CN112004852B - 以直链和环状脂肪族多异氰酸酯制备的核壳胶囊 - Google Patents

以直链和环状脂肪族多异氰酸酯制备的核壳胶囊 Download PDF

Info

Publication number
CN112004852B
CN112004852B CN201880092657.1A CN201880092657A CN112004852B CN 112004852 B CN112004852 B CN 112004852B CN 201880092657 A CN201880092657 A CN 201880092657A CN 112004852 B CN112004852 B CN 112004852B
Authority
CN
China
Prior art keywords
core
oil
aliphatic polyisocyanate
component
group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201880092657.1A
Other languages
English (en)
Chinese (zh)
Other versions
CN112004852A (zh
Inventor
帕特里克·奥特
科利亚·贝伦斯
蒂莫西·J·埃文斯-洛拉
约翰·M·特芬哈特
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Symrise AG
Original Assignee
Symrise AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Symrise AG filed Critical Symrise AG
Publication of CN112004852A publication Critical patent/CN112004852A/zh
Application granted granted Critical
Publication of CN112004852B publication Critical patent/CN112004852B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0039Coated compositions or coated components in the compositions, (micro)capsules
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72Polyisocyanates or polyisothiocyanates
    • C08G18/721Two or more polyisocyanates not provided for in one single group C08G18/73 - C08G18/80
    • C08G18/722Combination of two or more aliphatic and/or cycloaliphatic polyisocyanates
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/11Encapsulated compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/87Polyurethanes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00Formulations or additives for perfume preparations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • B01J13/06Making microcapsules or microballoons by phase separation
    • B01J13/14Polymerisation; cross-linking
    • B01J13/16Interfacial polymerisation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30Low-molecular-weight compounds
    • C08G18/32Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225Polyamines
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72Polyisocyanates or polyisothiocyanates
    • C08G18/73Polyisocyanates or polyisothiocyanates acyclic
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72Polyisocyanates or polyisothiocyanates
    • C08G18/74Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/75Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic
    • C08G18/758Polyisocyanates or polyisothiocyanates cyclic cycloaliphatic containing two or more cycloaliphatic rings
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/0005Other compounding ingredients characterised by their effect
    • C11D3/001Softening compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50Perfumes
    • C11D3/502Protected perfumes
    • C11D3/505Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41Particular ingredients further characterized by their size
    • A61K2800/412Microsized, i.e. having sizes between 0.1 and 100 microns
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/56Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Veterinary Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Dispersion Chemistry (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)
  • Medicinal Preparation (AREA)
CN201880092657.1A 2018-04-24 2018-04-24 以直链和环状脂肪族多异氰酸酯制备的核壳胶囊 Active CN112004852B (zh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/EP2018/060492 WO2019206404A1 (en) 2018-04-24 2018-04-24 Core-shell capsules prepared with linear and cyclic aliphatic polyisocyanates

Publications (2)

Publication Number Publication Date
CN112004852A CN112004852A (zh) 2020-11-27
CN112004852B true CN112004852B (zh) 2023-04-04

Family

ID=62063531

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201880092657.1A Active CN112004852B (zh) 2018-04-24 2018-04-24 以直链和环状脂肪族多异氰酸酯制备的核壳胶囊

Country Status (6)

Country Link
US (1) US12421480B2 (https=)
EP (1) EP3784713B1 (https=)
JP (1) JP7177855B2 (https=)
CN (1) CN112004852B (https=)
BR (1) BR112020021624B1 (https=)
WO (1) WO2019206404A1 (https=)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020164705A1 (de) * 2019-02-13 2020-08-20 Symrise Ag Verfahren zur herstellung von mikrokapseln
EP4499918A1 (en) 2022-03-30 2025-02-05 Symrise AG Paper roll as fragrance control release system
CN115008867B (zh) * 2022-04-19 2024-06-11 吴江市润升纺织有限公司 长效芳香复合织物的加工工艺及其使用方法

