CN111602682A - 一种复方禽舍消毒剂及其制备方法 - Google Patents

一种复方禽舍消毒剂及其制备方法 Download PDF

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CN111602682A
CN111602682A CN202010608615.8A CN202010608615A CN111602682A CN 111602682 A CN111602682 A CN 111602682A CN 202010608615 A CN202010608615 A CN 202010608615A CN 111602682 A CN111602682 A CN 111602682A
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poultry house
disinfectant
traditional chinese
chinese medicine
compound
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徐仕睿
刘勇
刘威
李鹏
李天书
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Liaoning Dongke Pharmaceutical Co ltd
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Abstract

本发明公开了一种复方禽舍消毒剂及其制备方法，包括如下组份及重量百分比：具有杀菌功效的中药提取物5.0‑7.0％；N，N‑双(3‑氨基丙基)十二胺0‑0.8％；EDTA二钠0‑0.5％；聚已亚甲基盐酸0‑0.5％；聚乙烯吡咯烷酮0‑0.5％；PEG‑40氢化蓖麻油0.2‑0.6％；异丙醇2.0‑3.0％，乙基己基甘油0.8‑2.0％，余量为纯化水。本发明复方禽舍消毒剂具有如下优点：由于采用了有别于以往常规的化学消毒剂和中药类型消毒剂的制备方法，在高效杀菌、抑菌的同时，通过高倍稀释可降低消毒剂中化工产品的浓度与使用量，还兼顾了使用安全性与环境友好的问题，适合在禽舍杀菌中的大规模推广应用。

Description

一种复方禽舍消毒剂及其制备方法
技术领域
本发明属于消毒剂技术领域，涉及一种复方禽舍消毒剂及其制备方法。
背景技术
春季家禽最易感染各种疫病，搞好禽舍消毒是预防各种疫病发生的重要工作之一。密闭禽舍采用消毒剂进行熏蒸消毒，是一种重要的消毒手段。禽舍中的细菌主要包括埃希氏大肠杆菌、沙门氏菌、金黄色葡萄球菌等在内的多种细菌，这些细菌的传播能力极强，并会对家禽产生致命作用。因此选用一种安全高效、化学成分低且无毒副作用的消毒剂，对于禽舍消毒具有十分重要的意义。
通常情况下，市场上的禽舍消毒剂以化学消毒剂为主，另外还有少量的中药类型消毒剂。化学消毒剂的优点是杀菌高效，具有较好的广谱性；缺点是大量化学消毒剂的使用，会对家禽机体造成伤害，浓度较大时对禽舍环境造成污染。中药消毒剂的优点是使用安全，对环境友好；缺点也显而易见，就是杀菌能力不足，无法满足多种细菌环境的使用。
发明内容
本发明的目的是提供一种复方禽舍消毒剂及其制备方法，该消毒剂能有效克服现有禽舍消毒剂的不足。
本发明采用的技术方案为：
一、本发明——一种复方禽舍消毒剂，包括如下组份及重量百分比：具有杀菌功效的中药提取物5.0-7.0％；N，N-双(3-氨基丙基)十二胺0-0.8％；EDTA二钠0-0.5％；聚已亚甲基盐酸0-0.5％；聚乙烯吡咯烷酮0-0.5％；PEG-40氢化蓖麻油0.2-0.6％；异丙醇2.0-3.0％；乙基己基甘油0.8-2.0％，余量为纯化水。
上述具有杀菌功效中药提取物所采用的中药包括：①防治埃希氏大肠杆菌的中药：鱼腥草、苍术、黄芩、五倍子、肉桂、黄连、银翘、桑菊；②防治沙门氏菌的中药：石榴皮、黄柏、半枝莲、蒲公英、板蓝根、秦皮、苦参、野菊花；③防治金黄色葡萄球菌的中药：大黄、柴胡、丹参、黄芪、大青叶、芦荟，白头翁、甘草、铁苋中的一种或多种。
上述具有杀菌功效的中药提取物所采用的提取方法包括：超临界萃取、水提取或超声波提取方法中的一种或两种。
上述具有杀菌功效的中药提取物用量为5.5-6.5％。
上述N，N-双(3-氨基丙基)十二胺用量为0.2-0.3％。
上述EDTA二钠用量为0.3-0.5％。
上述聚已亚甲基盐酸用量为0.2-0.3％。
上述聚乙烯吡咯烷酮用量为0.3-0.4％。
上述PEG-40氢化蓖麻油用量为0.5-0.6％。
上述异丙醇用量为2.2-2.5％。
上述乙基己基甘油用量为1.0-1.5％。
二、本发明——一种复方禽舍消毒剂的制备方法，包括如下步骤：将总含量50％的纯化水加入容器中，在缓慢搅拌状态下向其中依次加入N，N-双(3-氨基丙基)十二胺、EDTA二钠、聚已亚甲基盐酸、聚乙烯吡咯烷酮、PEG-40氢化蓖麻油、异丙醇及具有杀菌功效的中药提取物，搅拌均匀后补加剩余50％的纯化水，快速搅拌10分钟后出料即得。
本发明复方禽舍消毒剂具有如下优点：由于采用了有别于以往常规的化学消毒剂和中药类型消毒剂的制备方法，在高效杀菌、抑菌的同时，通过高倍稀释可降低消毒剂中化工产品的浓度与使用量，还兼顾了使用安全性与环境友好的问题，适合在禽舍杀菌中的大规模推广应用。
采用新型“0添加防腐剂”原料乙基己基甘油，除了自身具有很好的防腐功能，同时与聚已亚甲基盐酸还可起到较强的增效作用，可大大降低防腐杀菌剂的用量。
具体实施方式
实施例1：
预先采用超临界萃取方法分别对苍术、黄柏和柴胡进行中药精华成分提取，待用。将100g纯化水加入烧瓶中，在缓慢搅拌状态下向其中依次加入N，N-双(3-氨基丙基)十二胺1g、EDTA二钠0.6g、聚已亚甲基盐酸0.5g、聚乙烯吡咯烷酮0.5g、PEG-40氢化蓖麻油0.8g、异丙醇5g、乙基己基甘油2.4g以及苍术提取物3g、黄柏提取物4g、柴胡提取物4g，搅拌30分钟。待烧瓶内溶液均一后，再加入100g纯化水，快速搅拌10分钟后出料，得到本专利消毒液产品221.8g。
实施例2：
预先采用水提取方法分别对五倍子、石榴皮和大青叶进行中药精华成分提取，待用。将150g纯化水加入烧瓶中，在缓慢搅拌状态下向其中依次加入N，N-双(3-氨基丙基)十二胺1.2g、EDTA二钠0.9g、聚已亚甲基盐酸0.8g、聚乙烯吡咯烷酮0.8g、PEG-40氢化蓖麻油0.7g、异丙醇7g、乙基己基甘油5g以及五倍子提取物8g、石榴皮提取物6g、大青叶提取物7g，搅拌30分钟。待烧瓶内溶液均一后，再加入150g纯化水，快速搅拌10分钟后出料，得到本专利消毒液产品337.3g。
实施例3：
预先采用超声波提取方法分别对黄芩、蒲公英和白头翁进行中药精华成分提取，待用。将200g纯化水加入烧瓶中，在缓慢搅拌状态下向其中依次加入N，N-双(3-氨基丙基)十二胺2g、EDTA二钠1.2g、聚已亚甲基盐酸1g、聚乙烯吡咯烷酮1g、PEG-40氢化蓖麻油1.6g、异丙醇10g、乙基己基甘油4.5g以及黄芩提取物8g、蒲公英提取物6g、白头翁提取物8g，搅拌30分钟。待烧瓶内溶液均一后，再加入200g纯化水，快速搅拌10分钟后出料，得到本专利消毒液产品443.3g。
实施例4：
预先采用超临界萃取方法分别对鱼腥草、秦皮和芦荟进行中药精华成分提取，待用。将100g纯化水加入烧瓶中，在缓慢搅拌状态下向其中依次加入N，N-双(3-氨基丙基)十二胺0.8g、EDTA二钠1g、聚已亚甲基盐酸0.8g、聚乙烯吡咯烷酮0.7g、PEG-40氢化蓖麻油0.9g、异丙醇5g、乙基己基甘油4g以及鱼腥草提取物5g、蒲公英提取物3g、白头翁提取物4g，搅拌30分钟。待烧瓶内溶液均一后，再加入100g纯化水，快速搅拌10分钟后出料，得到本专利消毒液产品225.2g。
实施例5：
预先采用超声波提取方法分别对桑菊、黄柏和甘草进行中药精华成分提取，待用。将400g纯化水加入烧瓶中，在缓慢搅拌状态下向其中依次加入N，N-双(3-氨基丙基)十二胺3.8g、EDTA二钠2.2g、聚已亚甲基盐酸1.9g、聚乙烯吡咯烷酮1.6g、PEG-40氢化蓖麻油2.5g、异丙醇18g、乙基己基甘油10g以及桑菊提取物15g、黄柏提取物10g、甘草提取物19g，搅拌30分钟。待烧瓶内溶液均一后，再加入400g纯化水，快速搅拌10分钟后出料，得到本专利消毒液产品884g。

