CN111685201A - Method for preparing theabrownin by using instant tea powder as raw material - Google Patents
Method for preparing theabrownin by using instant tea powder as raw material Download PDFInfo
- Publication number
- CN111685201A CN111685201A CN202010608132.8A CN202010608132A CN111685201A CN 111685201 A CN111685201 A CN 111685201A CN 202010608132 A CN202010608132 A CN 202010608132A CN 111685201 A CN111685201 A CN 111685201A
- Authority
- CN
- China
- Prior art keywords
- theabrownin
- raw material
- tea
- preparing
- tea powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000843 powder Substances 0.000 title claims abstract description 33
- 239000002994 raw material Substances 0.000 title claims abstract description 31
- 235000020344 instant tea Nutrition 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title claims abstract description 19
- 235000013616 tea Nutrition 0.000 claims abstract description 39
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 15
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 102000004190 Enzymes Human genes 0.000 claims abstract description 9
- 108090000790 Enzymes Proteins 0.000 claims abstract description 9
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 9
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 9
- 238000001035 drying Methods 0.000 claims abstract description 5
- 241001122767 Theaceae Species 0.000 claims abstract 12
- 235000010987 pectin Nutrition 0.000 claims description 5
- 229920001277 pectin Polymers 0.000 claims description 5
- 239000001814 pectin Substances 0.000 claims description 5
- 238000001223 reverse osmosis Methods 0.000 claims description 5
- 230000035484 reaction time Effects 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- 239000000243 solution Substances 0.000 claims 9
- 239000007864 aqueous solution Substances 0.000 claims 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 1
- 239000008187 granular material Substances 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 14
- 230000008901 benefit Effects 0.000 abstract description 6
- 244000269722 Thea sinensis Species 0.000 description 27
- 238000002360 preparation method Methods 0.000 description 6
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 238000012824 chemical production Methods 0.000 description 2
- 230000035622 drinking Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000012847 fine chemical Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 description 1
- 235000019224 Camellia sinensis var Qingmao Nutrition 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 description 1
- 235000005487 catechin Nutrition 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 229950001002 cianidanol Drugs 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000009569 green tea Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 235000020339 pu-erh tea Nutrition 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/166—Addition of, or treatment with, enzymes or microorganisms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
- A23F3/22—Drying or concentrating tea extract
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Microbiology (AREA)
- Tea And Coffee (AREA)
Abstract
The invention aims to provide a method for preparing theabrownin by using instant tea powder as a raw material, which has the advantage of strong controllability, can improve the production efficiency and the product quality, broadens the source channel of the raw material, reduces the raw material cost and improves the economic benefit. The method for preparing theabrownin by using instant tea powder as a raw material comprises the following steps: A. selecting instant tea powder with the tea polyphenol content reaching the preset content; B. dissolving instant tea powder in water to obtain tea water solution; C. adding biological enzyme into the tea water solution for oxidation reaction; D. filtering and concentrating the tea water solution after the oxidation reaction to obtain a concentrated solution with a preset concentration; E. drying the concentrated solution to prepare powder to obtain the finished theabrownin product.
Description
Technical Field
The invention belongs to the technical field of food processing, and particularly relates to a preparation method of theabrownin.
Background
China is a world-wide tea-producing nation, and Chinese people have more than five thousand years of history of drinking tea, and the drinking tea is beneficial to the common knowledge of health people. Tea pigment, theabrownin and catechin in the tea have various effects of reducing blood fat, blood sugar and blood pressure, resisting oxidation, tumors, radiation, aging, cardiovascular and cerebrovascular diseases and the like, and the medicinal value of the tea is continuously valued by people. At present, people can extract and separate theabrownin from tea leaves, and the preparation method specifically comprises the steps of tea leaf leaching, multi-stage filtration, air-entrapping oxidation, reverse osmosis concentration, thermal concentration and the like, and has the following disadvantages:
the whole production process has long flow, large equipment investment and low production efficiency, and has ten working procedures from raw material input to theabrownin product output; the content of active ingredients of the product is low, and is only about 60 percent; the quality of the produced theabrownin is influenced by the quality of the raw materials and is not stable enough; a large amount of tea leaves and waste water are produced in the production process, the environmental pollution is great, and the site selection of a factory is greatly limited; the production process is very extensive, can not meet the requirements of fine chemical production, and has poor economic benefit.
