse powder to the ethanol in the step (1) is 1 (0.8-1).
7. A method for preparing a mold detoxification additive for animals according to claim 5, wherein: the solid-liquid ratio of the licorice coarse powder and the deionized water in the step (2) is 1: 2; the adding amount of the saccharifying enzyme is 0.2-0.5% of the licorice coarse powder.
8. A method for preparing a mold detoxification additive for animals according to claim 5, wherein: the ratio of the chrysanthemum coarse powder to 80% ethanol in the step (3) is 1: 20.
9. A method for preparing a mold detoxification additive for animals according to claim 5, wherein: the ethanol concentration of the gardenia coarse powder soaked in the step (1) is 75%.
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廖万清等: "《现代真菌病学》", 31 October 2017, 复旦大学出版社 * |
黄盛兴: "浅论猪霉菌毒素中毒危害及防治措施", 《中国畜禽种业》 * |
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