CN111773113A - 一种冻干精华面膜及其制作工艺 - Google Patents
一种冻干精华面膜及其制作工艺 Download PDFInfo
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- CN111773113A CN111773113A CN202010599311.XA CN202010599311A CN111773113A CN 111773113 A CN111773113 A CN 111773113A CN 202010599311 A CN202010599311 A CN 202010599311A CN 111773113 A CN111773113 A CN 111773113A
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Abstract
本发明提供一种冻干精华面膜及其制作工艺,涉及护肤品技术领域,本发明的冻干精华面膜由以下原料组成:二裂酵母发酵产物滤液、蚕丝胶蛋白、弹性蛋白、蛋白酶、蛋壳膜提取物、蛋清提取物、蜂花粉、蜂胶提取物、黄原胶、牛奶蛋白、虾青素、水解蚕丝、甜橙油、珍珠提取物、草本提取物和去离子水;本发明的冻干精华面膜原料成分安全,加工过程简单,无污染物产生,绿色环保;其配方中不含防腐剂,对皮肤无刺激性,适用于任何肤质,且具有美白、淡斑褪黑、抗衰防皱、保湿补水、杀菌收敛的作用,不会对肌肤造成过多负担,使用效果好。
Description
【技术领域】
本发明涉及护肤品技术领域,具体涉及一种冻干精华面膜及其制作工艺。
【背景技术】
随着我国人民生活水平的不断提高,越来越多的女性开始注重对于肌肤的保养,特别是对于面部肌肤的日常护理愈加重视。除了使用膏霜类产品对皮肤进行防护,日常护理中常用到产品就是面膜。市场常见的面膜具有清洁、补水保湿、美白、平衡油脂等丰富的功能。市面上的面膜种类繁多,但或多或少存在以下几点问题:1.在面膜生产过程中,大部分生产商都会在生产过冲中添加不同种类的防腐剂来抑制微生物的繁殖甚至是致其死亡,尽管防腐技术在不断进步,但是依然存在着致敏、影响产品气味、肤感、长时间使用损伤皮肤表层等问题;2.由于生产后面膜一直处于活性状态,面膜的成分还会不断产生各种反应变化,导致随着时间的推移,面膜的使用效果会打折扣;3.现有的面膜由于肌肤吸收十分有限,导致使用效果不明显,面膜的功效有待改进。
能否站在绿色、天然、安全和环保简约的角度满足人们对美的追求,已经成为新时期人们对护肤品、化妆品质量内涵与功能诉求所关注的焦点。
【发明内容】
有鉴于此,本发明的目的在于提供一种冻干精华面膜及其制作工艺,本发明的冻干精华面膜原料成分安全,加工过程简单,无污染物产生,绿色环保;其配方中不含防腐剂,对皮肤无刺激性,适用于任何肤质,且具有美白、淡斑褪黑、抗衰防皱、保湿补水、杀菌收敛的作用,不会对肌肤造成过多负担,使用效果好。
为了解决上述技术问题,本发明采用了如下的技术方案:
一种冻干精华面膜由以下重量份的原料组成:二裂酵母发酵产物滤液10-20份、蚕丝胶蛋白3-5份、弹性蛋白4-8份、蛋白酶5-10份、蛋壳膜提取物3-5份、蛋清提取物3-5份、蜂花粉4-8份、蜂胶提取物4-8份、黄原胶3-5份、牛奶蛋白8-18份、虾青素5-12份、水解蚕丝4-9份、甜橙油6-15份、珍珠提取物3-5份、草本提取物6-12份和去离子水20-35份。