Secondly, due to the long production process flow, the problem of frequent product quality fluctuation caused by human or equipment control errors in the production process is increased.
And thirdly, the raw materials can be purchased only nearby, so that the source of the raw materials is limited, the price of the raw materials is difficult to reduce, and the raw materials are easily influenced by natural disasters.
Disclosure of Invention
The invention aims to provide a method for preparing theabrownin by using instant tea powder as a raw material, which has the advantage of strong controllability, can improve the production efficiency and the product quality, broadens the source channel of the raw material, reduces the raw material cost and improves the economic benefit.
The method for preparing theabrownin by using instant tea powder as a raw material comprises the following steps:
A. selecting instant tea powder with the tea polyphenol content reaching the preset content;
B. dissolving instant tea powder in water to obtain tea water solution;
C. adding biological enzyme into the tea water solution for oxidation reaction;
D. filtering and concentrating the tea water solution after the oxidation reaction to obtain a concentrated solution with a preset concentration;
E. drying the concentrated solution to prepare powder to obtain the finished theabrownin product.
Specifically, the biological enzyme in the step C is pectin biological enzyme, and the tea water solution can better perform oxidation reaction under the catalytic action of the pectin biological enzyme.
In the preparation method of theabrownin, the instant tea powder with stable tea polyphenol content is directly adopted as the raw material, so that the source of the raw material is not limited by regions any more, the raw material can be imported from southeast Asia and the like, the price of the raw material is favorably reduced, the content of the tea polyphenol in the instant tea powder is 3-9 times of that of common tea or Pu' er tea, and the tea polyphenol is a main substance for converting the tea polyphenol into the theabrownin, so that the product produced by using the instant tea powder as the raw material has high theabrownin content, excellent quality and stable and reliable quality. The preparation method of the invention has the advantages that the production process flow is greatly shortened, the production procedures of tea extraction, slag discharge, filtration, fine filtration, membrane concentration and the like in the traditional preparation method are omitted, the fixed asset investment of a production line is saved, the production process is changed from a rough type to a fine chemical production mode, the human or equipment control errors in the production process are reduced, the preparation process is more accurate and controllable through the control of production process parameters, the quality of the produced theabrownin is more stable, and the content of effective components can reach more than 99%.
Drawings
Fig. 1 is a process flow diagram of the method for preparing theabrownin using instant tea powder as a raw material according to the present invention.
Detailed Description
The following description of the embodiments of the present invention, with reference to the accompanying drawings, will explain the working principles of the present invention in further detail.
Example 1:
the embodiment provides a method for preparing theabrownin by using instant tea powder as a raw material, which specifically comprises the following steps:
A. selecting instant tea powder with tea polyphenol content reaching a preset content, wherein the high-grade instant green tea powder is adopted in the embodiment, and the tea polyphenol content is more than or equal to 80%;
B. adding instant tea powder and purified water into a raw material extraction tank, heating to 40 ℃, and dynamically dissolving into a 10% tea water solution;
C. adding pectin biological enzyme into the tea water solution, and then carrying out oxidation reaction, wherein the addition standard of the pectin biological enzyme is that 100mg of biological enzyme is added into every 1Kg of tea water solution, the oxidation reaction is carried out by adding pure oxygen at 40 ℃ under two atmospheric pressures, and the oxidation reaction time is 60 minutes;
D. firstly, carrying out high-speed centrifugal separation on a tea water solution after oxidation reaction to remove particulate matters, and then sequentially carrying out super filtration, reverse osmosis concentration and vacuum concentration on the tea water solution to prepare a qualified concentrated solution; wherein the precision of the super filtration is 30 ten thousand of molecular weight, the multiple of the reverse osmosis concentration is 5-8 times, and the concentration mass percentage content of the concentrated solution after vacuum concentration reaches more than 30%;
E. spray drying the concentrated solution in a drying tower to prepare powder to obtain a theabrownin product, wherein the powder particles of the theabrownin finished product are smaller than 200 meshes, and the water content is smaller than 3%; and finally, carrying out product detection on the finished product of the theabrownin, packaging and warehousing.
The invention has been described in connection with the accompanying drawings, it is to be understood that the invention is not limited in its application to the details of construction and the arrangement of the components set forth in the following description, as long as the invention is capable of being practiced without modification in any way whatsoever, and is capable of other applications without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (8)
1. A method for preparing theabrownin by using instant tea powder as a raw material is characterized by comprising the following steps:
A. selecting instant tea powder with the tea polyphenol content reaching the preset content;
B. dissolving instant tea powder in water to obtain tea water solution;
C. adding biological enzyme into the tea water solution for oxidation reaction;
D. filtering and concentrating the tea water solution after the oxidation reaction to obtain a concentrated solution with a preset concentration;
E. drying the concentrated solution to prepare powder to obtain the finished theabrownin product.
2. The method for preparing theabrownin using instant tea powder as a raw material according to claim 1, wherein the bio-enzyme in the step C is pectin bio-enzyme.
3. The method for preparing theabrownin using instant tea powder as a raw material according to claim 1 or 2, wherein the predetermined content in the step a is 80% or more.
4. The method for preparing theabrownin using instant tea powder as a raw material according to claim 1 or 2, wherein the concentration of the aqueous tea solution in the step B is 10%.
5. The method for preparing theabrownin starting from instant tea powder as claimed in claim 1 or 2, wherein the standard of addition of the bio-enzyme in the step C is 100mg per 1Kg of tea aqueous solution.
6. The method for preparing theabrownin from instant tea powder as a raw material according to claim 1 or 2, wherein the step C is carried out by adding oxygen at 40 ℃ under two atmospheric pressures for an oxidation reaction time of 60 minutes.
7. The method for preparing theabrownin from instant tea powder as a raw material according to claim 1 or 2, characterized in that, in the step D, the tea aqueous solution after oxidation reaction is firstly subjected to centrifugal separation to remove particulate matters, and then the tea aqueous solution is subjected to super filtration, reverse osmosis concentration and vacuum concentration in sequence to obtain a concentrated solution; wherein the precision of the super filtration is 30 ten thousand molecular weight, the multiple of the reverse osmosis concentration is 5-8 times, and the concentration mass percentage content of the concentrated solution of the vacuum concentration reaches more than 30%.
