CN112120961A - Viscous eyeliner with strong false eyelashes and preparation method and application thereof - Google Patents
Viscous eyeliner with strong false eyelashes and preparation method and application thereof Download PDFInfo
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- CN112120961A CN112120961A CN202010383324.3A CN202010383324A CN112120961A CN 112120961 A CN112120961 A CN 112120961A CN 202010383324 A CN202010383324 A CN 202010383324A CN 112120961 A CN112120961 A CN 112120961A
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- eyeliner
- copolymer
- false eyelashes
- ester
- viscous
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- 210000000720 eyelash Anatomy 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 229920001577 copolymer Polymers 0.000 claims abstract description 43
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims abstract description 32
- 150000002148 esters Chemical class 0.000 claims abstract description 32
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims abstract description 24
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000003086 colorant Substances 0.000 claims abstract description 18
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 17
- 239000003755 preservative agent Substances 0.000 claims abstract description 17
- 230000002335 preservative effect Effects 0.000 claims abstract description 17
- 239000003906 humectant Substances 0.000 claims abstract description 16
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 12
- 239000002904 solvent Substances 0.000 claims abstract description 10
- FEWFXBUNENSNBQ-UHFFFAOYSA-N 2-hydroxyacrylic acid Chemical compound OC(=C)C(O)=O FEWFXBUNENSNBQ-UHFFFAOYSA-N 0.000 claims abstract description 8
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims abstract description 8
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims abstract description 8
- RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Natural products CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 claims abstract description 8
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims abstract description 8
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229920001485 poly(butyl acrylate) polymer Polymers 0.000 claims abstract description 8
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 claims abstract description 8
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 8
- 229940068968 polysorbate 80 Drugs 0.000 claims abstract description 8
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 8
- 229920005749 polyurethane resin Polymers 0.000 claims abstract description 8
- 229920002689 polyvinyl acetate Polymers 0.000 claims abstract description 8
- 239000011118 polyvinyl acetate Substances 0.000 claims abstract description 8
- 229920000915 polyvinyl chloride Polymers 0.000 claims abstract description 8
- 239000004800 polyvinyl chloride Substances 0.000 claims abstract description 8
- 229920005989 resin Polymers 0.000 claims abstract description 8
- 239000011347 resin Substances 0.000 claims abstract description 8
- 150000003505 terpenes Chemical class 0.000 claims abstract description 8
- 235000007586 terpenes Nutrition 0.000 claims abstract description 8
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims abstract description 8
- CUNWUEBNSZSNRX-RKGWDQTMSA-N (2r,3r,4r,5s)-hexane-1,2,3,4,5,6-hexol;(z)-octadec-9-enoic acid Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO.OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO.CCCCCCCC\C=C/CCCCCCCC(O)=O.CCCCCCCC\C=C/CCCCCCCC(O)=O.CCCCCCCC\C=C/CCCCCCCC(O)=O CUNWUEBNSZSNRX-RKGWDQTMSA-N 0.000 claims abstract description 7
- 229960005078 sorbitan sesquioleate Drugs 0.000 claims abstract description 7
- 229940117013 triethanolamine oleate Drugs 0.000 claims abstract description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 21
- 238000003756 stirring Methods 0.000 claims description 21
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 9
- 238000004945 emulsification Methods 0.000 claims description 9
- 229960005323 phenoxyethanol Drugs 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 8
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- MXOAEAUPQDYUQM-QMMMGPOBSA-N (S)-chlorphenesin Chemical compound OC[C@H](O)COC1=CC=C(Cl)C=C1 MXOAEAUPQDYUQM-QMMMGPOBSA-N 0.000 claims description 7
- 229940083957 1,2-butanediol Drugs 0.000 claims description 7
- BMRWNKZVCUKKSR-UHFFFAOYSA-N butane-1,2-diol Chemical compound CCC(O)CO BMRWNKZVCUKKSR-UHFFFAOYSA-N 0.000 claims description 7
- 229960003993 chlorphenesin Drugs 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- 238000007789 sealing Methods 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 239000004909 Moisturizer Substances 0.000 claims 1
- 230000001333 moisturizer Effects 0.000 claims 1
- 239000003292 glue Substances 0.000 abstract description 13
- 239000000853 adhesive Substances 0.000 abstract description 4
- 230000001070 adhesive effect Effects 0.000 abstract description 4
- 230000000638 stimulation Effects 0.000 abstract description 2
- 230000001804 emulsifying effect Effects 0.000 description 13
- 230000002421 anti-septic effect Effects 0.000 description 7
- 229960004418 trolamine Drugs 0.000 description 5
- 239000002537 cosmetic Substances 0.000 description 4
- 210000000744 eyelid Anatomy 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 description 1
- ZKYCLDTVJCJYIB-UHFFFAOYSA-N 2-methylidenedecanamide Chemical compound CCCCCCCCC(=C)C(N)=O ZKYCLDTVJCJYIB-UHFFFAOYSA-N 0.000 description 1
- 206010016322 Feeling abnormal Diseases 0.000 description 1
- 206010040914 Skin reaction Diseases 0.000 description 1
- 229920006322 acrylamide copolymer Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- RSAAVARFAITAFK-UHFFFAOYSA-N dodecane-1,2,11,12-tetrol Chemical compound OCC(O)CCCCCCCCC(O)CO RSAAVARFAITAFK-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229940049964 oleate Drugs 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000035483 skin reaction Effects 0.000 description 1
- 231100000430 skin reaction Toxicity 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8117—Homopolymers or copolymers of aromatic olefines, e.g. polystyrene; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8123—Compositions of homopolymers or copolymers of compounds having one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers, e.g. PVC, PTFE
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8158—Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/87—Polyurethanes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
Abstract
The invention relates to a viscous eyeliner with strong false eyelashes and a preparation method and application thereof, and the components of the eyeliner comprise a solvent, a humectant, a colorant, an emulsifier, a tackifying film-forming agent, a colorant and a preservative; the emulsifier is polysorbate-80, triethanolamine and sorbitan sesquioleate; the tackifying film forming agent comprises polybutyl acrylate, rosin acrylate, terpene resin, styrene/isoprene copolymer, polyvinyl acetate, hydroxyacrylic acid (ester) copolymer, polyvinyl chloride, acrylic acid (ester) copolymer/octylacrylamide copolymer, styrene/acrylic acid (ester) copolymer, polyurethane resin, acrylic acid (ester) copolymer/ethylhexyl acrylate copolymer; the eyeliner disclosed by the invention combines the functions of the eyeliner and the glue or the adhesive sticker for sticking the false eyelashes into a whole, and can reduce stimulation and damage to the skin compared with the traditional glue or adhesive sticker for sticking the false eyelashes.
Description
Technical Field
The invention belongs to the technical field of color cosmetics, and particularly relates to viscous eyeliner capable of strongly sticking false eyelashes as well as a preparation method and application of the viscous eyeliner.
Background
The eyeliner is a color cosmetic product which is commonly used in the life and work of the vast females at present, and the eyeliner is acted on the edge of the eyes in a linear form, so that the eyeliner can play the roles of enlarging the eyes and making the eyes more attractive, and can add charm to the vast females.
Modern eye makeup operations generally include eye line drawing and false eyelash sticking, and for a long time, the traditional eye makeup method is to draw eye lines on eyes separately and then glue or stick false eyelash on the corresponding positions. According to research and research, the fact that the skin is irritated by using or using the glue or the glue paste for a long time and the health state of the skin is damaged is found, the eyes are uncomfortable and the weight of eyelids is increased by applying the glue, the eyes are not attractive due to the fact that the glue spreading technology is not good, the makeup steps are complicated, the traditional eye makeup operation is not suitable for people who need to use false eyelashes for a long time, and the traditional eyeliner generally does not have the function of sticking the false eyelashes or can not be firmly stuck the false eyelashes. The existing eyeliner product has single function and only has the function of drawing eyeliner, and eyeliner and glue or glue paste are required for eyelids before false eyelashes are stuck on the eyelash, so that the burden of skin around the eyes is increased, the skin around the eyes is damaged in time, fine lines on the eyes are increased, and the like.
