CN112126379A - Adhesive for sticking false eyelashes and preparation method thereof - Google Patents
Adhesive for sticking false eyelashes and preparation method thereof Download PDFInfo
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- CN112126379A CN112126379A CN202010383901.9A CN202010383901A CN112126379A CN 112126379 A CN112126379 A CN 112126379A CN 202010383901 A CN202010383901 A CN 202010383901A CN 112126379 A CN112126379 A CN 112126379A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J125/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Adhesives based on derivatives of such polymers
- C09J125/02—Homopolymers or copolymers of hydrocarbons
- C09J125/04—Homopolymers or copolymers of styrene
- C09J125/08—Copolymers of styrene
- C09J125/14—Copolymers of styrene with unsaturated esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/04—Homopolymers or copolymers of esters
- C09J133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09J133/08—Homopolymers or copolymers of acrylic acid esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a sticky glue for sticking false eyelashes and a preparation method thereof. The adhesive glue comprises the following raw materials: solvent, humectant, emulsifier, neutralizer, viscous film-forming agent and preservative; counted by weight parts, the viscous film-forming agent comprises 6-12 parts of rosin acrylate, 5-15 parts of C5-6 alkane/naphthene/terpene copolymer, 5-40 parts of styrene/acrylate copolymer, 5-15 parts of acrylate/ethylhexyl acrylate copolymer, 3-13 parts of polyvinyl alcohol and 15-25 parts of polyurethane; the preservative is 0.1-0.5 part of phenoxyethanol, 0.1-0.5 part of octoglycol and 0.1-0.5 part of chlorphenesin. The preparation method of the adhesive comprises adding the above components in batches, heating at different temperatures, stirring, and adjusting pH to obtain the final product. The adhesive for sticking false eyelashes has strong adhesiveness, long makeup time, no corner lifting in the period of makeup, and no makeup in rainy and foggy days.
Description
Technical Field
The invention relates to the technical field of glue for makeup, in particular to a viscous glue for sticking false eyelashes and a preparation method thereof.
Background
The vast women loving beauty have the habit of using false eyelashes, and the false eyelashes can make the women good for looking, effectively improve the female quality, make it more confident and beautiful, are the beauty supplies that the woman likes deeply. When the false eyelashes are used, the false eyelashes need to be adhered to eyelids by glue which is used for sticking the false eyelashes. Generally, an adhesive line is drawn on eyelids with a glue for sticking false eyelashes or the glue is directly applied to roots of the false eyelashes, and then the false eyelashes are stuck on the glue to be stuck on the eyelids. The existing glue for sticking false eyelashes has insufficient viscosity, is easy to tilt corners after a long time, has short makeup holding time, and is removed in a severe rain and fog weather.
Disclosure of Invention
The invention aims to provide a sticky glue for sticking false eyelashes and a preparation method thereof. The problems that the viscosity of false eyelash sticking glue is insufficient, the corners are easy to warp after a long time, the makeup holding time is short, and makeup removal is aggravated in rainy and foggy days in the background technology are solved.
The technical scheme of the invention is as follows: a viscous gel for sticking false eyelashes comprises the following raw materials, solvent, humectant, emulsifier, neutralizer, viscous film-forming agent, and antiseptic; counting by weight parts, the solvent is 5-15 parts of water; the humectant comprises 2-4 parts of propylene glycol; the emulsifier is polysorbate-800.5-1.5 parts; the neutralizing agent is aminomethyl propanol 0.1-0.8 part; the adhesive film-forming agent comprises 6-12 parts of rosin acrylate, 5-15 parts of C5-6 alkane/naphthene/terpene copolymer, 5-40 parts of styrene/acrylate copolymer, 5-15 parts of acrylate/ethylhexyl acrylate copolymer, 3-13 parts of polyvinyl alcohol and 15-25 parts of polyurethane; the preservative is 0.1-0.5 part of phenoxyethanol, 0.1-0.5 part of octoglycol and 0.1-0.5 part of chlorphenesin.