8. The method for preparing theabrownin from instant tea powder as a raw material according to claim 1 or 2, wherein the step E is to dry the concentrated solution in a drying tower to prepare the theabrownin product, wherein the granule of the theabrownin product is less than 200 meshes and the water content is less than 3%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010608132.8A CN111685201A (en) | 2020-06-29 | 2020-06-29 | Method for preparing theabrownin by using instant tea powder as raw material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010608132.8A CN111685201A (en) | 2020-06-29 | 2020-06-29 | Method for preparing theabrownin by using instant tea powder as raw material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN111685201A true CN111685201A (en) | 2020-09-22 |
Family
ID=72484394
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010608132.8A Pending CN111685201A (en) | 2020-06-29 | 2020-06-29 | Method for preparing theabrownin by using instant tea powder as raw material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111685201A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3666484A (en) * | 1969-11-12 | 1972-05-30 | Lipton Inc Thomas J | Process for making a spray-dried instant tea of desired bulk density |
| CN1285152A (en) * | 2000-09-14 | 2001-02-28 | 龙坚 | High-active tawny agent and productive method thereof |
| CN1989851A (en) * | 2005-12-26 | 2007-07-04 | 康波 | Process for producing high purity food-grade tea pigment |
| CN103451233A (en) * | 2012-10-27 | 2013-12-18 | 陈小强 | Method for preparing theabrownin by taking tea polyphenol as active ingredients through adopting compound enzyme process |
-
2020
- 2020-06-29 CN CN202010608132.8A patent/CN111685201A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3666484A (en) * | 1969-11-12 | 1972-05-30 | Lipton Inc Thomas J | Process for making a spray-dried instant tea of desired bulk density |
| CN1285152A (en) * | 2000-09-14 | 2001-02-28 | 龙坚 | High-active tawny agent and productive method thereof |
| CN1989851A (en) * | 2005-12-26 | 2007-07-04 | 康波 | Process for producing high purity food-grade tea pigment |
| CN103451233A (en) * | 2012-10-27 | 2013-12-18 | 陈小强 | Method for preparing theabrownin by taking tea polyphenol as active ingredients through adopting compound enzyme process |
Non-Patent Citations (1)
| Title |
|---|
| 张芬等: "外源酶对六堡茶渥堆过程中色素转化规律影响", 《食品研究与开发》 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103265520B (en) | Method for preparing oligomeric proanthocyanidins and tannin pigment from grape seeds after winemaking | |
| CN109645304B (en) | Preparation method of mulberry leaf health food base material | |
| CN106381319A (en) | High-efficiency extraction and separation method of grape seed proanthocyanidin oligomer | |
| CN105255984A (en) | Method for converting ginsenoside through plant complex enzyme | |
| CN104788511A (en) | Method for preparing persimmon tannins with high micromolecular tannin content from persimmons | |
| CN106822196A (en) | A kind of method for extracting Ginkgo biloba polysaccharide and ginko leaves flavone simultaneously from ginkgo leaf | |
| CN104523836A (en) | Method for comprehensively extracting protein, polysaccharide and polyphenol from avocado kernels | |
| CN107114643B (en) | Red date health concentrated juice and preparation method thereof | |
| CN104478950A (en) | Method for extracting persimmon tannin high in small molecular tannin content from persimmon | |
| CN114515008A (en) | Cistanche tubulosa extract and preparation method thereof | |
| CN1927857A (en) | Extraction and purification process of buckwheat sprout total flavone | |
| CN104447897B (en) | A kind of method that persimmon tannin is extracted from persimmon | |
| CN101434972A (en) | Process for preparing Lonicera edulis anthocyanin by solid state biological reaction | |
| CN104450822A (en) | Method for producing theaflavin from tea polyphenol production wastewater | |
| CN111685201A (en) | Method for preparing theabrownin by using instant tea powder as raw material | |
| CN112806549A (en) | Ginger full-recycling treatment method | |
| CN107473979A (en) | A kind of processing method of film extraction theanine | |
| CN111574639B (en) | Method for separating and purifying nitraria tangutorum bobr polysaccharide | |
| CN104189087B (en) | A kind of method extracting total flavonoid functional materials from Folium Mori | |
| CN104876986B (en) | A kind of method of anthocyanin in extraction purple sweetpotato | |
| CN112375153A (en) | Method for extracting ginseng flower polysaccharide by utilizing multistage countercurrent-enzymolysis coupling technology | |
| CN112616976A (en) | Herbal medicine tea for sobering up, protecting liver, reducing blood fat and blood sugar | |
| KR101958442B1 (en) | Method for producing red ginseng extract concentrate with enhanced ginsenoside content | |
| CN108383891B (en) | Method for extracting saponin and co-producing kaempferol from camellia oleifera abel cake | |
| CN111096222A (en) | Method for improving content of ginsenoside in adventitious roots of ginseng by using immobilized chaetomium globosum spores |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200922 |