CN111544351A - A facial mask composition containing water extract of wood shavings, and its preparation method - Google Patents
A facial mask composition containing water extract of wood shavings, and its preparation method Download PDFInfo
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- CN111544351A CN111544351A CN202010411960.2A CN202010411960A CN111544351A CN 111544351 A CN111544351 A CN 111544351A CN 202010411960 A CN202010411960 A CN 202010411960A CN 111544351 A CN111544351 A CN 111544351A
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a hidden mark mask composition containing a wood shaving water extract and a preparation method thereof. The hidden mark mask composition comprises the following components in percentage by mass: 35.0-40.0% of wood shaving water extract (elm bark extract), 3.0-8.0% of glycerin, 0.1-0.3% of hydrolyzed collagen, 0.1-5.0% of panthenol, 0.1-0.5% of preservative and the balance of deionized water. The wood shaving water extract is an extract of the bark soak solution of the elm, belongs to a plant-extracted natural glycoprotein component, has high safety, contains various similar structures, can play the functions of the wood shaving water extract in multiple angles and multiple ways, and has the effects of tightening skin and reducing wrinkles. The preparation method comprises the following steps: pulverizing, soaking, extracting, filtering and compounding. The invention is not only simple and convenient to operate, but also has the advantages of good stability, low cost and simple application.
Description
Technical Field
The invention relates to a mask composition, belongs to the technical field of cosmetics, and particularly relates to a hidden mask composition containing a wood shaving water extract and a preparation method thereof.
Background
The wood shaving water is called sticking head tree in ancient times, Shanghai refers to coagulation wood shaving, which is the tree, and painters live friend and release the way in the self-speaking self-painting: "is also called" the elm. The wood shavings are elm wood shavings, contain glue juice in them, and are a necessary product for combing and caring hair for ancient women.
Ancient times, there were three hundred and sixty rows, of which the deal wood shavings were one row. A short foot long stool is carried by a vendor, a hole is formed in the front end of the stool surface, a bamboo rod with more than two feet is inserted into the hole, a string of serially overlapped condensed wood shavings is hung on the bamboo rod, the width of the bamboo rod is about two inches, the length of the bamboo rod is half of the length of the stool, a section of smooth yellowish rectangular elm wood is further arranged on the stool, the broad plane is slightly pushed, a piece of thin wavy condensed wood shavings form a commodity, the condensed wood shavings are soaked in hot water to seep viscous liquid, and then the liquid is filled into a shaving cylinder and is smeared on hair by a hairbrush. At a moment, the hair can be identified by shining, is convenient for combing and shaping, can emit light fragrance, has the effects of moistening and blackening the hair, and is a genuine natural green hair care product.
Until today, Beijing opera Danjiao is still under the ancient method, and the temple patches on the two sides of the cheek are not necessarily made of coagulated wood shavings. The white pulp inside the old elm bark is dried and called as wood shavings, and the wood shavings soaking water is the wood shavings water for the paster. The shaving lotion is skin-friendly, mild and non-irritating.
However, how to innovate again by using the 'condensed wood shavings' of the ancient method to obtain a brand-new facial mask product for the skin care product industry is a technical problem which needs to be solved urgently by technical personnel in the current field.
Disclosure of Invention
The invention aims to provide a hidden line mask composition containing a wood shaving water extract, which starts from the wisdom of the ancient traditional technology in China, and has various similar structures through modern technical innovation, so that the hidden line mask composition can play the functions of the mask in multiple angles and multiple ways and has the effects of tightening skin and fading wrinkles.
The invention also aims to provide a preparation method of the concealed mark facial mask composition containing the wood shaving water extract, which is simple and convenient to operate, and has the advantages of good stability, low cost and simplicity in application through crushing, soaking extraction, filtration and preparation processes.
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of a hidden mark mask composition containing a wood shaving water extract comprises the following raw materials in percentage by weight:
30.0 to 40.0 percent of wood shaving water extract (ulmus pumila bark extract);
3.0 to 8.0 percent of glycerin;
0.1 to 0.3 percent of hydrolyzed collagen;
0.1 to 5.0 percent of panthenol;
0.1 to 0.5 percent of preservative;
the balance being deionized water.