本发明中,进一步地,所述二裂酵母发酵产物滤液通过以下方法得到:
a.将摇床活化好的双歧杆菌接种到培养基中,在pH值为6.6-6.8,温度为35-40℃、摇床速度为100-150rpm的条件下发酵6-8小时;b.发酵结束后,灭活菌液,低速离心后收集上清液,得到发酵液,备用;c.将步骤b所得发酵液、透明质酸、烟酰胺按照体积比为3:1-2:0.5:0.5的比例混合,加热搅拌溶解,即可获得所述二裂酵母发酵产物滤液。
本发明中,进一步地,所述草本提取物由以下重量份的原料组成:白芨5-10份、白蔹3-8份、茯苓6-12份、白术5-10份、白鲜5-10份、白睡莲3-8份、白芍5-10份和北美金缕梅2-6份。
本发明中,进一步地,所述草本提取物通过以下方法得到:a.蒸馏:按重量份数,将白芨、白蔹、茯苓、白术、白鲜、白睡莲、白芍和北美金缕梅混合置于去离子水中浸泡40-60分钟,接着将上述混合药材置于蒸馏锅内,注入水蒸气,蒸馏处理得草本蒸馏液;取草本蒸馏液置于微波萃取仪内,微波处理12-18min,过滤得草本提取物。
本发明中,进一步地,所述虾青素通过以下方法得到:取天然雨生红球藻,在其中加入其质量的30-38倍,浓度为3-4mol/L的盐酸,接着在40-45℃下水浴8-12分钟后过滤取其滤渣,在惰性气体保护下加热,使滤渣溶解于甲醇中,得到滤渣溶解液,接着将滤渣溶解液于5-15℃环境中沉降15-22小时,取上清液进行浓缩干燥,即可得到所述虾青素。
本发明还提供上述一种冻干精华面膜的制作工艺,所述制作工艺包括以下步骤:
在反应罐中加入去离子水,加热至45-50℃时加入二裂酵母发酵产物滤液和草本提取物,于发酵罐中发酵30-35天,然后提取发酵滤液,在发酵滤液中分别加入花青素、蚕丝胶蛋白、弹性蛋白、蛋白酶、蛋壳膜提取物、蛋清提取物、蜂花粉、蜂胶提取物、黄原胶、牛奶蛋白、水解蚕丝、甜橙油,搅拌使这些物质完全分散,接着将上述混合物进行二次发酵萃取,萃取出的第二道精华再进行小肽分离,再将小肽分离后的精华送入微波真空罐中,然后进行抽真空处理至真空度为-0.09MPa~-0.06MPa;再进行微波处理,微波频率为300-380MHz,微波处理时间为0.5-1min,得到精华原液,备用;在真空休眠舱密封生产环境下,于-196℃的条件下对精华原液进行冷冻干燥,令高浓缩活性精华原液瞬间呈现无菌干燥休眠状态,以喷雾形式履盖到天然蚕丝膜布上,即可得到冻干精华面膜。
本发明中,进一步地,所述天然蚕丝膜布通过以下方法得到:以纯蚕丝短纤维为原料,采用水刺成网技术制备真丝无纺布;将真丝无纺布进行脱胶处理,然后用碳酸氢钠溶液浸泡使其溶胀,接着在其湿态下转移到纤维解离器中进行解离,得到纤维溶液;将解离后的纤维溶液用酸中和得到悬浮液,沉淀除水、在纸页成型器上进行抄纸再于纸页干燥器上进行干燥,制得天然蚕丝膜布。
本发明采用真空冻干技术,使面膜纸成分处于休眠状态,使用时,采用原液与带冻干粉的面膜纸混合,将成分激活,使成分保持最佳状态,延长面膜使用有效期。
本申请的蛋壳膜提取物通过以下方法得到:将蛋壳膜清洗烘干后粉碎成80目细粉,按照料液比为1g:20ml的比例加入离子液体,在70℃的条件下反应2h,接着加入蛋壳膜质量2-4%的蛋白酶进行酶解处理,酶解后过滤出去滤渣,在滤液中加入十六烷基吡啶进行沉淀,收集上清液,即为所述蛋壳膜提取物。
