CN111450009B - Anti-discoloration lipstick raincoat composition and preparation method thereof - Google Patents
Anti-discoloration lipstick raincoat composition and preparation method thereof Download PDFInfo
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- CN111450009B CN111450009B CN202010372771.9A CN202010372771A CN111450009B CN 111450009 B CN111450009 B CN 111450009B CN 202010372771 A CN202010372771 A CN 202010372771A CN 111450009 B CN111450009 B CN 111450009B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a color-fading-preventing lipstick raincoat composition and a preparation method thereof, wherein the color-fading-preventing lipstick raincoat composition comprises the following raw materials: fumed silica, pullulan, noni fruit extract and water; the preparation method comprises the steps of adding the fumed silica, the pullulan and the noni fruit extract into water according to the formula ratio, and carrying out ultrasonic treatment to obtain the noni fruit extract. According to the lipstick raincoat composition, fumed silica, pullulan and noni fruit extracts are used as main raw materials to be compounded to obtain the anti-decoloration lipstick raincoat composition, a layer of compact protective film can be formed to separate lipstick from the outside, the lipstick can be effectively prevented from being stained with a cup and losing color, a good moisturizing effect is achieved, moisture of lips can be locked, and lip chapping is avoided; meanwhile, the film forming effect of the pullulan polysaccharide and the noni fruit extract can be enhanced through ultrasonic treatment, the moisture-preserving and water-locking effect is enhanced, the stability of the lipstick raincoat under the high-temperature condition is improved, and the decoloring is effectively prevented.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a lipstick raincoat composition for preventing discoloration and a preparation method thereof.
Background
The makeup is to apply cosmetics and tools, and the face, five sense organs and other parts of the human body are rendered, drawn and arranged by adopting steps and skills according to rules, so that the three-dimensional impression is enhanced, the shape and color are adjusted, the defects are covered, and the expression is magical, thereby achieving the purpose of beautifying the visual perception. In recent years, the market demand of color cosmetics products is rapidly rising, lip products are diversified, and lipstick is one of the cosmetics which are used most by women in daily life. The lipstick can color the lips and improve the mental appearance of people, but the traditional lipstick is lack of substantivity, is easy to dry or aggregate or crack on the lips along with the time, has low persistence and is easy to fade.
The lipstick raincoat is used for fixing the lipstick, the main components of the raincoat are silica extract and poly-perfluoromethyl isopropyl ether, and after the raincoat is smeared on the lips, a layer of protective film is formed to separate the lipstick from the external environment, so that the lipstick can be effectively prevented from being stained on a cup and removed from the makeup.
CN108815019A discloses an anti-discoloration lipstick raincoat, which comprises the following raw materials in parts by weight: 0.5-6 parts of polydimethylsiloxane and polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked copolymer, 5-15 parts of polydimethylsiloxane, 60-70 parts of spherical silicon resin powder, 2-3 parts of jojoba oil, 1-3 parts of shea butter and 0.1-1 part of tocopherol. The lipstick can prevent lips from drying and cracking, and prevent lipstick from being stained on a cup and losing color.
CN109864896A discloses an anti-discoloration lipstick raincoat composition, which comprises the following raw materials in parts by weight: 95-98% of poly-perfluoromethyl isopropyl ether, 1-2% of fumed silica, 0.1-1% of vitamin C, 0.1-1% of glycerol and the balance of aloe extract. The lipstick can prevent lipstick from being stained on the cup, has good moistening and moisturizing effects, and can prevent lips from being chapped.
The research shows that the research on the lipstick raincoat is less at present, and the existing lipstick raincoat has poor stability under the high-temperature condition and is easy to decolor. Therefore, it is highly desirable to provide an anti-discoloring lipstick raincoat composition with good stability under high temperature conditions and a preparation method thereof.
Disclosure of Invention
In order to solve the technical problems, the invention provides an anti-decoloring lipstick raincoat composition and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
the anti-fading lipstick raincoat composition comprises the following raw materials: fumed silica, pullulan, noni fruit extract and water.
Preferably, the anti-fading lipstick raincoat composition comprises the following raw materials in parts by weight: 30-50 parts of fumed silica, 5-10 parts of pullulan, 7-13 parts of noni extract and 50-70 parts of water.
Further preferably, the anti-fading lipstick raincoat composition comprises the following raw materials in parts by weight: 32-48 parts of fumed silica, 6-9 parts of pullulan, 8-12 parts of noni extract and 55-65 parts of water.
Further preferably, the mass ratio of the pullulan polysaccharide to the noni fruit extract is 7: 9-11.