The adhesive for adhering false eyelashes comprises the following raw materials in parts by weight, and the solvent is 5-10 parts of water; the humectant is 2-4 parts of propylene glycol and 1-3 parts of 1, 2-butanediol; the emulsifier is polysorbate-80.5-1.5 parts; the neutralizing agent is aminomethyl propanol 0.2-0.8 part; the adhesive film-forming agent comprises 6-12 parts of rosin acrylate, 5-10 parts of C5-6 alkane/naphthene/terpene copolymer, 20-40 parts of styrene/acrylic acid (ester) copolymer, 6-12 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer, 5-11 parts of polyvinyl alcohol and 110-20 parts of polyurethane; the preservative is 0.1-0.3 part of phenoxyethanol, 0.1-0.3 part of octoglycol and 0.1-0.3 part of chlorphenesin.
The adhesive for sticking false eyelashes comprises the following raw materials in parts by weight, and the solvent is 10 parts of water; the humectant is 3 parts of propylene glycol and 2 parts of 1, 2-butanediol; the emulsifier is polysorbate-81 parts; the neutralizing agent is 0.5 part of aminomethyl propanol; the adhesive film-forming agent comprises 9 parts of rosin acrylate, 10 parts of C5-6 alkane/naphthene/terpene copolymer, 30.2 parts of styrene/acrylic acid (ester) copolymer, 11 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer, 8 parts of polyvinyl alcohol and 115 parts of polyurethane; the preservative is 0.1 part of phenoxyethanol, 0.1 part of octoglycol and 0.1 part of chlorphenesin.
The preparation method of the sticky glue for sticking false eyelashes comprises the following steps,
a. putting water, propylene glycol, 1, 2-butanediol, and polysorbate-80 into emulsifying pot, mixing, dissolving, and heating to 80-90 deg.C to obtain product A;
b. sequentially adding rosin acrylate, C5-6 alkane/naphthene/terpene copolymer, styrene/acrylic acid (ester) copolymer, acrylic acid (ester) or ethylhexyl acrylate copolymer, polyvinyl alcohol and polyurethane-1 into the product A, maintaining the temperature at 80-90 ℃, and homogenizing and stirring for 3-8min to obtain a product B;
c. adding phenoxyethanol, caprylyl glycol and chlorphenesin to product C, homogenizing and stirring for 1-5min to obtain product C;
d. cooling product C to 30-50 deg.C, adding aminomethyl propanol to pH of 6.5-8.5, homogenizing and stirring for 1-3min, and discharging to obtain the final product.
The sticky glue for sticking false eyelashes comprises 3-5 parts by weight of a styrene/isoprene copolymer.
The adhesive for sticking false eyelashes further comprises the following raw materials, by weight, 20-40 parts of polybutyl acrylate, 5-15 parts of polyvinyl acetate and 5-10 parts of polyvinylpyrrolidone. The polybutyl acrylate, the polyvinyl acetate and the polyvinylpyrrolidone are used together, so that the adhesive has the characteristic of lasting adhesion when being wetted, namely the adhesive recovers viscosity when being wetted after being dried, can be used as glue for repeatedly adhering false eyelashes, is simple to make up, and can save the makeup cost.
The viscous glue for sticking false eyelashes comprises the following raw materials in parts by weight, and the solvent is 3-8 parts of water; the humectant is 1-5 parts of propylene glycol; the emulsifier is polysorbate-800.5-1.5 parts; the neutralizing agent is aminomethyl propanol 0.2-0.8 part; the adhesive film-forming agent is 6-10 parts of rosin acrylate, 3-8 parts of polyvinyl alcohol, 3-8 parts of C5-6 alkane/naphthene/terpene copolymer, 2-6 parts of styrene/isoprene copolymer, 3-8 parts of styrene/acrylic acid (ester) copolymer, 6-8 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer and 16-10 parts of polyurethane; the preservative is 0.1 to 0.3 part of phenoxyethanol, 0.1 to 0.3 part of octoglycol and 0.1 to 0.3 part of chlorphenesin; also comprises 20-40 parts of polybutyl acrylate, 8-12 parts of polyvinyl acetate and 6-10 parts of polyvinylpyrrolidone.
