CN103494717B - Non-irritant mascara cream and preparation method thereof - Google Patents
Non-irritant mascara cream and preparation method thereof Download PDFInfo
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- CN103494717B CN103494717B CN201310357403.7A CN201310357403A CN103494717B CN 103494717 B CN103494717 B CN 103494717B CN 201310357403 A CN201310357403 A CN 201310357403A CN 103494717 B CN103494717 B CN 103494717B
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Abstract
The invention discloses a non-irritant mascara cream and a preparation method thereof. The mascara cream is composed of following components: decyl glucoside, lauryl glucoside, beeswax, candelilla wax, cetanol, silicone oil, polyvinylpyrrolidone, acrylic polymer, ferric oxide, polyacrylamide, (and) C13-C14 isoparaffin, (and) laureth-7, water, and addictive. The mascara cream adopts alkyl glucosides (decyl glucoside and lauryl glucoside) as the emulsifier, combines the vitamin E functions of preventing oxidation, nourishing, and repairing, and generates no allergy or discomfort to eyes after using the mascara cream. The mascara cream has the advantages of uniform coating of mascara cream body, good waterproof effect, long lasting make-up effect, no irritation, and safe using.
Description
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of non-stimulated mascara and preparation method thereof.
Background technology
Mascara product is of a great variety in the market, has dense type, fine elongated, volume sticks up type, plentiful volume sticks up type, dense fine elongated etc., gets consumer reception very much.But because eye part skin is thinner, after use mascara is made up, because causing nictation mastic to contact eye part skin, be easy to cause ocular allergies.So non-stimulated mascara product has just become the focus of cosmetics research staff research instantly.
Summary of the invention
The object of this invention is to provide a kind of safe, gentle non-stimulated mascara, meet the demand of market to the non-stimulated mascara makeup cosmetic of gentleness.
In order to reach object of the present invention, take following technical scheme:
A kind of non-stimulated mascara, it is characterized in that according to mass percent composed of the following components: alkyl glucosides glycoside emulsifying agent 4.0%-8.0%, waxiness 8.0%-18.0%, oils and fats 3.0%-8.0%, film former 5.0%-18.0%, coloring agent 8.0%-20.0%, thickening agent 0.5%-2.0%, antiseptic 0.3%-0.5%, surplus is deionized water.Wherein said alkyl androstanediol emulsifying agent is at least one in following alkyl androstanediol: decyl glucoside 2.0%-4.0%, lauryl glucoside 2.0%-4.0%; Described waxiness be following waxiness at least one and more than: Apis cerana Fabricius 5%-10%, candelilla wax 3%-6%, spermol 1.0%-2.0%; Described oils and fats be at least 2 kinds of following oils and fats or two or more: Cyclomethicone 2-5%, tocopherol acetas 0.5-1%, polydimethylsiloxane 0.5%-2%; Described film former is one or more of following film former: polyvinylpyrrolidone 2.0%-10.0%, acrylate copolymer 3%-8%; Described coloring agent is ferrum oxide 8%-20%; Described thickening agent be polyacrylamide (with) C13-C14 isoparaffin (with) lauryl alcohol-70.5%-2%.
Another object of the present invention is to provide the preparation method of above-mentioned mascara.
In order to reach this purpose, present invention employs following technical scheme:
(1) polyvinylpyrrolidone and deionized water are weighed up in proportion, join successively in vacuum high-shear homogenizer in order, be heated to 75 ~ 78 DEG C and make it dissolve completely, add ferrum oxide and carry out high speed homogenization 3300 ~ 3400r/min, homogenizing 6 minutes; And being kept temperature 75 DEG C, this is aqueous phase;
(2) alkyl glucosides glycoside, waxiness, antiseptic are weighed up in proportion, join heating and stirring pot successively in order, heated and stirred makes it dissolve completely to 75 ~ 78 DEG C, and is kept temperature 75 DEG C, and this is oil phase;
(3) after silicone oil being added oil phase mixing, be heated rapidly to 75 DEG C and slowly join immediately in aqueous phase, open high-shear homogenizer 3000 ~ 3100r/min, homogenizing 12 minutes simultaneously, and keep 75 DEG C;
(4) temperature of emulsion after emulsifying is well down to 60 DEG C, add D phase acrylate copolymer and keep temperature and carry out high speed homogenization 2000 ~ 2500r/min, homogenizing is after 5 minutes, add E heterophasic polypropylene amide (with) C13-C14 isoparaffin (with) after lauryl alcohol-7, low speed homogenizing 1500 ~ 2000r/min, homogenizing 15min opens vacuum machine simultaneously and carries out vacuum defoamation, opens attached stirring 20 ~ 30r/min and lowers the temperature, discharging after being cooled to 35 DEG C.
Beneficial effect of the present invention: the emulsifying agent in formula is with the non-stimulated alkyl polyglucoside of gentleness for emulsifying agent, and the mastic made is gentle, contact non-stimulated afterwards with eye part skin after eyelashes are smeared.
Detailed description of the invention
Below by way of specific embodiment, the present invention is further illustrated, but these embodiments are just in order to illustrate, do not do any type of restriction to the present invention.
Embodiment 1: a kind of non-stimulated mascara
Formula is shown in Table 1.Table 1
Described in the present embodiment 1, a kind of non-stimulated mascara is prepared by following steps:
(1) the alkyl glucosides glycoside of A phase, waxiness, antiseptic are weighed up in proportion, join heating and stirring pot successively in order, heated and stirred makes it dissolve completely to 75 ~ 78 DEG C, and is kept temperature 75 DEG C;
(2) polyvinylpyrrolidone of C phase and deionized water are weighed up in proportion, join successively in order in vacuum high-shear homogenizer, being heated to 75 ~ 78 DEG C makes it dissolve completely, adds ferrum oxide and carries out high speed homogenization 3300 ~ 3400r/min, homogenizing 6 minutes; And being kept temperature 75 DEG C, this is aqueous phase;
(3) B is added to after A phase mixes, is heated rapidly to 75 DEG C and slowly joins immediately in aqueous phase, open high-shear homogenizer 3000 ~ 3100r/min, homogenizing 12 minutes simultaneously, and keep 75 DEG C;
(4) temperature of emulsion after emulsifying is well down to 60 DEG C, add D phase acrylate copolymer and keep temperature and carry out high speed homogenization 2000 ~ 2500r/min, homogenizing is after 5 minutes, add E heterophasic polypropylene amide (with) C13-C14 isoparaffin (with) after lauryl alcohol-7, low speed homogenizing 1500 ~ 2000r/min, homogenizing 15min opens vacuum machine simultaneously and carries out vacuum defoamation, opens attached stirring 20 ~ 30r/min and lowers the temperature, discharging after being cooled to 35 DEG C.
Embodiment 2: a kind of non-stimulated mascara
Formula is shown in Table 2 table 2
Embodiment 3: a kind of non-stimulated mascara
Formula is shown in Table 3.
Table 3
Described in embodiment 2,3, a kind of non-stimulated mascara is prepared by following steps:
(1) the alkyl glucosides glycoside of A phase, waxiness, antiseptic are weighed up in proportion, join heating and stirring pot successively in order, heated and stirred makes it dissolve completely to 75 ~ 78 DEG C, and is kept temperature 75 DEG C;
(2) polyvinylpyrrolidone of C phase and deionized water are weighed up in proportion, join successively in order in vacuum high-shear homogenizer, being heated to 75 ~ 78 DEG C makes it dissolve completely, adds ferrum oxide and carries out high speed homogenization 3300 ~ 3400r/min, homogenizing 6 minutes; And being kept temperature 75 DEG C, this is aqueous phase;
(3) B is added to after A phase mixes, is heated rapidly to 75 DEG C and slowly joins immediately in aqueous phase, open high-shear homogenizer 3000 ~ 3100r/min, homogenizing 12 minutes simultaneously, and keep 75 DEG C;
(4) temperature of emulsion after emulsifying is well down to 60 DEG C, add D phase acrylate copolymer and keep temperature and carry out high speed homogenization 2000 ~ 2500r/min, homogenizing is after 5 minutes, add E heterophasic polypropylene amide (with) C13-C14 isoparaffin (with) after lauryl alcohol-7, low speed homogenizing 1500 ~ 2000r/min, homogenizing 15min opens vacuum machine simultaneously and carries out vacuum defoamation, opens attached stirring 20 ~ 30r/min and lowers the temperature, discharging after being cooled to 35 DEG C.
The common mascara of comparative example 1
Formula is shown in Table 4.
Table 4
Its preparation method is as follows:
1, by A heat phase to 85 DEG C, all melt, stir;
2, by B heat phase to 85 DEG C, C is added to B phase, stirs, three rollers grind three times, mix homogeneously, recovery temperature to 85 DEG C;
3, B, C mixed phase is slowly joined A phase 85 DEG C time, and homogenizing 5 minutes;
4, D to be added in the emulsion of ABC homogenizing 3 minutes, and to be incubated 30 minutes, then cool to DEG C 45;
5, add E phase, and stir, discharging.
