CN112090387B - Fluid loss agent raw materials polymerization reaction unit - Google Patents
Fluid loss agent raw materials polymerization reaction unit Download PDFInfo
- Publication number
- CN112090387B CN112090387B CN202011151581.0A CN202011151581A CN112090387B CN 112090387 B CN112090387 B CN 112090387B CN 202011151581 A CN202011151581 A CN 202011151581A CN 112090387 B CN112090387 B CN 112090387B
- Authority
- CN
- China
- Prior art keywords
- polymerization reaction
- reaction kettle
- shaft
- rotating
- stirring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000006116 polymerization reaction Methods 0.000 title claims abstract description 93
- 239000002994 raw material Substances 0.000 title claims abstract description 29
- 238000003756 stirring Methods 0.000 claims abstract description 65
- 238000004140 cleaning Methods 0.000 claims abstract description 35
- 239000007921 spray Substances 0.000 claims abstract description 31
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 31
- 239000007788 liquid Substances 0.000 claims description 26
- 235000014676 Phragmites communis Nutrition 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 8
- 239000010865 sewage Substances 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- 238000001802 infusion Methods 0.000 claims description 4
- 230000000379 polymerizing effect Effects 0.000 claims description 4
- 238000007599 discharging Methods 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 abstract description 12
- 238000007790 scraping Methods 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 5
- 238000005299 abrasion Methods 0.000 abstract description 3
- 239000000463 material Substances 0.000 description 5
- 238000005507 spraying Methods 0.000 description 5
- 239000000654 additive Substances 0.000 description 2
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000011368 organic material Substances 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 229920003169 water-soluble polymer Polymers 0.000 description 2
- 239000004908 Emulsion polymer Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 229910001870 ammonium persulfate Inorganic materials 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 230000005465 channeling Effects 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000003999 initiator Substances 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 239000004816 latex Substances 0.000 description 1
- 229920000126 latex Polymers 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 239000003129 oil well Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 229920001059 synthetic polymer Polymers 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/093—Cleaning containers, e.g. tanks by the force of jets or sprays
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/30—Filling of barrels or casks
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Polymerisation Methods In General (AREA)
- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
Abstract
The invention discloses a fluid loss agent raw material polymerization reaction device which comprises a polymerization reaction kettle and a group of support frames fixedly arranged at the bottom of the polymerization reaction kettle, wherein the polymerization reaction kettle is respectively provided with a stirring mechanism and a cleaning mechanism, and one side of the polymerization reaction kettle is provided with a filling mechanism. The invention has the advantages that the stirring mechanism positioned in the polymerization reaction kettle can stir the raw materials of the fluid loss agent in the polymerization reaction kettle, a group of stirring shafts rotate around the rotating shaft and simultaneously rotate, so that the polymerization reaction effect of the raw materials of the fluid loss agent is effectively improved, the cleaning scraping plate is in linear contact with the inner wall of the polymerization reaction kettle in the stirring state, the abrasion of the cleaning scraping plate on the inner wall of the polymerization reaction kettle is reduced, the cleaning mechanism can automatically clean the adhered polymer on the inner wall of the polymerization reaction kettle, in the cleaning state, a group of stirring shafts rotate around the rotating shaft and simultaneously spray and clean in cooperation with the spray head, and the filling mechanism can automatically weigh and fill the polymer after the polymerization reaction, so that the invention is convenient to use.
Description
Technical Field
The invention relates to the field of fluid loss additives, in particular to a fluid loss additive raw material polymerization reaction device.
Background
The fluid loss agent product can be divided into a granular material, a water-soluble polymer and an organic material. Among the granular materials, latex becomes a research hot spot at home and abroad by virtue of the advantages of good filtration loss reduction, gas channeling prevention, toughness enhancement and the like. At present, most of the fluid loss agent products are water-soluble polymers and organic materials, and the products can be divided into modified natural products and synthetic polymers. In addition, many studies have been made on environmental protection type fluid loss agents abroad.
The method comprises the steps of transferring emulsified raw materials in an emulsifying kettle into a reaction kettle, starting stirring, heating the materials to 60-65 ℃, adding an initiator solution prepared from 0.2kg of ammonium persulfate and 10kg of distilled water, regulating the rotation speed of a stirring motor to be 300r/min for stirring and initiating, increasing the speed of the stirring motor to 1200+/-2 r/min when the temperature of the materials is raised to 70 ℃, controlling the temperature of the materials to be below 100 ℃, and regulating the rotation speed of the stirring motor to be 600r/min when the temperature of the materials is lowered to 70 ℃, so that the materials are kept at a constant temperature of 80 ℃ for continuous reaction for 1h, thus obtaining the oil well cement emulsion polymer fluid loss agent product. The existing polymerization reaction equipment for the raw materials of the fluid loss agent is used for stirring the raw materials of the fluid loss agent, the stirring of the raw materials is uneven, the polymerization reaction effect is affected, and the cooled polymer is easy to adhere to the inner wall of the polymerization reaction kettle, so that the wall built-up phenomenon occurs, the polymer is not discharged cleanly, the cleaning is labor-consuming, and the automatic filling function is not provided.