The adhesive for adhering false eyelashes comprises the following raw materials in parts by weight, and the solvent is 5 parts of water; the humectant is 3 parts of propylene glycol; the emulsifier is polysorbate-801 parts; the neutralizing agent is 0.5 part of aminomethyl propanol; the adhesive film-forming agent comprises 8 parts of rosin acrylate, 5 parts of polyvinyl alcohol, 5.2 parts of C5-6 alkane/naphthene/terpene copolymer, 4 parts of styrene/isoprene copolymer, 5 parts of styrene/acrylic acid (ester) copolymer, 7 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer and 18 parts of polyurethane; the preservative is 0.1 part of phenoxyethanol, 0.1 part of octoglycol and 0.1 part of chlorphenesin; also comprises 31 parts of polybutyl acrylate, 10 parts of polyvinyl acetate and 8 parts of polyvinylpyrrolidone.
The preparation method of the sticky glue for sticking false eyelashes comprises the following steps,
step a, putting water, propylene glycol and polysorbate-80 into an emulsifying pot, uniformly mixing and dissolving, and heating to 80-90 ℃ to obtain a product A;
b, sequentially adding polybutyl acrylate, polyvinyl acetate, polyvinylpyrrolidone, rosin acrylate, polyvinyl alcohol, C5-6 alkane/naphthene/terpene copolymer, styrene/isoprene copolymer, styrene/acrylic acid (ester) copolymer, acrylic acid (ester) or ethylhexyl acrylate copolymer and polyurethane-1 into the product A, maintaining the temperature at 80-90 ℃, and homogenizing and stirring for 3-8min to obtain a product B;
step C, adding phenoxyethanol, caprylyl glycol and chlorphenesin to the product B, and homogenizing and stirring for 1-5min to obtain a product C;
and d, cooling the product C to 30-50 ℃, adding aminomethyl propanol to adjust the pH value to 6.5-8.5, homogenizing and stirring for 1-3min, and discharging to obtain a finished product.
Compared with the prior art, the rosin acrylic ester, the C5-6 alkane/naphthene/terpene copolymer, the styrene/acrylate copolymer, the acrylate/ethylhexyl acrylate copolymer, the polyvinyl alcohol and the polyurethane-1 have strong viscosity, and the components are mixed according to the proportion of the invention to generate synergistic effect, so that the viscosity stronger than that of any single component is generated, and the false eyelashes can be effectively adhered. The proportion of the components of the adhesive can ensure that the adhesive for adhering false eyelashes firmly adheres the false eyelashes to eyelids, has no tight feeling when being adhered to skin, can keep the makeup time for 12 hours, does not warp corners in the period, and does not make up in rainy and foggy weather. The adhesive for sticking false eyelashes has strong adhesiveness, long makeup time, no corner lifting in the period of makeup, and no makeup in rainy and foggy days.
Detailed Description
The present invention is further illustrated by the following examples, which are not to be construed as limiting the invention.
Example 1. The adhesive for sticking false eyelashes comprises the following raw materials in parts by weight and a solvent: 5 parts of water; humectant: 2 parts of propylene glycol; emulsifier: polysorbate-800.5 parts; neutralizing agent: 0.1 part of aminomethyl propanol; a sticky film forming agent: 6 parts of rosin acrylate, 5 parts of C5-6 alkane/naphthene/terpene copolymer, 5 parts of styrene/acrylate copolymer, 5 parts of acrylate/ethylhexyl acrylate copolymer, 3 parts of polyvinyl alcohol and 15 parts of polyurethane; preservative: 0.1 part of phenoxyethanol, 0.1 part of octoglycol and 0.1 part of chlorphenesin.
The preparation method of the sticky glue for sticking false eyelashes comprises the following steps,
a. putting water, propylene glycol, 1, 2-butanediol, and polysorbate-80 into emulsifying pot, mixing, dissolving, and heating to 80 deg.C to obtain product A;
b. sequentially adding rosin acrylate, C5-6 alkane/naphthene/terpene copolymer, styrene/acrylic acid (ester) copolymer, acrylic acid (ester) or ethylhexyl acrylate copolymer, polyvinyl alcohol and polyurethane-1 into the product A, maintaining the temperature at 80-90 ℃, and homogenizing and stirring for 3-8min to obtain a product B;
c. adding phenoxyethanol, caprylyl glycol and chlorphenesin to product C, homogenizing and stirring for 1min to obtain product C;
d. cooling product C to 30 deg.C, adding aminomethyl propanol to pH of 6.7, homogenizing and stirring for 1min, discharging to obtain final product, and sealing and storing.
The makeup time of the adhesive glue for sticking false eyelashes is 12 hours.
Example 2. A sticky glue for sticking false eyelashes comprises the following raw materials in parts by weight; solvent: 15 parts of water; humectant: 4 parts of propylene glycol; emulsifier: polysorbate-801.5 parts; neutralizing agent: 0.8 part of aminomethyl propanol; a sticky film forming agent: 12 parts of rosin acrylate, 15 parts of C5-6 alkane/naphthene/terpene copolymer, 40 parts of styrene/acrylate copolymer, 15 parts of acrylate/ethylhexyl acrylate copolymer, 13 parts of polyvinyl alcohol and 125 parts of polyurethane; preservative: 0.5 part of phenoxyethanol, 0.5 part of octoglycol and 0.5 part of chlorphenesin.
The preparation method of the sticky glue for sticking false eyelashes comprises the following steps,
a. putting water, propylene glycol, 1, 2-butanediol, and polysorbate-80 into emulsifying pot, mixing, dissolving, and heating to 90 deg.C to obtain product A;
b. sequentially adding rosin acrylate, C5-6 alkane/naphthene/terpene copolymer, styrene/acrylic acid (ester) copolymer, acrylic acid (ester) or ethylhexyl acrylate copolymer, polyvinyl alcohol and polyurethane-1 into the product A, maintaining the temperature at 90 ℃, and homogenizing and stirring for 8min to obtain a product B;
c. adding phenoxyethanol, caprylyl glycol and chlorphenesin to product C, homogenizing and stirring for 5min to obtain product C;
d. cooling product C to 50 deg.C, adding aminomethyl propanol to pH of 7.9, homogenizing and stirring for 3min, discharging to obtain final product, and sealing and storing.
The makeup time of the adhesive glue for sticking false eyelashes is 12 hours.
Example 3. The adhesive for sticking false eyelashes comprises the following raw materials in parts by weight and a solvent: 10 parts of water; humectant: 3 parts of propylene glycol and 2 parts of 1, 2-butanediol; emulsifier: polysorbate-81 parts; neutralizing agent: 0.5 part of aminomethyl propanol; a sticky film forming agent: 9 parts of rosin acrylate, 10 parts of C5-6 alkane/naphthene/terpene copolymer, 30.2 parts of styrene/acrylic acid (ester) copolymer, 11 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer, 8 parts of polyvinyl alcohol and 115 parts of polyurethane; preservative: 0.1 part of phenoxyethanol, 0.1 part of octoglycol and 0.1 part of chlorphenesin.
The preparation method of the sticky glue for sticking false eyelashes comprises the following steps,
a. putting water, propylene glycol, 1, 2-butanediol, and polysorbate-80 into emulsifying pot, mixing, dissolving, and heating to 85 deg.C to obtain product A;
b. sequentially adding rosin acrylate, C5-6 alkane/naphthene/terpene copolymer, styrene/acrylic acid (ester) copolymer, acrylic acid (ester) or ethylhexyl acrylate copolymer, polyvinyl alcohol and polyurethane-1 into the product A, maintaining the temperature at 85 ℃, and homogenizing and stirring for 5min to obtain a product B;
c. adding phenoxyethanol, caprylyl glycol and chlorphenesin to product C, homogenizing and stirring for 3min to obtain product C;
d. cooling product C to 45 deg.C, adding aminomethyl propanol with pH of 7.2, homogenizing and stirring for 2min, discharging to obtain final product, and sealing and storing.
The makeup time of the adhesive glue for sticking false eyelashes is 12 hours.
The composition of the tacky gum for sticking false eyelashes in the examples 1 to 3 is shown in Table 1. The substance with "/" in the present invention is a conventional cosmetic raw material of a body mixture type determined by ingredients.
Table 1 composition table (1) of tacky adhesive for tacky false eyelashes
Example 4. The adhesive for sticking false eyelashes comprises the following raw materials in parts by weight and a solvent: 3 parts of water; humectant: 1 part of propylene glycol; emulsifier: polysorbate-800.5 parts; neutralizing agent: 0.2 part of aminomethyl propanol; a sticky film forming agent: 6 parts of rosin acrylate, 3 parts of polyvinyl alcohol, 3 parts of C5-6 alkane/naphthene/terpene copolymer, 2 parts of styrene/isoprene copolymer, 3 parts of styrene/acrylic acid (ester) copolymer, 6 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer and 16 parts of polyurethane; preservative: 0.1 part of phenoxyethanol, 0.1 part of octoglycol and 0.1 part of chlorphenesin; also comprises 20 parts of polybutyl acrylate, 8 parts of polyvinyl acetate and 6 parts of polyvinylpyrrolidone.