本申请的蛋清提取物通过以下方法得到:将蛋清离心或过滤除去不溶性的杂蛋白,分离出含生物活性成分的蛋清上清粗提液;将蛋清上清粗提液,离心或过滤除去不溶性的杂蛋白提取清液,将此清液通过阴离子树脂交换柱,分离出蛋清生物活性成分。
本申请的蜂胶提取物通过以下方法得到:将蜂胶原料低温粉碎、置于去离子水中并加入分散剂,搅拌均匀后加入无机盐溶液,加热并搅拌后冷却静置、除去固体后溶于非临界流体溶剂中加热加压浸提2-7小时,减压蒸馏并回收溶剂,得蜂胶提取物。
本申请的珍珠提取物通过以下方法得到:将珍珠研磨成粒径为80nm的纳米珍珠粉,采用弱酸溶液在35-40℃溶解纳米珍珠粉,搅拌反应2h,在6000rpm的速度离心;取上清液,在去离子水中透析4天,冷冻干燥得到珍珠提取物。
综上所述,由于采用了上述技术方案,本发明的有益效果是:
1.本发明的冻干精华面膜原料成分安全,加工过程简单,无污染物产生,绿色环保;其配方中不含防腐剂,对皮肤无刺激性,适用于任何肤质,且具有美白、淡斑褪黑、抗衰防皱、保湿补水、杀菌收敛的作用,不会对肌肤造成过多负担,使用效果好。
2.采用本申请冻干技术生产出来的面膜,可以长时间保留精华的活性纯度,并且活性成份高达95%以上,没有防腐剂、增稠剂、化学品,完全可以做到天然绿色无毒无添加剂,任何肌肤都可以使用,是真正的0敏感,0添加的产品。
3.本发明的冻干精华面膜各原料相互结合,具有高效保湿、排毒养颜、淡化色斑、抗衰防皱、美白护肤等美容功效,现有的面膜存在吸收效果不佳的问题,导致面膜利用率低,研究表明,具有脂溶性又具有水溶性的物质最易被皮肤渗透吸收,申请人发现,天然虾青素是至今发现的唯一一种既具有脂溶性又具有水溶性的高效抗氧化药物,本申请的虾青素是通过从雨生红球藻中提取得到,在加热溶解过程中,采取惰性气体保护,减少虾青素的损失,精制得到的虾青素的转移率高,对面部肌肤起到抗氧化,保护皮肤健康的作用。
4.本申请组成面膜的原料中包括二裂酵母发酵产物滤液,利用微生物发酵技术,在二裂酵母发酵产物滤液原有的基础上,通过添加其他活性物,增强发酵产品在美白和保湿方面的功效,采用二裂酵母发酵过的中草药,能完全去除掉中草药中的微毒性,并能使中草药的药效成份提高到原来的4倍以上。
5.本申请选用蚕丝作为面膜基布,蚕丝中含有极高的胶原蛋白和弹力纤维,氨基酸、核糖、核酸等营养成份,它与人体胶原蛋白完全相同,因而容易被肌肤吸收,促进细胞再生,紧致细胞间隙距离,提升肌肤柔韧度和紧致度。
6.本申请在面膜制备过程中,在混合精华原料时,通过微波真空处理,各组分同时发生热效应和非热效应,微波辐射加热时,微波中的电磁场以每秒数亿次甚至数十亿次的频率转换方向,使得材料内部不同电荷的极化以及这种极化不具备迅速跟上交变电场的能力,导致材料内部摩擦而发热,即所谓的“内加热”,使得面膜中的各组分相互交融,并可能发生若干反应,最终使本发明的面膜成分发挥防老减皱、增强皮肤弹性、清理毛孔内堵塞物的优良效果。
【具体实施方式】
下面的实施例可以帮助本领域的技术人员更全面地理解本发明,但不可以以任何方式限制本发明。
实施例1
本实施例提供的一种冻干精华面膜由以下重量份的原料组成:二裂酵母发酵产物滤液10份、蚕丝胶蛋白3份、弹性蛋白4份、蛋白酶5份、蛋壳膜提取物3份、蛋清提取物3份、蜂花粉4份、蜂胶提取物4份、黄原胶3份、牛奶蛋白8份、虾青素5份、水解蚕丝4份、甜橙油6份、珍珠提取物3份、草本提取物6份和去离子水20份;其中,草本提取物由以下重量份的原料组成:白芨5份、白蔹3份、茯苓6份、白术5份、白鲜5份、白睡莲3份、白芍5份和北美金缕梅2份。
本实施例还提供上述一种冻干精华面膜的制作工艺,包括以下步骤:
(一)制备二裂酵母发酵产物滤液
a.将摇床活化好的双歧杆菌接种到培养基中,在pH值为6.6,温度为35℃、摇床速度为100rpm的条件下发酵6小时;b.发酵结束后,灭活菌液,低速离心后收集上清液,得到发酵液,备用;c.将步骤b所得发酵液、透明质酸、烟酰胺按照体积比为3:1:0.5:0.5的比例混合,加热搅拌溶解,即可获得所述二裂酵母发酵产物滤液;
(二)制备虾青素
取天然雨生红球藻,在其中加入其质量的30倍,浓度为3mol/L的盐酸,接着在40℃下水浴8分钟后过滤取其滤渣,在惰性气体保护下加热,使滤渣溶解于甲醇中,得到滤渣溶解液,接着将滤渣溶解液于5℃环境中沉降15小时,取上清液进行浓缩干燥,即可得到所述虾青素;
(三)制备草本提取物
按重量份数,将白芨、白蔹、茯苓、白术、白鲜、白睡莲、白芍和北美金缕梅混合置于去离子水中浸泡40分钟,接着将上述混合药材置于蒸馏锅内,注入水蒸气,蒸馏处理得草本蒸馏液;取草本蒸馏液置于微波萃取仪内,微波处理12min,过滤得草本提取物;
(四)制作冻干精华面膜
在反应罐中加入去离子水,加热至45℃时加入二裂酵母发酵产物滤液和草本提取物,于发酵罐中发酵30天,然后提取发酵滤液,在发酵滤液中分别加入花青素、蚕丝胶蛋白、弹性蛋白、蛋白酶、蛋壳膜提取物、蛋清提取物、蜂花粉、蜂胶提取物、黄原胶、牛奶蛋白、水解蚕丝、甜橙油,搅拌使这些物质完全分散,接着将上述混合物进行二次发酵萃取,萃取出的第二道精华再进行小肽分离,再将小肽分离后的精华送入微波真空罐中,然后进行抽真空处理至真空度为-0.09MPa;再进行微波处理,微波频率为300MHz,微波处理时间为0.5min,得到精华原液,备用;在真空休眠舱密封生产环境下,于-196℃的条件下对精华原液进行冷冻干燥,使高浓缩活性精华原液瞬间呈现无菌干燥休眠状态,以喷雾形式履盖到天然蚕丝膜布上,即可得到冻干精华面膜;其中,天然蚕丝膜布通过以下方法得到:以纯蚕丝短纤维为原料,采用水刺成网技术制备真丝无纺布;将真丝无纺布进行脱胶处理,然后用碳酸氢钠溶液浸泡使其溶胀,接着在其湿态下转移到纤维解离器中进行解离,得到纤维溶液;将解离后的纤维溶液用酸中和得到悬浮液,沉淀除水、在纸页成型器上进行抄纸再于纸页干燥器上进行干燥,制得天然蚕丝膜布。
实施例2
本实施例提供的一种冻干精华面膜由以下重量份的原料组成:二裂酵母发酵产物滤液15份、蚕丝胶蛋白4份、弹性蛋白6份、蛋白酶7份、蛋壳膜提取物4份、蛋清提取物4份、蜂花粉7份、蜂胶提取物6份、黄原胶4份、牛奶蛋白13份、虾青素8份、水解蚕丝7份、甜橙油10份、珍珠提取物4份、草本提取物8份和去离子水28份;其中,草本提取物由以下重量份的原料组成:白芨7份、白蔹6份、茯苓9份、白术7份、白鲜7份、白睡莲6份、白芍7份和北美金缕梅4份。
本实施例还提供上述一种冻干精华面膜的制作工艺,包括以下步骤:
(一)制备二裂酵母发酵产物滤液
a.将摇床活化好的双歧杆菌接种到培养基中,在pH值为6.7,温度为37℃、摇床速度为125rpm的条件下发酵7小时;b.发酵结束后,灭活菌液,低速离心后收集上清液,得到发酵液,备用;c.将步骤b所得发酵液、透明质酸、烟酰胺按照体积比为3:1:0.5:0.5的比例混合,加热搅拌溶解,即可获得所述二裂酵母发酵产物滤液;
(二)制备虾青素
取天然雨生红球藻,在其中加入其质量的34倍,浓度为3.5mol/L的盐酸,接着在42℃下水浴10分钟后过滤取其滤渣,在惰性气体保护下加热,使滤渣溶解于甲醇中,得到滤渣溶解液,接着将滤渣溶解液于10℃环境中沉降18小时,取上清液进行浓缩干燥,即可得到所述虾青素;
(三)制备草本提取物
按重量份数,将白芨、白蔹、茯苓、白术、白鲜、白睡莲、白芍和北美金缕梅混合置于去离子水中浸泡50分钟,接着将上述混合药材置于蒸馏锅内,注入水蒸气,蒸馏处理得草本蒸馏液;取草本蒸馏液置于微波萃取仪内,微波处理16min,过滤得草本提取物;
(四)制作冻干精华面膜
在反应罐中加入去离子水,加热至47℃时加入二裂酵母发酵产物滤液和草本提取物,于发酵罐中发酵32天,然后提取发酵滤液,在发酵滤液中分别加入花青素、蚕丝胶蛋白、弹性蛋白、蛋白酶、蛋壳膜提取物、蛋清提取物、蜂花粉、蜂胶提取物、黄原胶、牛奶蛋白、水解蚕丝、甜橙油,搅拌使这些物质完全分散,接着将上述混合物进行二次发酵萃取,萃取出的第二道精华再进行小肽分离,再将小肽分离后的精华送入微波真空罐中,然后进行抽真空处理至真空度为-0.08MPa;再进行微波处理,微波频率为340MHz,微波处理时间为0.7min,得到精华原液,备用;在真空休眠舱密封生产环境下,于-196℃的条件下对精华原液进行冷冻干燥,使高浓缩活性精华原液瞬间呈现无菌干燥休眠状态,以喷雾形式履盖到天然蚕丝膜布上,即可得到冻干精华面膜;其中,天然蚕丝膜布通过以下方法得到:以纯蚕丝短纤维为原料,采用水刺成网技术制备真丝无纺布;将真丝无纺布进行脱胶处理,然后用碳酸氢钠溶液浸泡使其溶胀,接着在其湿态下转移到纤维解离器中进行解离,得到纤维溶液;将解离后的纤维溶液用酸中和得到悬浮液,沉淀除水、在纸页成型器上进行抄纸再于纸页干燥器上进行干燥,制得天然蚕丝膜布。
实施例3
本实施例提供的一种冻干精华面膜由以下重量份的原料组成:二裂酵母发酵产物滤液20份、蚕丝胶蛋白5份、弹性蛋白8份、蛋白酶10份、蛋壳膜提取物5份、蛋清提取物5份、蜂花粉8份、蜂胶提取物8份、黄原胶5份、牛奶蛋白18份、虾青素12份、水解蚕丝9份、甜橙油15份、珍珠提取物5份、草本提取物12份和去离子水35份;其中,草本提取物由以下重量份的原料组成:白芨10份、白蔹8份、茯苓12份、白术10份、白鲜10份、白睡莲8份、白芍10份和北美金缕梅6份。
本实施例还提供上述一种冻干精华面膜的制作工艺,包括以下步骤:
(一)制备二裂酵母发酵产物滤液
a.将摇床活化好的双歧杆菌接种到培养基中,在pH值为6.8,温度为40℃、摇床速度为150rpm的条件下发酵8小时;b.发酵结束后,灭活菌液,低速离心后收集上清液,得到发酵液,备用;c.将步骤b所得发酵液、透明质酸、烟酰胺按照体积比为3:2:0.5:0.5的比例混合,加热搅拌溶解,即可获得所述二裂酵母发酵产物滤液;
(二)制备虾青素
取天然雨生红球藻,在其中加入其质量的38倍,浓度为4mol/L的盐酸,接着在45℃下水浴12分钟后过滤取其滤渣,在惰性气体保护下加热,使滤渣溶解于甲醇中,得到滤渣溶解液,接着将滤渣溶解液于15℃环境中沉降22小时,取上清液进行浓缩干燥,即可得到所述虾青素;
(三)制备草本提取物
按重量份数,将白芨、白蔹、茯苓、白术、白鲜、白睡莲、白芍和北美金缕梅混合置于去离子水中浸泡60分钟,接着将上述混合药材置于蒸馏锅内,注入水蒸气,蒸馏处理得草本蒸馏液;取草本蒸馏液置于微波萃取仪内,微波处理18min,过滤得草本提取物;
(四)制作冻干精华面膜
在反应罐中加入去离子水,加热至50℃时加入二裂酵母发酵产物滤液和草本提取物,于发酵罐中发酵35天,然后提取发酵滤液,在发酵滤液中分别加入花青素、蚕丝胶蛋白、弹性蛋白、蛋白酶、蛋壳膜提取物、蛋清提取物、蜂花粉、蜂胶提取物、黄原胶、牛奶蛋白、水解蚕丝、甜橙油,搅拌使这些物质完全分散,接着将上述混合物进行二次发酵萃取,萃取出的第二道精华再进行小肽分离,再将小肽分离后的精华送入微波真空罐中,然后进行抽真空处理至真空度为-0.06MPa;再进行微波处理,微波频率为380MHz,微波处理时间为1min,得到精华原液,备用;在真空休眠舱密封生产环境下,于-196℃的条件下对精华原液进行冷冻干燥,使高浓缩活性精华原液瞬间呈现无菌干燥休眠状态,以喷雾形式履盖到天然蚕丝膜布上,即可得到冻干精华面膜;其中,天然蚕丝膜布通过以下方法得到:以纯蚕丝短纤维为原料,采用水刺成网技术制备真丝无纺布;将真丝无纺布进行脱胶处理,然后用碳酸氢钠溶液浸泡使其溶胀,接着在其湿态下转移到纤维解离器中进行解离,得到纤维溶液;将解离后的纤维溶液用酸中和得到悬浮液,沉淀除水、在纸页成型器上进行抄纸再于纸页干燥器上进行干燥,制得天然蚕丝膜布。
效果验证
为了进一步说明本发明沃柑贮藏保鲜效果方法的实用价值,申请人做一下对比试验:
第一组:本发明实施例2所述的冻干精华面膜;
第二组:去掉原料中的虾青素,其他原料和制作工艺严格按照实施例2进行;
第三组:去掉原料中的二裂酵母发酵产物滤液,其他原料和制作工艺严格按照实施例2进行;
第四组:将天然蚕丝膜布换为普通面膜基布,其他原料和制作工艺严格按照实施例2进行;
第五组:去掉微波处理的步骤,其他原料和制作工艺严格按照实施例2进行;
第六组:将“在真空休眠舱密封生产环境下,于-196℃的条件下对精华原液进行冷冻干燥,使高浓缩活性精华原液瞬间呈现无菌干燥休眠状态,以喷雾形式履盖到天然蚕丝膜布上...”的步骤修改为“将精华原液经过喷雾形式覆盖到天然蚕丝膜布上,即可得到面膜...”;其他原料和制作工艺严格按照实施例2进行;
第七组:市面上的普通蚕丝面膜,购自广州市嘉美化妆品有限公司。
选择40名测试者(男女各20人,年龄段15-55岁),对上述七组面膜进行盲测。每组平行测定3次,测试者根据自己的使用感觉进行评分,评价项目设计铺展性、泡沫丰富度、香味、冲水感,清洁度、用后舒适度。评分标准采用5分制,1分为最差,5分为最佳。评价结果为所有测试者分数的平均分,平均分越高,效果越好。
保湿效果为使用面膜后肌肤含水率的差值与原肌肤含水率。
结果记录如表1所示:
表1七组面膜使用感评价结果
根据表1可知,本申请的冻干精华面膜具有温和滋润,用后舒适佳等特点,且其保湿美白、抗衰防皱、淡斑腿黑、收敛抑菌效果优于其他组别,本申请中的每一种原料均起到举足轻重的作用,原料间的相互作用结合科学的制作工艺得到了本发明冻干精华面膜。
虽然,上文中已经用一般性说明及具体实施方案对本发明作了详尽的描述,但在本发明基础上,可以对之作一些修改或改进,这对本领域技术人员而言是显而易见的。因此,在不偏离本发明精神的基础上所做的这些修改或改进,均属于本发明要求保护的范围。
Claims (7)