Disclosure of Invention
In order to solve the above problems, an object of the present invention is to provide a viscous eyeliner having a function of strongly sticking false eyelashes, a method for preparing the same, and an application thereof, and to provide an eyeliner (or eyeliner) having a function of strongly sticking false eyelashes, which can perform operations of drawing eyeliners for making up the eyes and sticking the false eyelashes in one step.
The technical content of the invention is as follows:
a viscous eyeliner with strong adhesion to false eyelashes comprises solvent, humectant, colorant, emulsifier, viscosity-increasing film-forming agent, colorant and antiseptic;
the water-based adhesive comprises, by mass, 5-8% of a solvent, 5-8% of a humectant, 3-5% of a colorant, 4-8% of an emulsifier, 74-81% of a tackifying film-forming agent and 0.1-0.3% of a preservative.
The solvent comprises water, and the humectant comprises propylene glycol and 1, 2-butanediol;
the preservative comprises phenoxyethanol and caprylyl glycol;
the colorant comprises CI 77266;
the emulsifier is polysorbate-80, triethanolamine and sorbitan sesquioleate;
the tackifying film forming agent comprises polybutyl acrylate, rosin acrylate, terpene resin, styrene/isoprene copolymer, polyvinyl acetate, hydroxyacrylic acid (ester) copolymer, polyvinyl chloride, acrylic acid (ester) copolymer/octylacrylamide copolymer, styrene/acrylic acid (ester) copolymer, polyurethane resin, acrylic acid (ester) copolymer/ethylhexyl acrylate copolymer;
the antiseptic comprises phenoxyethanol, octoglycol and chlorphenesin.
The invention also provides a viscous eyeliner with strong false eyelash sticking effect, which is applied to draw eyeliner and/or stick false eyelash.
The invention also provides a preparation method of the viscous eyeliner with strong false eyelashes, which comprises the following steps: mixing solvent, humectant and emulsifier, and placing at 10-2～10-1Heating to 80-90 ℃ under the vacuum environment of MPa for vacuum emulsification reaction, then adding a preservative for constant-temperature homogeneous stirring, then adding a tackifying film-forming agent and a colorant for constant-temperature homogeneous stirring, finally adding the rest preservative and a humectant for stirring, cooling the obtained product, and then sealing and storing.
The invention has the following beneficial effects:
the eyeliner can be directly adhered to false eyelashes, the functions of the eyeliner and glue or glue paste for adhering the false eyelashes are combined into a whole, the irritation and damage to skin can be reduced compared with the traditional glue or glue paste for adhering the false eyelashes, the adhesion enhancing film forming agent of the eyeliner can enable the eyeliner to have strong adhesion and to adhere the false eyelashes, the skin-friendly feeling and the soft feeling of the eyeliner are improved by adding the emulsifier, the irritation to the skin by the eyeliner is greatly reduced, the oxidation resistance of the skin is improved compared with the traditional eyeliner, the skin around the eyes is protected, the problem that the eyeliner is not attractive in eye makeup or the false eyelashes are easy to fall off is solved, the damage to the eyes and the skin around the eyes is reduced, and the eyeliner product can be also applied to eyeliners or eyeliners.
Drawings
Fig. 1 is a schematic view of an eyeliner product and an adhesive eyelash.
Detailed Description
The present invention is described in further detail in the following description of specific embodiments and the accompanying drawings, it is to be understood that these embodiments are merely illustrative of the present invention and are not intended to limit the scope of the invention, which is defined by the appended claims, and modifications thereof by those skilled in the art after reading this disclosure that are equivalent to the above described embodiments.
All the raw materials and reagents of the invention are conventional market raw materials and reagents unless otherwise specified.
The sources of the raw materials used in the preparation of the viscous eyeliner of the present invention having strongly adhered false eyelashes are shown in table 1:
TABLE 1 eyeliner raw material ingredient Table
The eyeliner comprises, by mass, 5-8% of a solvent, 5-8% of a humectant, 3-5% of a colorant, 4-8% of an emulsifier, 75-85% of a tackifying film-forming agent and 0.1-0.3% of a preservative.