The preparation method of the sticky glue for sticking false eyelashes comprises the following steps,
step a, putting water, propylene glycol and polysorbate-80 into an emulsifying pot, uniformly mixing and dissolving, and heating to 80 ℃ to obtain a product A;
b, sequentially adding polybutyl acrylate, polyvinyl acetate, polyvinylpyrrolidone, rosin acrylate, polyvinyl alcohol, C5-6 alkane/naphthene/terpene copolymer, styrene/isoprene copolymer, styrene/acrylic acid (ester) copolymer, acrylic acid (ester) or ethylhexyl acrylate copolymer and polyurethane-1 into the product A, maintaining the temperature at 80 ℃, and carrying out homogeneous stirring for 3min to obtain a product B;
adding phenoxyethanol, caprylyl glycol and chlorphenesin to the product B, and homogenizing and stirring for 1min to obtain a product C;
and d, cooling the product C to 30 ℃, adding aminomethyl propanol to adjust the pH value to 6.6, homogenizing and stirring for 1min, discharging to obtain a finished product, and sealing and storing.
The makeup time of the adhesive glue for sticking false eyelashes is 12 hours.
Example 5. The adhesive for sticking false eyelashes comprises the following raw materials in parts by weight and a solvent: 8 parts of water; humectant: 5 parts of propylene glycol; emulsifier: polysorbate-801.5 parts; neutralizing agent: 0.8 part of aminomethyl propanol; a sticky film forming agent: 10 parts of rosin acrylic ester, 8 parts of polyvinyl alcohol, 8 parts of C5-6 alkane/naphthene/terpene copolymer, 6 parts of styrene/isoprene copolymer, 8 parts of styrene/acrylic acid (ester) copolymer, 8 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer and 110 parts of polyurethane; preservative: 0.3 part of phenoxyethanol, 0.3 part of octoglycol and 0.3 part of chlorphenesin; also comprises 40 parts of polybutyl acrylate, 12 parts of polyvinyl acetate and 10 parts of polyvinylpyrrolidone.
The preparation method of the sticky glue for sticking false eyelashes comprises the following steps,
step a, putting water, propylene glycol and polysorbate-80 into an emulsifying pot, uniformly mixing and dissolving, and heating to 90 ℃ to obtain a product A;
b, sequentially adding polybutyl acrylate, polyvinyl acetate, polyvinylpyrrolidone, rosin acrylate, polyvinyl alcohol, C5-6 alkane/naphthene/terpene copolymer, styrene/isoprene copolymer, styrene/acrylic acid (ester) copolymer, acrylic acid (ester) or ethylhexyl acrylate copolymer and polyurethane-1 into the product A, maintaining the temperature at 90 ℃, and carrying out homogeneous stirring for 8min to obtain a product B;
adding phenoxyethanol, caprylyl glycol and chlorphenesin to the product B, homogenizing and stirring for 5min to obtain a product C;
and d, cooling the product C to 50 ℃, adding aminomethyl propanol to adjust the pH value to 8.2, homogenizing and stirring for 3min, discharging to obtain a finished product, and sealing and storing.
The makeup time of the adhesive glue for sticking false eyelashes is 12 hours.
Example 6. The adhesive for sticking false eyelashes comprises the following raw materials in parts by weight and a solvent: 5 parts of water; humectant: 3 parts of propylene glycol; emulsifier: polysorbate-801 parts; neutralizing agent: 0.5 part of aminomethyl propanol; a sticky film forming agent: 8 parts of rosin acrylic ester, 5 parts of polyvinyl alcohol, 5.2 parts of C5-6 alkane/naphthene/terpene copolymer, 4 parts of styrene/isoprene copolymer, 5 parts of styrene/acrylic acid (ester) copolymer, 7 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer and 18 parts of polyurethane; preservative: 0.1 part of phenoxyethanol, 0.1 part of octoglycol and 0.1 part of chlorphenesin; also comprises 31 parts of polybutyl acrylate, 10 parts of polyvinyl acetate and 8 parts of polyvinylpyrrolidone.
The preparation method of the sticky glue for sticking false eyelashes comprises the following steps,
step a, putting water, propylene glycol and polysorbate-80 into an emulsifying pot, uniformly mixing and dissolving, and heating to 85 ℃ to obtain a product A;
b, sequentially adding polybutyl acrylate, polyvinyl acetate, polyvinylpyrrolidone, rosin acrylate, polyvinyl alcohol, C5-6 alkane/naphthene/terpene copolymer, styrene/isoprene copolymer, styrene/acrylic acid (ester) copolymer and propylene into the product A, and homogenizing and stirring at 85 ℃ for 5min to obtain a product B;
adding phenoxyethanol, caprylyl glycol and chlorphenesin to the product B, homogenizing and stirring for 3min to obtain a product C;
and d, cooling the product C to 45 ℃, adding aminomethyl propanol to adjust the pH value to 7.1, homogenizing and stirring for 2min, discharging to obtain a finished product, and sealing and storing.
The makeup time of the adhesive glue for sticking false eyelashes is 12 hours.
The composition of the tacky gum for sticking false eyelashes in the examples 4 to 6 is shown in Table 2.
TABLE 2 composition table (2) of tacky gums for sticking false eyelashes
The present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof, and it should be understood that various changes and modifications can be effected therein by one skilled in the art without departing from the spirit and scope of the invention as defined in the appended claims.
Claims (9)
1. The adhesive glue for sticking false eyelashes is characterized in that: comprises the following raw materials, solvent, humectant, emulsifier, neutralizer, viscous film-forming agent and preservative; counting by weight parts, the solvent is 5-15 parts of water; the humectant comprises 2-4 parts of propylene glycol; the emulsifier is polysorbate-800.5-1.5 parts; the neutralizing agent is aminomethyl propanol 0.1-0.8 part; the adhesive film-forming agent comprises 6-12 parts of rosin acrylate, 5-15 parts of C5-6 alkane/naphthene/terpene copolymer, 5-40 parts of styrene/acrylate copolymer, 5-15 parts of acrylate/ethylhexyl acrylate copolymer, 3-13 parts of polyvinyl alcohol and 15-25 parts of polyurethane; the preservative is 0.1-0.5 part of phenoxyethanol, 0.1-0.5 part of octoglycol and 0.1-0.5 part of chlorphenesin.
2. The adhesive gum for sticking false eyelashes according to claim 1, wherein: the solvent is 5-10 parts of water; the humectant is 2-4 parts of propylene glycol and 1-3 parts of 1, 2-butanediol; the emulsifier is polysorbate-80.5-1.5 parts; the neutralizing agent is aminomethyl propanol 0.2-0.8 part; the adhesive film-forming agent comprises 6-12 parts of rosin acrylate, 5-10 parts of C5-6 alkane/naphthene/terpene copolymer, 20-40 parts of styrene/acrylic acid (ester) copolymer, 6-12 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer, 5-11 parts of polyvinyl alcohol and 110-20 parts of polyurethane; the preservative is 0.1-0.3 part of phenoxyethanol, 0.1-0.3 part of octoglycol and 0.1-0.3 part of chlorphenesin.
3. The adhesive gum for sticking false eyelashes according to claim 2, wherein: the solvent is 10 parts of water; the humectant is 3 parts of propylene glycol and 2 parts of 1, 2-butanediol; the emulsifier is polysorbate-81 parts; the neutralizing agent is 0.5 part of aminomethyl propanol; the adhesive film-forming agent comprises 9 parts of rosin acrylate, 10 parts of C5-6 alkane/naphthene/terpene copolymer, 30.2 parts of styrene/acrylic acid (ester) copolymer, 11 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer, 8 parts of polyvinyl alcohol and 115 parts of polyurethane; the preservative is 0.1 part of phenoxyethanol, 0.1 part of octoglycol and 0.1 part of chlorphenesin.
4. The method for preparing a tacky gum for sticking false eyelashes according to claim 2 or 3, wherein: comprises the following steps of (a) carrying out,
a. putting water, propylene glycol, 1, 2-butanediol, and polysorbate-80 into emulsifying pot, mixing, dissolving, and heating to 80-90 deg.C to obtain product A;
b. sequentially adding rosin acrylate, C5-6 alkane/naphthene/terpene copolymer, styrene/acrylic acid (ester) copolymer, acrylic acid (ester) or ethylhexyl acrylate copolymer, polyvinyl alcohol and polyurethane-1 into the product A, maintaining the temperature at 80-90 ℃, and homogenizing and stirring for 3-8min to obtain a product B;
c. adding phenoxyethanol, caprylyl glycol and chlorphenesin to product C, homogenizing and stirring for 1-5min to obtain product C;
d. cooling product C to 30-50 deg.C, adding aminomethyl propanol to pH of 6.5-8.5, homogenizing and stirring for 1-3min, and discharging to obtain the final product.
5. The adhesive gum for sticking false eyelashes according to claim 1, wherein: the adhesive film-forming agent also comprises 3-5 parts by weight of styrene/isoprene copolymer.
6. The adhesive gum for sticking false eyelashes according to claim 5, wherein: the material also comprises the following raw materials, by weight, 20-40 parts of polybutyl acrylate, 5-15 parts of polyvinyl acetate and 5-10 parts of polyvinylpyrrolidone.
7. The adhesive according to claim 6, wherein: the solvent is 3-8 parts of water; the humectant is 1-5 parts of propylene glycol; the emulsifier is polysorbate-800.5-1.5 parts; the neutralizing agent is aminomethyl propanol 0.2-0.8 part; the adhesive film-forming agent is 6-10 parts of rosin acrylate, 3-8 parts of polyvinyl alcohol, 3-8 parts of C5-6 alkane/naphthene/terpene copolymer, 2-6 parts of styrene/isoprene copolymer, 3-8 parts of styrene/acrylic acid (ester) copolymer, 6-8 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer and 16-10 parts of polyurethane; the preservative is 0.1 to 0.3 part of phenoxyethanol, 0.1 to 0.3 part of octoglycol and 0.1 to 0.3 part of chlorphenesin; also comprises 20-40 parts of polybutyl acrylate, 8-12 parts of polyvinyl acetate and 6-10 parts of polyvinylpyrrolidone.
8. The adhesive gum for sticking false eyelashes according to claim 7, wherein: the solvent is 5 parts of water; the humectant is 3 parts of propylene glycol; the emulsifier is polysorbate-801 parts; the neutralizing agent is 0.5 part of aminomethyl propanol; the adhesive film-forming agent comprises 8 parts of rosin acrylate, 5 parts of polyvinyl alcohol, 5.2 parts of C5-6 alkane/naphthene/terpene copolymer, 4 parts of styrene/isoprene copolymer, 5 parts of styrene/acrylic acid (ester) copolymer, 7 parts of acrylic acid (ester)/ethylhexyl acrylate copolymer and 18 parts of polyurethane; the preservative is 0.1 part of phenoxyethanol, 0.1 part of octoglycol and 0.1 part of chlorphenesin; also comprises 31 parts of polybutyl acrylate, 10 parts of polyvinyl acetate and 8 parts of polyvinylpyrrolidone.
9. The method for preparing a tacky gum for sticking false eyelashes according to claim 7 or 8, wherein: comprises the following steps of (a) carrying out,
step a, putting water, propylene glycol and polysorbate-80 into an emulsifying pot, uniformly mixing and dissolving, and heating to 80-90 ℃ to obtain a product A;
b, sequentially adding polybutyl acrylate, polyvinyl acetate, polyvinylpyrrolidone, rosin acrylate, polyvinyl alcohol, C5-6 alkane/naphthene/terpene copolymer, styrene/isoprene copolymer, styrene/acrylic acid (ester) copolymer, acrylic acid (ester) or ethylhexyl acrylate copolymer and polyurethane-1 into the product A, maintaining the temperature at 80-90 ℃, and homogenizing and stirring for 3-8min to obtain a product B;
step C, adding phenoxyethanol, caprylyl glycol and chlorphenesin to the product B, and homogenizing and stirring for 1-5min to obtain a product C;
and d, cooling the product C to 30-50 ℃, adding aminomethyl propanol to adjust the pH value to 6.5-8.5, homogenizing and stirring for 1-3min, and discharging to obtain a finished product.
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