Claims (10)

1.一种复方禽舍消毒剂，包括如下组份及重量百分比：具有杀菌功效的中药提取物5.0-7.0％；N，N-双(3-氨基丙基)十二胺0-0.8％；EDTA二钠0-0.5％；聚已亚甲基盐酸0-0.5％；聚乙烯吡咯烷酮0-0.5％；PEG-40氢化蓖麻油0.2-0.6％；异丙醇2.0-3.0％，乙基己基甘油0.8-2.0％，余量为纯化水。
2.根据权利要求1所述的一种复方禽舍消毒剂，其特征是：所述具有杀菌功效中药提取物所采用的中药包括：①防治埃希氏大肠杆菌的中药：鱼腥草、苍术、黄芩、五倍子、肉桂、黄连、银翘、桑菊；②防治沙门氏菌的中药：石榴皮、黄柏、半枝莲、蒲公英、板蓝根、秦皮、苦参、野菊花；③防治金黄色葡萄球菌的中药：大黄、柴胡、丹参、黄芪、大青叶、芦荟，白头翁、甘草、铁苋中的一种或多种。
3.根据权利要求1所述的一种复方禽舍消毒剂，其特征是：所述具有杀菌功效的中药提取物用量为5.5-6.5％。
4.根据权利要求1所述的一种复方禽舍消毒剂，其特征是：所述N，N-双(3-氨基丙基)十二胺用量为0.2-0.3％。
5.根据权利要求1所述的一种复方禽舍消毒剂，其特征是：所述EDTA二钠用量为0.3-0.5％。
6.根据权利要求1所述的一种复方禽舍消毒剂，其特征是：所述聚已亚甲基盐酸用量为0.2-0.3％。
7.根据权利要求1所述的一种复方禽舍消毒剂，其特征是：所述聚乙烯吡咯烷酮用量为0.3-0.4％。
8.根据权利要求1所述的一种复方禽舍消毒剂，其特征是：所述PEG-40氢化蓖麻油用量为0.5-0.6％。
9.根据权利要求1所述的一种复方禽舍消毒剂，其特征是：所述乙基己基甘油用量为1.0-1.5％。
10.一种复方禽舍消毒剂的制备方法，包括如下步骤：将总含量50％的纯化水加入容器中，在缓慢搅拌状态下向其中依次加入N，N-双(3-氨基丙基)十二胺、EDTA二钠、聚已亚甲基盐酸、聚乙烯吡咯烷酮、PEG-40氢化蓖麻油、异丙醇、乙基己基甘油，及具有杀菌功效的中药提取物，搅拌均匀后补加剩余50％的纯化水，快速搅拌10分钟后出料即得。
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