Further, the hidden-line mask composition containing the wood shaving water extract comprises the following components in percentage by mass:
35.0 to 40.0 percent of wood shaving water extract (ulmus pumila bark extract);
3.0 to 5.0 percent of glycerin;
0.1 to 0.3 percent of hydrolyzed collagen;
0.1 to 3.0 percent of panthenol;
0.5 percent of preservative;
the balance being deionized water.
Further, the mask composition comprises the following components in percentage by mass:
wood shaving water extract (Ulmus davidiana bark extract) 36.0%;
5.0% of glycerin;
0.2% of hydrolyzed collagen;
0.1% of panthenol;
0.5 percent of preservative;
the balance being deionized water.
By adopting the technical scheme, the manufacturing raw material is viscous liquid separated out by soaking the elm shavings in water, and the viscous liquid contains rich polysaccharide substances and has various effects of lifting and compacting instantly, smoothing wrinkles and the like.
Further, the aqueous extract of wood shavings is prepared by the following process steps, including raw material crushing, soaking, extraction, filtration and formulation. The method specifically comprises the following operation steps:
1) crushing: pulverizing cortex Ulmi Pumilae (wood shavings);
2) extraction: adding hot water (65-85 deg.C) into cortex Ulmi Pumilae (wood shavings), soaking for at least 6h, adding complex enzyme for extraction, and removing residue to obtain crude extractive solution;
3) and (3) filtering: settling the crude extract and filtering to obtain filtrate;
4) and (3) microfiltration: the filtrate is microfiltered to obtain percolate, and then water is added for continuous microfiltration until the total amount of the percolate is equal
The initial amount obtained in step three in the filtrate;
5) and (3) ultrafiltration: carrying out ultrafiltration on the percolate obtained in the step four, removing clear liquid and leaving concentrated solution;
6) preparation: and (3) preparing the concentrated solution in the step into a solution which is 20 percent of the crude drug by using deionized water.
Through adopting above-mentioned technical scheme, above-mentioned wood shavings (elm bark) raw and other materials are all adopted natural plant to be raw and other materials, and green is pollution-free, adopts the compound enzyme (for example, collagenase, cellulase and protease) extraction of plant class, can effective enzymolysis raw and other materials (the medicinal material) for the active ingredient in the raw and other materials can be fully decomposed out.
Then, primary filtration, microfiltration and ultrafiltration are adopted, namely, a plurality of filtration modes are matched for use, so that complex enzyme can be effectively screened, and effective separation between the enzyme and filtrate (also can be concentrated solution or percolate) is effectively realized; but also can remove insoluble substances in the filtrate, reduce the stimulation effect of the insoluble substances on the skin, obtain the filtrate with relatively low molecular weight, and be beneficial to promoting the absorption effect on the skin.
Furthermore, in the step 1), the particle size of the wood shavings (elm bark) obtained after crushing is controlled between 100 meshes and 120 meshes.
Because the wood shavings (elm barks) are blocky, the extraction efficiency of the complex enzyme is lower by directly adopting the complex enzyme, the contact area between the complex enzyme and the wood shavings (elm barks) can be effectively improved after the crushing treatment, and the enzymolysis efficiency and quality are greatly improved.
Further, in the step 2), the complex enzyme is a mixture of two or three of 0.6-2.2% of pectinase, 0.6-2.2% of cellulase and 0.6-1.5% of protease.
Further, the cellulase is one or more of C-1 enzyme, C-x enzyme and beta glucosidase; the C-1 enzyme is an enzyme that acts initially on cellulose, disrupting the crystalline structure of the cellulose chain; the C-x enzyme is cellulase which acts on cellulose activated by the C-1 enzyme and decomposes beta-1, 4-glycosidic bonds; beta-glucosidase can break down cellobiose, cellotriose and other low molecular cellodextrins to glucose.
Further, the protease is plant protease, preferably papain. The natural plant is rich in pectin, cellulose and protein, and is extracted by using complex enzyme (pectinase, cellulase and protease), so that the enzymolysis effect on the raw materials can be effectively improved, and the active ingredients (namely effective ingredients) in the raw materials are more efficiently released.
