CN112057371A - Apricot kernel hair-growing cream, composition and preparation method thereof - Google Patents
Apricot kernel hair-growing cream, composition and preparation method thereof Download PDFInfo
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- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 3
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses an almond hair-growing cream, a composition and a preparation method thereof, and relates to the technical field of cosmetics. The almond hair-growing milk comprises 18-45 parts of almond oil and 1.3-3.4 parts of cacumen biotae extract as raw materials, and the inventor finds that the almond hair-growing milk prepared by mixing the almond oil and the cacumen biotae extract according to the specific proportion can achieve the effects of safely growing hair, and reducing alopecia and hair breakage.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to almond hair growing cream, a composition and a preparation method thereof.
Background
With the increasing living and working pressure of modern human beings, a plurality of people have alopecia or even baldness, part of the alopecia is pathological, and the baldness is caused by bad living habits and stress, so that the personal image is seriously influenced.
For hair loss problems, there are many hair-growing and even hair-grafting products on the market, and the quality of the products becomes a concern for these consumers. Then, products which are safe to human bodies and can effectively solve the problems of alopecia and hair breakage are lacked at present.
In view of this, the invention is particularly proposed.
Disclosure of Invention
The invention aims to provide almond hair growing cream, a composition thereof and a preparation method thereof.
The invention is realized by the following steps:
in a first aspect, an embodiment provides an almond hair-growing cream composition, which comprises the following components in parts by weight: 18-45 parts of almond oil and 1.3-3.4 parts of cacumen biotae extract.
In a second aspect, embodiments provide a method for preparing an almond hair-growing milk, which comprises mixing the components of the almond hair-growing milk composition as described in the previous embodiments to prepare the almond hair-growing milk.
In a third aspect, the embodiment provides an almond hair-growing milk which is prepared by the preparation method described in the previous embodiment.
The invention has the following beneficial effects:
the embodiment of the invention provides almond hair-growing milk, a composition and a preparation method thereof, wherein the preparation raw materials of the almond hair-growing milk comprise 18-45 parts of almond oil and 1.3-3.4 parts of cacumen biotae extract, and the inventor finds that the almond hair-growing milk prepared by the almond oil and the cacumen biotae extract in the specific proportion can achieve the effects of safely growing hair, and reducing alopecia and hair breakage.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
Firstly, the embodiment of the invention provides an almond hair-growing cream composition which comprises the following components in parts by weight: 18-45 parts of almond oil and 1.3-3.4 parts of cacumen biotae extract.
The almond oil is slightly yellow and transparent, has faint scent, is not only an excellent edible oil, but also an advanced lubricating oil, can resist the low temperature below 20 ℃ below zero, can be used as an important raw material of advanced paint, cosmetics and high-quality perfumed soap, and can extract essence and vitamins.
The inventor finds that the almond oil and the cacumen biotae extract have synergistic effect, and the prepared almond hair-growing emulsion has the effects of reducing alopecia and hair breakage in the specific proportion, is safe in components and harmless to human bodies.
Specifically, in some embodiments, the parts by weight of the almond oil may be 18 parts, 20 parts, 22 parts, 24 parts, 26 parts, 28 parts, 30 parts, 32 parts, 34 parts, 36 parts, 38 parts, 40 parts, 42 parts, 44 parts, or 45 parts.
The biota orientalis leaf extract is the branch tip and leaf of the Franco of the Platycladus orientalis (L.) of the cypress family, is matched with the almond oil in a specific proportion for use, and has the unexpected technical effect of preventing alopecia.
In some embodiments, the weight parts of the cacumen biotae extract may be 1.3 parts, 1.5 parts, 1.7 parts, 1.9 parts, 2.1 parts, 2.3 parts, 2.5 parts, 2.7 parts, 2.9 parts, 3.1 parts or 3.4 parts.
In some embodiments, the almond hair growth cream composition further comprises: any one or more of an emollient, an emulsifier, a solvent, a pH adjuster, a chelating agent, a thickener, and an antioxidant.
In some embodiments, the almond hair-nourishing cream composition comprises the following components in parts by weight: 18-45 parts of almond oil, 1.3-3.4 parts of cacumen biotae extract, 3.5-6.8 parts of emollient, 0.4-1.8 parts of emulsifier, 58.7-101.35 parts of solvent, 0.005-0.01 part of pH regulator, 0.06-0.2 part of chelating agent, 1.6-4.2 parts of thickening agent and 0.01-0.08 part of antioxidant.
In some embodiments, the emollient is glycerin.
Preferably, the emulsifier is selected from: at least one of ceteareth-6 and ceteareth-25.
Preferably, the solvent is selected to be water.
Preferably, the pH adjuster is sodium hydroxide or a solution thereof.
Preferably, the chelating agent is disodium EDTA.
Preferably, the thickening agent is selected from: at least one of cetyl alcohol, carbomer, and xanthan gum.
Preferably, the antioxidant is selected from: at least one of tocopherol and wheat germ oil.
The inventor develops the specific composition and the proportion thereof through a series of experiments, and the effect of the almond hair-nourishing cream prepared by the composition on hair nourishing, hair loss reduction and hair breakage is more obvious under the conditions.
The embodiment of the invention also provides a preparation method of the almond hair-nourishing milk, which comprises the step of mixing the components of the almond hair-nourishing milk composition in any one of the embodiments to prepare the almond hair-nourishing milk.
In some embodiments, when the components include almond oil, cacumen biotae extract, emollient, emulsifier, solvent, pH adjuster, chelating agent, thickener, and antioxidant, the preparation method comprises: the components of the cacumen biotae extracting solution, the oil phase material, the water phase material and the pH regulator are uniformly stirred at the temperature of 15-35 ℃ to prepare the almond hair-growing emulsion.
Wherein the oil phase material is a mixed dissolved substance of almond oil, a thickening agent, an emulsifying agent and an antioxidant; the partial amount of the solvent is 58.7 to 101.35 parts by weight based on the above-mentioned partial weight parts. Preferably, the weight part of the solvent mixed in the water phase material is 25-45 parts.
The water phase material is a mixed dissolved substance of an emollient, a chelating agent and a partial solvent. The amount of the solvent used in the aqueous phase may be 45% to 100% by weight based on the total weight of the solvent. Specifically, a partial amount of the solvent used in the aqueous phase material accounts for any one of 50%, 60%, 70%, 80%, 90% and 100% of the total amount of the solvent. The remaining amount of solvent is used to disperse the cacumen biotae extract to form a cacumen biotae extract.
The cacumen biotae extracting solution is a solution formed by mixing cacumen biotae extract and the rest solvent.
In the mixing process, the components are mixed according to the weight parts of the components in the above embodiment without specific limitation.
The inventor finds that the oil phase material and the water phase material are respectively dissolved and then emulsified together according to the properties of each component in the composition and the efficacy required by the almond hair-nourishing cream, so that the product can be prepared more quickly and effectively, and the prepared almond hair-nourishing cream has remarkable efficacy of preventing alopecia and hair breakage.
In some embodiments, the mass ratio of the cacumen biotae extract to the solvent in the cacumen biotae extracting solution is 1 (8-12). Specifically, the mass ratio may be any one of 1:8, 1:9, 1:10, and 1: 11. In the preparation process, the amount of the solvent required for the cacumen biotae extract solution may be determined based on the mass ratio, and the remaining solvent may be used for the preparation of the aqueous material after the determination.
In some embodiments, the mix is prepared by: and mixing the oil phase material and the water phase material and emulsifying.
Preferably, the emulsifying temperature is 60-85 ℃, and the emulsifying time is 10-50 min;
preferably, the emulsification is vacuum emulsification.
In some embodiments, the oil phase is prepared by: mixing and dissolving the almond oil, the thickening agent, the emulsifier and the antioxidant at the temperature of 70-90 ℃.
In some embodiments, the aqueous phase is prepared by: mixing and dissolving the emollient, the chelating agent and part of the solvent at 70-90 ℃.
The oil phase material or the water phase material is prepared according to the preparation method of the embodiment, and can be better mixed, so that the almond hair-growing cream prepared by mixing the cacumen biotae extracting solution can better exert the efficacy.
In addition, the embodiment of the invention also provides the almond hair growing milk which is prepared by the preparation method of the almond hair growing milk in any one of the embodiments.
In some embodiments, the almond hair-growing milk is used in the following way: cleaning hair, drying, applying appropriate amount of the product on hair root, and massaging for 5-10 min until the product is completely absorbed. Preferably, once, twice or three times daily.
In some embodiments, the amount of almond hair tonic used is 3-15 mL.
The features and properties of the present invention are described in further detail below with reference to examples.
Example 1
An almond hair-growing cream is prepared by the following steps.
(1) The almond hair-nourishing milk composition (raw materials) comprises:
30 parts of almond oil, 2 parts of cacumen biotae extract, 5 parts of emollient, 1.2 parts of emulsifier, 60 parts of solvent, 0.08 part of pH regulator, 0.1 part of chelating agent, 2.5 parts of thickening agent and 0.04 part of antioxidant.
Wherein the emollient is glycerol, the emulsifier is ceteareth-6, the solvent is water, the pH regulator is sodium hydroxide solution, the chelating agent is disodium EDTA, the thickener is cetyl alcohol, and the antioxidant is tocopherol.
(2) Preparation of water phase material:
pumping 40 parts of solvent into a water phase pot, starting a stirrer of the water phase pot, weighing glycerol and EDTA disodium according to the weight part ratio, putting the glycerol and the EDTA disodium into the water phase pot, starting a steam heater and stirring at the stirring speed of 800r/min, and heating to 85 ℃ until the glycerol and the EDTA disodium are completely dissolved to obtain a water phase material.
(3) Preparing an oil phase material:
weighing the almond oil, the cetyl alcohol, the ceteareth-6 and the tocopherol (vitamin E) according to the weight parts, putting the mixture into an oil phase pot, starting a steam heater, starting stirring at the stirring speed of 800r/min, and heating to 85 ℃ until the mixture is completely dissolved to obtain the oil phase material.
(4) Preparing a mixture of an oil phase material and a water phase material:
starting a vacuum emulsifying pot, sucking the prepared water phase material into the vacuum emulsifying pot, and controlling the temperature to be 75 ℃; sucking the prepared oil phase material, starting stirring at the stirring speed of 55r/min for 30min, starting a homogenizer after uniformly stirring, and homogenizing for 10min to obtain a mixture of the oil phase material and the water phase material.
(5) Preparing a cacumen biotae extracting solution:
mixing the cacumen biotae extract with the rest water (the mass mixing ratio is 1:10) in parts by weight, and dispersing the cacumen biotae extract in water to obtain a cacumen biotae extracting solution.
The preparation process of the cacumen biotae extracting solution comprises the following steps: water extraction, filtration, concentration, drying and pulverization.
(6) Preparation of almond hair-growing cream
And uniformly stirring the prepared mixture of the oil phase material and the water phase material, the cacumen biotae extracting solution and the pH regulator at the temperature of 30 ℃ for 35 r/min. And cooling to normal temperature, sampling, detecting and discharging after the product is qualified.
Example 2
This example also provides an almond hair-growing milk whose composition and preparation method are substantially the same as those provided in example 1, except that the composition parameters are different, as follows.
The almond hair-nourishing milk composition (raw materials) comprises: 45 parts of almond oil, 2 parts of cacumen biotae extract, 5 parts of emollient, 1.2 parts of emulsifier, 67 parts of solvent, 0.08 part of pH regulator, 0.1 part of chelating agent, 2.5 parts of thickening agent and 0.04 part of antioxidant.
Example 3
This example also provides an almond hair-growing milk whose composition and preparation method are substantially the same as those provided in example 1, except that the composition parameters are different, as follows.
The almond hair-nourishing milk composition (raw materials) comprises: 40 parts of almond oil, 2 parts of cacumen biotae extract, 5 parts of emollient, 1.2 parts of emulsifier, 60 parts of solvent, 0.08 part of pH regulator, 0.1 part of chelating agent, 2.5 parts of thickening agent and 0.04 part of antioxidant.
Example 4
This example also provides an almond hair-growing milk whose composition and preparation method are substantially the same as those provided in example 1, except that the composition parameters are different, as follows.
The almond hair-nourishing milk composition (raw materials) comprises: 48 parts of almond oil, 1.5 parts of cacumen biotae extract, 5 parts of emollient, 1.2 parts of emulsifier, 62 parts of solvent, 0.08 part of pH regulator, 0.1 part of chelating agent, 3.0 parts of thickening agent and 0.04 part of antioxidant.
Comparative example 1
The present comparative example provides an almond hair-growing cream, the components and the preparation method of which are substantially the same as those provided in example 1, except that the proportions of the components are different, as follows.
The almond hair-nourishing milk composition (raw materials) comprises: 50 parts of almond oil, 1.3 parts of cacumen biotae extract, 5 parts of emollient, 1.2 parts of emulsifier, 60 parts of solvent, 0.08 part of pH regulator, 0.1 part of chelating agent, 2.5 parts of thickener and 0.04 part of antioxidant.
Comparative example 2
The present comparative example provides an almond hair-growing cream, the components and the preparation method of which are substantially the same as those provided in example 1, except that the proportions of the components are different, as follows.
The almond hair-nourishing milk composition (raw materials) comprises: 15 parts of almond oil, 3.5 parts of cacumen biotae extract, 5 parts of emollient, 1.2 parts of emulsifier, 50 parts of solvent, 0.08 part of pH regulator, 0.1 part of chelating agent, 2.5 parts of thickener and 0.04 part of antioxidant.
Comparative example 3
This comparative example provides an almond hair-growing milk whose composition and method of preparation are substantially the same as those provided in example 1, except that the compositions are different, as follows.
Replacing folium Platycladi extract with herba Taraxaci extract.
Comparative example 4
This comparative example provides an almond hair-growing milk whose composition and method of preparation are substantially the same as those provided in example 1, except that the compositions are different, as follows.
Replacing cacumen Platycladi extract with rhizoma Coptidis extract.
Comparative example 5
This comparative example provides an almond hair-growing milk whose composition and method of preparation are substantially the same as those provided in example 1, except that the compositions are different, as follows.
Replacing the cacumen biotae extract with a mulberry extract.
Test example 1
The preparation method and the raw materials provided by the embodiment 1 of the invention are adopted to prepare the almond hair-growing cream, and the prepared product is applied to human bodies.
Experimental methods
10 persons with serious alopecia and local baldness are selected, the scalp of 10 persons is smeared with 3-5 mL of the product once every morning and evening, and the finger abdomen is massaged for 10 min. The hair was tried for 10 days, 20 days and 30 days, and then the condition of hair loss and hair growth before and after use was observed (observation means: comparing the total hair density before and after use, number of local hair).
The evaluation criteria were:
a. the effect is shown: the hair loss is obviously reduced, and small villi obviously grow on bald tops;
b. the method has the following advantages: the hair loss is reduced, and a small amount of fine hair is obviously grown at the bald position;
c. and (4) invalidation: alopecia and baldness were unchanged.
The test results are shown in Table 1.
TABLE 1 test results
The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. The almond hair nourishing cream composition is characterized by comprising the following components in parts by weight: 18-45 parts of almond oil and 1.3-3.4 parts of cacumen biotae extract.
2. The almond hair nourishing cream composition of claim 1, wherein said almond hair nourishing cream composition further comprises at least one of the following components: emollients, emulsifiers, solvents, pH modifiers, chelating agents, thickeners and antioxidants.
3. The almond hair nourishing cream composition of claim 2, wherein the almond hair nourishing cream composition comprises the following components in parts by weight: 18-45 parts of almond oil, 1.3-3.4 parts of cacumen biotae extract, 3.5-6.8 parts of emollient, 0.4-1.8 parts of emulsifier, 58.7-101.35 parts of solvent, 0.005-0.01 part of pH regulator, 0.06-0.2 part of chelating agent, 1.6-4.2 parts of thickening agent and 0.01-0.08 part of antioxidant.
4. An almond hair nourishing cream composition according to claim 2 or 3 wherein said emollient is glycerin;
preferably, the emulsifier is selected from: at least one of ceteareth-6 and ceteareth-25;
preferably, the solvent is water;
preferably, the pH adjuster is sodium hydroxide or a solution thereof;
preferably, the chelating agent is disodium EDTA;
preferably, the thickening agent is selected from: at least one of cetyl alcohol, carbomer, and xanthan gum;
preferably, the antioxidant is selected from: at least one of tocopherol and wheat germ oil.
5. A method for preparing almond hair-growing milk, which is characterized by mixing the components of the almond hair-growing milk composition as claimed in any one of claims 1 to 4.
6. The method for preparing almond hair growing emulsion of claim 5 wherein, when said components include almond oil, biota orientalis extract, emollient, emulsifier, solvent, pH adjuster, chelating agent, thickener and antioxidant, said mixing comprises: uniformly stirring the mixture of the oil-phase material and the water-phase material, the cacumen biotae extract and the pH regulator in the components at 15-35 ℃;
wherein the oil phase material is a mixed dissolved substance of almond oil, a thickening agent, an emulsifying agent and an antioxidant; the water phase material is a mixed dissolved substance of an emollient, a chelating agent and a partial solvent; the cacumen biotae extracting solution is a solution obtained by mixing cacumen biotae extract and the rest of solvent;
preferably, in the cacumen biotae extracting solution, the mass ratio of the cacumen biotae extract to the solvent is 1: 8-12.
7. The preparation method of the almond hair-growing milk according to claim 6, characterized in that the preparation method of the mixture is as follows: mixing the oil phase material and the water phase material and emulsifying;
preferably, the emulsifying temperature is 60-85 ℃, and the emulsifying time is 10-50 min;
preferably, the emulsification is vacuum emulsification.
8. The preparation method of the almond hair-growing milk according to claim 6, characterized in that the oil phase material is prepared by the following steps: mixing and dissolving the almond oil, the thickening agent, the emulsifier and the antioxidant at the temperature of 70-90 ℃.
9. The preparation method of the almond hair-growing milk according to claim 6, characterized in that the preparation method of the water phase material is as follows: mixing and dissolving the emollient, the chelating agent and part of the solvent at 70-90 ℃.
10. An almond hair-growing milk characterized by being prepared by the preparation method of the almond hair-growing milk as claimed in any one of claims 5 to 9.
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Application publication date: 20201211 |