Experimental example 1 skin irritation test
With 60 women for object, getting 0.03ml sample with syringe is placed in the coyote hole of speckle examination adhesive tape, longitudinally be affixed on the normal skin of left forearm by the speckle examination adhesive tape being equipped with sample from bottom immediately, light pressing room, to drive away air, and makes trier be uniformly distributed one by one simultaneously.Labelling is carried out, to observe in test position.Pasted skin once every 24 hours, open half an hour after paster, then check according to the term of CTFA guide (1981).Carrying out 6 patch experiments altogether, the 6th day after subsides skin terminates, in order to observe late response, having carried out additional inspection.Data then utilize last check result, compare.Identify with table 5 as standard is carried out.Substances is respectively the non-stimulated mascara of embodiment 1 and the common mascara of comparative example, and result is as shown in table 6.
Table 5 standard of perfection
| Grade | Symbol | Standard of perfection |
| 0 | - | Negative reaction: non-stimulated, without erythema |
| 1 | ± | Suspicious reaction: slight erythema |
| 2 | + | Weak positive reaction: erythema |
| 3 | ++ | Strong positive reaction: erythema, pimple, vesicle |
| 4 | +++ | Extremely strong positive reaction: serious edema, bulla |
The irritant test result of the non-stimulated mascara of table 6 and common mascara
| Lagging number of times. | Comparative example 1 | Blank experiment | Embodiment 1 |
| 1 | 0 | 0 | 0 |
| 2 | 0 | 0 | 0 |
| 3 | 1 time ± | 0 | 0 |
| 4 | 1 time ± | 0 | 0 |
| 5 | 1 time ± | 0 | 0 |
| 6 | 1 time ± | 0 | 0 |
| Terminate latter 6th day | 1 time ± | 0 | 0 |
| Add up to | 5 times ± | 0 | 0 |
By this result of the test, can recognize that blank experiment is non-stimulated, the non-stimulated mascara of embodiment 1 is non-stimulated to skin, and the irritant reaction of common mascara to skin of comparative example still exists.Thus use after non-stimulated mascara to human body without any allergy and discomfort, the present invention is relatively general, and mascara product has safe and non-stimulating feature.
Claims (1)
1. a non-stimulated mascara, it is characterized in that being made up of according to certain mass percent following component: alkyl glucosides glycoside emulsifying agent 4.0%-8.0%, waxiness 8.0%-18.0%, oils and fats 3.0%-8.0%, film former 5.0%-18.0%, coloring agent 8.0%-20.0%, thickening agent 0.5%-2.0%, antiseptic 0.3%-0.5%, deionized water 5%-65%, all components mass percent sum is 100%; Described alkyl androstanediol emulsifying agent is following two kinds: decyl glucoside 2.0%-4.0% and lauryl glucoside 2.0%-4.0%; Described waxiness is following three kinds: Apis cerana Fabricius 5%-10% and candelilla wax 3%-6% and spermol 1.0%-2.0%; Described oils and fats is following three kinds: Cyclomethicone 2-5% and tocopherol acetas 0.5-1% and polydimethylsiloxane 0.5%-2%; Described film former is following two kinds: polyvinylpyrrolidone 2.0%-10.0% and acrylate copolymer 3%-8%; Described coloring agent is ferrum oxide 8%-20%; Described thickening agent be polyacrylamide (with) C13-C14 isoparaffin (with) lauryl alcohol-7 0.5%-2%.
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| CN109662914B (en) * | 2019-02-18 | 2021-11-26 | 广州卡迪莲化妆品科技有限公司 | Soap-based wax-free mascara and preparation method thereof |
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Address after: 510663 No. 15, Colin Road, Guangzhou Science City, Guangzhou high tech Industrial Development Zone, Guangdong Province Patentee after: Guangzhou Huanya cosmetics technology Co.,Ltd. Address before: 510663 No.15, Kelin Road, Guangzhou Science City, Guangzhou high tech Industrial Development Zone, Guangdong Province Patentee before: GUANGZHOU HUANYA COSMETICS TECHNOLOGY Co.,Ltd. |
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Application publication date: 20140108 Assignee: Guangzhou nabion Biotechnology Co.,Ltd. Assignor: Guangzhou Huanya cosmetics technology Co.,Ltd. Contract record no.: X2022980010117 Denomination of invention: A non irritating eye black and its preparation method Granted publication date: 20150325 License type: Common License Record date: 20220712 |
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