Disclosure of Invention
The invention provides a device for polymerizing the raw materials of the fluid loss agent to solve the problem of the polymerization of the raw materials of the fluid loss agent.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
the device comprises a polymerization reaction kettle and a group of support frames fixedly arranged at the bottom of the polymerization reaction kettle, wherein a stirring mechanism and a cleaning mechanism are respectively arranged in the polymerization reaction kettle, and a filling mechanism is arranged at one side of the polymerization reaction kettle;
the stirring mechanism comprises a rotating motor, a first driving gear, a rotating shaft, a first driven gear, a movable shaft sleeve, a connecting rod, a rotating handle, a ratchet wheel, a brake pawl, a reed, a second driving gear, a third driving gear, a group of opposite fixed rods, a fixed shaft sleeve, a stirring shaft, a second driven gear, a third driven gear, stirring paddles and a discharge port, wherein the rotating motor is arranged on one side of the upper end of the polymerization reaction kettle, the rotating end is vertically upwards, the first driving gear is arranged on the rotating end of the rotating motor, the rotating shaft is vertically inserted in the polymerization reaction kettle and is hollow, the upper end of the driving gear extends out of the polymerization reaction kettle, the first driven gear is arranged at the upper end of the rotating shaft and is meshed with the first driving gear, the movable shaft sleeve is movably sleeved on the rotating shaft, the connecting rod is arranged at the upper front end of the movable shaft sleeve, the rotating handle is arranged at the front end of the connecting rod and is positioned on the outer surface of the polymerization reaction kettle, the brake pawl is arranged on the rotating handle, the brake pawl is arranged on the front surface of the polymerization reaction kettle and is positioned above the ratchet wheel, the second driving gear is arranged on one side of the brake pawl, the movable shaft sleeve is arranged on the movable shaft sleeve, the third driven shaft is arranged at the bottom of the fixed shaft sleeve, the movable shaft is arranged at the bottom of the fixed shaft sleeve, the hollow shaft is arranged at the bottom of the fixed shaft, the stirring shaft is arranged at the bottom of the fixed shaft is arranged at the front end of the stirring shaft, and is meshed with the movable shaft is arranged at the front side;
the cleaning mechanism comprises a water inlet pipeline, a water storage cavity, two groups of opposite rotary spray nozzles, a group of opposite spray pipelines, a plurality of spray heads, a limiting groove, a sliding plate, a limiting plate, a cleaning scraping plate and a sewage outlet, wherein the water inlet pipeline is fixedly inserted into the rotating shaft;
the filling mechanism comprises a liquid outlet pipeline, a liquid pump, a filling base, a mounting plate, a sliding rod, a filling gun, a roller conveying frame, an inner cavity, a stepping motor, a driving shaft, a set of opposite external threads, a set of opposite first screw threads, a clamping plate, a weighing sensor, a driving bevel gear, a screw rod, a driven bevel gear and a second screw thread, wherein the liquid outlet pipeline is inserted into a discharging hole, the liquid pump is mounted on the liquid outlet pipeline, the filling base is positioned on one side of a polymerization reaction kettle, the mounting plate is vertically mounted at the upper rear end of the filling base, the rear end of the sliding rod is slidably mounted on the mounting plate, the filling gun is mounted at the front end of the sliding rod, the roller conveying frame is mounted on the filling base, the inner cavity is opened in the filling base, the stepping motor is mounted at the front end of the filling base, the rotating end is inserted into the inner cavity, the driving shaft is mounted on the rotating end of the stepping motor, the rear end extends out of the inner cavity, the set of opposite external threads are respectively arranged on two sides of the outer surface of the driving shaft, the set of the opposite first screw threads are respectively sleeved on one set of opposite first external threads, the driving bevel gear is mounted on the driving bevel gear and the driving screw threads are fixedly mounted at the two sides of the driving screw threads, the driving screw rod and the driving screw is fixedly mounted at the front end.
Further, a heat conduction oil heating layer is arranged outside the polymerization reaction kettle.
Further, the back end of the reed is connected with a pulling handle.
Further, the water inlet pipeline is communicated with an external water pipe.
Further, the upper ends of the group of opposite spray pipelines are movably connected with the water inlet pipeline through rotary joints.
Further, a spring is arranged in the limiting groove, and the front end of the spring is connected with the limiting plate.
Further, a first sliding groove is formed in the upper end of the mounting plate, and the rear end of the sliding rod is slidably mounted on the first sliding groove through a sliding block.
Further, an infusion hose is connected between the liquid outlet pipeline and the filling gun.
Further, a second sliding groove is formed in the bottom of the inner cavity, and the bottom of the first nut is slidably arranged on the second sliding groove through a sliding block.
Further, a group of strip-shaped holes corresponding to the clamping plates are formed in the filling base.
The invention provides a polymerization reaction device for a fluid loss agent raw material, which has the advantages that the fluid loss agent raw material in a polymerization reaction kettle can be stirred through a stirring mechanism positioned in the polymerization reaction kettle, a group of stirring shafts rotate around a rotating shaft and simultaneously rotate, so that the polymerization reaction effect of the fluid loss agent raw material is effectively improved, a cleaning scraper is in linear contact with the inner wall of the polymerization reaction kettle in a stirring state, the abrasion of the cleaning scraper on the inner wall of the polymerization reaction kettle is reduced, the cleaning mechanism can automatically clean adhered polymers on the inner wall of the polymerization reaction kettle, the stirring shafts rotate around the rotating shaft in a cleaning state and simultaneously spray-clean in cooperation with a spray head, and the filling mechanism can automatically weigh and fill the polymers after the polymerization reaction, so that the device is convenient to use.