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1572011A (en) 1976-02-11 1980-07-23 Commw Scient Ind Res Org Bisulphite adducts of biuret-polyisocyanates
AU5960380A (en) 1979-08-30 1981-03-05 A. Ehrenreich G.m.b.H. & Co. KG Bellows seal and retaining ring
US4855490A (en) 1982-06-18 1989-08-08 Mobay Corporation Liquid polyisocyanate adduct mixtures possessing good compatibility with apolar solvents
DE3605552A1 (de) 1986-02-21 1987-08-27 Bayer Ag Hochkonzentrierte, stabile loesungen von farbbildnern
DE3622262A1 (de) 1986-07-02 1988-01-07 Bayer Ag Chromogene 3,1-benzoxazine
DE3738240A1 (de) 1987-11-11 1989-05-24 Bayer Ag Tetraindolyl-heptamethin-ether, -alkohole und farbstoffe
DE59307983D1 (de) 1992-09-30 1998-02-19 Ciba Geigy Ag Konzentrierte, wässrige Flüssigformulierungen von Farbbildnern
DE10051190A1 (de) 2000-10-16 2002-04-25 Bayer Ag Mikrokapseln mit Wänden aus Polyharnstoff
GB0221697D0 (en) 2002-09-18 2002-10-30 Unilever Plc Novel compouds and their uses
EP1958627A3 (de) 2007-01-04 2010-09-01 Symrise GmbH & Co. KG Verwendung bestimmter Menthyl-3-oxocarbonsäureester als physiologisch wirksame Kühlsubstanzen
EP2187871B1 (en) 2007-08-16 2016-04-13 Symrise AG Mixtures comprising pellitorin and uses thereof
EP2033688B1 (de) 2007-08-20 2012-10-17 Symrise AG Oxalsäurederivate und deren Verwendung als physiologische Kühlwirkstoffe
DE102008002145A1 (de) 2008-06-02 2009-12-03 Symrise Gmbh & Co. Kg Kapsel mit organisch-anorganischer Hybridwand
WO2015023961A1 (en) 2013-08-15 2015-02-19 International Flavors & Fragrances Inc. Polyurea or polyurethane capsules
US20160166480A1 (en) * 2009-09-18 2016-06-16 International Flavors & Fragrances Inc. Microcapsule compositions
ES2628087T3 (es) 2010-06-25 2017-08-01 Cognis Ip Management Gmbh Procedimiento para producir microcápsulas
EP2585034A2 (en) 2010-06-25 2013-05-01 Givaudan SA Encapsulated compositions comprising aldehyde fragrance precursors
GB201010701D0 (en) * 2010-06-25 2010-08-11 Givaudan Sa Process for producing microcapsules
EP2763749B1 (en) * 2011-10-19 2018-02-21 Rohm and Haas Company Encapsulation of personal care actives
BR112014015213A8 (pt) 2011-12-22 2017-06-13 Givaudan Sa melhoras na, ou relacionadas à encapsulação de perfumes
JP6615121B2 (ja) * 2014-04-29 2019-12-04 ビーエーエスエフ ソシエタス・ヨーロピア マイクロカプセルの製造方法
EP2954785B1 (de) 2014-06-13 2018-06-06 Symrise AG Neue Stoffmischung zur Verbesserung des Süssgeschmacks enthaltend Rubusosid oder alpha-Glycosylrubusosid
EP2979751B1 (de) 2014-07-29 2020-10-28 Symrise AG Verfahren zur herstellung von festen kühlstoffen
US10398632B2 (en) 2014-11-07 2019-09-03 Givaudan S.A. Capsule composition
WO2016144798A1 (en) * 2015-03-06 2016-09-15 International Flavors & Fragrances Inc. Microcapsule compositions with high performance
EP3170552A1 (en) * 2015-11-23 2017-05-24 Basf Se Microcapsule comprising a polymeric shell and a hydrophilic or hydrophobic core material
US9974720B2 (en) * 2015-12-30 2018-05-22 International Flavors & Fragrances Inc. Compositions containing microcapsules coated with deposition proteins
US20180015009A1 (en) * 2015-12-30 2018-01-18 International Flavors & Fragrances Inc. Microcapsule compositions with improved deposition
EP3295929A1 (en) 2016-09-19 2018-03-21 S.P.C.M. Sa Use of an ampholyte copolymer as colloidal stabilizer in a process of encapsulating fragrance

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
1,4-环己烷二异氰酸酯合成研究进展;赵博,等;《精细与专用化学品》;20041231;第14卷;第7-9页 *
Biocompatibility and hemocompatibility evaluation of polyether urethanes synthesized using DBU organocatalyst;Andere Basterretxea,等;《European Polymer Journal》;20160812;第84卷;第750-758页 *

Also Published As

Publication number Publication date
JP2021528226A (ja) 2021-10-21
WO2019206404A1 (en) 2019-10-31
JP7177855B2 (ja) 2022-11-24
EP3784713B1 (en) 2024-02-21
BR112020021624A2 (pt) 2021-01-26
BR112020021624B1 (pt) 2024-02-06
US20210238510A1 (en) 2021-08-05
EP3784713A1 (en) 2021-03-03
US12421480B2 (en) 2025-09-23
CN112004852A (zh) 2020-11-27

Similar Documents

Publication Publication Date Title
JP7809100B2 (ja) マイクロカプセルの調製プロセス
CN104918694B (zh) 香精油包囊
CN101990572B (zh) 羧酸酯作为香味物质的用途
JP7546145B2 (ja) 生分解性ポリ尿素/ポリウレタンマイクロカプセル
EP3197421B1 (en) High-coverage, low odor malodor counteractant compounds and methods of use
CN113766969A (zh) 用于制备微胶囊的方法
JP2021191838A (ja) カプセル化されたフレグランス組成物
CN112004852B (zh) 以直链和环状脂肪族多异氰酸酯制备的核壳胶囊
CN115103719A (zh) 基于天然氨基酸的经封装的香味剂
JP7547612B2 (ja) 生分解性ポリ尿素/ポリウレタンマイクロカプセル
JP7546146B2 (ja) ポリ尿素/ポリウレタンマイクロカプセル
US20250144589A1 (en) Method for Producing Microcapsules
GB2630880A (en) Method for producing microcapsules
BR122025016552A2 (pt) Processo para a preparação de microcápsulas
WO2019170222A1 (en) Encapsulated active substance deposition on hairs and textile

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant