CN112022758A - Lipstick and preparation method thereof - Google Patents

Lipstick and preparation method thereof Download PDF

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Publication number
CN112022758A
CN112022758A CN202011003644.8A CN202011003644A CN112022758A CN 112022758 A CN112022758 A CN 112022758A CN 202011003644 A CN202011003644 A CN 202011003644A CN 112022758 A CN112022758 A CN 112022758A
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parts
paste
paste body
lipstick
mixture
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方锦寿
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Guangzhou Qianzhi Herbal Cosmetics Co ltd
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Guangzhou Qianzhi Herbal Cosmetics Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9755Gymnosperms [Coniferophyta]
    • A61K8/9767Pinaceae [Pine family], e.g. pine or cedar
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06Lipsticks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)

Abstract

The application relates to the field of cosmetics, and particularly discloses lipstick and a preparation method thereof. The lipstick comprises a first paste body and a second paste body, wherein the length of the first paste body is consistent with that of the second paste body, the first paste body and the second paste body are bonded together along the length direction, and the surfaces of the first paste body and the second paste body which are bonded with each other are overlapped; the first paste comprises: the first coloring agent, rosin extract, hydrogenated castor oil dimer linoleate, di-diglycerol polyacyl adipate-2, an emulsifying agent, deionized water and a plasticizer; the second paste comprises: a second colorant, rosin extract, hydrogenated castor oil dimer linoleate, di-diglycerol polyacyl adipate-2, an emulsifier, deionized water and a plasticizer. The lipstick has the advantages of excellent moistening degree, difficult color fading and three colors in one tube.

Description

Lipstick and preparation method thereof
Technical Field
The application relates to the technical field of cosmetics, in particular to lipstick and a preparation method thereof.
Background
In recent years, with the increasing demand for cosmetics, lipstick as a common cosmetic has been improved, and high demands have been made on color types, color fastness, moisture, safety, and the like.
The color fastness and the moistening degree are a pair of contradictory combinations, the lipstick with high moistening degree has poor color fastness because the content of the emollient is higher, if the color fastness is required to be ensured to be better, the amount of the emollient is greatly reduced, but at the same time, the moistening degree of the lipstick is reduced, so that the phenomena of fine lines, dry peeling and the like are caused by the loss of water of lips.
In order to improve the moistening degree and the color fastness of lipstick on the market, functional emollients can be added, the functional emollients can bring a certain color fixing effect, in order to make the color fastness better, multiple functional emollients are generally considered to be compounded, but the compounding of different functional emollients can not always achieve the positive superposition effect, and the condition that the color fastness is reduced or basically unchanged can exist, so that the lipstick which has better moistening degree and color fastness on the market is not too much, the requirements of consumers are difficult to meet, and the improvement space is provided.
Disclosure of Invention
To the not enough that prior art exists, one of the purpose of this application is to provide a lipstick, its effect that has better moist degree and colour fastness simultaneously.
In view of the deficiencies of the prior art, another object of the present application is to provide a method for preparing a lipstick having the effect that three colors can be used together.
One of the above objects of the present invention is achieved by the following technical solutions:
a lipstick, characterized in that: the paste comprises a first paste body and a second paste body, wherein the length of the first paste body is consistent with that of the second paste body, the first paste body and the second paste body are bonded together along the length direction, and the surfaces of the first paste body and the second paste body which are bonded with each other are overlapped;
the first paste comprises the following components in parts by mass: 3-4 parts of a first coloring agent; 5-7 parts of rosin extract; 2.5-3.5 parts of hydrogenated castor oil dimer linoleate; 24-6 parts of di-diglycerol polyacyladipate; 1-1.5 parts of an emulsifier; 7-9 parts of a plasticizer; 6-8 parts of deionized water.
The second paste comprises the following components in parts by mass: 2-3 parts of a second colorant; 5-7 parts of rosin extract; 2.5-3.5 parts of hydrogenated castor oil dimer linoleate; 24-6 parts of di-diglycerol polyacyladipate; 1-1.5 parts of an emulsifier; 7-9 parts of a plasticizer; 6-8 parts of deionized water.
By adopting the technical scheme, the moistening degree of the lipstick is better by adding the rosin extracting solution, and the coloring agent in the lipstick is better wrapped in the crystal formed by the terpenoid through the terpenoid in the rosin extracting solution, so that the lipstick is not easy to fade, and has better moistening degree and color fastness.