Drawings
FIG. 1 is a schematic diagram of a polymerization reaction device for a fluid loss agent raw material.
Fig. 2 is a schematic view of the movable sleeve according to the present invention.
FIG. 3 is a schematic view showing a cleaning operation state of the polymerization reactor according to the present invention.
Fig. 4 is a schematic view of a rotating shaft according to the present invention.
Fig. 5 is an enlarged view of a portion of fig. 4 at a in accordance with the present invention.
FIG. 6 is a cross-sectional view of a stirring shaft according to the present invention.
Fig. 7 is an enlarged view of a portion of fig. 6 at B in accordance with the present invention.
Fig. 8 is a schematic view of two working states of the rotary handle according to the present invention.
Fig. 9 is a schematic diagram of two working states of the connecting rod according to the present invention.
Fig. 10 is a schematic view of the filling mechanism according to the present invention.
In the figure: 1. a polymerization reaction kettle; 2. a support frame; 3. a rotating electric machine; 4. a first driving gear; 5. a rotation shaft; 6. a driven gear I; 7. a movable shaft sleeve; 8. a connecting rod; 9. rotating the handle; 10. a ratchet wheel; 11. a brake pawl; 12. a reed; 13. a driving gear II; 14. a driving gear III; 15. a fixed rod; 16. fixing the shaft sleeve; 17. a stirring shaft; 18. a driven gear II; 19. driven gear III; 20. stirring paddles; 21. a discharge port; 22. a water inlet pipe; 23. a water storage chamber; 24. rotating the spray head; 25. a spray pipe; 26. a spray header; 27. a limit groove; 28. a sliding plate; 29. a limiting plate; 30. cleaning a scraping plate; 31. a sewage outlet; 32. a liquid outlet pipe; 33. a liquid pump; 34. filling a base; 35. a mounting plate; 36. a slide bar; 37. filling gun; 38. a roller carriage; 39. an inner cavity; 40. a stepping motor; 41. a drive shaft; 42. an external thread; 43. a first nut; 44. a clamping plate; 45. a weighing sensor; 46. a driving helical gear; 47. a screw rod; 48. driven helical gears; 49. a second nut; 50. a conduction oil heating layer; 51. pulling the handle; 52. a spring; 53. a first chute; 54. an infusion hose; 55. a second chute; 56. and a strip-shaped hole.
Detailed Description
The invention is described in detail below with reference to the accompanying drawings, as shown in fig. 1-10: the device comprises a polymerization reaction kettle 1 and a group of support frames 2 fixedly arranged at the bottom of the polymerization reaction kettle 1, wherein a stirring mechanism and a cleaning mechanism are respectively arranged in the polymerization reaction kettle 1, and a filling mechanism is arranged at one side of the polymerization reaction kettle 1;
the stirring mechanism comprises a rotating motor 3, a first driving gear 4, a rotating shaft 5, a first driven gear 6, a movable shaft sleeve 7, a connecting rod 8, a rotating handle 9, a ratchet wheel 10, a brake pawl 11, a reed 12, a second driving gear 13, a third driving gear 14, a group of opposite fixed rods 15, a fixed shaft sleeve 16, a stirring shaft 17, a second driven gear 18, a third driven gear 19, a stirring paddle 20 and a discharge hole 21, wherein the rotating motor 3 is arranged on one side of the upper end of the polymerization reaction kettle 1, the rotating end is vertically upwards, the first driving gear 4 is arranged on the rotating end of the rotating motor 3, the rotating shaft 5 is vertically inserted in the polymerization reaction kettle 1 and is hollow, the upper end extends out of the polymerization reaction kettle 1, the first driven gear 6 is arranged at the upper end of the rotating shaft 5 and is meshed with the first driving gear 4, the movable shaft sleeve 7 is movably sleeved on the rotating shaft 5, the connecting rod 8 is arranged at the front end of the movable shaft sleeve 7, the rotating handle 9 is arranged at the front end of the connecting rod 8 and is positioned on the outer surface of the polymerization reaction kettle 1, the ratchet wheel 10 is arranged on the rotating handle 9, the brake pawl 11 is arranged on the front surface of the polymerization reaction kettle 1 and is positioned above the ratchet wheel 10, the reed 12 is positioned at one side of the brake pawl 11, the driving gear II 13 is arranged on the movable shaft sleeve 7, the driving gear III 14 is arranged at the bottom of the movable shaft sleeve 7, a group of opposite fixed rods 15 are arranged at two sides of the rotating shaft 5, the fixed shaft sleeve 16 is arranged at the front end of the fixed rod 15, the stirring shaft 17 is movably inserted into the fixed shaft sleeve 16 and is hollow, the driven gear II 18 is arranged at the upper end of the stirring shaft 17, the driven gear III 19 is arranged on the fixed shaft sleeve 16, the stirring paddle 20 is arranged at the bottom of the rotating shaft 5, the discharge hole 21 is formed in the bottom of the polymerization reaction kettle 1;
