CN114053980A - A reation kettle for production of tert-butyl alcohol sodium - Google Patents

A reation kettle for production of tert-butyl alcohol sodium Download PDF

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Publication number
CN114053980A
CN114053980A CN202111453630.0A CN202111453630A CN114053980A CN 114053980 A CN114053980 A CN 114053980A CN 202111453630 A CN202111453630 A CN 202111453630A CN 114053980 A CN114053980 A CN 114053980A
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CN
China
Prior art keywords
cleaning
ring
kettle body
storage tank
liquid storage
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202111453630.0A
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Chinese (zh)
Inventor
余奋玉
衡永刚
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Jinbang Pharmaceutical Chemical Co ltd
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Anhui Jinbang Pharmaceutical Chemical Co ltd
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Publication date
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Priority to CN202111453630.0A priority Critical patent/CN114053980A/en
Publication of CN114053980A publication Critical patent/CN114053980A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto 
    • B08B9/08Cleaning containers, e.g. tanks
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto 
    • B08B9/08Cleaning containers, e.g. tanks
    • B08B9/087Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/68Preparation of metal alcoholates
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/28Metal alcoholates
    • C07C31/30Alkali metal or alkaline earth metal alcoholates

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a reaction kettle for producing sodium tert-butoxide, which comprises a kettle body, wherein a reaction cavity is arranged in the kettle body, and a feed inlet and a discharge outlet which are communicated with the reaction cavity are arranged on the kettle body; a liquid storage tank for storing cleaning liquid is arranged in the reaction cavity, and a liquid inlet is formed in the liquid storage tank; the lower end of the liquid storage tank is rotatably connected with a cleaning ring, and a plurality of cleaning plates for cleaning the inner wall of the reaction cavity are fixedly connected onto the cleaning ring; the cleaning plate for cleaning the inner wall is arranged, and the stirring and cleaning work can be respectively completed through the forward rotation and the reverse rotation of the stirring motor by utilizing the matching of the driving wheel and the blocking ring, so that the manufacturing cost is reduced, and the space utilization rate is improved; in the cleaning process, the cleaning solution in the liquid storage tank is only sprayed to the periphery of each cleaning plate through the through holes, the flow channels and the cleaning holes, so that the cleaning efficiency is improved, and meanwhile, the waste of the cleaning solution is avoided.