Further, in the step 2), the temperature during extraction is controlled to be 0-82 ℃, and the extraction time is 3-4 h. During extraction, the preferred extraction temperature is 50-55 ℃; the pH during extraction is 4-6.5, preferably 5.5-6.5. The pectinase is obtained by fermenting and refining Aspergillus niger. The pectinase is mainly used for juicing and clarifying fruit and vegetable juice beverages and fruit wine, and has a good effect of decomposing pectin. The appropriate temperature of the pectinase is about 20-55 ℃, and the optimal temperature is 50 ℃; the pH is 4-6.
The cellulase is a complex enzyme system consisting of a plurality of hydrolytic enzymes, and a plurality of fungi in nature can secrete the cellulase. The cellulase is suitably at a temperature of 25-30 deg.C and a pH of 5.5-6.5.
In addition, proteases are a class of enzymes (enzymes) in the body that are effective in breaking down proteins. The breakdown method is to break peptide bonds that link amino acids into polypeptide chains. Wherein the papain is extracted from fructus Chaenomelis, and the optimum temperature is about 50 deg.C. Therefore, the complex enzyme has the strongest activity at the temperature of 50-55 ℃ and the pH value of 5.5-5.5.
Further, in the step 4), the aperture of the filtering membrane is 30nm, the pressure for microfiltration is 3-5bar, and the microfiltration is carried out at the temperature of 50-80 ℃ until the percolate can not seep out. The pressurized microfiltration operation is carried out under the filtering membrane with the aperture of 30nm, so that the filtering efficiency is effectively improved.
Further, in the step 5), the cut-off molecular weight of the filtering membrane is controlled at 50000D, the ultrafiltration is carried out at the pressure of 10-15bar and the temperature of 50-80 ℃. The pressurization operation is carried out in the ultrafiltration process, and the ultramicro efficiency can be improved on the basis of ensuring the effective ultramicro.
Further, in the step 6), 0.3 to 1 weight percent of preservative is added, and sterilization treatment is carried out; the preservative is selected from one or more of methylparaben, chlorphenesin and phenoxyethanol.
Further, the preservative comprises 0.5% of menthone and 0.5% of hexanediol by weight percentage. Preservative such as carithamine and 0.5% hexanediol are added to improve the storage time of the composition.
In addition, the preparation method of the hidden mark mask containing the wood shaving water extract comprises the following steps:
1) adding glycerol into a water phase pot, starting stirring, sequentially adding hydrolyzed collagen and panthenol, heating to 82 ℃, and keeping the temperature for 12 minutes until the glycerol is completely dissolved;
2) keeping the stirring speed of an emulsifying pot at 350 r/min, sucking the components obtained in the step 1) in vacuum, homogenizing at low speed for 3 min, and cooling; cooling to 55 deg.C, adding the water extract of wood shavings into the emulsifying pot, stirring, and stirring;
3) stirring and cooling to below 42 ℃, adding the preservatives in sequence, and stirring for 15 minutes until the mixture is uniform; cooling to 37 deg.C, filtering and discharging; and (5) inspecting, discharging and filling.
In conclusion, the invention has the following beneficial effects:
1) the invention has the advantages of immediate compactness, fine grain fading, good stability, low cost and simple application;
2) the hidden mark mask composition disclosed by the invention is prepared from natural plants, so that pollution is avoided, and the safety is high;
3) the invention adopts a plurality of filtering modes to be matched for use, not only can effectively screen the complex enzyme, but also can effectively realize the effective separation between the enzyme and the filtrate (also can be concentrated solution or percolate); but also can remove insoluble substances in the filtrate, reduce the stimulation effect of the insoluble substances on the skin, obtain the filtrate with relatively low molecular weight, and be beneficial to promoting the absorption effect on the skin.
Drawings
FIG. 1 is a process flow diagram of a method for preparing an aqueous extract of wood wool in accordance with an embodiment of the present invention.
Detailed Description
The present invention will be described in more detail below with reference to specific preferred embodiments and examples of effects, but the present invention is not limited to the following examples.