1.一种冻干精华面膜,其特征在于,所述冻干精华面膜主要由以下重量份的原料组成:二裂酵母发酵产物滤液10-20份、蚕丝胶蛋白3-5份、弹性蛋白4-8份、蛋白酶5-10份、蛋壳膜提取物3-5份、蛋清提取物3-5份、蜂花粉4-8份、蜂胶提取物4-8份、黄原胶3-5份、牛奶蛋白8-18份、虾青素5-12份、水解蚕丝4-9份、甜橙油6-15份、珍珠提取物3-5份、草本提取物6-12份和去离子水20-35份。
2.根据权利要求1所述的一种冻干精华面膜,其特征在于,所述二裂酵母发酵产物滤液通过以下方法得到:
a.将摇床活化好的双歧杆菌接种到培养基中,在pH值为6.6-6.8,温度为35-40℃、摇床速度为100-150rpm的条件下发酵6-8小时;b.发酵结束后,灭活菌液,低速离心后收集上清液,得到发酵液,备用;c.将步骤b所得发酵液、透明质酸、烟酰胺按照体积比为3:1-2:0.5:0.5的比例混合,加热搅拌溶解,即可获得所述二裂酵母发酵产物滤液。
3.根据权利要求1所述的一种冻干精华面膜,其特征在于,所述草本提取物由以下重量份的原料组成:白芨5-10份、白蔹提3-8份、茯苓6-12份、白术5-10份、白鲜5-10份、白睡莲3-8份、白芍5-10份和北美金缕梅2-6份。
4.根据权利要求3所述的一种冻干精华面膜,其特征在于,所述草本提取物通过以下方法得到:按重量份数,将白芨、白蔹、茯苓、白术、白鲜、白睡莲、白芍和北美金缕梅混合置于去离子水中浸泡40-60分钟,接着将上述混合药材置于蒸馏锅内,注入水蒸气,蒸馏处理得草本蒸馏液;取草本蒸馏液置于微波萃取仪内,微波处理12-18min,过滤得草本提取物。
5.根据权利要求1所述的一种冻干精华面膜,其特征在于,所述虾青素通过以下方法得到:取天然雨生红球藻,在其中加入其质量的30-38倍,浓度为3-4mol/L的盐酸,接着在40-45℃下水浴8-12分钟后过滤取其滤渣,在惰性气体保护下加热,使滤渣溶解于甲醇中,得到滤渣溶解液,接着将滤渣溶解液于5-15℃环境中沉降15-22小时,取上清液进行浓缩干燥,即可得到所述虾青素。
6.根据权利要求1-5任一项所述的一种冻干精华面膜的制作工艺,其特征在于,所述制作工艺包括以下步骤:
在反应罐中加入去离子水,加热至45-50℃时加入二裂酵母发酵产物滤液和草本提取物,于发酵罐中发酵30-35天,然后提取发酵滤液,在发酵滤液中分别加入花青素、蚕丝胶蛋白、弹性蛋白、蛋白酶、蛋壳膜提取物、蛋清提取物、蜂花粉、蜂胶提取物、黄原胶、牛奶蛋白、水解蚕丝、甜橙油,搅拌使这些物质完全分散,接着将上述混合物进行二次发酵萃取,萃取出的第二道精华再进行小肽分离,再将小肽分离后的精华送入微波真空罐中,然后进行抽真空处理至真空度为-0.09MPa~-0.06MPa;再进行微波处理,微波频率为300-380MHz,微波处理时间为0.5-1min,得到精华原液,备用;在真空休眠舱密封生产环境下,于-196℃的条件下对精华原液进行冷冻干燥,使高浓缩活性精华原液瞬间呈现无菌干燥休眠状态,以喷雾形式履盖到天然蚕丝膜布上,即可得到冻干精华面膜。
7.根据权利要求6所述的一种冻干精华面膜的制作工艺,其特征在于,所述天然蚕丝膜布通过以下方法得到:以纯蚕丝短纤维为原料,采用水刺成网技术制备真丝无纺布;将真丝无纺布进行脱胶处理,然后用碳酸氢钠溶液浸泡使其溶胀,接着在其湿态下转移到纤维解离器中进行解离,得到纤维溶液;将解离后的纤维溶液用酸中和得到悬浮液,沉淀除水、在纸页成型器上进行抄纸再于纸页干燥器上进行干燥,制得天然蚕丝膜布。
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