the cleaning mechanism comprises a water inlet pipeline 22, a water storage cavity 23, two groups of opposite rotary spray heads 24, a group of opposite spray pipelines 25, a plurality of spray heads 26, a limiting groove 27, a sliding plate 28, a limiting plate 29, a cleaning scraper 30 and a drain outlet 31, wherein the water inlet pipeline 22 is fixedly inserted into the rotating shaft 5, the water storage cavity 23 is arranged in the rotating shaft 5, the two groups of opposite rotary spray heads 24 are respectively arranged on two sides of the water storage cavity 23, the group of opposite spray pipelines 25 are respectively inserted into the stirring shaft 17, the plurality of spray heads 26 are respectively arranged on the spray pipelines 25, the limiting groove 27 is arranged on one side of the stirring shaft 17, the sliding plate 28 is slidably arranged in the limiting groove 27, the limiting plate 29 is arranged at the rear end of the sliding plate 28, the cleaning scraper 30 is arranged at the front end of the sliding plate 28, and the drain outlet 31 is arranged on one side of the bottom of the polymerization reaction kettle 1;
the filling mechanism comprises a liquid outlet pipe 32, a liquid pump 33, a filling base 34, a mounting plate 35, a sliding rod 36, a filling gun 37, a roller conveying frame 38, an inner cavity 39, a stepping motor 40, a driving shaft 41, a set of opposite external threads 42, a set of opposite nuts one 43, a clamping plate 44, a weighing sensor 45, a driving bevel gear 46, a screw rod 47, a driven bevel gear 48 and two nuts 49, wherein the liquid outlet pipe 32 is inserted in the liquid outlet 21, the liquid pump 33 is mounted on the liquid outlet pipe 32, the filling base 34 is positioned on one side of the polymerization reaction kettle 1, the mounting plate 35 is vertically mounted on the rear end of the filling base 34, the rear end of the sliding rod 36 is slidably mounted on the mounting plate 35, the filling gun 37 is mounted on the front end of the sliding rod 36, the roller conveying frame 38 is mounted on the filling base 34, the inner cavity 39 is opened in the filling base 34, the stepping motor 40 is mounted on the front end of the filling base 34, the rotating end is inserted in the inner cavity 39, the driving shaft 41 is mounted on the rotating end of the stepping motor 40, the driving bevel gear 40 is mounted on the rear end of the screw rod 47, the opposite to the screw rod one side of the screw rod 45 is mounted on the screw rod one side of the driving bevel gear 46, the opposite to the screw rod 45 is mounted on the two sides of the screw rod 47, the threaded end of the threaded rod one side of the driving bevel gear 45 is mounted on the opposite to the screw rod 46, the threaded end is mounted on the threaded end of the threaded rod one side of the driving motor 46 is mounted on the screw rod 45 and the threaded end is meshed with the threaded end of the threaded rod one side of the threaded rod 43 is mounted on the outer side of the threaded 4.
The outside of the polymerization reaction kettle 1 is provided with a heat conduction oil heating layer 50.
The back end of the reed 12 is connected with a pulling handle 51.
The water intake pipe 22 communicates with an external water pipe.
The upper ends of a group of opposite spray pipes 25 are movably connected with the water inlet pipe 22 through rotary joints.
A spring 52 is arranged in the limiting groove 27, and the front end of the spring 52 is connected with the limiting plate 29.
The upper end of the mounting plate 35 is provided with a first chute 53, and the rear end of the sliding rod 36 is slidably arranged on the first chute 53 through a sliding block.
An infusion hose 54 is connected between the outlet pipe 32 and the filling gun 37.
The bottom of the inner cavity 39 is provided with a second chute 55, and the bottom of the first screw 43 is slidably arranged on the second chute 55 through a sliding block.
The filling base 34 is provided with a set of strip-shaped holes 56 corresponding to the clamping plates 44.
The working principle of the embodiment is as follows: the electric equipment used by the device is controlled by an external controller, a heat conduction oil heating layer 50 is arranged outside the polymerization reaction kettle 1, the heat conduction oil heating layer 50 is used for heating the raw materials of the fluid loss agent put into the polymerization reaction kettle 1, a feed inlet is arranged at the upper end of the polymerization reaction kettle 1, and when the device is used, a user sequentially puts the raw materials of the fluid loss agent into the polymerization reaction kettle 1 through the feed inlet;
stirring: the movable shaft sleeve 7 is movably sleeved on the rotating shaft 5, the connecting rod 8 is arranged at the front end of the movable shaft sleeve 7, the rotating handle 9 is arranged at the front end of the connecting rod 8 and is positioned on the outer surface of the polymerization reaction kettle 1, the ratchet wheel 10 is arranged on the rotating handle 9, the brake pawl 11 is arranged on the front surface of the polymerization reaction kettle 1 and is positioned above the ratchet wheel 10, the reed 12 is positioned on one side of the brake pawl 11, a user can adjust the position of the movable shaft sleeve 7 through the rotating handle 9, the driving gear II 13 is arranged on the movable shaft sleeve 7, the driving gear III 14 is arranged at the bottom of the movable shaft sleeve 7, the initial position of the movable shaft sleeve 7 is positioned at the upper end of the rotating shaft 5, as shown in figure 1, at the moment, the driving gear II 13 is meshed with the driven gear II 18, the rotating motor 3 starts to work firstly, the driving gear I4 on the rotating end is driven to start rotating, the rotating shaft 5 is movably inserted in the polymerization reaction kettle 1 through the fastening bearing, the inside of the stirring shaft is hollow, the upper end of the stirring shaft is extended out of the polymerization reaction