Description

A reation kettle for production of tert-butyl alcohol sodium
Technical Field
The invention relates to the field of chemistry, in particular to a reaction kettle for producing sodium tert-butoxide.
Background
Sodium tert-butoxide, white crystals, widely used as strong base in condensation, rearrangement and ring-opening reactions in chemical, pharmaceutical, pesticide and organic synthesis, sodium tert-butoxide is usually prepared in a reaction kettle, which is a container for physical or chemical reaction, by the structural design and parameter configuration of the container, the heating, evaporation, cooling and low-speed mixing functions required by the process are realized, the reaction kettle is widely used in petroleum, chemical, rubber, pesticide, dye, medicine, food, pressure vessels for completing the processes of vulcanization, nitration, hydrogenation, alkylation, polymerization, condensation, etc., such as reactors, reaction kettles, decomposition kettles, polymerization kettles, etc., and the materials are generally carbon manganese steel, stainless steel, zirconium, nickel-based alloy and other composite materials; after reaction is accomplished usually, need wash the material of cauldron internal wall, avoid causing the influence to follow-up production, the cauldron body need be opened to traditional cleaning methods more to wash away the processing to cauldron internal wall, this mode is wasted time and energy, and the treatment effeciency remains to be improved.
Disclosure of Invention
The invention aims to provide a reaction kettle for producing sodium tert-butoxide, and aims to solve the problem of low cleaning efficiency of the inner wall of the kettle body in the prior art.
In order to solve the technical problem, the reaction kettle for producing the sodium tert-butoxide provided by the invention comprises a kettle body, wherein a reaction cavity is arranged in the kettle body, and a feeding hole and a discharging hole which are communicated with the reaction cavity are arranged on the kettle body; a liquid storage tank for storing cleaning liquid is arranged in the reaction cavity, and a liquid inlet is formed in the liquid storage tank; the lower end of the liquid storage tank is rotationally connected with a cleaning ring; the cleaning ring is fixedly connected with a plurality of cleaning plates for cleaning the inner wall of the reaction cavity, each cleaning plate is provided with a flow channel, the cleaning ring is provided with a plurality of through holes respectively communicated with the corresponding flow channels, and each cleaning plate is provided with a plurality of cleaning holes communicated with the flow channels;
the kettle body is provided with a stirring motor, and an output shaft of the stirring motor is fixedly connected with a stirring rod; one side of the stirring rod is rotatably connected with a baffle plate, and the lower end of the stirring rod is fixedly connected with a driving wheel; the reaction cavity is internally provided with a blocking ring, the blocking ring is rotatably connected with the kettle body, the blocking ring is fixedly connected with the cleaning plate, the blocking ring is provided with a ratchet part, a notch is arranged in the driving wheel, a driving rod is rotatably connected in the notch, when the driving wheel rotates forwards, a first inclined plane on the ratchet part pushes the driving rod to enter the notch, the driving wheel cannot drive the blocking ring to rotate, when the driving wheel rotates backwards, a third inclined plane on the driving rod is abutted against a second inclined plane on the ratchet part, and the driving rod drives the blocking ring to rotate.
Preferably, a sealing ring is arranged between the kettle body and the blocking ring.
Preferably, a sealing ring is arranged between the blocking ring and the baffle plate.
After adopting the structure, compared with the prior art, the invention has the following advantages: the cleaning plate for cleaning the inner wall is arranged, and the stirring and cleaning work can be respectively completed through the forward rotation and the reverse rotation of the stirring motor by utilizing the matching of the driving wheel and the blocking ring, so that the manufacturing cost is reduced, and the space utilization rate is improved; in the cleaning process, the cleaning solution in the liquid storage tank is only sprayed to the periphery of each cleaning plate through the through holes, the flow channels and the cleaning holes, so that the cleaning efficiency is improved, and meanwhile, the waste of the cleaning solution is avoided.
Drawings
FIG. 1 is a schematic view of the internal structure of the present invention;
FIG. 2 is a cross-sectional view taken along line A-A of FIG. 1 in accordance with the present invention;
FIG. 3 is a cross-sectional view taken along line B-B of FIG. 1 in accordance with the present invention;
FIG. 4 is a schematic three-dimensional structure of a cleaning plate and a reservoir of the present invention;
fig. 5 is a schematic view of another perspective three-dimensional structure of the cleaning plate and reservoir of the present invention.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings and specific embodiments.
As shown in fig. 1 to 5, the reaction kettle for producing sodium tert-butoxide of the present invention includes a kettle body 1, a reaction chamber 11 is provided in the kettle body 1, and a feed inlet 12 and a discharge outlet 13 which are communicated with the reaction chamber 11 are provided on the kettle body 1; a liquid storage tank 14 for storing cleaning liquid is arranged in the reaction chamber 11, and a liquid inlet 141 is arranged on the liquid storage tank 14; the lower end of the liquid storage tank 14 is rotatably connected with a cleaning ring 142; a plurality of cleaning plates 143 for cleaning the inner wall of the reaction chamber 11 are fixedly connected to the cleaning ring 142, each cleaning plate 143 is provided with a flow channel 144, the cleaning ring 142 is provided with a plurality of through holes 145 respectively communicated with the corresponding flow channels 144, and each cleaning plate 143 is provided with a plurality of cleaning holes 146 communicated with the flow channels 144;
the stirring motor 2 is arranged on the kettle body 1, and an output shaft of the stirring motor 2 is fixedly connected with a stirring rod 21; one side of the stirring rod 21 is rotatably connected with a baffle 22, and the lower end of the stirring rod 21 is fixedly connected with a driving wheel 3; a blocking ring 23 is arranged in the reaction chamber 11, the blocking ring 23 is rotatably connected with the kettle body 1, the blocking ring 23 is fixedly connected with the cleaning plate 143, a ratchet portion 231 is arranged on the blocking ring 23, a notch 31 is arranged in the driving wheel 3, a driving rod 32 is rotatably connected in the notch 31, when the driving wheel 3 rotates forwards, a first inclined surface 232 on the ratchet portion 231 pushes the driving rod 32 to enter the notch 31, the driving wheel 3 cannot drive the blocking ring 23 to rotate, when the driving wheel 3 rotates backwards, a third inclined surface 321 on the driving rod 32 abuts against a second inclined surface 233 on the ratchet portion 231, and the driving rod 32 drives the blocking ring 23 to rotate.
When the stirring operation is carried out, the stirring motor 2 drives the driving wheel 3 to rotate forwards, and at the moment, when the driving rod 32 passes through one ratchet, the driving rod 32 is pushed into the notch 31 by the first inclined surface 232 on the corresponding ratchet, so that the driving wheel 3 cannot drive the blocking ring 23 to rotate in the process, and the cleaning plate 143 does not work; when the inner wall is cleaned after the reaction is finished, cleaning liquid is firstly introduced into the liquid storage tank 14, then the stirring motor 2 drives the driving wheel 3 to rotate reversely, the third inclined surface 321 on the driving rod 32 abuts against the corresponding second inclined surface 233 on the ratchet part 231, meanwhile, the driving rod 32 abuts against the notch 31, in the process, the driving rod 32 drives the blocking ring 23 to rotate, the cleaning plate 143 rotates to clean the inner wall, and the stirring and cleaning work can be respectively completed through the forward rotation and the reverse rotation of the stirring motor 2 by utilizing the matching of the driving wheel 3 and the blocking ring 23, so that the manufacturing cost is reduced, and the space utilization rate is improved; meanwhile, in the cleaning process, the cleaning liquid in the liquid storage tank 14 is only sprayed to the periphery of each cleaning plate 143 through the through holes 145, the flow channels 144 and the cleaning holes 146, so that the cleaning efficiency is improved, and the waste of the cleaning liquid is avoided; it should be noted that the forward rotation and the reverse rotation are only described for convenience of expression, and only correspond to the viewing angle shown in fig. 3, the forward rotation is the clockwise rotation of the driving wheel 3, and the determination should be made according to the structural position of each part during the specific production.
And a sealing ring is arranged between the kettle body 1 and the blocking ring 23.
And a sealing ring is arranged between the blocking ring 23 and the baffle plate 22.
The above description is only about the preferred embodiment of the present invention, but it should not be understood as limiting the claims, and the present invention may be modified in other structures, not limited to the above structures. In general, all changes which come within the scope of the invention as defined by the independent claims are intended to be embraced therein.