Example 1
A preparation method of viscous eyeliner with strong adhesion to false eyelashes comprises:
1) mixing 5% water, 3% propylene glycol, 3% polysorbate-80, 1% triethanolamine and 1% sorbitan sesquialterPlacing oleate into a vacuum emulsifying pot with vacuum degree of 10-2Heating an emulsifying pot to 85 ℃ under MPa to perform vacuum emulsification reaction;
2) adding 0.1% phenoxyethanol and 0.1% caprylyl glycol antiseptic into the emulsifying pot, maintaining the temperature at 85 deg.C, homogenizing and stirring for 10 min;
3) then adding 5.2% of polybutyl acrylate, 5.5% of rosin acrylate, 7% of terpene resin, 6% of styrene/isoprene copolymer, 7% of polyvinyl acetate, 8% of hydroxy acrylic acid (ester) copolymer, 9% of polyvinyl chloride, 8% of acrylic acid (ester)/octyl acrylamide copolymer, 7% of styrene/acrylic acid (ester) copolymer, 9% of polyurethane resin, 9% of acrylic acid (ester)/ethylhexyl acrylate copolymer and other tackifying film forming agents and 4% of CI77266 coloring agent, keeping the temperature at 85 ℃, and homogenizing and stirring for 10 minutes;
4) and finally, adding the rest 0.1% of chlorphenesin preservative and 2% of 1, 2-butanediol humectant, continuing homogenizing and stirring for minutes, cooling to 50 ℃ after the products are completely fused, putting the obtained product into a heat-resistant bag, and sealing and storing to obtain the eyeliner product.
Example 2
A preparation method of viscous eyeliner with strong adhesion to false eyelashes comprises:
1) putting 6% of water, 3% of propylene glycol, 3% of polysorbate-80, 3% of triethanolamine and 2% of sorbitan sesquioleate into a vacuum emulsifying pot, and setting the vacuum degree to 10-2Heating an emulsifying pot to 87 ℃ under MPa to perform vacuum emulsification reaction;
2) adding 0.1% phenoxyethanol and 0.1% caprylyl glycol antiseptic into the emulsifying pot, maintaining the temperature at 87 deg.C, homogenizing and stirring for 10 min;
3) adding tackifying film forming agents such as 5.5% of polybutyl acrylate, 6.2% of rosin acrylate, 6% of terpene resin, 8% of styrene/isoprene copolymer, 7% of polyvinyl acetate, 8% of hydroxyacrylic acid (ester) copolymer, 7% of polyvinyl chloride, 6% of acrylic acid (ester)/octylacrylamide copolymer, 6% of styrene/acrylic acid (ester) copolymer, 9% of polyurethane resin, 8% of acrylic acid (ester)/ethylhexyl acrylate copolymer and the like, maintaining the temperature at 87 ℃, and homogenizing and stirring for 10 minutes;
4) and finally, adding the rest 0.1% of chlorphenesin preservative and 3% of 1, 2-butanediol humectant, continuing homogenizing and stirring for minutes, cooling to 50 ℃ after the products are completely fused, adding 3% of CI77266 colorant, putting the obtained product into a heat-resistant bag, and sealing and storing to obtain the eyeliner product.
Example 3
A preparation method of viscous eyeliner with strong adhesion to false eyelashes comprises:
1) putting 6.5% of water, 4% of 1, 2-butanediol, 2% of polysorbate-80, 3% of triethanolamine and 1% of sorbitan sesquioleate into a vacuum emulsifying pot, setting the vacuum degree to be 0.1MPa, and heating the emulsifying pot to 83 ℃ for vacuum emulsification reaction;
2) adding 0.1% phenoxyethanol and 0.1% caprylyl glycol antiseptic into the emulsifying pot, maintaining the temperature at 83 deg.C, homogenizing and stirring for 10 min;
3) then adding tackifying film forming agents such as 5% of polybutyl acrylate, 4.2% of rosin acrylate, 7% of terpene resin, 7% of styrene/isoprene copolymer, 8% of polyvinyl acetate, 8% of hydroxyacrylic acid (ester) copolymer, 7% of polyvinyl chloride, 7% of acrylic acid (ester)/octylacrylamide copolymer, 6% of styrene/acrylic acid (ester) copolymer, 8% of polyurethane resin, 8% of acrylic acid (ester)/ethylhexyl acrylate copolymer and the like, and 4% of a coloring agent CI77266, keeping the temperature at 83 ℃, and uniformly stirring for 10 minutes;
4) and finally, adding the rest 0.1% of chlorphenesin preservative and 4% of propylene glycol humectant, continuing homogenizing and stirring for minutes, cooling to 50 ℃ after the products are completely fused, putting the obtained product into a heat-resistant bag, and sealing and storing to obtain the eyeliner product.