kettle 1, the driven gear I6 is arranged at the upper end of the rotating shaft 5 and meshed with the driving gear I4, the rotating motor 3 drives the rotating shaft 5 to start rotating, a group of opposite fixed rods 15 are arranged at two sides of the rotating shaft 5, a fixed shaft sleeve 16 is arranged at the front end of the fixed rod 15, a stirring shaft 17 is movably inserted in the fixed shaft sleeve 16 and is hollow, the rotating shaft 5 drives a group of stirring shafts 17 to start rotating, the driven gear II 18 is arranged at the upper end of the stirring shaft 17, the driving gear II 13 is meshed with the driven gear II 18 in a stirring state, the stirring shaft 17 rotates around the rotating shaft 5 and simultaneously rotates, the raw materials of the fluid loss agent in the polymerization reaction kettle 1 are effectively stirred, the polymerization reaction effect of the raw materials of the fluid loss agent is improved, the stirring paddle 20 is arranged at the bottom of the rotating shaft 5, the stirring paddles 20 can stir the raw materials of the fluid loss agent at the bottom in the polymerization reaction kettle 1, the raw materials of the fluid loss agent in the polymerization reaction kettle 1 can be stirred through the stirring mechanism in the polymerization reaction kettle 1, a group of stirring shafts 17 rotate around the rotating shaft 5 and simultaneously rotate, so that the polymerization reaction effect of the raw materials of the fluid loss agent is effectively improved, the cleaning scraping plate 30 is in linear contact with the inner wall of the polymerization reaction kettle 1 in a stirring state, and the abrasion of the cleaning scraping plate 30 to the inner wall of the polymerization reaction kettle 1 is reduced;
the cleaning process comprises the following steps: a user firstly adjusts the movable shaft sleeve 7 to the lower part of the rotating shaft 5 through rotating the handle 9, as shown in fig. 3, at the moment, the driving gear III 14 and the driven gear III 19 are meshed with each other, during cleaning, the rotating motor 3 firstly starts to work to drive the rotating shaft 5 to rotate, at the moment, a group of stirring shafts 17 only rotate around the rotating shaft 5, a limit groove 27 is formed on one side of the stirring shafts 17, a sliding plate 28 is slidably arranged in the limit groove 27, a limit plate 29 is arranged at the rear end of the sliding plate 28, a cleaning scraper 30 is arranged at the front end of the sliding plate 28, a spring 52 is arranged in the limit groove 27, the front end of the spring 52 is connected with the limit plate 29, the spring 52 can enable the cleaning scraper 30 to be closely attached to the inner wall of the polymerization reaction kettle 1, a group of cleaning scrapers 30 are alternately arranged, the stirring shafts 17 can drive the cleaning scraper 30 to clean polymers adhered to the inner wall of the polymerization reaction kettle 1, the water inlet pipe 22 is fixedly inserted in the rotating shaft 5 through a fastening bearing, the water inlet pipe 22 is communicated with an external water pipe, the water storage cavity 23 is formed in the rotating shaft 5, two groups of opposite rotating spray heads 24 are respectively arranged at two sides of the water storage cavity 23, the rotating shaft 5 drives the two groups of opposite rotating spray heads 24 to rotate up and down while rotating, the inner wall at the upper end of the polymerization reaction kettle 1 is sprayed and cleaned, one group of opposite spraying pipelines 25 are respectively inserted in the stirring shaft 17, the upper end of the spraying pipelines are movably connected with the water inlet pipe 22 through a rotating joint, the stirring shaft 17 is convenient to rotate during stirring, a plurality of spraying heads 26 are respectively arranged on the spraying pipelines 25, the spraying heads 26 can spray and clean the inner wall at the bottom of the polymerization reaction kettle 1, the cleaned sewage can be discharged through a sewage outlet 31, and the cleaning mechanism can automatically clean adhered polymers on the inner wall of the polymerization reaction kettle 1 in a cleaning state, the stirring shafts 17 rotate around the rotating shaft 5 and are matched with the spray heads to carry out spray cleaning, so that the manual cleaning labor force is reduced;
when filling, the following steps are carried out: after the polymerization reaction of the fluid loss agent raw materials in the polymerization reaction kettle 1 is completed, the fluid loss agent raw materials are discharged through the discharge hole 21, the liquid outlet pipeline 32 is inserted into the discharge hole 21, the liquid pump 33 is arranged on the liquid outlet pipeline 32, the liquid pump 33 can pump the reacted polymer into the liquid outlet pipeline 32, the roller conveying frame 38 is arranged on the filling base 34, a user places a ton barrel to be filled at the upper end of the roller conveying frame 38, the position of the feeding hole of the ton barrel is opposite to the position of the filling gun 37 at the upper end, when in filling, the stepping motor 40 starts to work, the rotating end of the stepping motor 40 is movably inserted into the inner cavity 39 of the filling base 34 through a fastening bearing, the driving shaft 41 is arranged on the rotating end of the stepping motor 40, the rear end extends out of the inner cavity 39, the stepping motor 40 drives the driving shaft 41 on the rotating end to start to rotate, a group of opposite external threads 42 are respectively arranged on two sides of the outer surface of the driving shaft 41, the clamping plate 44 is arranged at the upper end of the first screw 43, the bottom of the inner cavity 39 is provided with a second chute 55, the bottom of the first screw 43 is slidably arranged on the second chute 55 through a sliding block, the filling base 34 is provided with a group of strip-shaped holes 56 corresponding to the clamping plate 44, the stepping motor 40 rotates positively to drive the clamping plate 44 to clamp and fix the ton barrel on the roller conveying frame 38, the phenomenon of position deviation is prevented when the ton barrel is filled, the driving helical gear 46 is arranged at the rear end of the driving shaft 41, the bottom of the screw 47 is movably arranged on the filling base 34 through a fastening bearing and positioned at one side of the mounting plate 35, the driven helical gear 48 is arranged at the bottom of the screw 47 and is meshed with the driving helical gear 46, the second screw 49 is arranged at the upper end of the screw 47 and fixedly connected with the sliding rod 36, the rear end of the sliding rod 36 is slidably arranged on the mounting plate 35, the filling gun 37 is installed at the front end of the sliding rod 36, the liquid outlet pipe 32 and the filling gun 37 are connected with the transfusion hose 54, the clamping plate 44 clamps the ton barrel on the roller conveying frame 38, meanwhile, the sliding rod 36 drives the front-end filling gun 37 to move downwards and enter the ton barrel feeding hole to fill, the weighing sensor 45 is installed at the top of the inner cavity 39, the display is installed on one side of the filling base 34 and used for displaying the weight of polymer in the ton barrel, after filling, the stepping motor 40 reverses and drives the clamping plate 44 to loosen the ton barrel on the roller conveying frame 38, meanwhile, the filling gun 37 moves upwards and breaks away from the ton barrel, a user can transport the ton barrel on the roller conveying frame 38, and the filling mechanism can automatically weigh and fill the polymer after polymerization, so that the polymer is convenient to use.
The above technical solution only represents the preferred technical solution of the present invention, and some changes that may be made by those skilled in the art to some parts of the technical solution represent the principles of the present invention, and the technical solution falls within the scope of the present invention.
Claims (6)
1. The device comprises a polymerization reaction kettle (1) and a group of support frames (2) fixedly arranged at the bottom of the polymerization reaction kettle (1), and is characterized in that a stirring mechanism and a cleaning mechanism are respectively arranged in the polymerization reaction kettle (1), and a filling mechanism is arranged at one side of the polymerization reaction kettle (1);
the stirring mechanism comprises a rotating motor (3), a first driving gear (4), a rotating shaft (5), a first driven gear (6), a movable shaft sleeve (7), a connecting rod (8), a rotating handle (9), a ratchet wheel (10), a brake pawl (11), a reed (12), a second driving gear (13), a third driving gear (14), a group of opposite fixed rods (15), a fixed shaft sleeve (16), a stirring shaft (17), a second driven gear (18), a third driven gear (19), a stirring paddle (20) and a discharge hole (21), wherein the rotating motor (3) is arranged on one side of the upper end of the polymerization reaction kettle (1), the rotating end is vertically upwards, the first driving gear (4) is arranged on the rotating end of the rotating motor (3), the rotating shaft (5) is vertically inserted in the polymerization reaction kettle (1) and is hollow, the upper end extends out of the polymerization reaction kettle (1), the first driven gear (6) is arranged at the upper end of the rotating shaft (5) and is meshed with the first driving gear (4), the movable shaft sleeve (7) is movably arranged on the rotating shaft (5), the connecting rod (8) is sleeved on the front end of the connecting rod (8) and is arranged on the outer surface of the polymerization reaction kettle (9), the ratchet wheel (10) is arranged on the rotating handle (9), the brake pawl (11) is arranged on the front surface of the polymerization reaction kettle (1) and is positioned above the ratchet wheel (10), the reed (12) is positioned on one side of the brake pawl (11), the driving gear II (13) is arranged on the movable shaft sleeve (7), the driving gear III (14) is arranged at the bottom of the movable shaft sleeve (7), a group of opposite fixed rods (15) are arranged on two sides of the rotating shaft (5), the fixed shaft sleeve (16) is arranged at the front end of the fixed rod (15), the stirring shaft (17) is movably inserted in the fixed shaft sleeve (16) and is hollow, the driven gear II (18) is arranged at the upper end of the stirring shaft (17), the driven gear III (19) is arranged on the fixed shaft sleeve (16), the stirring paddle (20) is arranged at the bottom of the rotating shaft (5), and the discharging port (21) is arranged at the bottom of the polymerization reaction kettle (1);
