CN112043858A - Chinese yew sanitary towel and preparation method thereof - Google Patents
Chinese yew sanitary towel and preparation method thereof Download PDFInfo
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- CN112043858A CN112043858A CN202010823909.2A CN202010823909A CN112043858A CN 112043858 A CN112043858 A CN 112043858A CN 202010823909 A CN202010823909 A CN 202010823909A CN 112043858 A CN112043858 A CN 112043858A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/40—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing ingredients of undetermined constitution or reaction products thereof, e.g. plant or animal extracts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F13/15—Absorbent pads, e.g. sanitary towels, swabs or tampons for external or internal application to the body; Supporting or fastening means therefor; Tampon applicators
- A61F13/45—Absorbent pads, e.g. sanitary towels, swabs or tampons for external or internal application to the body; Supporting or fastening means therefor; Tampon applicators characterised by the shape
- A61F13/47—Sanitary towels, incontinence pads or napkins
- A61F13/472—Sanitary towels, incontinence pads or napkins specially adapted for female use
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- A—HUMAN NECESSITIES
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- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F13/15—Absorbent pads, e.g. sanitary towels, swabs or tampons for external or internal application to the body; Supporting or fastening means therefor; Tampon applicators
- A61F13/84—Accessories, not otherwise provided for, for absorbent pads
- A61F13/8405—Additives, e.g. for odour, disinfectant or pH control
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- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/33—Heterocyclic compounds
- A61K31/335—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin
- A61K31/35—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom
- A61K31/352—Heterocyclic compounds having oxygen as the only ring hetero atom, e.g. fungichromin having six-membered rings with one oxygen as the only ring hetero atom condensed with carbocyclic rings, e.g. methantheline
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- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
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- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
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- A61F13/00—Bandages or dressings; Absorbent pads
- A61F13/15—Absorbent pads, e.g. sanitary towels, swabs or tampons for external or internal application to the body; Supporting or fastening means therefor; Tampon applicators
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- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
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- A61F13/84—Accessories, not otherwise provided for, for absorbent pads
- A61F13/8405—Additives, e.g. for odour, disinfectant or pH control
- A61F2013/8408—Additives, e.g. for odour, disinfectant or pH control with odour control
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Abstract
The invention discloses a Chinese yew sanitary towel and a preparation method in the technical field of Chinese yew sanitary towels, wherein the Chinese yew sanitary towel comprises a Chinese yew pad body, the Chinese yew pad body comprises an upper surface layer, a lower surface layer and a medicine composite layer arranged between the upper surface layer and the lower surface layer, the medicine composite layer comprises a traditional Chinese medicine chip and a coating layer for coating the traditional Chinese medicine chip, and the preparation material of the traditional Chinese medicine chip is specifically as follows: 4-8 parts of taxus chinensis, 4-8 parts of chicory, 4-8 parts of dandelion, 4-8 parts of soybean isoflavone, 3-6 parts of salvia miltiorrhiza bunge, 3-6 parts of semen cuscutae, 1-2 parts of safflower, 1 part of eucommia bark, 1 part of radix bupleuri, 1 part of motherwort and 1-2 parts of alcohol, wherein the components are used as raw materials and are prepared according to proper weight proportion, an upper surface layer, a medicine composite layer and a lower surface layer are sequentially overlapped together, and composite pressing is realized, so that the preparation of the taxus chinensis sanitary towel is realized, various medicine components play a role in synergy, and the effects of effectively relieving and treating dysmenorrheal, diminishing inflammation and sterilizing are jointly played.
Description
Technical Field
The invention relates to the technical field of Chinese yew sanitary napkins, and particularly relates to a Chinese yew sanitary napkin and a preparation method thereof.
Background
Dysmenorrhea is one of common and frequently encountered diseases of women, is commonly seen in women of 25-45 years old, and means that the women have lower abdomen or waist pain, even lumbosacral pain, during and before menstrual period, which seriously affects the work and study of the vast women and reduces the quality of life. The design of side is for preventing the edge leakage, and the gum of the thin soft cotton of silk is waterproof material, can keep the menstrual blood in the thin soft cotton of silk, and dry and comfortable not anti-seepage adopts high ventilative combined material, makes the inside and outside oxygen passageway of piece of cloth body open, makes private skin freely breathe, 360 full-sealed packages, and the refuse pollutes, lets the bacterium be wushich. Compared with the existing product, the Chinese yew sanitary towel has better effects on diminishing inflammation, sterilizing, relieving dysmenorrheal and eliminating peculiar smell, and therefore the Chinese yew sanitary towel and the preparation method are provided.
Disclosure of Invention
The invention aims to provide a taxus chinensis sanitary towel and a preparation method thereof, and aims to solve the problems in the background art.
In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a chinese yew sanitary towel and preparation method, chinese yew sanitary towel includes chinese yew protection pad body, and chinese yew protection pad body includes upper surface layer, lower surface layer and sets up the medicine composite bed between upper surface layer and lower surface layer, and the medicine composite bed includes traditional chinese medicine chip and the coating of parcel traditional chinese medicine chip, and traditional chinese medicine chip's preparation material specifically is: 4-8 parts of taxus chinensis, 4-8 parts of chicory, 4-8 parts of dandelion, 4-8 parts of soybean isoflavone, 3-6 parts of salvia miltiorrhiza bunge, 3-6 parts of semen cuscutae, 1-2 parts of safflower, 1 part of eucommia bark, 1 part of radix bupleuri, 1 part of motherwort and 1-2 parts of alcohol, wherein the medicine composite layer is prepared by the following method:
the method comprises the following steps: extracting Taxus chinensis, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain Taxus chinensis fine powder: putting 200Kg of taxus raw material into a stainless steel extraction tank with the volume of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, feeding the feed liquid into a decompression solvent recoverer, and recovering the alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step two: externally purchasing soybean isoflavone fine powder with the effective component content of 80 percent: purchasing soybean isoflavone with 80% of effective component content, oven drying, and pulverizing into superfine powder;
step three: extracting Saviae Miltiorrhizae radix, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain Saviae Miltiorrhizae radix fine powder: putting 200Kg of radix Salviae Miltiorrhizae into a stainless steel extraction tank of 3 cubic meters, extracting with 30% ethanol as extraction medium at 60 deg.C under stirring for 1 hr, recovering ethanol from the feed liquid in a vacuum solvent recoverer at 60 deg.C under negative pressure. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step four: extracting semen Cuscutae, separating by column chromatography to obtain semen Cuscutae fine powder with effective component content of 80%, drying, and pulverizing to obtain semen Cuscutae fine powder: putting 200Kg of dodder raw material into a stainless steel extraction tank with the volume of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, putting the feed liquid into a decompression solvent recoverer, and recovering the alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step five: extracting safflower, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain fine powder of safflower: putting 200Kg of safflower raw material into a stainless steel extraction tank with 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, feeding the feed liquid into a decompression solvent recoverer, and recovering alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step six: extracting a mixture of eucommia bark, bupleurum and motherwort, wherein the content of effective components is 80%, drying and crushing to obtain mixture fine powder of the eucommia bark, the bupleurum and the motherwort: putting 300Kg of mixture raw materials of eucommia bark, bupleurum and motherwort 100Kg into a stainless steel extraction tank of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃, stirring and extracting for 1 hour at intervals (20 minutes), feeding the feed liquid into a decompression solvent recoverer, and recovering alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step seven: preparing a traditional Chinese medicine paste: dissolving 6 parts of taxus chinensis extract, 3 parts of salvia miltiorrhiza extract, 3 parts of semen cuscutae extract, 1 part of safflower extract, 3 parts of eucommia bark, radix bupleuri and motherwort mixed extract in 30% alcohol dissolving solution which is 10 times of the weight of all the traditional Chinese medicine extracts, stirring for 20 minutes, putting the dissolving solution into a decompression solvent recoverer, recovering alcohol at the negative pressure of 60 ℃, and concentrating the traditional Chinese medicine dissolving solution into paste (the density is 1.7) to form a preparation raw material of a coating layer;