Claims (3)

1. A reaction kettle for producing sodium tert-butoxide is characterized by comprising a kettle body (1), wherein a reaction cavity (11) is arranged in the kettle body (1), and a feed inlet (12) and a discharge outlet (13) which are communicated with the reaction cavity (11) are arranged on the kettle body (1); a liquid storage tank (14) for storing cleaning liquid is arranged in the reaction cavity (11), and a liquid inlet (141) is arranged on the liquid storage tank (14); the lower end of the liquid storage tank (14) is rotationally connected with a cleaning ring (142); a plurality of cleaning plates (143) used for cleaning the inner wall of the reaction cavity (11) are fixedly connected to the cleaning ring (142), each cleaning plate (143) is provided with a flow channel (144), the cleaning ring (142) is provided with a plurality of through holes (145) respectively communicated with the corresponding flow channels (144), and each cleaning plate (143) is provided with a plurality of cleaning holes (146) communicated with the flow channels (144);
a stirring motor (2) is arranged on the kettle body (1), and an output shaft of the stirring motor (2) is fixedly connected with a stirring rod (21); one side of the stirring rod (21) is rotatably connected with a baffle plate (22), and the lower end of the stirring rod (21) is fixedly connected with a driving wheel (3); be equipped with separation ring (23) in reaction chamber (11), separation ring (23) and cauldron body (1) rotate to be connected, separation ring (23) and cleaning plate (143) fixed connection, be equipped with ratchet portion (231) on separation ring (23), be equipped with notch (31) in drive wheel (3), notch (31) internal rotation is connected with actuating lever (32), when drive wheel (3) corotation, first inclined plane (232) promote in ratchet portion (231) actuating lever (32) get into in notch (31), drive wheel (3) can not drive separation ring (23) rotatory, when drive wheel (3) reversal, second inclined plane (233) offset on third inclined plane (321) and ratchet portion (231) on actuating lever (32), actuating lever (32) will drive separation ring (23) and rotate.
2. The reaction kettle for producing sodium tert-butoxide according to claim 1, characterized in that a sealing ring is arranged between the kettle body (1) and the barrier ring (23).
3. The reaction kettle for sodium tert-butoxide production according to claim 1, characterized in that a sealing ring is provided between the barrier ring (23) and the baffle plate (22).
CN202111453630.0A 2021-12-01 2021-12-01 A reation kettle for production of tert-butyl alcohol sodium Pending CN114053980A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111453630.0A CN114053980A (en) 2021-12-01 2021-12-01 A reation kettle for production of tert-butyl alcohol sodium

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111453630.0A CN114053980A (en) 2021-12-01 2021-12-01 A reation kettle for production of tert-butyl alcohol sodium

Publications (1)

Publication Number Publication Date
CN114053980A true CN114053980A (en) 2022-02-18

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CN202111453630.0A Pending CN114053980A (en) 2021-12-01 2021-12-01 A reation kettle for production of tert-butyl alcohol sodium

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CN (1) CN114053980A (en)

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI235698B (en) * 2004-07-21 2005-07-11 Wan-Chuan Li A tool ratchet device having a rotary disc
CN207254201U (en) * 2017-09-30 2018-04-20 淄博职业学院 Liquid fast deployment equipment
CN209952840U (en) * 2019-02-28 2020-01-17 大连盛瑞贝尔科技有限公司 Novel wall scraping type reaction kettle
CN210058267U (en) * 2019-05-30 2020-02-14 漯河市天龙化工有限公司 Emulsifier reation kettle belt cleaning device
CN210827712U (en) * 2019-07-15 2020-06-23 河钢股份有限公司承德分公司 Water-saving device
CN112090387A (en) * 2020-10-26 2020-12-18 河北峰林永茂化工科技有限公司 Polymerization reaction device for water loss reducing agent raw materials
CN112833022A (en) * 2021-02-05 2021-05-25 陈少同 Submersible pump
CN112880357A (en) * 2021-04-27 2021-06-01 山东云豪卫生用品股份有限公司 Non-woven fabrics drying device is used in processing of panty-shape diapers
CN213854561U (en) * 2020-11-27 2021-08-03 贵港市微芯科技有限公司 Glass lining reaction kettle with wall sticking prevention function
CN214163482U (en) * 2020-06-05 2021-09-10 青岛建科工程检测有限公司 Mortar mixer easy to clean
CN214716629U (en) * 2021-04-20 2021-11-16 上海鼎素精细化工有限公司 Residual cleaning equipment for reaction kettle pigment kettle
CN214765403U (en) * 2020-12-23 2021-11-19 山东沾化奥仕化学有限公司 Reation kettle for chemical industry equipment

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI235698B (en) * 2004-07-21 2005-07-11 Wan-Chuan Li A tool ratchet device having a rotary disc
CN207254201U (en) * 2017-09-30 2018-04-20 淄博职业学院 Liquid fast deployment equipment
CN209952840U (en) * 2019-02-28 2020-01-17 大连盛瑞贝尔科技有限公司 Novel wall scraping type reaction kettle
CN210058267U (en) * 2019-05-30 2020-02-14 漯河市天龙化工有限公司 Emulsifier reation kettle belt cleaning device
CN210827712U (en) * 2019-07-15 2020-06-23 河钢股份有限公司承德分公司 Water-saving device
CN214163482U (en) * 2020-06-05 2021-09-10 青岛建科工程检测有限公司 Mortar mixer easy to clean
CN112090387A (en) * 2020-10-26 2020-12-18 河北峰林永茂化工科技有限公司 Polymerization reaction device for water loss reducing agent raw materials
CN213854561U (en) * 2020-11-27 2021-08-03 贵港市微芯科技有限公司 Glass lining reaction kettle with wall sticking prevention function
CN214765403U (en) * 2020-12-23 2021-11-19 山东沾化奥仕化学有限公司 Reation kettle for chemical industry equipment
CN112833022A (en) * 2021-02-05 2021-05-25 陈少同 Submersible pump
CN214716629U (en) * 2021-04-20 2021-11-16 上海鼎素精细化工有限公司 Residual cleaning equipment for reaction kettle pigment kettle
CN112880357A (en) * 2021-04-27 2021-06-01 山东云豪卫生用品股份有限公司 Non-woven fabrics drying device is used in processing of panty-shape diapers

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Application publication date: 20220218