the cleaning mechanism comprises a water inlet pipeline (22), a water storage cavity (23), two groups of opposite rotary spray heads (24), a group of opposite spray pipelines (25), a plurality of spray heads (26), a limiting groove (27), a sliding plate (28), a limiting plate (29), a cleaning scraper (30) and a sewage draining outlet (31), wherein the water inlet pipeline (22) is fixedly inserted into the rotary shaft (5), the water storage cavity (23) is arranged in the rotary shaft (5), the two groups of opposite rotary spray heads (24) are respectively arranged at two sides of the water storage cavity (23), the group of opposite spray pipelines (25) are respectively inserted into a stirring shaft (17), the spray heads (26) are respectively arranged on the spray pipelines (25), the limiting groove (27) is arranged at one side of the stirring shaft (17), the sliding plate (28) is slidably arranged in the limiting groove (27), the limiting plate (29) is arranged at the rear end of the sliding plate (28), the cleaning scraper (30) is arranged at the front end of the sliding plate (28), and the sewage draining outlet (31) is arranged at one side of the bottom of the polymerization kettle (1);
the filling mechanism comprises a liquid outlet pipe (32), a liquid pump (33), a filling base (34), a mounting plate (35), a sliding rod (36), a filling gun (37), a roller conveying frame (38), an inner cavity (39), a stepping motor (40), a driving shaft (41), a group of opposite external threads (42), a group of opposite nuts (43), a clamping plate (44), a weighing sensor (45), a driving bevel gear (46), a screw rod (47), a driven bevel gear (48) and two nuts (49), the liquid outlet pipe (32) is inserted in a discharge hole (21), the liquid pump (33) is mounted on the liquid outlet pipe (32), the filling base (34) is positioned on one side of the polymerization reaction kettle (1), the mounting plate (35) is vertically mounted at the rear end of the filling base (34), the rear end of the sliding rod (36) is slidably mounted on the mounting plate (35), the filling gun (37) is mounted at the front end of the sliding rod (36), the roller conveying frame (38) is mounted on the inner cavity (34) and the inner cavity (34) is mounted at the front end of the stepping motor (39), the driving shaft (41) is arranged on the rotating end of the stepping motor (40), the rear end of the driving shaft extends out of the inner cavity (39), a group of opposite external threads (42) are respectively tapped on two sides of the outer surface of the driving shaft (41), a group of opposite screw nuts (43) are respectively sleeved on the group of opposite external threads (42), the clamping plate (44) is arranged at the upper end of the screw nut (43), the weighing sensor (45) is arranged at the top of the inner cavity (39), the driving bevel gear (46) is arranged at the rear end of the driving shaft (41), the screw rod (47) is movably arranged on the filling base (34) and is positioned on one side of the mounting plate (35), the driven bevel gear (48) is arranged at the bottom of the screw rod (47) and is meshed with the driving bevel gear (46), and the screw nut (49) is arranged at the upper end of the screw rod (47) and is fixedly connected with the sliding rod (36);
a heat conducting oil heating layer (50) is arranged outside the polymerization reaction kettle (1);
the rear end of the reed (12) is connected with a pulling handle (51);
the water inlet pipeline (22) is communicated with an external water pipe;
the upper ends of the group of opposite spray pipelines (25) are movably connected with the water inlet pipeline (22) through rotary joints.
2. The device for polymerizing the fluid loss agent raw materials according to claim 1, wherein a spring (52) is installed in the limiting groove (27), and the front end of the spring (52) is connected with the limiting plate (29).
3. The device for polymerizing the raw materials of the fluid loss agent according to claim 1, wherein a first chute (53) is arranged at the upper end of the mounting plate (35), and the rear end of the sliding rod (36) is slidably arranged on the first chute (53) through a sliding block.
4. The fluid loss agent raw material polymerization reaction device according to claim 1, wherein an infusion hose (54) is connected between the liquid outlet pipe (32) and the filling gun (37).
5. The device for polymerizing the raw materials of the fluid loss agent according to claim 1, wherein a second chute (55) is arranged at the bottom of the inner cavity (39), and the bottom of the first screw (43) is slidably arranged on the second chute (55) through a sliding block.
6. A fluid loss agent feed polymerization apparatus according to claim 1, wherein the filling base (34) is provided with a plurality of strip-shaped holes (56) corresponding to the clamping plates (44).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011151581.0A CN112090387B (en) | 2020-10-26 | 2020-10-26 | Fluid loss agent raw materials polymerization reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011151581.0A CN112090387B (en) | 2020-10-26 | 2020-10-26 | Fluid loss agent raw materials polymerization reaction unit |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN112090387A CN112090387A (en) | 2020-12-18 |
| CN112090387B true CN112090387B (en) | 2023-11-28 |
Family
ID=73785513
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011151581.0A Active CN112090387B (en) | 2020-10-26 | 2020-10-26 | Fluid loss agent raw materials polymerization reaction unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112090387B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114053980A (en) * | 2021-12-01 | 2022-02-18 | 安徽金邦医药化工有限公司 | A reation kettle for production of tert-butyl alcohol sodium |