Example 4
A preparation method of viscous eyeliner with strong adhesion to false eyelashes comprises:
1) putting 7% of water, 2.5% of propylene glycol, 2% of polysorbate-80, 2% of triethanolamine and 3% of sorbitan sesquioleate into a vacuum emulsification pot, setting the vacuum degree to be 0.05MPa, and heating the emulsification pot to 88 ℃ for vacuum emulsification reaction;
2) adding 0.05% phenoxyethanol and 0.03% caprylyl glycol antiseptic into the emulsifying pan, maintaining the temperature at 88 deg.C, homogenizing and stirring for 10 min;
3) adding tackifying film forming agents such as 4.9% of polybutyl acrylate, 4% of rosin acrylate, 8% of terpene resin, 7% of styrene/isoprene copolymer, 6% of polyvinyl acetate, 6% of hydroxyacrylic acid (ester) copolymer, 7% of polyvinyl chloride, 8% of acrylic acid (ester)/octylacrylamide copolymer, 9% of styrene/acrylic acid (ester) copolymer, 7% of polyurethane resin, 8% of acrylic acid (ester)/ethylhexyl acrylate copolymer and the like, and 5% of a coloring agent CI77266, keeping the temperature at 88 ℃, and homogenizing and stirring for 10 minutes;
4) and finally, adding the rest 0.02 percent of chlorphenesin preservative and 3.5 percent of 1, 2-butanediol humectant, continuing homogenizing and stirring for 8 minutes, cooling to 50 ℃ after the products are completely fused, putting the obtained product into a heat-resistant bag, and sealing and storing to obtain the eyeliner product.
Example 5
A preparation method of viscous eyeliner with strong adhesion to false eyelashes comprises:
1) putting 8% of water, 2.5% of 1, 2-butanediol, 2% of polysorbate-80, 2% of triethanolamine and 1% of sorbitan sesquioleate into a vacuum emulsifying pot, setting the vacuum degree to be 0.1MPa, and heating the emulsifying pot to 90 ℃ for vacuum emulsification reaction;
2) adding 0.05% phenoxyethanol and 0.05% caprylyl glycol antiseptic into the emulsifying pan, maintaining the temperature at 90 deg.C, homogenizing and stirring for 12 min;
3) then adding 5.8% of polybutyl acrylate, 6% of rosin acrylate, 8% of terpene resin, 7% of styrene/isoprene copolymer, 8% of polyvinyl acetate, 6% of hydroxyacrylic acid (ester) copolymer, 7% of polyvinyl chloride, 8% of acrylic acid (ester)/octylacrylamide copolymer, 9% of styrene/acrylic acid (ester) copolymer, 7% of polyurethane resin, 7% of acrylic acid (ester)/ethylhexyl acrylate copolymer and other tackifying film forming agents and 3% of a coloring agent CI77266, keeping the temperature at 90 ℃, and carrying out homogeneous stirring for 12 minutes;
4) and finally, adding the rest 0.1 percent of chlorphenesin preservative and 2.5 percent of propylene glycol humectant, continuing homogenizing and stirring for 10 minutes, cooling to 50 ℃ after the products are completely fused, putting the obtained product into a heat-resistant bag, and sealing and storing to obtain the eyeliner product.
The application method of the eyeliner comprises the following steps:
the eyeliner is loaded in an eyeliner box or an eyeliner pen, the eyeliner is drawn according to a desired line, and the eyeliner is formed after the eyeliner is air-dried without bonding false eyelashes; if the false eyelashes need to be adhered, the false eyelashes need to be adhered after the eyelash lines are drawn.
The products of the above 5 examples were tested as follows:
1. patch test on human skin
Selecting 25 female volunteers, wherein the female volunteers are 20-30 years old, the volunteers all conform to a subject selection principle in technical specification for cosmetic safety (2015 edition), averagely dividing the 25 female volunteers into 5 groups, and performing a human skin spot test on the 5 groups of female volunteers according to a test method in the human skin spot test in technical specification for cosmetic safety (2015 edition) by using the products of the 5 embodiments, wherein the tests comprise arm and back tests, and the result shows that the skin reaction degrees of the 15 female volunteers are negative, namely negative reactions, namely the products have no stimulation on the human skin, and the eye liner liquid used by users for expressing is mild in touch and not easy to make up.
Fig. 1 shows a line drawn on the hand of the eyeliner product of example 1 and false eyelashes, which show that the false eyelashes can be firmly stuck on the eyeliner and can be removed only by hand, which shows that the eyeliner product of the present invention can perform the function of combining eyeliner and sticking false eyelashes, which can strongly stick false eyelashes.
2. Efficacy use test
The above 5 groups of female volunteers used the products of examples 1-5, respectively, and prepared false eyelashes, each with eyelids painted with eye lines, left eye not adhered to false eyelash, and right eye adhered to false eyelash.
Each of 5 female volunteers had 5 women, each group used eyeliner and adhered false eyelashes, and according to the survey results, the eye makeup effect among 25 women was: the eyeliner of the left eye is smooth, the false eyelashes of the right eye are firmly adhered, and the false eyelashes can be kept on eyelids for half a day or more, so that the eyeliner in the embodiment can be directly adhered to the false eyelashes, has no discomfort to skin, and brings great convenience to makeup of the eyeliner of women.
Claims (10)
1. The viscous eyeliner capable of strongly sticking false eyelashes is characterized by comprising a solvent, a humectant, a colorant, an emulsifier, a tackifying film forming agent, a colorant and a preservative.
2. The viscous eyeliner of claim 1, wherein the solvent is 5-8 wt%, the humectant is 5-8 wt%, the colorant is 3-5 wt%, the emulsifier is 4-8 wt%, the viscosity-increasing film-forming agent is 74-81 wt%, and the preservative is 0.1-0.3 wt%.
3. The viscous eyeliner having strong adhesion to false eyelashes of claim 1 or 2, wherein the solvent comprises water, and the moisturizer comprises propylene glycol and 1, 2-butanediol.
4. The viscous eyeliner having strongly adhered false eyelashes of claim 1 or 2, wherein the preservative comprises phenoxyethanol and caprylyl glycol.
5. A viscous eyeliner having a strong adhesion to false eyelashes of claim 3, wherein the colorant comprises CI 77266.
6. The viscous eyeliner with strong adhesion to false eyelashes of claim 1 or 2, wherein the emulsifiers polysorbate-80, triethanolamine and sorbitan sesquioleate.
7. The viscous eyeliner of claim 1 or 2, wherein the viscosity-increasing film-forming agent comprises polybutyl acrylate, rosin acrylate, terpene resin, styrene/isoprene copolymer, polyvinyl acetate, hydroxyacrylic acid (ester) copolymer, polyvinyl chloride, acrylic acid (ester)/octylacrylamide copolymer, styrene/acrylic acid (ester) copolymer, polyurethane resin, acrylic acid (ester)/ethylhexyl acrylate copolymer.
8. The viscous eyeliner having strong adhesion to false eyelashes of claim 1 or 2, wherein the preservative comprises phenoxyethanol, caprylyl glycol and chlorphenesin.
9. A viscous eyeliner having strongly adhered eyelash as claimed in any one of claims 1 to 8, which is applied to draw eyeliner and/or adhere eyelash.
10. A method for preparing the viscous eyeliner of any one of claims 1 to 8 having strongly adhered false eyelashes by: mixing solvent, humectant and emulsifier, and placing at 10-2~10-1 Heating to 80-90 ℃ under the vacuum environment of MPa for vacuum emulsification reaction, then adding a preservative for constant-temperature homogeneous stirring, then adding a tackifying film-forming agent and a colorant for constant-temperature homogeneous stirring, finally adding the rest preservative and a humectant for stirring, cooling the obtained product, and then sealing and storing.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114209611A (en) * | 2021-12-10 | 2022-03-22 | 上海创元化妆品有限公司 | Eyeliner based on aqueous polyurethane dispersion and preparation method thereof |
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Application publication date: 20201225 |