The invention discloses a hidden mark mask composition containing a wood shaving water extract and a preparation method thereof. According to the total mass percentage of the composition, the hidden mark mask composition comprises the following raw material components: 35.0-40.0% of wood shaving water extract (elm bark extract), 3.0-8.0% of glycerin, 0.1-0.3% of hydrolyzed collagen, 0.1-5.0% of panthenol, 0.1-0.5% of preservative and the balance of deionized water.
The wood shaving water extract is an extract of a bark soak solution of Ulmus pumila (Ulmus Campesris), belongs to a plant extract natural glycoprotein component, is safe, contains various similar structures, can play a role in multiple angles and ways, and has the effects of tightening skin and smoothing wrinkles. The formula is as follows: the raw materials comprise 100 percent of elm bark and the balance of water.
The preparation method of the mask composition comprises the following steps: pulverizing, soaking, extracting, filtering and compounding. The invention is not only simple and convenient to operate, but also has the advantages of good stability, low cost and simple application. The hidden-line mask prepared by using the wood shaving water extract creates innovation on the dosage form and the application range of the mask.
The invention makes a major breakthrough in the biological enzymolysis technology and the innovative extraction technology and develops the wood shaving water extract for preparing the hidden-line mask. The water extract of wood shavings has the characteristics of instant effect, instant invisible wrinkles and instant beautiful and plastic contours, and the usage is very simple and only needs to be smeared.
After the facial mask is applied to the face, a layer of invisible transparent firm film is formed on the surface of the skin. The drying thickness is about 50 microns, the invisible sticking on the skin is more than 18 hours, and the user can independently control the sticking time on the skin.
The wrinkles on the skin can be instantly hidden and disappear under the action of the 'hidden line mask' attachment. The effect of improving rough and large wrinkles of the skin after use is particularly obvious. The invisible wrinkles of the invisible line mask can simultaneously play a role in tightening and lifting, so that the mandible, the cheek and the statute lines are visualized, and the clear change of the face contour can be seen at a glance.
Example 1 preparation of aqueous extract of wood shavings
A preparation method of water extract of wood shavings is shown in figure 1, and comprises the following operation steps:
firstly, crushing: dried elm bark is added into a universal pulverizer small-sized pulverizer (the manufacturer is Jiangyin union mechanical equipment Co., Ltd.) with the model of WF-180 for pulverizing operation, and the obtained particle size is 100-120 meshes.
II, extraction: soaking 50kg of raw materials (i.e. 50kg of pulverized elm bark) in 500kg of deionized water for 6h, and then adding 0.8kg of pectinase, 0.6kg of cellulase and 0.4kg of papain; then extracting at 65 deg.C for 3 hr with traditional Chinese medicine extraction, filtration, concentration and external circulation equipment (manufacturer is Zhongli filtration equipment Co., Ltd., Hainin), and removing residue with filter (manufacturer is Zhongli filtration equipment Co., Ltd., Hainin) to obtain crude extractive solution.
The plant extraction device with patent number CN201620115696.7 can also be used as the equipment required in the specific production process.
Thirdly, filtering: and (3) standing the crude extract obtained in the step two for 30 minutes, and filtering substances in the crude extract after the substances are settled through a B870 model plate-frame type polypropylene filter plate (which is environment-friendly and is a source-developing source), so as to obtain a filtrate.
Fourthly, microfiltration: filtering the filtrate with a filter membrane with a cut-off pore size of 30nm at 4bar and 60 deg.C, microfiltering until the percolate can no longer seep out, and supplementing equal amount of water to continue microfiltering until the amount of percolate is equal to that of the initial filtrate.
Fifthly, ultrafiltration: and (3) adopting a filtering membrane with the molecular weight cutoff of 50000D to filter the filtrate obtained in the fourth step at the operating pressure of 12bar and the temperature of 60 ℃ to carry out ultrafiltration operation, and removing the filtered clear liquid to leave a concentrated solution.
Sixthly, preparation: preparing the concentrated solution from the above steps with deionized water to 40% of the crude drug, adding 0.13W/W% (weight percent) methyl hydroxybenzoate and 0.13W/W% (weight percent) chlorphenesin, and sterilizing at 90 deg.C for 30 min.
Example 2 preparation of aqueous extract of wood shavings
A preparation method of a wood shaving water extract comprises the following operation steps:
firstly, crushing: dried elm bark is added into a universal pulverizer small-sized pulverizer (the manufacturer is Jiangyin union mechanical equipment Co., Ltd.) with the model of WF-180 for pulverizing operation, and the particle size of the obtained elm bark is all 100-120 meshes.
II, extraction: soaking 50kg of raw materials (i.e. 50kg of pulverized elm bark) in 650kg of deionized water for 5h, and then adding 1kg of pectinase, 0.6kg of cellulase and 0.5kg of papain; then extracting at 80 deg.C for 3.5h by using traditional Chinese medicine extraction, filtration and concentration external circulation equipment (manufacturer is Zhongli filtration equipment Co., Ltd., Hainin), and removing residue by using filter (manufacturer is Zhongli filtration equipment Co., Ltd., Hainin) to obtain crude extract. The plant extraction device with patent number CN201620115696.7 can also be used as the equipment required in the specific production process.
Thirdly, filtering: and (3) standing the crude extract obtained in the step two for 2 hours, and filtering substances in the crude extract after the substances are settled through a B870 model plate-frame type polypropylene filter plate (environmental friendly, and source is created) to obtain a filtrate.
Fourthly, microfiltration: filtering the filtrate with a filter membrane with a cut-off pore diameter of 30nm at 5bar and 55 deg.C, microfiltering until the percolate can not seep out, and supplementing equal amount of water to continue microfiltering until the amount of percolate is equal to that of the initial filtrate.
Fifthly, ultrafiltration: and D, adopting a filtering membrane with the molecular weight cutoff of 50000D to filter the filtrate obtained in the fourth step, wherein the operating pressure is 15bar, and the temperature is 80 ℃ for ultrafiltration operation, and removing the filtered clear liquid to leave a concentrated solution.
Sixthly, preparation: preparing the concentrated solution from the above steps with deionized water to 40% of crude drug, adding 0.13W/W% methyl hydroxybenzoate and 0.13W/W% chlorphenesin, and sterilizing at 95 deg.C for 30 min.
Example 3 preparation of aqueous extract of wood shavings
A preparation method of a wood shaving water extract comprises the following operation steps:
firstly, crushing: dried elm bark is added into a universal pulverizer small-sized pulverizer (the manufacturer is Jiangyin union mechanical equipment Co., Ltd.) with the model of WF-180 for pulverizing operation, and the obtained elm bark particles are all 120 meshes 100-.
II, extraction: soaking 60kg of raw materials (60 kg of pulverized elm bark) in 1000kg of deionized water for 8h, and then adding 2kg of pectinase, 1.5kg of cellulase and 1kg of papain; then extracting at 50 deg.C for 3 hr with traditional Chinese medicine extraction, filtration and concentration external circulation equipment (manufacturer is Zhongli filtration equipment Co., Ltd., Hainin), and removing residue with filter (manufacturer is Zhongli filtration equipment Co., Ltd., Hainin) to obtain crude extractive solution.
Thirdly, filtering: and (3) standing the crude extract obtained in the step two for 2 hours, and filtering substances in the crude extract after the substances are settled through a B870 model plate-frame type polypropylene filter plate (environmental friendly, and source is created) to obtain a filtrate.
Fourthly, microfiltration: filtering the filtrate with a filter membrane with a cut-off pore diameter of 30nm at an operating pressure of 3bar and a temperature of 85 deg.C, microfiltering until the percolate can no longer seep out, and then supplementing an equal amount of water to continue microfiltering until the amount of percolate is equal to the amount of the initial filtrate.
Fifthly, ultrafiltration: and D, adopting a filtering membrane with the molecular weight cutoff of 50000D to filter the filtrate obtained in the fourth step, wherein the operating pressure is 10bar, and the temperature is 85 ℃ for ultrafiltration operation, and removing the filtered clear liquid to leave a concentrated solution.