| CN115069122B (en) * | 2022-07-06 | 2023-12-05 | 珠海市中浆纳米材料科技有限公司 | Liquid material dispersing mechanism and paint preparation system provided with same |
Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101239290A (en) * | 2007-11-19 | 2008-08-13 | 深圳和而泰智能控制股份有限公司 | Stirrer |
| JP2009136730A (en) * | 2007-12-04 | 2009-06-25 | Sumitomo Heavy Industries Environment Co Ltd | Vertical axis type stirring device |
| CN103583125A (en) * | 2013-11-29 | 2014-02-19 | 东北农业大学 | Gear-driven pot seedling transplantation longitudinal seedling feeding mechanism |
| CN105752793A (en) * | 2016-05-11 | 2016-07-13 | 汪加军 | Anti-falling device of elevator |
| CN206715900U (en) * | 2017-04-18 | 2017-12-08 | 上海蓝木化工有限公司 | Chemical Manufacture reactor washing and brushing device |
| CN208115585U (en) * | 2018-01-12 | 2018-11-20 | 东莞市润天化工有限公司 | A kind of mixing plant of hardware baking vanish |
| CN209049385U (en) * | 2018-10-30 | 2019-07-02 | 广东衡光新材料科技有限公司 | Stainless steel cauldron is used in industrial adhesive production |
| CN111440907A (en) * | 2020-04-10 | 2020-07-24 | 湖州瑞博鞋业有限公司 | Leather shoe leather dyeing device based on planetary gear transmission principle |
| CN111450785A (en) * | 2019-01-22 | 2020-07-28 | 甘肃施可丰生态科技有限公司 | Compound fertilizer raw material reaction barrel |
| CN112957951A (en) * | 2021-02-05 | 2021-06-15 | 青岛市中医医院(青岛市海慈医院、青岛市康复医学研究所) | Traditional Chinese medicine raw material mixing and stirring equipment and method |
| CN213726469U (en) * | 2020-10-26 | 2021-07-20 | 河北峰林永茂化工科技有限公司 | Polymerization reaction device for water loss reducing agent raw materials |
| CN214715979U (en) * | 2021-04-08 | 2021-11-16 | 河北恒创环保科技有限公司 | Electroplating effluent pretreatment flocculation agitating unit |
-
2020
- 2020-10-26 CN CN202011151581.0A patent/CN112090387B/en active Active
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101239290A (en) * | 2007-11-19 | 2008-08-13 | 深圳和而泰智能控制股份有限公司 | Stirrer |
| JP2009136730A (en) * | 2007-12-04 | 2009-06-25 | Sumitomo Heavy Industries Environment Co Ltd | Vertical axis type stirring device |
| CN103583125A (en) * | 2013-11-29 | 2014-02-19 | 东北农业大学 | Gear-driven pot seedling transplantation longitudinal seedling feeding mechanism |
| CN105752793A (en) * | 2016-05-11 | 2016-07-13 | 汪加军 | Anti-falling device of elevator |
| CN206715900U (en) * | 2017-04-18 | 2017-12-08 | 上海蓝木化工有限公司 | Chemical Manufacture reactor washing and brushing device |
| CN208115585U (en) * | 2018-01-12 | 2018-11-20 | 东莞市润天化工有限公司 | A kind of mixing plant of hardware baking vanish |
| CN209049385U (en) * | 2018-10-30 | 2019-07-02 | 广东衡光新材料科技有限公司 | Stainless steel cauldron is used in industrial adhesive production |
| CN111450785A (en) * | 2019-01-22 | 2020-07-28 | 甘肃施可丰生态科技有限公司 | Compound fertilizer raw material reaction barrel |
| CN111440907A (en) * | 2020-04-10 | 2020-07-24 | 湖州瑞博鞋业有限公司 | Leather shoe leather dyeing device based on planetary gear transmission principle |
| CN213726469U (en) * | 2020-10-26 | 2021-07-20 | 河北峰林永茂化工科技有限公司 | Polymerization reaction device for water loss reducing agent raw materials |
| CN112957951A (en) * | 2021-02-05 | 2021-06-15 | 青岛市中医医院(青岛市海慈医院、青岛市康复医学研究所) | Traditional Chinese medicine raw material mixing and stirring equipment and method |
| CN214715979U (en) * | 2021-04-08 | 2021-11-16 | 河北恒创环保科技有限公司 | Electroplating effluent pretreatment flocculation agitating unit |
Also Published As
| Publication number | Publication date |
|---|---|
| CN112090387A (en) | 2020-12-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN112090387B (en) | Fluid loss agent raw materials polymerization reaction unit | |
| CN100420547C (en) | Multiple steel tube and reinforcing steel bar delivery and derusting device | |
| CN113458107B (en) | Automatic movable cleaning equipment for chemical storage tanks | |
| CN213726469U (en) | Polymerization reaction device for water loss reducing agent raw materials | |
| CN110542222B (en) | Internal dirt removing device of solar water heating pipe | |
| CN207769306U (en) | A kind of filter press | |
| CN219964871U (en) | Lubricating oil preparation device | |
| CN218133884U (en) | Ball mill convenient to clearance | |
| CN207533192U (en) | A kind of stirred tank | |
| CN212819675U (en) | Feeding control system | |
| CN111941683A (en) | Raw material melting device for polyester film production and processing | |
| CN117207379B (en) | Marine rubber tube apparatus for producing that corrosion resistance is high | |
| CN207254156U (en) | A kind of efficient food additive mixed stirring device easy to cleaning | |
| CN220386303U (en) | Portable carborundum suspension agitating unit | |
| CN220360037U (en) | Syrup heating barrel | |
| CN220657127U (en) | Chemical industry is with vertical material mixing arrangement of rotatory liquid feeding formula | |
| CN213996914U (en) | Belt cleaning device is used in plastic products processing | |
| CN215389223U (en) | Homogeneous stirrer | |
| CN116492969B (en) | High conversion preparation facilities of methyl methacrylate | |
| CN219722873U (en) | Stirrer for producing rust-proof grease | |
| CN216093618U (en) | Reation kettle is used in paint remover production | |
| CN220265266U (en) | Automatic filling device for polyurethane coating production | |
| CN220834215U (en) | Traditional chinese medicine leaching tank that heat preservation effect is good | |
| CN114541695B (en) | Ceramic tile back cement of building decoration usefulness is paintd equipment | |
| CN219359908U (en) | Stirring device for polypropylene resin production |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |