CN111961250A - 一种阻燃聚氨酯软泡材料的制备方法 - Google Patents
一种阻燃聚氨酯软泡材料的制备方法 Download PDFInfo
- Publication number
- CN111961250A CN111961250A CN202010886896.3A CN202010886896A CN111961250A CN 111961250 A CN111961250 A CN 111961250A CN 202010886896 A CN202010886896 A CN 202010886896A CN 111961250 A CN111961250 A CN 111961250A
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- Prior art keywords
- polyurethane
- foam
- soft foam
- phytic acid
- flame
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229920002635 polyurethane Polymers 0.000 title claims abstract description 62
- 239000004814 polyurethane Substances 0.000 title claims abstract description 62
- 239000003063 flame retardant Substances 0.000 title claims abstract description 38
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 35
- 239000006261 foam material Substances 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000006260 foam Substances 0.000 claims abstract description 40
- IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 claims abstract description 33
- 238000003756 stirring Methods 0.000 claims abstract description 17
- 238000000034 method Methods 0.000 claims abstract description 15
- 229920005830 Polyurethane Foam Polymers 0.000 claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 14
- 239000011496 polyurethane foam Substances 0.000 claims abstract description 14
- 238000001035 drying Methods 0.000 claims abstract description 13
- 239000006087 Silane Coupling Agent Substances 0.000 claims abstract description 11
- 239000008367 deionised water Substances 0.000 claims abstract description 11
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000004140 cleaning Methods 0.000 claims abstract description 7
- 238000006243 chemical reaction Methods 0.000 claims abstract description 6
- 238000001816 cooling Methods 0.000 claims abstract description 6
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 claims description 10
- 235000002949 phytic acid Nutrition 0.000 claims description 10
- 229940068041 phytic acid Drugs 0.000 claims description 10
- 239000000467 phytic acid Substances 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 5
- 238000001914 filtration Methods 0.000 abstract description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 5
- 229910052760 oxygen Inorganic materials 0.000 abstract description 5
- 239000001301 oxygen Substances 0.000 abstract description 5
- 231100000252 nontoxic Toxicity 0.000 abstract description 3
- 230000003000 nontoxic effect Effects 0.000 abstract description 3
- 230000008569 process Effects 0.000 abstract description 3
- 230000003139 buffering effect Effects 0.000 abstract description 2
- 238000009413 insulation Methods 0.000 abstract description 2
- 238000007598 dipping method Methods 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 9
- 230000007613 environmental effect Effects 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 2
- 239000012774 insulation material Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 230000001988 toxicity Effects 0.000 description 2
- 231100000419 toxicity Toxicity 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000004721 Polyphenylene oxide Substances 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000009841 combustion method Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000012948 isocyanate Substances 0.000 description 1
- 150000002513 isocyanates Chemical class 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/36—After-treatment
- C08J9/40—Impregnation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/36—After-treatment
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
- C08J2375/04—Polyurethanes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyurethanes Or Polyureas (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
Claims (5)
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CN202010886896.3A CN111961250B (zh) | 2020-08-28 | 2020-08-28 | 一种阻燃聚氨酯软泡材料的制备方法 |
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CN111961250A true CN111961250A (zh) | 2020-11-20 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114027552A (zh) * | 2021-10-28 | 2022-02-11 | 盐城工学院 | 一种过滤嘴的制备方法及其产品 |
Citations (8)
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CN101565511A (zh) * | 2009-06-05 | 2009-10-28 | 圣诺盟聚氨脂(上海)有限公司 | 一种物理浸渍液及物理浸渍法制备高性能柔性聚氨酯泡沫塑料 |
CN104892667A (zh) * | 2015-06-16 | 2015-09-09 | 青岛格瑞烯金属防护科技有限公司 | 一种植酸聚合物的制备方法及其在金属表面预处理领域的应用 |
CN106191833A (zh) * | 2016-07-11 | 2016-12-07 | 张卫东 | 一种阻燃型播种机表面处理用水基防锈剂及其制作方法 |
CN106948172A (zh) * | 2017-04-06 | 2017-07-14 | 天津工业大学 | 一种基于硅‑磷‑氮协同体系的阻燃聚丙烯腈织物的制备方法 |
CN107828081A (zh) * | 2017-10-18 | 2018-03-23 | 西南交通大学 | 一种软质聚氨酯泡沫阻燃材料的制备方法 |
CN108047494A (zh) * | 2017-11-15 | 2018-05-18 | 四川大学 | 植酸铵盐阻燃剂及其制备方法和用以制备的阻燃增韧聚乳酸材料 |
US20200056057A1 (en) * | 2018-08-17 | 2020-02-20 | The University Of Massachusetts | Synergistic flame retardant compositions and fiber blends including the same |
CN110922632A (zh) * | 2019-12-13 | 2020-03-27 | 中国民用航空飞行学院 | 阻燃聚氨酯软泡塑料及其制备方法 |
-
2020
- 2020-08-28 CN CN202010886896.3A patent/CN111961250B/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101565511A (zh) * | 2009-06-05 | 2009-10-28 | 圣诺盟聚氨脂(上海)有限公司 | 一种物理浸渍液及物理浸渍法制备高性能柔性聚氨酯泡沫塑料 |
CN104892667A (zh) * | 2015-06-16 | 2015-09-09 | 青岛格瑞烯金属防护科技有限公司 | 一种植酸聚合物的制备方法及其在金属表面预处理领域的应用 |
CN106191833A (zh) * | 2016-07-11 | 2016-12-07 | 张卫东 | 一种阻燃型播种机表面处理用水基防锈剂及其制作方法 |
CN106948172A (zh) * | 2017-04-06 | 2017-07-14 | 天津工业大学 | 一种基于硅‑磷‑氮协同体系的阻燃聚丙烯腈织物的制备方法 |
CN107828081A (zh) * | 2017-10-18 | 2018-03-23 | 西南交通大学 | 一种软质聚氨酯泡沫阻燃材料的制备方法 |
CN108047494A (zh) * | 2017-11-15 | 2018-05-18 | 四川大学 | 植酸铵盐阻燃剂及其制备方法和用以制备的阻燃增韧聚乳酸材料 |
US20200056057A1 (en) * | 2018-08-17 | 2020-02-20 | The University Of Massachusetts | Synergistic flame retardant compositions and fiber blends including the same |
CN110922632A (zh) * | 2019-12-13 | 2020-03-27 | 中国民用航空飞行学院 | 阻燃聚氨酯软泡塑料及其制备方法 |
Non-Patent Citations (4)
Title |
---|
SHIBIN NIE等: ""Fabrication of environmentally-benign flame retardant cotton fabrics with hydrophobicity by a facile chemical modification"", 《CELLULOSE》 * |
SHIBIN NIE等: ""Fabrication of environmentally-benign flame retardant cotton fabrics with hydrophobicity by a facile chemical modification"", 《CELLULOSE》, vol. 26, no. 8, 16 April 2019 (2019-04-16), pages 5147 - 5158, XP036774986, DOI: 10.1007/s10570-019-02431-y * |
XIAN-WEI CHENG等: "Flame retardant and hydrophobic properties of novel sol-gel derived phytic acid/silica hybrid organic-inorganic coatings for silk fabric", 《APPLIED SURFACE SCIENCE》 * |
XIAN-WEI CHENG等: "Flame retardant and hydrophobic properties of novel sol-gel derived phytic acid/silica hybrid organic-inorganic coatings for silk fabric", 《APPLIED SURFACE SCIENCE》, vol. 427, 1 January 2018 (2018-01-01), pages 69 - 80, XP085228820, DOI: 10.1016/j.apsusc.2017.08.021 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114027552A (zh) * | 2021-10-28 | 2022-02-11 | 盐城工学院 | 一种过滤嘴的制备方法及其产品 |
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Application publication date: 20201120 Assignee: DONGTAI GAOKE TECHNOLOGY INNOVATION PARK Co.,Ltd. Assignor: YANCHENG INSTITUTE OF TECHNOLOGY Contract record no.: X2024980001369 Denomination of invention: Preparation method of a flame-retardant polyurethane soft foam material Granted publication date: 20230131 License type: Common License Record date: 20240124 |
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Assignee: DONGTAI GAOKE TECHNOLOGY INNOVATION PARK Co.,Ltd. Assignor: YANCHENG INSTITUTE OF TECHNOLOGY Contract record no.: X2024980001369 Date of cancellation: 20240407 |