step eight: preparing a traditional Chinese medicine chip: respectively drying chicory, taxus chinensis and dandelion, crushing and grinding the chicory, the taxus chinensis and the dandelion into superfine powder, adding the taxus chinensis powder into 95-degree alcohol, soaking for 24 hours, wherein the mass ratio of the alcohol to the taxus chinensis powder is 3:1, then mixing the cichorium chinensis and the dandelion powder in proportion, adding purified water after the alcohol is evaporated, decocting for 35-40 minutes, filtering, and adding 6 parts of soybean isoflavone extract to obtain a traditional Chinese medicine composition liquid medicine for later use; then, under the environment of aseptic temperature of 0-10 ℃, the common suction core of the non-woven fabric is soaked in the liquid medicine of the traditional Chinese medicine composition for 2-3 days; taking out the soaked non-woven fabric wick, and air-drying with dry air at 0-10 deg.C under sterile condition to obtain traditional Chinese medicine chip;
step nine: preparation of a medicine composite layer: in a sterile environment, attaching the Chinese medicinal paste obtained by distillation in the seventh step to a Chinese medicinal chip, and processing by ultraviolet irradiation to obtain a medicinal composite layer;
step ten: and sequentially superposing the upper surface layer, the medicine composite layer and the lower surface layer together, and realizing composite pressing, thereby realizing the preparation of the taxus chinensis sanitary towel.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the Chinese yew protective pad, the medicine composite layer is added into the Chinese yew protective pad body, so that the Chinese yew protective pad can effectively sterilize, diminish inflammation, relieve dysmenorrheal and eliminate peculiar smell, various medicine components play a synergistic role, and the Chinese yew protective pad has the effects of effectively relieving and treating dysmenorrheal, diminishing inflammation, sterilizing, eliminating peculiar smell, overcoming infertility and the like, and protects the health of women;
2. the Chinese yew extract has obvious effects on aging resistance, human immunity improvement and free radical capture, so that the sanitary towel has good antibacterial and bacteriostatic effects, the chicory and the taraxacum contain biological protein, the soaking-out of the effective components and the active components of the Chinese yew can be greatly increased, the anticancer drug effect of the Chinese yew is enhanced, under the same drug effect, the using amount of the Chinese yew is small, the production cost can be greatly reduced, the chicory component can effectively eliminate HPV, and the blank of defending the HPV in the field of female sanitary products at present is filled.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The utility model provides a chinese yew sanitary towel and preparation method, chinese yew sanitary towel includes chinese yew protection pad body, and chinese yew protection pad body includes upper surface layer, lower surface layer and sets up the medicine composite bed between upper surface layer and lower surface layer, and the medicine composite bed includes traditional chinese medicine chip and the coating of parcel traditional chinese medicine chip, and traditional chinese medicine chip's preparation material specifically is: 8 parts of taxus chinensis, 8 parts of chicory, 8 parts of dandelion, 8 parts of soybean isoflavone, 6 parts of salvia miltiorrhiza, 6 parts of semen cuscutae, 2 parts of safflower, 1 part of eucommia bark, 1 part of radix bupleuri, 1 part of motherwort and 2 parts of alcohol, wherein the medicine composite layer is prepared by the following method:
the method comprises the following steps: extracting Taxus chinensis, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain Taxus chinensis fine powder: putting 200Kg of taxus raw material into a stainless steel extraction tank with the volume of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, feeding the feed liquid into a decompression solvent recoverer, and recovering the alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step two: externally purchasing soybean isoflavone fine powder with the effective component content of 80 percent: purchasing soybean isoflavone with 80% of effective component content, oven drying, and pulverizing into superfine powder;
step three: extracting Saviae Miltiorrhizae radix, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain Saviae Miltiorrhizae radix fine powder: putting 200Kg of radix Salviae Miltiorrhizae into a stainless steel extraction tank of 3 cubic meters, extracting with 30% ethanol as extraction medium at 60 deg.C under stirring for 1 hr, recovering ethanol from the feed liquid in a vacuum solvent recoverer at 60 deg.C under negative pressure. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step four: extracting semen Cuscutae, separating by column chromatography to obtain semen Cuscutae fine powder with effective component content of 80%, drying, and pulverizing to obtain semen Cuscutae fine powder: putting 200Kg of dodder raw material into a stainless steel extraction tank with the volume of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, putting the feed liquid into a decompression solvent recoverer, and recovering the alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step five: extracting safflower, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain fine powder of safflower: putting 200Kg of safflower raw material into a stainless steel extraction tank with 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, feeding the feed liquid into a decompression solvent recoverer, and recovering alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step six: extracting a mixture of eucommia bark, bupleurum and motherwort, wherein the content of effective components is 80%, drying and crushing to obtain mixture fine powder of the eucommia bark, the bupleurum and the motherwort: putting 300Kg of mixture raw materials of eucommia bark, bupleurum and motherwort 100Kg into a stainless steel extraction tank of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃, stirring and extracting for 1 hour at intervals (20 minutes), feeding the feed liquid into a decompression solvent recoverer, and recovering alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step seven: preparing a traditional Chinese medicine paste: dissolving 6 parts of taxus chinensis extract, 3 parts of salvia miltiorrhiza extract, 3 parts of semen cuscutae extract, 1 part of safflower extract, 3 parts of eucommia bark, radix bupleuri and motherwort mixed extract in 30% alcohol dissolving solution which is 10 times of the weight of all the traditional Chinese medicine extracts, stirring for 20 minutes, putting the dissolving solution into a decompression solvent recoverer, recovering alcohol at the negative pressure of 60 ℃, and concentrating the traditional Chinese medicine dissolving solution into paste (the density is 1.7) to form a preparation raw material of a coating layer;
step eight: preparing a traditional Chinese medicine chip: respectively drying chicory, taxus chinensis and dandelion, crushing and grinding the chicory, the taxus chinensis and the dandelion into superfine powder, adding the taxus chinensis powder into 95-degree alcohol, soaking for 24 hours, wherein the mass ratio of the alcohol to the taxus chinensis powder is 3:1, then mixing the cichorium intybus and the dandelion powder in proportion, adding purified water after the alcohol is evaporated, decocting for 340 minutes, filtering, and adding 6 parts of soybean isoflavone extract to obtain a traditional Chinese medicine composition liquid medicine for later use; then, under the environment of asepsis and 10 ℃, the common suction core of the non-woven fabric is soaked in the liquid medicine of the traditional Chinese medicine composition for 3 days; taking out the soaked non-woven fabric wick, and air-drying with dry air at 10 deg.C under sterile condition to obtain traditional Chinese medicine chip;
step nine: preparation of a medicine composite layer: in a sterile environment, attaching the Chinese medicinal paste obtained by distillation in the seventh step to a Chinese medicinal chip, and processing by ultraviolet irradiation to obtain a medicinal composite layer;
step ten: and sequentially superposing the upper surface layer, the medicine composite layer and the lower surface layer together, and realizing composite pressing, thereby realizing the preparation of the taxus chinensis sanitary towel.
Example 2
The utility model provides a chinese yew sanitary towel and preparation method, chinese yew sanitary towel includes chinese yew protection pad body, and chinese yew protection pad body includes upper surface layer, lower surface layer and sets up the medicine composite bed between upper surface layer and lower surface layer, and the medicine composite bed includes traditional chinese medicine chip and the coating of parcel traditional chinese medicine chip, and traditional chinese medicine chip's preparation material specifically is: 4 parts of taxus chinensis, 4 parts of chicory, 4 parts of dandelion, 4 parts of soybean isoflavone, 3 parts of salvia miltiorrhiza, 3 parts of semen cuscutae, 1 part of safflower, 1 part of eucommia bark, 1 part of radix bupleuri, 1 part of motherwort and 1 part of alcohol, wherein the medicine composite layer is prepared by the following method:
the method comprises the following steps: extracting Taxus chinensis, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain Taxus chinensis fine powder: putting 200Kg of taxus raw material into a stainless steel extraction tank with the volume of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, feeding the feed liquid into a decompression solvent recoverer, and recovering the alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step two: externally purchasing soybean isoflavone fine powder with the effective component content of 80 percent: purchasing soybean isoflavone with 80% of effective component content, oven drying, and pulverizing into superfine powder;
step three: extracting Saviae Miltiorrhizae radix, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain Saviae Miltiorrhizae radix fine powder: putting 200Kg of radix Salviae Miltiorrhizae into a stainless steel extraction tank of 3 cubic meters, extracting with 30% ethanol as extraction medium at 60 deg.C under stirring for 1 hr, recovering ethanol from the feed liquid in a vacuum solvent recoverer at 60 deg.C under negative pressure. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step four: extracting semen Cuscutae, separating by column chromatography to obtain semen Cuscutae fine powder with effective component content of 80%, drying, and pulverizing to obtain semen Cuscutae fine powder: putting 200Kg of dodder raw material into a stainless steel extraction tank with the volume of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, putting the feed liquid into a decompression solvent recoverer, and recovering the alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step five: extracting safflower, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain fine powder of safflower: putting 200Kg of safflower raw material into a stainless steel extraction tank with 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, feeding the feed liquid into a decompression solvent recoverer, and recovering alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step six: extracting a mixture of eucommia bark, bupleurum and motherwort, wherein the content of effective components is 80%, drying and crushing to obtain mixture fine powder of the eucommia bark, the bupleurum and the motherwort: putting 300Kg of mixture raw materials of eucommia bark, bupleurum and motherwort 100Kg into a stainless steel extraction tank of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃, stirring and extracting for 1 hour at intervals (20 minutes), feeding the feed liquid into a decompression solvent recoverer, and recovering alcohol at the negative pressure of 60 ℃. Purified water is added to adjust the density of the feed liquid to 1, and the feed liquid enters column chromatography for adsorption at the flow rate of 3 cubic meters per hour. Eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step seven: preparing a traditional Chinese medicine paste: dissolving 6 parts of taxus chinensis extract, 3 parts of salvia miltiorrhiza extract, 3 parts of semen cuscutae extract, 1 part of safflower extract, 3 parts of eucommia bark, radix bupleuri and motherwort mixed extract in 30% alcohol dissolving solution which is 10 times of the weight of all the traditional Chinese medicine extracts, stirring for 20 minutes, putting the dissolving solution into a decompression solvent recoverer, recovering alcohol at the negative pressure of 60 ℃, and concentrating the traditional Chinese medicine dissolving solution into paste (the density is 1.7) to form a preparation raw material of a coating layer;
step eight: preparing a traditional Chinese medicine chip: respectively drying chicory, taxus chinensis and dandelion, crushing and grinding the chicory, the taxus chinensis and the dandelion into superfine powder, adding the taxus chinensis powder into 95-degree alcohol, soaking for 24 hours, wherein the mass ratio of the alcohol to the taxus chinensis powder is 3:1, then mixing the cichorium intybus and the dandelion powder in proportion, adding purified water after the alcohol is evaporated, decocting for 35 minutes, filtering, and adding 6 parts of soybean isoflavone extract to obtain a traditional Chinese medicine composition liquid medicine for later use; then, under the environment of asepsis and 0 ℃, the common suction core of the non-woven fabric is soaked in the liquid medicine of the traditional Chinese medicine composition for 2 days; taking out the soaked non-woven fabric wick, and air-drying with dry air at 0 deg.C under sterile condition to obtain traditional Chinese medicine chip;
step nine: preparation of a medicine composite layer: in a sterile environment, attaching the Chinese medicinal paste obtained by distillation in the seventh step to a Chinese medicinal chip, and processing by ultraviolet irradiation to obtain a medicinal composite layer;
step ten: and sequentially superposing the upper surface layer, the medicine composite layer and the lower surface layer together, and realizing composite pressing, thereby realizing the preparation of the taxus chinensis sanitary towel.
The Chinese yew extract has obvious effects on anti-aging, human immunity improvement and free radical capture, so that the sanitary towel has better antibacterial and bacteriostatic effects, the chicory and the taraxacum contain biological protein, the stain of the effective components and the active components of the Chinese yew can be greatly increased, the anticancer drug effect of the Chinese yew is enhanced, the using amount of the Chinese yew is small under the same drug effect, the production cost can be greatly reduced, the chicory components can effectively eliminate HPV virus, and the blank of defending HPV virus in the field of female sanitary products at present is filled.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (1)
1. A Chinese yew sanitary towel and a preparation method thereof are characterized in that: the chinese yew sanitary towel includes chinese yew protection pad body, and chinese yew protection pad body includes upper surface layer, lower surface layer and sets up the medicine composite bed between upper surface layer and lower surface layer, and the medicine composite bed includes traditional chinese medicine chip and the coating of parcel traditional chinese medicine chip, and the preparation material of traditional chinese medicine chip specifically is: 4-8 parts of taxus chinensis, 4-8 parts of chicory, 4-8 parts of dandelion, 4-8 parts of soybean isoflavone, 3-6 parts of salvia miltiorrhiza bunge, 3-6 parts of semen cuscutae, 1-2 parts of safflower, 1 part of eucommia bark, 1 part of radix bupleuri, 1 part of motherwort and 1-2 parts of alcohol, wherein the medicine composite layer is prepared by the following method:
the method comprises the following steps: extracting Taxus chinensis, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain Taxus chinensis fine powder: putting 200Kg of taxus raw material into a stainless steel extraction tank with the volume of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, feeding the feed liquid into a decompression solvent recoverer, and recovering the alcohol at the negative pressure of 60 ℃; adding purified water to adjust the density of the feed liquid to 1, and allowing the feed liquid to enter column chromatography for adsorption at a flow rate of 3 cubic meters per hour; eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step two: externally purchasing soybean isoflavone fine powder with the effective component content of 80 percent: purchasing soybean isoflavone with 80% of effective component content, oven drying, and pulverizing into superfine powder;
step three: extracting Saviae Miltiorrhizae radix, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain Saviae Miltiorrhizae radix fine powder: putting 200Kg of radix Salviae Miltiorrhizae into a stainless steel extraction tank of 3 cubic meters, extracting with 30% ethanol as extraction medium at 60 deg.C under stirring for 1 hr, recovering ethanol from the feed liquid in a decompression solvent recoverer at 60 deg.C under negative pressure; adding purified water to adjust the density of the feed liquid to 1, and allowing the feed liquid to enter column chromatography for adsorption at a flow rate of 3 cubic meters per hour; eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step four: extracting semen Cuscutae, separating by column chromatography to obtain semen Cuscutae fine powder with effective component content of 80%, drying, and pulverizing to obtain semen Cuscutae fine powder: putting 200Kg of dodder raw material into a stainless steel extraction tank with the volume of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, putting the feed liquid into a decompression solvent recoverer, and recovering the alcohol at the negative pressure of 60 ℃; adding purified water to adjust the density of the feed liquid to 1, and allowing the feed liquid to enter column chromatography for adsorption at a flow rate of 3 cubic meters per hour; eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step five: extracting safflower, separating by column chromatography to obtain 80% effective component, drying, and pulverizing to obtain fine powder of safflower: putting 200Kg of safflower raw material into a stainless steel extraction tank with the volume of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃ under stirring at intervals (20 minutes) for 1 hour, feeding the feed liquid into a decompression solvent recoverer, and recovering alcohol at the negative pressure of 60 ℃; adding purified water to adjust the density of the feed liquid to 1, and allowing the feed liquid to enter column chromatography for adsorption at a flow rate of 3 cubic meters per hour; eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step six: extracting a mixture of eucommia bark, bupleurum and motherwort, wherein the content of effective components is 80%, drying and crushing to obtain mixture fine powder of the eucommia bark, the bupleurum and the motherwort: putting 300Kg of mixture raw materials of 100Kg of eucommia bark, bupleurum and motherwort into a stainless steel extraction tank of 3 cubic meters, taking 30% alcohol as an extraction medium, extracting at 60 ℃, stirring and extracting for 1 hour at intervals (20 minutes), putting feed liquid into a decompression solvent recoverer, and recovering alcohol at the negative pressure of 60 ℃; adding purified water to adjust the density of the feed liquid to 1, and allowing the feed liquid to enter column chromatography for adsorption at a flow rate of 3 cubic meters per hour; eluting with 24% alcohol at a flow rate of 1 cubic meter per hour for 3 hours to remove impurities, then eluting with 70% alcohol at a flow rate of 1 cubic meter per hour for 1 hour, introducing the eluate into a reduced-pressure solvent recoverer, recovering alcohol at a negative pressure of 60 ℃, introducing the residual product-containing liquid into a spray drying tower to dry to obtain a product, analyzing the effective content by liquid chromatography, calculating the mixing amount of each batch of products according to the effective content of 80%, and mixing in a stainless steel mixer for 10 minutes to obtain a standard product with the effective content of 80%;
step seven: preparing a traditional Chinese medicine paste: dissolving 6 parts of taxus chinensis extract, 3 parts of salvia miltiorrhiza extract, 3 parts of semen cuscutae extract, 1 part of safflower extract, 3 parts of eucommia bark, radix bupleuri and motherwort mixed extract in 30% alcohol dissolving solution which is 10 times of the weight of all the traditional Chinese medicine extracts, stirring for 20 minutes, putting the dissolving solution into a decompression solvent recoverer, recovering alcohol at the negative pressure of 60 ℃, and concentrating the traditional Chinese medicine dissolving solution into paste (the density is 1.7) to form a preparation raw material of a coating layer;
step eight: preparing a traditional Chinese medicine chip: respectively drying chicory, taxus chinensis and dandelion, crushing and grinding the chicory, the taxus chinensis and the dandelion into superfine powder, adding the taxus chinensis powder into 95-degree alcohol, soaking for 24 hours, wherein the mass ratio of the alcohol to the taxus chinensis powder is 3:1, then mixing the cichorium chinensis and the dandelion powder in proportion, adding purified water after the alcohol is evaporated, decocting for 35-40 minutes, filtering, and adding 6 parts of soybean isoflavone extract to obtain a traditional Chinese medicine composition liquid medicine for later use; then, under the environment of aseptic temperature of 0-10 ℃, the common suction core of the non-woven fabric is soaked in the liquid medicine of the traditional Chinese medicine composition for 2-3 days; taking out the soaked non-woven fabric wick, and air-drying with dry air at 0-10 deg.C under sterile condition to obtain traditional Chinese medicine chip;
step nine: preparation of a medicine composite layer: in a sterile environment, attaching the Chinese medicinal paste obtained by distillation in the seventh step to a Chinese medicinal chip, and processing by ultraviolet irradiation to obtain a medicinal composite layer;
step ten: and sequentially superposing the upper surface layer, the medicine composite layer and the lower surface layer together, and realizing composite pressing, thereby realizing the preparation of the taxus chinensis sanitary towel.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113133870A (en) * | 2021-04-14 | 2021-07-20 | 王游 | Chinese yew sanitary towel and preparation method thereof |
| CN113577367A (en) * | 2021-08-13 | 2021-11-02 | 东莞市金保利卫生用品有限公司 | Sanitary towel for recuperating and detoxifying and preparation method thereof |
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| CN102335454A (en) * | 2011-09-29 | 2012-02-01 | 胡红节 | Sanitary napkin, toilet paper or care wings containing Taxus chinensis and preparing methods thereof |
| CN107281536A (en) * | 2017-08-17 | 2017-10-24 | 成都市梦之城农业开发有限公司 | A kind of wick for being used for sanitary napkin and protection pad and preparation method thereof |
| CN109701067A (en) * | 2019-03-12 | 2019-05-03 | 大连桃花传媒有限公司 | Chinese yew negative ion dysmenorrhea pad |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102335454A (en) * | 2011-09-29 | 2012-02-01 | 胡红节 | Sanitary napkin, toilet paper or care wings containing Taxus chinensis and preparing methods thereof |
| CN107281536A (en) * | 2017-08-17 | 2017-10-24 | 成都市梦之城农业开发有限公司 | A kind of wick for being used for sanitary napkin and protection pad and preparation method thereof |
| CN109701067A (en) * | 2019-03-12 | 2019-05-03 | 大连桃花传媒有限公司 | Chinese yew negative ion dysmenorrhea pad |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113133870A (en) * | 2021-04-14 | 2021-07-20 | 王游 | Chinese yew sanitary towel and preparation method thereof |
| CN113577367A (en) * | 2021-08-13 | 2021-11-02 | 东莞市金保利卫生用品有限公司 | Sanitary towel for recuperating and detoxifying and preparation method thereof |
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Application publication date: 20201208 |