Sixthly, preparation: preparing the concentrated solution from the above steps with deionized water to 40% of crude drug, adding 0.13W/W% methyl hydroxybenzoate and 0.13W/W% chlorphenesin, and sterilizing at 90 deg.C for 30 min.
Example 4 (preparation of a mask pack containing aqueous extracts of wood shavings)
The mask composition comprises the following raw material components in percentage by mass:
the wood shaving water extract (ulmus pumila bark extract) of example 1 was 35.0%, glycerin was 3.0%, hydrolyzed collagen was 0.3%, panthenol was 5.0%, preservative was 0.1%, and the balance was deionized water.
Example 5 (preparation of a mask pack containing aqueous extracts of wood shavings)
The mask composition comprises the following raw material components in percentage by mass:
the wood shaving water extract (ulmus pumila bark extract) of example 2 was 38.0%, glycerin was 5.0%, hydrolyzed collagen was 0.2%, panthenol was 0.5%, preservative was 0.3%, and the balance was deionized water.
Example 6 (preparation of a mask pack containing aqueous extracts of wood shavings)
The mask composition comprises the following raw material components in percentage by mass:
the wood shaving water extract (ulmus pumila bark extract) of example 3 was 40.0%, glycerin was 8.0%, hydrolyzed collagen was 0.3%, panthenol was 0.2%, preservative was 0.1%, and the balance was deionized water.
The method for preparing the mask pack containing the wood shaving water extract of the above examples 4 to 6 includes the steps of:
1) adding glycerol into water phase pot, stirring, sequentially adding hydrolyzed collagen and panthenol, heating to 82 deg.C, and maintaining the temperature until completely dissolved;
2) keeping the stirring speed of the emulsifying pot at 350 r/min, sucking the components obtained in the step 1) in vacuum, homogenizing at low speed, and cooling; cooling to 55 deg.C, adding the water extract of wood shavings into the emulsifying pot, stirring, and stirring;
3) stirring and cooling to below 42 ℃, adding the preservatives in sequence, and stirring for 15 minutes until the mixture is uniform; cooling to 37 deg.C, filtering and discharging; and (5) inspecting, discharging and filling.
Comparative example 1
An aqueous extract of wood wool, differing from example 1 in that: the formulation was identical to that of example 1, but the preparation process was different.
The formula is as follows: the raw materials comprise 100 percent of elm bark and the balance of water.
The method of preparing the aqueous extract of wood wool of comparative example 1 above, comprising the steps of:
1) extraction: extracting 50kg of raw material (50 kg of pulverized elm bark) with 500kg of deionized water at 95 deg.C under stirring for 4 hr, and removing residue to obtain crude extractive solution;
2) and (3) refrigerating: putting the crude extract into a refrigeration house at 4 ℃, and refrigerating for 8 h;
3) and (3) filtering: filtering with diatomite via a plate and frame diatomite filter (Shandong engineering and mechanical Co., Ltd.);
4) preparation: preparing the extract solution by deionized water into 40 percent of the crude drug, adding 0.13W/W percent of methylparaben and 0.13W/W percent of chlorphenesin, and sterilizing at 90 ℃ for 30min to obtain the extract solution of the scheme.
Comparative example 2
An aqueous extract of wood wool, differing from example 1 in that: the formulation was identical to that of example 1, but the preparation process was different.
The formula is as follows: the raw materials comprise 100 percent of elm bark and the balance of water.
The method of preparing the aqueous extract of wood wool of comparative example 2 above, comprising the steps of:
1) extraction: extracting 50kg of raw materials (50 kg of pulverized elm bark) with 6500kg of deionized water at 40 deg.C under stirring for 2 hr, and mixing the crude extractive solutions;
2) and (3) refrigerating: putting the crude extract into a refrigeration house at 4 ℃, and refrigerating for 5 h;
3) and (3) filtering: filtering with gauze;
4) preparation: preparing 40% of the crude drug by deionized water, adding 0.13W/W% of methylparaben and 0.13W/W% of chlorphenesin, and sterilizing at 90 ℃ for 30min to obtain the aqueous extract of the wood shaving.
The following is a content of the effect application test example section.
Effect test example 1 (detection analysis)
1) The instant tightening effect experiment test object comprises the following steps:
s1, taking 35W/W% of the water extract of the shavings obtained in examples 1-3 and comparative examples 1-2 with instant tightening and anti-aging effects and 50ml of deionized water for later use.
S2, sequentially adding A, D phase raw materials (namely deionized water, glycerol, methyl hydroxybenzoate and chlorphenesin) into a main pot according to the mixture ratio of the hidden pattern mask of the wood shaving water extract shown in the table 2, stirring and heating to 85 ℃ for 20min to completely dissolve the raw materials; cooling to 50 deg.C, adding B, C phase (35W/W% of the water extract of the wood shavings with immediate firmness and anti-aging property obtained in example 1, hydrolyzed collagen protein and panthenol), and stirring to obtain test sample 1.
S3, sequentially replacing the composition with immediate tightness and anti-aging effect obtained in the example 1 with 50W/W% of the phase B raw material with the compositions with immediate tightness and anti-aging effect obtained in the example 2, the example 3, the comparative example 1 and the comparative example 2 with equal amount, and deionized water. Then, test sample 2, test sample 3, control sample 2, and blank control were obtained in this order according to the preparation method in S2.
TABLE 1 index results for aqueous wood wool extract
TABLE 2 hidden pattern mask formula of wood shavings water extract (weight percentage content%)
The test method comprises the following steps: 30 healthy volunteers participated in the experiment (different from the above experiment), and the age of the male and female was between 25-55 years, and each group had 5 members. And 30 healthy volunteers (i.e., subjects) had not participated in any clinical test method for drugs, cosmetics or health products in the last three months: random, double blind, control methods were used.
The specific operation steps are as follows:
1) marking the regions of the subject to be examined with the instrument by using a template prepared in advance, wherein each region has a size of 2.5cm2；
2) Respectively smearing any one of sample samples 1-3 and control samples 1-2 on random 5 areas of the left arm and the right arm of a subject, and smearing blank control on the remaining 2 areas;
3) removing blank control areas of left and right arms, marking all test areas with skin marker pen, continuously using sample for 4 months in the morning and evening respectively, with sample usage amount of 2-2.5mg/cm2；
3) Any other skin care products or medicines cannot be used within 30 days;
4) the test instrument is Corneometer (CK) and skin elasticity tester; the test time points are before the sample is used and after the sample is used for 4 months (the control group is before the sample is smeared, and the test is carried out after the sample 1-3 and the control sample 1-2 are used for 4 months), before the test, the skin is cleaned by water, and after the skin is dried for 30min, the measurement is carried out (the environment temperature of a laboratory is controlled to be 20 +/-1 ℃, and the relative humidity is 48 +/-2%);
5. the original life rule is kept during the experiment.
The formula for detection is: r5 ═ Ur/Ue
Where Ur refers to the portion of the skin that recovers quickly and Ue refers to the portion that springs up quickly due to suction.
In table 3: significance is high, P < 0.01; indicates significant difference, P < 0.05.
Table 3 skin elasticity test results
As can be seen from the test results in Table 3, R5 values for test samples 1-3 were all greater than 0.8, the skin viscoelasticity of test samples 1-3 increased significantly from that before application, with P < 0.01; whereas the control samples 1-2 showed no significant change in R5, P <0.05, which remained around 0.78. From the above results, it can be seen that the test samples 1-3 have the effects of increasing skin elasticity and long-acting anti-aging, and have significant statistical significance.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.
Claims (10)
1. A mask composition comprising a wood shaving water extract, characterized in that: according to the total mass percentage of the composition, the hidden mark mask consists of the following components:
30.0 to 40.0 percent of wood shaving water extract; the wood shaving water extract is a ulmus pumila bark extract;
3.0 to 8.0 percent of glycerin;
0.1 to 0.3 percent of hydrolyzed collagen;
0.1 to 5.0 percent of panthenol;
0.1 to 0.5 percent of preservative;
the balance being deionized water.
