CN112220703A - Anti-wrinkle cosmetic composition and preparation method thereof - Google Patents

Anti-wrinkle cosmetic composition and preparation method thereof Download PDF

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Publication number
CN112220703A
CN112220703A CN202011264515.4A CN202011264515A CN112220703A CN 112220703 A CN112220703 A CN 112220703A CN 202011264515 A CN202011264515 A CN 202011264515A CN 112220703 A CN112220703 A CN 112220703A
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molecular weight
cosmetic composition
high molecular
extract
wrinkle cosmetic
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Inventor
章明旺
陈林香
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Xiamen Eagle Don Pharmaceutical Co ltd
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Xiamen Eagle Don Pharmaceutical Co ltd
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Priority to CN202011264515.4A priority Critical patent/CN112220703A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

Abstract

The invention belongs to the technical field of cosmetics, and particularly relates to an anti-wrinkle cosmetic composition and a preparation method thereof, wherein the anti-wrinkle cosmetic composition comprises the following raw material components, by weight, 90-100 parts of cyclopentadimethylsiloxane, 0.1-0.5 part of high molecular weight polysiloxane, 0.5-1.5 parts of olive oil, 0.1-0.7 part of rose oil, 0.1-0.8 part of dendrobium extract and 0.03-0.2 part of ginseng extract. According to the invention, the high molecular weight polysiloxane is added into the formula of the anti-wrinkle cosmetic, so that when the anti-wrinkle cosmetic is applied to skin, the high molecular weight polysiloxane forms a film on the skin, the absorption efficiency of essence components is improved, and waste is avoided.

Description

Anti-wrinkle cosmetic composition and preparation method thereof
Technical Field
The invention belongs to the technical field of cosmetics, and relates to an anti-wrinkle cosmetic composition and a preparation method thereof.
Background
The essential oil contains various essential components and can regulate and improve the skin. The essential oils can be classified into whitening, anti-wrinkle, repairing, etc. according to their effects. The essential oil mainly contains fat-soluble essential components, so that the essential oil is easier to absorb by human skin than water-soluble essential components, but the problems of insufficient absorption or incomplete absorption exist due to the fact that the essential oil is not uniform during coating and the relatively large number of the essential components are locally gathered under the action of gravity after coating, namely a part of the essential components are wasted, and the effect of the essential oil is not fast enough visually. From the perspective of consumers, cosmetics which can quickly exert the anti-wrinkle effect are more popular with consumers.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide the anti-wrinkle cosmetic composition which can enable the essence components to be more uniformly coated on the skin and fully exert the anti-wrinkle effect of the essence oil.
Another object of the present invention is to provide a method for preparing an anti-wrinkle cosmetic.
The technical scheme of the invention is as follows:
an anti-wrinkle cosmetic composition comprises, by weight, 90-100 parts of cyclopentadimethylsiloxane, 0.1-0.5 part of high molecular weight polysiloxane, 0.5-1.5 parts of olive, 0.1-0.7 part of rose oil, 0.1-0.8 part of dendrobium extract and 0.03-0.2 part of ginseng extract.
Preferably, the composition comprises 92-99 parts of cyclopentadidimethyl siloxane, 0.13-0.4 part of high molecular weight polysiloxane, 0.8-1.4 parts of olive, 0.15-0.6 part of rose oil, 0.13-0.6 part of dendrobium extract and 0.06-0.14 part of ginseng extract.
More preferably, the composition comprises 94-98 parts of cyclopentadidimethyl siloxane, 0.15-0.3 part of high molecular weight polysiloxane, 0.9-1.3 parts of olive, 0.2-0.5 part of rose oil, 0.16-0.5 part of dendrobium extract and 0.09-0.12 part of ginseng extract.
Preferably, the high molecular weight polysiloxane is polydimethylsiloxane or alkyl modified polydimethylsiloxane. In the present invention, the high molecular weight polysiloxane is more preferably alkyl-modified polydimethylsiloxane, and examples thereof include dodecyl-modified high molecular weight polydimethylsiloxane, tetradecyl-modified high molecular weight polydimethylsiloxane, hexadecyl-modified high molecular weight polydimethylsiloxane, and octadecyl-modified high molecular weight polydimethylsiloxane. The preparation method of the high molecular weight alkyl modified polydimethylsiloxane has been disclosed, for example, CN 109880106A.
Preferably, the high molecular weight polysiloxane has an average relative molecular weight of 20 to 120 ten thousand. In the present invention, the average relative molecular weight of the high molecular weight polysiloxane is more preferably 30 to 80 ten thousand.
Preferably, the dendrobium extract is a dendrobium officinale extract.
A method of making an anti-wrinkle cosmetic composition according to any of the above embodiments, comprising mixing the high molecular weight polysiloxane and the cyclopentadecylpolydimethylsiloxane, stirring the mixture uniformly for a first time, adding the olea europaea, the rose oil, the dendrobium extract, and the ginseng extract, and stirring the mixture uniformly for a second time to obtain the anti-wrinkle cosmetic composition.
Preferably, the second time of uniform stirring further comprises filtration with microporous filter membranes with pore size of 0.22 μm and pore size of 0.11 μm.
Preferably, the storage in an aging tank for aging is also included after the second stirring to be uniform for 60-100 days.
The invention has the beneficial effects that: according to the invention, the high molecular weight polysiloxane is added into the anti-wrinkle cosmetic composition, so that the cosmetic composition can form a relatively uniform film after being coated on human skin, and the phenomenon that the essential components are unevenly distributed on the human skin due to uneven coating or aggregation of the essential components under the action of gravity after coating is avoided, on one hand, the absorption amount of the essential components by the human skin is inconsistent, the anti-wrinkle effect is inconsistent, and on the other hand, the waste of the essential components at the aggregation part of the essential components is also caused due to incomplete absorption. Therefore, the high molecular weight polysiloxane forms a film on human skin, so that the essential components are more uniformly distributed and absorbed on the human skin, and the essential components are more fully absorbed, thereby achieving better and faster anti-wrinkle effect.
Detailed Description
The technical solution of the present invention is further illustrated and described by the following detailed description.
Unless otherwise specified, the parts described in the following examples are parts by weight.
Example 1
The raw material components are 92 portions of cyclopentadidimethyl siloxane, 0.15 portion of high molecular weight polydimethylsiloxane (with average relative molecular weight of 50 ten thousand), 0.7 portion of olive, 0.15 portion of rose oil, 0.3 portion of dendrobium officinale extract and 0.12 portion of ginseng extract,
mixing high molecular weight polydimethylsiloxane and cyclopentasiloxane, stirring uniformly, adding olive oil, rose oil, dendrobium officinale extract and ginseng extract, stirring uniformly, filtering with microporous filter membranes with the pore diameter of 0.22 mu m and the pore diameter of 0.11 mu m respectively, storing in an aging tank, and aging for 70 days to obtain the anti-wrinkle cosmetic composition, which is marked as K-1.
Example 2
Comprises the following raw material components of 100 parts of cyclopentadidimethyl siloxane, 0.45 part of dodecyl modified polysiloxane with high molecular weight (average relative molecular weight is 60 ten thousand, the mass percent of dodecyl is 1.2%), 1.1 parts of olive, 0.5 part of rose oil, 0.4 part of dendrobium officinale extract and 0.13 part of ginseng extract,
mixing high molecular weight dodecyl modified polysiloxane and cyclopentadienyldimethyl siloxane, stirring uniformly, adding olive oil, rose oil, dendrobium officinale extract and ginseng extract, stirring uniformly, filtering by using microporous filter membranes with the pore diameter of 0.22 mu m and the pore diameter of 0.11 mu m respectively, storing in an aging tank, and aging for 90 days to obtain the anti-wrinkle cosmetic composition, which is marked as K-2.
Example 3
The raw material components are 95 parts of cyclopentadidimethyl siloxane, 0.24 part of high molecular weight octadecyl modified polysiloxane (average relative molecular weight is 76 ten thousand, the mass percent of octadecyl is 1.3%), 0.8 part of olive, 0.16 part of rose oil, 0.7 part of dendrobium officinale extract and 0.08 part of ginseng extract,
mixing high molecular weight octadecyl modified polysiloxane and cyclopentadimethylsiloxane, stirring uniformly, adding olive oil, rose oil, dendrobium officinale extract and ginseng extract, stirring uniformly, filtering with microporous filter membranes with the pore diameter of 0.22 μm and the pore diameter of 0.11 μm respectively, storing in an aging tank, aging for 70 days, and obtaining the anti-wrinkle cosmetic composition, which is marked as K-3.
Example 4
Comprises the following raw material components of 96 parts of cyclopentadidimethyl siloxane, 0.22 part of high molecular weight octadecyl modified polysiloxane (average relative molecular weight is 76 ten thousand, the mass percent of octadecyl is 1.3%), 1.2 parts of olive, 0.34 part of rose oil, 0.35 part of dendrobium officinale extract and 0.11 part of ginseng extract,
mixing high molecular weight octadecyl modified polysiloxane and cyclopentadimethylsiloxane, stirring uniformly, adding olive oil, rose oil, dendrobium officinale extract and ginseng extract, stirring uniformly, filtering with microporous filter membranes with the pore diameter of 0.22 μm and the pore diameter of 0.11 μm respectively, storing in an aging tank, aging for 90 days to obtain the anti-wrinkle cosmetic composition, which is marked as K-4.
Example 5
93 portions of cyclopentadidimethyl siloxane, 0.4 portion of high molecular weight docosyl modified polysiloxane (average relative molecular weight is 42 ten thousand, the mass percent of docosyl is 0.9%), 1.2 portions of olive, 0.4 portion of rose oil, 0.5 portion of dendrobium officinale extract and 0.16 portion of ginseng extract,
mixing high molecular weight octadecyl modified polysiloxane and cyclopentadimethylsiloxane, stirring uniformly, adding olive oil, rose oil, dendrobium officinale extract and ginseng extract, stirring uniformly, filtering with microporous filter membranes with the pore diameter of 0.22 μm and the pore diameter of 0.11 μm respectively, storing in an aging tank, aging for 85 days, and obtaining the anti-wrinkle cosmetic composition, which is marked as K-5.
Comparative example 1
Comprises the following raw material components of 96 parts of cyclopentadidimethyl siloxane, 0.35 part of polydimethylsiloxane (viscosity of 2400mPa.s at 25 ℃), 1.2 parts of olive, 0.34 part of rose oil, 0.35 part of dendrobium officinale extract and 0.11 part of ginseng extract,
mixing polydimethylsiloxane, cyclopentadimethicone, olive oil, rose oil, dendrobium officinale extract and ginseng extract, stirring uniformly, filtering by using microporous filter membranes with the pore diameter of 0.22 mu m and the pore diameter of 0.11 mu m respectively, storing in an aging tank, and aging for 90 days to obtain the anti-wrinkle cosmetic composition, which is marked as K-6.
Comparative example 2
Comprises the following raw material components of 96 parts of cyclopentadidimethyl siloxane, 0.22 part of octadecyl modified polysiloxane (viscosity of 3700mPa.s at 25 ℃), 1.2 parts of olive, 0.34 part of rose oil, 0.35 part of dendrobium officinale extract and 0.11 part of ginseng extract,
mixing octadecyl modified polysiloxane, cyclopentadidimethyl siloxane, olive oil, rose oil, dendrobium officinale extract and ginseng extract, stirring uniformly, filtering by using microporous filter membranes with the pore diameter of 0.22 mu m and the pore diameter of 0.11 mu m respectively, storing in an aging tank, and aging for 90 days to obtain the anti-wrinkle cosmetic composition, which is marked as K-7.
Comparative example 3
Comprises the following raw material components of 96 parts of cyclopentadidimethyl siloxane, 1.2 parts of olive oil, 0.34 part of rose oil, 0.35 part of dendrobium officinale extract and 0.11 part of ginseng extract,
mixing cyclopentadimethylsiloxane, olive oil, rose oil, dendrobium officinale extract and ginseng extract, stirring uniformly, filtering by using microporous filter membranes with the pore diameter of 0.22 mu m and the pore diameter of 0.11 mu m respectively, and storing in an aging tank for aging for 90 days to obtain the anti-wrinkle cosmetic composition which is marked as K-8.
Comparative example 4
Comprises the following raw material components of 96 parts of cyclopentadidimethyl siloxane, 0.22 part of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 1.2 parts of olive, 0.34 part of rose oil, 0.35 part of dendrobium officinale extract and 0.11 part of ginseng extract,
mixing the polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and the cyclopenta polydimethylsiloxane, uniformly stirring, adding olive oil, rose oil, a dendrobium officinale extract and a ginseng extract, uniformly stirring, respectively filtering by using microporous filter membranes with the pore diameter of 0.22 mu m and the pore diameter of 0.11 mu m, storing in an aging tank, and aging for 90 days to obtain the anti-wrinkle cosmetic composition, wherein the mark is K-9.
Effect testing
90 healthy women with the age of 40-55 years are selected, and the skin is loose and rough and has more wrinkles. The 90 women were randomly divided into 9 groups on average, with 10 people per group.
The test method comprises the following steps: after 8 to 9 o' clock per night and thorough skin cleaning, the anti-wrinkle cosmetic compositions K-1 to K-9 of examples 1 to 5 and comparative examples 1 to 4 are evenly smeared on the facial skin with the smearing amount of 3.0 +/-0.2 mg/cm2And after 30 minutes, cleaning is carried out. Every 14 days is a course of treatment.
Anti-wrinkle effect evaluation criterion: (1) the remarkable effect is that the user feels very satisfactory, the skin becomes more elastic, compact and glossy, wrinkles are obviously reduced, and no allergy or other side effects exist; (2) effective, users feel generally satisfied, the skin condition is improved, wrinkles are reduced, and allergy or other side effects are avoided; (3) and (4) invalidation: the user had no satisfaction with the user, no improvement in skin condition, and no reduction in wrinkles.
Sensory evaluation criteria were used: and (3) scoring according to the feeling of the subject in the using process, wherein the scoring adopts 5 grades, 1 grade is the worst effect, 5 grades is the best effect, and the average value is taken in each group of tests.
The evaluation statistics of the anti-wrinkle effect are shown in table 1.
The sensory evaluation is shown in table 2.
TABLE 1
Figure BDA0002775686260000051
Therefore, from the above results, it is understood that the anti-wrinkle cosmetic composition of the present invention has a good anti-wrinkle effect and exhibits an anti-wrinkle effect more rapidly.
TABLE 2
Figure BDA0002775686260000052
Figure BDA0002775686260000061
Therefore, the anti-wrinkle cosmetic composition provided by the invention is better in use feeling, and is uniform and not greasy to apply.
The foregoing has shown and described the fundamental principles, principal features and advantages of the invention. It should be understood by those skilled in the art that the present invention is not limited by the foregoing embodiments, which are merely preferred embodiments of the present invention, and the scope of the present invention should not be limited thereby, and that equivalent changes and modifications made within the scope of the present invention and the specification should be covered thereby. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (9)

1. An anti-wrinkle cosmetic composition is characterized by comprising, by weight, 90-100 parts of cyclopentadimethylsiloxane, 0.1-0.5 part of high molecular weight polysiloxane, 0.5-1.5 parts of olive, 0.1-0.7 part of rose oil, 0.1-0.8 part of dendrobium extract and 0.03-0.2 part of ginseng extract.
2. The anti-wrinkle cosmetic composition according to claim 1, which comprises 92-99 parts of cyclopentadimethylsiloxane, 0.13-0.4 part of high molecular weight polysiloxane, 0.8-1.4 parts of olea europaea, 0.15-0.6 part of rose oil, 0.13-0.6 part of dendrobium extract and 0.06-0.14 part of ginseng extract.
3. The anti-wrinkle cosmetic composition according to claim 2, which consists of 94-98 parts of cyclopentadimethylsiloxane, 0.15-0.3 part of high molecular weight polysiloxane, 0.9-1.3 parts of olea europaea, 0.2-0.5 part of rose oil, 0.16-0.5 part of dendrobium extract and 0.09-0.12 part of ginseng extract.
4. The anti-wrinkle cosmetic composition according to any one of claims 1 to 3, wherein the high molecular weight polysiloxane is polydimethylsiloxane or alkyl-modified polydimethylsiloxane.
5. The anti-wrinkle cosmetic composition according to any one of claims 1 to 3, wherein the high molecular weight polysiloxane has an average relative molecular weight of 20 to 120 ten thousand.
6. The anti-wrinkle cosmetic composition according to any one of claims 1 to 3, wherein the dendrobium extract is dendrobium officinale extract.
7. A method of preparing an anti-wrinkle cosmetic composition according to any one of claims 1 to 6, characterized in that the high molecular weight polysiloxane and the cyclopentadecylpolydimethylsiloxane are mixed, stirred uniformly for the first time, the olea europaea, the rose oil, the dendrobium extract and the ginseng extract are added, and stirred uniformly for the second time, so as to obtain the anti-wrinkle cosmetic composition.
8. The preparation method according to claim 7, further comprising filtering with microporous membranes having a pore size of 0.22 μm and a pore size of 0.11 μm after the second stirring.
9. The method of claim 7, further comprising aging in an aging tank for 60-100 days after the second stirring.
CN202011264515.4A 2020-11-12 2020-11-12 Anti-wrinkle cosmetic composition and preparation method thereof Pending CN112220703A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115025007A (en) * 2022-06-30 2022-09-09 广州长生康生物科技有限公司 Polypeptide anti-wrinkle essence and preparation method thereof

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中国科学院兰州化学物理研究所: "《硅油》", 31 August 1973, 甘肃人民出版社 *
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115025007A (en) * 2022-06-30 2022-09-09 广州长生康生物科技有限公司 Polypeptide anti-wrinkle essence and preparation method thereof

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Application publication date: 20210115