The moisturizing degree of the lipstick is good by adding the hydrogenated castor oil dilinoleate and adding the hydrogenated castor oil dilinoleate, an oil wax structure formed by the hydrogenated castor oil dilinoleate contains grease and a coloring agent to form a DA-L wrapping framework, and the space structure is maintained by crystallization, so that the pigment is not easy to migrate out of the framework, and the lipstick has good moisturizing degree and color fastness.
By adding the di-diglycerol polyacyladipate-2, the di-diglycerol polyacyladipate-2 has high water locking property, excellent skin adhesion and smooth feeling, so that the lipstick has better moisturizing effect and skin feeling in use.
Through the matching of the rosin extract, the hydrogenated castor oil dimer linoleate and the di-diglycerol polyacyl adipate-2, the lipstick has more excellent moistening degree, the inhibiting effect of the rosin extract and the hydrogenated castor oil dimer linoleate on the color fastness is relieved by the di-diglycerol polyacyl adipate-2, the color fastness of the lipstick is also improved, and the lipstick is not easy to fade while having better moistening degree.
The present application may be further configured in a preferred example to: the paint also comprises the following components in parts by mass:
the first paste body and the second paste body respectively comprise the following components in parts by mass: 9-12 parts of an adhesive;
by adopting the technical scheme, the components in the lipstick are well bonded together by adding the adhesive, so that the components in the lipstick are not easy to scatter, and the pressure resistance of the lipstick is improved.
The present application may be further configured in a preferred example to: the paint also comprises the following components in parts by mass:
the first paste body and the second paste body respectively comprise the following components in parts by mass: 20-23 parts of a spreading agent;
by adopting the technical scheme, the ductility of the lipstick is better by adding the ductility agent, so that the lipstick is easy to push away in the using process.
The present application may be further configured in a preferred example to: the paint also comprises the following components in parts by mass:
the first paste body and the second paste body respectively comprise the following components in parts by mass: 3-5 parts of a skin conditioner.
By adopting the technical scheme, the skin conditioner can remove free radicals to a certain degree, so that the lipstick has better oxidation resistance, and the skin on the lips is not easy to become dull under ultraviolet rays.
The present application may be further configured in a preferred example to: the paint also comprises the following components in parts by mass:
the first paste body and the second paste body respectively comprise the following components in parts by mass: 10-12 parts of a humectant.
By adopting the technical scheme, the moisturizing agent is added, so that the skin absorbs moisture from a humid environment, the water content of the surface of the lips is improved, and the dry state of the lips is improved.
The present application may be further configured in a preferred example to: the paint also comprises the following components in parts by mass:
the first paste body and the second paste body respectively comprise the following components in parts by mass: 0.08-0.14 part of aromatizer.
By adopting the technical scheme, the flavor of the oil and fat composition in the lipstick is covered by adding the aromatizer, so that the lipstick has better smell.
The second purpose of the application is realized by the following technical scheme:
the preparation method of the lipstick comprises the following steps:
step 1), preparing a first paste specifically comprises:
step 1-1), adding a rosin extracting solution, hydrogenated castor oil dimer linoleate, di-diglycerol polyacyl adipate, an emulsifier and a plasticizer into part of deionized water, wherein the part of deionized water accounts for 20% -30% of the total amount of the deionized water, heating to 60-70 ℃ while stirring, and stirring until the mixture is uniformly mixed to obtain a first mixture;
step 1-2), adding the first colorant into the rest 70% -80% of deionized water, heating to 80-90 ℃ while stirring, and uniformly stirring to obtain a second mixture;
step 1-3), cooling the first mixture and the second mixture to 35-45 ℃, and uniformly stirring to obtain a first composition;
and 1-4), injecting the first composition into a mold for cooling and molding, wherein a partition plate which divides the inner space of the mold into two containing cavities and extends along the length direction is arranged inside the mold, and adding the first composition into one containing cavity of the mold to obtain a first paste.
Step 2), the preparation of the second paste specifically comprises:
step 2-1), adding the rosin extract, hydrogenated castor oil dimer linoleate, di-diglycerol polyacyl adipate, an emulsifier and a plasticizer into partial deionized water, wherein the partial deionized water accounts for 20% -30% of the total amount of the deionized water, heating to 60-70 ℃ while stirring, and uniformly stirring to obtain a third mixture;
step 2-2), adding the second colorant into the residual 70% -80% of deionized water, heating to 80-90 ℃ while stirring, and stirring until the mixture is uniformly mixed to obtain a fourth mixture;
step 2-3), cooling the third mixture and the fourth mixture to 35-45 ℃, and uniformly stirring to obtain a second composition;
step 2-4), taking down the partition plate, adding the second composition into the other accommodating cavity of the mold, and cooling and molding to obtain a second paste;
step 3), demolding the first paste body and the second paste body which are bonded together to obtain the lipstick;
the step 1) and the step 2) are not performed in sequence and are not performed at the same time.
By adopting the technical scheme, the heating temperature in the step 1-1) and the step 2-1) is 60-70 ℃, so that the activity of each oil and fat component in the lipstick is not easy to damage.
The heating temperature in the step 1-2) and the step 2-2) is 80-90 ℃, so that the activity of the colorant in the lipstick is not easily damaged, and the lipstick is better developed.
The temperature is reduced to 35-45 ℃ through the steps 1-3) and 2-3), so that the mixture is mixed together more stably.
The first paste and the second paste are shaped by cooling and forming in the steps 1-4) and 2-4).
Demolding is carried out in the step 3), so that the complete three-color lipstick is obtained.
The present application may be further configured in a preferred example to: cetyl ethyl hexanoate, ethylhexyl palmitate, tridecyl trimellitate, candelilla wax, ceresin B, polyisobutylene and triisodecyl trimellitate are respectively added in the step 1-1) and the step 2-1), and are heated to 60-70 ℃ while stirring, and are uniformly stirred;
in the step 1-2) and the step 2-2), a humectant is respectively added, and the mixture is heated to 80-90 ℃ while stirring, and is uniformly stirred;
in the step 1-3) and the step 2-3), phenoxyethanol and an excipient are respectively added after the temperature is reduced to 35-45 ℃, and the mixture is stirred uniformly.
By adopting the technical scheme, the heating temperature in the step 1-2) and the step 2-2) is 80-90 ℃, so that the activity of each component in the lipstick is not easy to damage.
The temperature is reduced to 35-45 ℃ through the steps 1-3) and 2-3), so that the mixture is mixed together more stably.
In summary, the present application has the following beneficial effects:
1. the inhibition effect between the rosin extract and the hydrogenated castor oil dimer linoleate on the aspect of color fastness is relieved through the di-diglycerol polyacyl adipate-2, the color fastness of the lipstick is also improved, and the lipstick is not easy to fade while the moistening degree is improved.
2. By adding cetyl ethyl hexanoate, ethylhexyl palmitate and tridecyl trimellitate, the lipstick has better ductility, and is easy to push away in the using process.
3. By adding the skin conditioner, the skin conditioner can remove free radicals to a certain degree, so that the lipstick has better oxidation resistance, and lips are not easy to become dull.
Detailed Description
The present application will be described in further detail with reference to examples.
The information on the source of the main raw material components in the following examples and comparative examples is shown in Table 1
TABLE 1
Figure BDA0002695159900000071
Figure BDA0002695159900000081
Examples 1 to 3:
a lipstick comprises a first paste body and a second paste body, wherein the length of the first paste body is consistent with that of the second paste body, the first paste body and the second paste body are bonded together along the length direction, and the surfaces of the first paste body and the second paste body which are bonded with each other are overlapped;
the first paste is prepared from the following components:
the composition comprises rosin extracting solution, hydrogenated castor oil dilinoleate, di-diglycerol polyacyl adipate-2, an emulsifier, a first colorant, a plasticizer and deionized water.
The second paste is prepared from the following components:
the composition comprises rosin extract, hydrogenated castor oil dilinoleate, di-diglycerol polyacyl adipate-2, an emulsifier, a plasticizer, a second colorant and deionized water.
The emulsifier in the first ointment and the emulsifier in the second ointment are both compounded by cetyl polyethylene glycol/polypropylene glycol-10/polydimethylsiloxane and cetyl polyethylene glycol.
The plasticizer in the first paste body and the plasticizer in the second paste body are both compounded by beeswax and polyethylene wax.