2. The mask pack composition comprising an aqueous extract of wood shavings according to claim 1, wherein: according to the total mass percentage of the composition, the hidden mark mask consists of the following components:
35.0 to 40.0 percent of wood shaving water extract; the wood shaving water extract is a ulmus pumila bark extract;
3.0 to 5.0 percent of glycerin;
0.1 to 0.3 percent of hydrolyzed collagen;
0.1 to 3.0 percent of panthenol;
0.5 percent of preservative;
the balance being deionized water.
3. The mask pack composition comprising an aqueous extract of wood shavings according to claim 1, wherein: according to the total mass percentage of the composition, the hidden mark mask consists of the following components:
36.0% of wood shaving water extract; the wood shaving water extract is a ulmus pumila bark extract;
5.0% of glycerin;
0.2% of hydrolyzed collagen;
0.1% of panthenol;
0.5 percent of preservative;
the balance being deionized water.
4. The mask pack composition according to any one of claims 1 to 3, comprising an aqueous extract of wood shavings: the wood shaving water extract is prepared by the following steps:
1) crushing: pulverizing cortex Ulmi Pumilae (wood shavings);
2) extraction: adding hot water into cortex Ulmi Pumilae (wood shavings), soaking at 65-85 deg.C for at least 6 hr, adding complex enzyme for extraction, and removing residue to obtain crude extractive solution;
3) and (3) filtering: settling the crude extract and filtering to obtain filtrate;
4) and (3) microfiltration: carrying out microfiltration on the filtrate to obtain a percolate, and then adding water for continuous microfiltration until the total amount of the percolate is equal to the initial amount of the filtrate obtained in the step 3);
5) and (3) ultrafiltration: carrying out ultrafiltration on the percolate obtained in the step 4), removing clear liquid and leaving concentrated solution;
6) preparation: and preparing the concentrated solution in the step into a liquid medicine which is 20 percent of the weight of the crude drug by using deionized water.
5. The mask pack composition comprising an aqueous extract of wood shavings according to claim 4, wherein: in the step 1), the particle size of the bark (wood shavings) of the ulmus pumila obtained after crushing is controlled to be between 100 meshes and 120 meshes.
6. The mask pack composition comprising an aqueous extract of wood shavings according to claim 4, wherein: in the step 2), the complex enzyme is a mixture of two or three of 0.6-2.2% of pectinase, 0.6-2.2% of cellulase and 0.6-1.5% of protease; the extraction temperature is controlled at 0-82 deg.C, and the extraction time is 3-4 h.
7. The mask pack composition comprising an aqueous extract of wood shavings according to claim 4, wherein: in the step 3), the aperture of the filter membrane is 30nm, the pressure for microfiltration is 3-4bar, and the microfiltration is carried out at the temperature of 50-80 ℃ until the percolate can not seep out.
8. The mask pack containing the wood wool water extract according to claim 4, wherein: in the step 4), the cut-off molecular weight of the filtering membrane is controlled at 50000D, the ultrafiltration pressure is 10-15bar, and the ultrafiltration operation is carried out at the temperature of 50-80 ℃.
9. The mask pack containing the wood wool water extract according to claim 4, wherein: in the step 6), 0.1 to 0.5 weight percent of preservative is also added, and sterilization treatment is carried out; the antiseptic is selected from one or more of menthone, hexanediol, methyl paraben, chlorphenesin and phenoxyethanol.
10. The method for preparing a mask pack containing an aqueous extract of wood shavings according to any one of claims 1 to 9, comprising the steps of:
1) adding glycerol into water phase pot, stirring, sequentially adding hydrolyzed collagen and panthenol, heating to 82 deg.C, and maintaining the temperature until completely dissolved;
2) keeping the stirring speed of the emulsifying pot at 350 r/min, sucking the components obtained in the step 1) in vacuum, homogenizing at low speed, and cooling; cooling to 55 deg.C, adding the water extract of wood shavings into the emulsifying pot, stirring, and stirring;
3) stirring and cooling to below 42 ℃, adding the preservatives in sequence, and stirring for 15 minutes until the mixture is uniform; cooling to 37 deg.C, filtering and discharging; and (5) inspecting, discharging and filling.
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| KR960021002A (en) * | 1994-12-23 | 1996-07-18 | 성재갑 | Radical scavenger containing extract of elm and anti-aging cosmetic composition containing same |
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