The first colorant and the second colorant are compounded by orange 501, red 104-1, red 102-1 and water-soluble black powder, and the compounding ratio of the first colorant to the second colorant is different.
In examples 1-3, the amounts (in Kg) of the ingredients of the first and second pastes are detailed in Table 2
TABLE 2
Figure BDA0002695159900000091
Figure BDA0002695159900000101
The process for preparing the lipsticks of examples 1-3 includes the steps of:
step 1), preparing a first paste, specifically comprising:
step 1-1), adding a rosin extracting solution, hydrogenated castor oil dimer linoleate, di-diglycerol polyacyladipate, cetyl polyethylene glycol/polypropylene glycol-10/polydimethylsiloxane and part of deionized water into a first stirring kettle, wherein the part of deionized water accounts for 25% of the total amount of the deionized water, the rotating speed is 80r/min, heating to 65 ℃ while stirring, and stirring for 20 minutes to obtain a first mixture;
step 1-2), adding the remaining 75% of deionized water and the first colorant into a second stirring kettle at a rotating speed of 100r/min, heating to 85 ℃ while stirring, and stirring for 25 minutes to obtain a second mixture;
step 1-3), naturally cooling the first mixture and the second mixture to 40 ℃, adding the first mixture into a second stirring kettle, rotating at the speed of 80r/min, and stirring for 20 minutes to obtain a first composition;
step 1-4), injecting the first composition into a mold for cooling and molding, wherein a partition plate which divides the inner space of the mold into two containing cavities and extends along the length direction is arranged inside the mold, adding the first composition into one containing cavity of the mold, and cooling to-8 ℃ on a cooling table to obtain a first paste;
step 2), preparing a second paste, which specifically comprises:
step 2-1), adding the rosin extract, hydrogenated castor oil dimer linoleate, di-diglycerol polyacyladipate, cetyl polyethylene glycol/polypropylene glycol-10/polydimethylsiloxane and part of deionized water into a third stirring kettle, wherein the part of deionized water accounts for 25% of the total amount of the deionized water, the rotating speed is 80r/min, heating to 65 ℃ while stirring, and stirring for 20 minutes to obtain a third mixture;
step 2-2), adding the remaining 75% of deionized water and the second colorant into a fourth stirring kettle at a rotating speed of 100r/min, heating to 85 ℃ while stirring, and stirring for 25 minutes to obtain a fourth mixture;
step 2-3), naturally cooling the third mixture and the fourth mixture to 40 ℃, adding the third mixture into a fourth stirring kettle, rotating at the speed of 80r/min, and stirring for 20 minutes to obtain a second composition;
step 2-4), taking down the partition plate of the mold, adding the second composition into the other accommodating cavity of the mold, and cooling to-8 ℃ on a cooling table to obtain a second paste;
and 3) demolding the first paste body and the second paste body which are bonded together to obtain the lipstick.
Example 4
A lipstick, which differs from example 2 only in that:
in step 1-1), the mixture is heated to 70 ℃ while stirring, and stirred for 25 minutes.
In the step 1-2), the mixture is heated to 90 ℃ while stirring, and stirred for 30 minutes.
In the step 1-3), the mixture is naturally cooled to 50 ℃, stirred for 30 minutes and then cooled to-5 ℃.
In step 2-1), the mixture is heated to 60 ℃ while stirring, and stirred for 15 minutes.
In step 2-2), the mixture is heated to 80 ℃ while stirring, and stirred for 20 minutes.
In the step 2-3), the mixture is naturally cooled to 40 ℃.
In step 2-4), cooling to-10 ℃.
Example 5
A lipstick, differing from example 6 only in that:
in step 1-1), the mixture is heated to 70 ℃ while stirring, and stirred for 25 minutes.
In the step 1-2), the mixture is heated to 90 ℃ while stirring, and stirred for 30 minutes.
In the step 1-3), the mixture is naturally cooled to 50 ℃, stirred for 30 minutes and then cooled to-5 ℃.
In step 2-1), the mixture is heated to 60 ℃ while stirring, and stirred for 15 minutes.
In step 2-2), the mixture is heated to 80 ℃ while stirring, and stirred for 20 minutes.
In the step 2-3), the mixture is naturally cooled to 40 ℃.
In step 2-4), cooling to-10 ℃.
Examples 6 to 8
A lipstick, which differs from example 2 only in that: the components of the first paste and the second paste also each include a binder.
The adhesive of the first paste body and the second paste body is the compound of candelilla wax, ceresin B and polyisobutylene.
In examples 6 to 8, the amounts (in Kg) of the respective components added are specified in Table 3
TABLE 3
Figure BDA0002695159900000131
Candelilla wax, ceresin B and polyisobutylene were added to the first stirred tank together with the rosin extract in step 1-1) and step 2-1).
Examples 9 to 11
Compared with example 2, the difference is only that: the components of the first paste and the second paste respectively comprise pentaerythritol tetraisostearic acid and phytosterol ester.
In examples 9 to 11, the amounts (in Kg) of the respective components added are specified in Table 4
TABLE 4
Figure BDA0002695159900000132
Pentaerythritol tetraisostearic acid and phytosterol ester are added into a first stirring kettle together with the rosin extract in the step 1-1) and the step 2-1).
Examples 12 to 14
A lipstick, which differs from example 2 only in that: the components of the first paste and the second paste respectively comprise a ductility agent.
The extending agent of the first paste and the second paste is the compound of cetyl ethyl hexanoate, ethylhexyl palmitate and tridecyl trimellitate.
In examples 12 to 14, the amounts (in Kg) of the respective components added are specified in Table 5
TABLE 5
Figure BDA0002695159900000141
Cetyl ethylhexanoate, ethylhexyl palmitate and tridecyl trimellitate were added to the first stirred tank in step 1-1) and step 2-1) together with the rosin extract.
Examples 15 to 17
A lipstick, which differs from example 2 only in that: the components of the first paste and the second paste respectively comprise an adhesive, pentaerythritol tetraisostearate, phytosterol ester, an extending agent, a skin conditioner, a humectant, a preservative and an aromatizer.
The adhesive of the first paste body and the second paste body is the compound of candelilla wax, ceresin B and polyisobutylene.
The extending agent of the first paste and the second paste is the compound of cetyl ethyl hexanoate, ethylhexyl palmitate and tridecyl trimellitate.
The skin conditioning agent of the first ointment and the second ointment is triisodecanol trimellitate.
The humectants of the first paste body and the second paste body are both compounded of glycerol and propylene glycol.
The preservatives of the first paste body and the second paste body are compounded by methyl ester, propyl ester and phenoxyethanol.
The flavoring agents of the first paste and the second paste are Vanilla HS-2116.
In examples 15 to 17, the amounts (in Kg) of the respective components added are specified in Table 6
TABLE 6
Figure BDA0002695159900000151
Figure BDA0002695159900000161
Candelilla wax, ceresin B, polyisobutylene, pentaerythritol tetraisostearic acid, phytosterol ester, cetyl ethyl hexanoate, ethylhexyl palmitate, tridecyl trimellitate, triisodecyl trimellitate, methyl ester, propyl ester, glycerol, propylene glycol in step 1-1) and step 2-1) are added to a first stirred tank together with the rosin extract.
Adding phenoxyethanol and vanilla HS-2116 into the second stirring kettle together with the first mixture in the steps 1-3) and 2-3).
Comparative example 1
A lipstick, which differs from example 2 only in that: step 1-1) and step 2-1), beeswax and polyethylene wax are mixed according to the proportion of 1:1 and then equivalently replace the rosin extract, the di-diglycol polyacyladipate-2 and the hydrogenated castor oil dimer linoleate.
Comparative example 2
A lipstick, which differs from example 2 only in that: step 1-1) and step 2-1), beeswax and polyethylene wax are mixed according to the proportion of 1:1 and then are equivalently used for replacing the diglycerol polyacyladipate-2 and the hydrogenated castor oil dimer linoleate.
Comparative example 3
A lipstick, which differs from example 2 only in that: in the step 1-1) and the step 2-1), beeswax and polyethylene wax are mixed according to the proportion of 1:1 and then replace the rosin extract and the di-diglycerol polyacyladipate-2 in equal amount.
Comparative example 4
A lipstick, which differs from example 2 only in that: in the step 1-1) and the step 2-1), beeswax and polyethylene wax are mixed according to the proportion of 1:1 and then replace the rosin extract and the hydrogenated castor oil dimer linoleate in equal amount.
Comparative example 5
A lipstick, which differs from example 2 only in that: in the step 1-1) and the step 2-1), beeswax and polyethylene wax are mixed according to the proportion of 1:1 and then replace the diglycerol polyacyladipate-2 by equal amount.
Comparative example 6
A lipstick, which differs from example 2 only in that: in the step 1-1) and the step 2-1), beeswax and polyethylene wax are mixed according to the proportion of 1:1 and then are equivalently used for replacing hydrogenated castor oil dimer linoleate.
Comparative example 7
A lipstick, which differs from example 2 only in that: in the step 1-1) and the step 2-1), beeswax and polyethylene wax are mixed according to the proportion of 1:1, and then the equal amount of the mixture replaces the turpentine extracting solution.
Experiment 1
The safety performance of the lipsticks prepared in each example and comparative example was examined according to technical specifications for cosmetic safety (2015 edition). The data for the partial detection of microorganisms are detailed in Table 7:
TABLE 7
Figure BDA0002695159900000171
Figure BDA0002695159900000181
According to the detection data in table 7, the safety performance detection of the lipsticks prepared in examples 1 to 17 and comparative examples 1 to 7 both meet the standard requirements, and are not easy to cause harm to human bodies.
Experiment 2
The moisturizing and moisturizing effects of the lipstick prepared in each example and each comparative example are detected according to QB/T4256-2011 evaluation guidance for moisturizing efficacy of cosmetics in the light industry.
The test method comprises the following steps: 72 healthy volunteers were randomly selected, aged 20-50 years, and divided into 24 groups at random, each group consisting of 3 persons, and then lipsticks prepared in the examples and comparative examples of the present invention were tested correspondingly, and the lipsticks prepared in the examples and comparative examples were applied to the lips of the subjects respectively at a constant temperature (22. + -. 2 ℃ C.) and a relative humidity of 50. + -. 5% in an amount of 7. + -. 0.1) mg, and simultaneously tested, and the moisture content of the skin was tested at 2h, 4h, 6h, and 8h after the application of the lipsticks prepared in the examples and comparative examples respectively, and the evaluation results were expressed as the average value of the hydration. The assay data are detailed in table 8:
TABLE 8
Figure BDA0002695159900000182
Figure BDA0002695159900000191
Figure BDA0002695159900000201
According to the comparison of the data of comparative example 5 and comparative examples 2 and 3 in table 8, the degree of hydration is reduced significantly by adding the rosin extract and the hydrogenated castor oil dilinoleate, which indicates that the rosin extract, the hydrogenated castor oil dilinoleate, has a synergistic effect on the degree of moisturizing, and has a moisturizing effect on lips, so that the lipstick is more moisturizing.
According to the comparison of the data of comparative example 6 and comparative examples 2 and 4 in table 8, the degree of hydration is reduced significantly by adding the rosin extract and the di-diglycerol polyacyladipate-2, which indicates that the rosin extract and the di-diglycerol polyacyladipate-2 have a synergistic effect on the degree of moisturizing, and have the effects of moisturizing lips, so that the lipstick is more moisturizing.
According to the comparison of the data of comparative example 7, comparative example 3 and comparative example 4 in table 8, the degree of hydration is reduced significantly by adding the hydrogenated castor oil dilinoleate and the bis-diglycerol polyacyladipate-2, which indicates that the hydrogenated castor oil dilinoleate and the bis-diglycerol polyacyladipate-2 play a synergistic role in moisturizing the lips, and have the effect of moisturizing the lips, so that the lipstick is more moist.
According to the comparison of the data of examples 1 to 3 and comparative examples 2 to 4 in table 8, the degree of hydration is reduced significantly by adding the rosin extract, the hydrogenated castor oil dilinoleate and the bis-diglycerol polyacyladipate-2, which indicates that the rosin extract, the hydrogenated castor oil dilinoleate and the bis-diglycerol polyacyladipate-2 play a synergistic role in moisturizing the lips and have moisturizing effect on the lips, so that the lipstick is more moisturizing.
According to the comparison of the data of examples 9-11 and example 2 in Table 8, the degree of hydration decreases with the addition of pentaerythritol tetraisostearate and phytosterol ester, indicating that pentaerythritol tetraisostearate and phytosterol ester have the moisturizing effect, so that the lipstick is more moist.
Experiment 3
72 healthy volunteers aged 20-50 years were randomly selected, and divided into 24 groups of 3, and then lipsticks prepared in the examples and comparative examples were tested correspondingly, and applied to the lips of the subjects in an amount of (7. + -. 0.1mg) in a constant temperature environment (26. + -.1 ℃ C.), after standing for 2 hours, test papers were pressed against the lips of the volunteers under a pressure of 0.1N, L values of the test papers after pressing were measured by a color difference meter three times, and the evaluation results were expressed as an average value of L values for each time. The data are shown in Table 9:
TABLE 9
Figure BDA0002695159900000211
Figure BDA0002695159900000221
As can be seen from comparison of the data of comparative example 2 with that of comparative example 1 in Table 9, the L value becomes larger by adding the rosin extract, indicating that the color fastness of the rosin extract to lipstick is improved, so that lipstick is not easily discolored.
As can be seen from comparison of the data of comparative example 3 with that of comparative example 1 in Table 9, the L value becomes larger by adding the hydrogenated castor oil dilinoleate, which shows that the color fastness of the hydrogenated castor oil dilinoleate to lipstick is improved, so that lipstick is not easily faded.
As can be seen from the comparison of the data of comparative example 4 with that of comparative example 1 in Table 9, the L value is substantially unchanged by the addition of bis-diglycerol polyacyladipate 2, indicating that bis-diglycerol polyacyladipate 2 does not adversely affect the color fastness of lipstick.
According to the comparison of the data of comparative example 5 and comparative examples 2 and 3 in table 9, the L value of the hydrogenated castor oil dilinoleate and the pine resin extract added is larger than that of the hydrogenated castor oil dilinoleate added alone but smaller than that of the pine resin extract added alone, which shows that the hydrogenated castor oil dilinoleate has an inhibiting effect on the pine resin extract in improving the color fastness of lipstick, so that the color fastness of lipstick is deteriorated, and the lipstick is more likely to fade.
As can be seen from comparison of the data of comparative example 6 and comparative example 2 in Table 9, the L value is substantially unchanged by the addition of bis-diglycerol polyacyladipate 2, indicating that the effect of bis-diglycerol polyacyladipate 2 on the improvement of the color fastness to lipstick of the rosin extract is small.
As can be seen from comparison of the data in Table 9 in comparative example 7 with that in comparative example 3, the L value is substantially unchanged by the addition of bis-diglycerol polyacyladipate 2, indicating that the effect of bis-diglycerol polyacyladipate 2 on the improvement of the lipstick fastness is small.
As can be seen from comparison of the data of examples 1 to 3 with comparative example 5 in Table 9, the addition of bis-diglycerol polyacyladipate 2 resulted in an increase in L value, indicating that bis-diglycerol polyacyladipate 2 alleviated the mutual inhibition between the rosin extract and the hydrogenated castor oil dilinoleate, and that a synergistic effect was exhibited between the rosin extract and the hydrogenated castor oil dilinoleate, resulting in more excellent color fastness of lipstick.
As can be seen from a comparison of the data from examples 6 to 8 and example 2 in Table 9, the addition of candelilla wax, ceresin B and polyisobutene results in substantially unchanged L values, indicating that candelilla wax, ceresin B and polyisobutene have no negative effect on the fastness to redness.
As can be seen from a comparison of the data in Table 9 for examples 9-11 with example 2, the addition of pentaerythritol tetraisostearate and phytosterol ester resulted in a substantially unchanged L value, indicating that pentaerythritol tetraisostearate and phytosterol ester did not have a negative effect on the fastness to redness.
As can be seen from a comparison of the data from examples 15 to 17 and example 2 in Table 9, with the addition of candelilla wax, ceresin B, polyisobutylene, pentaerythritol tetraisostearate, phytosterol esters, cetyl ethylhexanoate, ethylhexyl palmitate, tridecyl trimellitate, triisodecyl trimellitate, glycerol, propylene glycol, methyl ester, propyl ester, phenoxyethanol, and vanilla HS-2116, the L values are essentially unchanged, indicating that the combination of these ingredients does not have a negative effect on the fastness to redness.
The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.

Claims (8)

1. A lipstick, characterized in that: the paste comprises a first paste body and a second paste body, wherein the length of the first paste body is consistent with that of the second paste body, the first paste body and the second paste body are bonded together along the length direction, and the surfaces of the first paste body and the second paste body which are bonded with each other are overlapped;
the first paste comprises the following components in parts by mass:
3-4 parts of a first coloring agent;
5-7 parts of rosin extract;
2.5-3.5 parts of hydrogenated castor oil dimer linoleate;
24-6 parts of di-diglycerol polyacyladipate;
1-1.5 parts of an emulsifier;
7-9 parts of a plasticizer;
6-8 parts of deionized water;
the second paste comprises the following components in parts by mass:
2-3 parts of a second colorant;
5-7 parts of rosin extract;
2.5-3.5 parts of hydrogenated castor oil dimer linoleate;
24-6 parts of di-diglycerol polyacyladipate;
1-1.5 parts of an emulsifier;
7-9 parts of a plasticizer;
6-8 parts of deionized water.
2. A lipstick according to claim 1 wherein:
the first paste body and the second paste body respectively comprise the following components in parts by mass:
9-12 parts of an adhesive.
3. A lipstick according to claim 1 wherein:
the first paste body and the second paste body respectively comprise the following components in parts by mass:
20-23 parts of a spreading agent.
4. A lipstick according to claim 1 wherein: the first paste body and the second paste body respectively comprise the following components in parts by mass:
3-5 parts of a skin conditioner.
5. A lipstick according to claim 1 wherein: the first paste body and the second paste body respectively comprise the following components in parts by mass:
10-12 parts of a humectant.
6. A lipstick according to claim 1 wherein: the first paste body and the second paste body respectively comprise the following components in parts by mass:
0.08-0.14 part of aromatizer.
7. The process for producing a lipstick according to claim 1, characterized in that:
step 1), preparing a first paste specifically comprises:
step 1-1), adding a rosin extracting solution, hydrogenated castor oil dimer linoleate, di-diglycerol polyacyl adipate, an emulsifier and a plasticizer into part of deionized water, wherein the part of deionized water accounts for 20% -30% of the total amount of the deionized water, heating to 60-70 ℃ while stirring, and stirring until the mixture is uniformly mixed to obtain a first mixture;
step 1-2), adding the first colorant into the rest 70% -80% of deionized water, heating to 80-90 ℃ while stirring, and uniformly stirring to obtain a second mixture;
step 1-3), cooling the first mixture and the second mixture to 35-45 ℃, and uniformly stirring to obtain a first composition;
step 1-4), injecting the first composition into a mold for cooling and molding, wherein a partition plate which divides the inner space of the mold into two containing cavities and extends along the length direction is arranged inside the mold, and adding the first composition into one containing cavity of the mold to obtain a first paste;
step 2), the preparation of the second paste specifically comprises:
step 2-1), adding the rosin extract, hydrogenated castor oil dimer linoleate, di-diglycerol polyacyl adipate, an emulsifier and a plasticizer into partial deionized water, wherein the partial deionized water accounts for 20% -30% of the total amount of the deionized water, heating to 60-70 ℃ while stirring, and uniformly stirring to obtain a third mixture;
step 2-2), adding the second colorant into the residual 70% -80% of deionized water, heating to 80-90 ℃ while stirring, and stirring until the mixture is uniformly mixed to obtain a fourth mixture;
step 2-3), cooling the third mixture and the fourth mixture to 35-45 ℃, and uniformly stirring to obtain a second composition;
step 2-4), taking down the partition plate, adding the second composition into the other accommodating cavity of the mold, and cooling and molding to obtain a second paste;
step 3), demolding the first paste body and the second paste body which are bonded together to obtain the lipstick;
the step 1) and the step 2) are not performed in sequence and are not performed at the same time.
8. The process for producing a lipstick according to claim 7, characterized in that: cetyl ethyl hexanoate, ethylhexyl palmitate, tridecyl trimellitate, candelilla wax, ceresin B, polyisobutylene and a skin conditioner are respectively added in the step 1-1) and the step 2-1), and are heated to 60-70 ℃ while being stirred and are uniformly stirred;
in the step 1-2) and the step 2-2), respectively adding a humectant, heating to 80-90 ℃ while stirring, and stirring until the mixture is uniformly mixed;
in the step 1-3) and the step 2-3), after the temperature is reduced to 35-45 ℃, the aromatizer is respectively added and stirred uniformly.
CN202011003644.8A 2020-09-22 2020-09-22 Lipstick and preparation method thereof Pending CN112022758A (en)

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