Preferably, the preparation method of the noni fruit extract comprises the following steps:
(1) slicing, drying and crushing noni to obtain noni powder;
(2) adding a cyclodextrin aqueous solution into the noni powder obtained in the step (1), and performing ultrasonic extraction, suction filtration and concentration to obtain a concentrated solution;
(3) and (3) adding absolute ethyl alcohol into the concentrated solution obtained in the step (2), precipitating with ethanol, and centrifuging to remove supernatant to obtain the noni extract.
Preferably, the pulverization in step (1) is to a particle size of 20 to 30 μm.
Preferably, the mass percentage of the cyclodextrin water solution in the step (2) is 1-3%, and the ultrasonic extraction conditions are as follows: the ultrasonic power is 200-300kw, and the time is 10-15 min.
Preferably, the addition amount of the absolute ethyl alcohol in the step (3) is 4-5 times of the volume of the concentrated solution; the alcohol precipitation is performed by standing for 12-24h at 1-4 ℃; the centrifugation is carried out for 10-15min at 3000r/min 2000-.
The invention also provides a preparation method of the lipstick raincoat composition, which comprises the following steps: adding the fumed silica, the pullulan and the noni fruit extract into water according to the formula ratio, and carrying out ultrasonic treatment to obtain the lipstick raincoat composition.
Preferably, the conditions of the ultrasonic treatment are: the temperature is 30-45 ℃, the ultrasonic power is 450-500kw, and the time is 5-10 min.
The invention has the beneficial effects that:
(1) according to the invention, the fumed silica, the pullulan and the noni fruit extract are compounded as main raw materials to obtain the anti-decoloration lipstick raincoat composition, a layer of compact protective film can be formed to separate lipstick from the outside, the lipstick can be effectively prevented from being stained with a cup and fading, and meanwhile, the lipstick raincoat composition has a good moisturizing effect, can lock water in the lips and avoids lip chapping.
(2) In the preparation process, the film forming effect of the pullulan polysaccharide and the noni fruit extract can be enhanced through ultrasonic treatment, the moisturizing and water locking effect is enhanced, the stability of the lipstick raincoat under the high-temperature condition is improved, and the decoloring is effectively prevented.
Detailed Description
The embodiments of the present invention are described below with reference to specific embodiments, and other advantages and effects of the present invention will be easily understood by those skilled in the art from the disclosure of the present specification. The invention is capable of other and different embodiments and of being practiced or of being carried out in various ways, and its several details are capable of modification in various respects, all without departing from the spirit and scope of the present invention.
Before the present embodiments are further described, it is to be understood that the scope of the invention is not limited to the particular embodiments described below; it is also to be understood that the terminology used in the examples is for the purpose of describing particular embodiments only, and is not intended to limit the scope of the present invention.
When numerical ranges are given in the examples, it is understood that both endpoints of each of the numerical ranges and any value therebetween can be selected unless the invention otherwise indicated. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
The sources of the raw materials used in the present invention are not limited, and the raw materials used in the present invention are all those commonly available in the art unless otherwise specified.
Example 1
The anti-fading lipstick raincoat composition comprises the following raw materials in parts by weight: 30 parts of fumed silica, 5 parts of pullulan, 7 parts of noni fruit extract and 50 parts of water;
the preparation method of the noni fruit extract comprises the following steps:
(1) slicing noni fruit, drying, and pulverizing to particle size of 20 μm to obtain noni fruit powder;
(2) according to the mass ratio of 1: 5, adding 1% of cyclodextrin water solution in percentage by mass into the noni powder obtained in the step (1), performing ultrasonic extraction for 10min at the power of 300kw, performing suction filtration, and concentrating to obtain a concentrated solution;
(3) according to the volume ratio of 1: 4, adding absolute ethyl alcohol into the concentrated solution obtained in the step (2), standing at 1 ℃ for alcohol precipitation for 12 hours, and then centrifuging at 2000r/min for 15min to remove supernatant, so as to obtain the noni fruit extract;
the preparation method of the lipstick raincoat composition comprises the following steps: adding the formula amount of fumed silica, pullulan and noni fruit extract into water, and treating for 10min at the temperature of 30 ℃ and the ultrasonic power of 450kw to obtain the lipstick raincoat composition.
Example 2
The anti-fading lipstick raincoat composition comprises the following raw materials in parts by weight: 50 parts of fumed silica, 10 parts of pullulan, 13 parts of noni fruit extract and 70 parts of water;
the preparation method of the noni fruit extract comprises the following steps:
(1) slicing noni fruit, drying, and pulverizing to 30 μm to obtain noni fruit powder;
(2) according to the mass ratio of 1: 5, adding a 3% cyclodextrin aqueous solution in percentage by mass into the noni powder obtained in the step (1), performing ultrasonic extraction for 15min at the power of 200kw, performing suction filtration, and concentrating to obtain a concentrated solution;
(3) according to the volume ratio of 1: 5, adding absolute ethyl alcohol into the concentrated solution obtained in the step (2), standing at 4 ℃, precipitating with ethanol for 24 hours, and then centrifuging at 3000r/min for 10 minutes to remove supernatant, so as to obtain the noni fruit extract;
the preparation method of the lipstick raincoat composition comprises the following steps: adding the formula amount of fumed silica, pullulan and noni fruit extract into water, and treating for 5min at 45 ℃ and 500kw of ultrasonic power to obtain the lipstick raincoat composition.
Example 3
The anti-fading lipstick raincoat composition comprises the following raw materials in parts by weight: 40 parts of fumed silica, 7 parts of pullulan, 10 parts of noni fruit extract and 60 parts of water.
The preparation method of the noni fruit extract comprises the following steps:
(1) slicing noni fruit, drying, and pulverizing to particle size of 25 μm to obtain noni fruit powder;
(2) adding 2% by mass of cyclodextrin aqueous solution into the noni powder obtained in the step (1), performing ultrasonic extraction for 12min at the power of 250kw, performing suction filtration, and concentrating to obtain a concentrated solution;
(3) according to the volume ratio of 1: 4.5, adding absolute ethyl alcohol into the concentrated solution obtained in the step (2), standing at the temperature of 2 ℃, precipitating with ethanol for 18h, and centrifuging at the speed of 2500r/min for 13min to remove supernatant, thus obtaining the noni fruit extract.
The invention also provides a preparation method of the lipstick raincoat composition, which comprises the following steps: adding the formula amount of fumed silica, pullulan and noni fruit extract into water, and carrying out ultrasonic treatment for 7min at the temperature of 40 ℃ and the ultrasonic power of 480kw to obtain the lipstick raincoat composition.
Example 4
The difference between the embodiment and the embodiment 3 is that the lipstick raincoat composition comprises the following raw materials in parts by weight: 35 parts of fumed silica, 7 parts of pullulan, 9 parts of noni fruit extract and 58 parts of water.
Example 5
The difference between the embodiment and the embodiment 3 is that the lipstick raincoat composition comprises the following raw materials in parts by weight: 45 parts of fumed silica, 7 parts of pullulan, 11 parts of noni fruit extract and 68 parts of water.
Example 6
The difference between the embodiment and the embodiment 3 is that the lipstick raincoat composition comprises the following raw materials in parts by weight: 40 parts of fumed silica, 8 parts of pullulan, 8 parts of noni fruit extract and 60 parts of water.
Comparative example 1
This comparative example differs from example 3 in that it does not contain noni fruit extract.
Comparative example 2
This comparative example differs from example 3 in that no pullulan was included.
Comparative example 3
This comparative example differs from example 3 in that fumed silica is not included.
Comparative example 4
The comparative example is different from example 3 in that the ultrasonic treatment is replaced by stirring in the preparation process of the lipstick raincoat composition, the stirring speed is 300rpm, and the stirring time is 30 min.
Comparative example 5
The comparative example is different from example 3 in that the ultrasonic treatment temperature is 50 ℃ and the ultrasonic power is 550kw during the preparation of the lipstick raincoat composition for 5 min.
Comparative example 6
This comparative example differs from example 3 in that water is used instead of the aqueous cyclodextrin solution in the preparation of the noni powder extract.
Experimental example A lipstick dipping cup test
325 female volunteers aged 25-55 years were selected, randomly divided into 13 groups by age, 25 persons in each group, the volunteers painted with lipstick of the same type for 2min, respectively painted with the lipstick raincoat compositions prepared in examples 1-6 and comparative examples 1-6 with a cotton swab, and after 3min, respectively tested for the condition of dipping in the lipstick with a paper cup, a white porcelain cup and a clear glass cup, wherein the control group was not painted with the lipstick raincoat composition, and the statistical results are shown in table 1.
TABLE 1
From the above-mentioned examples 1-6, the lipstick raincoat composition prepared by the present invention has a good non-stick effect on paper cups, porcelain cups and glass cups, and meanwhile, according to the examples 3-5, when the mass ratio of pullulan to noni fruit extract is 7:9-11, the prepared lipstick raincoat composition has a good non-stick effect.
Experimental example II high temperature cup adhesion detection
325 female volunteers aged 25-55 years were selected, randomly divided into 13 groups by age, 25 persons in each group, the volunteers painted with lipstick of the same type for 2min, respectively painted with the lipstick raincoat compositions prepared in examples 1-6 and comparative examples 1-6 with cotton sticks, and 5min later, the condition of dipping the cups with transparent glass cups at 40 ℃ was tested, wherein the lipstick raincoat composition was not painted in the control group, and the statistical results are shown in table 2.
TABLE 2
From the above-mentioned examples 1-6, it can be seen that the high-temperature glass cup non-stick effect of the lipstick raincoat composition prepared by the invention is good, and meanwhile, according to the examples 3-5, when the mass ratio of the pullulan polysaccharide to the noni fruit extract is 7:9-11, the prepared lipstick raincoat composition has good high-temperature stability and good non-stick effect.
Experimental example three moisturizing effect test
325 female volunteers were randomly divided into 13 groups of 25 persons, and lipstick (2 mg/cm) of the same type was first applied to lips2) After 2min, the lipstick raincoat compositions prepared in examples 1-6 and comparative examples 1-6 were applied by cotton swab (1 mg/cm)2) Lip skin humidity was measured using a skin hygrometer model CM825 (CK, germany) at 25 ℃ under an environment of 50% relative humidity at 1h, 2h, and 4h after using the product, respectively, wherein the control group was not coated with the lipstick raincoat composition, 3 times per measurement, and the average value was taken, as shown in table 3.
Table 3 lip skin moisture content%
As can be seen from the above table of examples 1-6, the lipstick raincoat composition prepared by the invention has good moisturizing and water locking effects, and still keeps higher moisture content in 4 h; according to the lip skin content of the examples 3-5, when the mass ratio of the pullulan polysaccharide to the noni fruit extract is 7:9-11, the prepared lipstick raincoat composition has better moisturizing and water locking performances.
In conclusion, the anti-decoloring lipstick raincoat composition is obtained by compounding the fumed silica, the pullulan and the noni fruit extract serving as main raw materials, can form a layer of compact protective film to separate lipstick from the outside, can effectively prevent the lipstick from sticking to a cup and fading, has a good moisturizing effect, can lock water on lips, and avoids lip chapping.
Meanwhile, the film forming effect of the pullulan polysaccharide and the noni fruit extract can be enhanced through ultrasonic treatment in the preparation process, the moisturizing and water locking effect is enhanced, the stability of the lipstick raincoat under the high-temperature condition is improved, and the decoloring is effectively prevented.
The present invention has been further described with reference to specific embodiments, which are only exemplary and do not limit the scope of the present invention. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention, and that such changes and modifications may be made without departing from the spirit and scope of the invention.
Claims (6)
1. The anti-fading lipstick raincoat composition is characterized by comprising the following raw materials in parts by weight: 30-50 parts of fumed silica, 5-10 parts of pullulan, 7-13 parts of noni extract and 50-70 parts of water;
the preparation method of the noni fruit extract comprises the following steps:
(1) slicing, drying and crushing noni to obtain noni powder;
(2) adding a cyclodextrin aqueous solution into the noni powder obtained in the step (1), and performing ultrasonic extraction, suction filtration and concentration to obtain a concentrated solution;
(3) adding absolute ethyl alcohol into the concentrated solution obtained in the step (2), precipitating with ethanol, and centrifuging to remove supernatant to obtain the noni extract;
the mass percentage of the cyclodextrin water solution in the step (2) is 1-3%;
the preparation method of the lipstick raincoat composition comprises the following steps: adding the fumed silica, the pullulan and the noni fruit extract into water according to the formula ratio, and carrying out ultrasonic treatment to obtain the lipstick raincoat composition; the ultrasonic treatment conditions are as follows: the temperature is 30-45 ℃, the ultrasonic power is 450-500kw, and the time is 5-10 min.
2. The lipstick raincoat composition as claimed in claim 1, comprising the following raw materials in parts by weight: 32-48 parts of fumed silica, 6-9 parts of pullulan, 8-12 parts of noni extract and 55-65 parts of water.
3. The lipstick raincoat composition as claimed in claim 1, wherein the mass ratio of the pullulan to the noni fruit extract is 7: 9-11.
4. The lipstick raincoat composition as claimed in claim 1, wherein the pulverization in step (1) is to a particle size of 20-30 μm.
5. The lipstick raincoat composition as claimed in claim 1, wherein the ultrasonic extraction conditions in step (2) are as follows: the ultrasonic power is 200-300kw, and the time is 10-15 min.
6. The lipstick raincoat composition as claimed in claim 1, wherein the absolute ethyl alcohol is added in the step (3) in an amount of 4-5 times the volume of the concentrate; the alcohol precipitation is performed by standing for 12-24h at 1-4 ℃; the centrifugation is carried out for 10-15min at 3000r/min 2000-.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3972997A (en) * | 1973-10-16 | 1976-08-03 | Sumitomo Chemical Company, Limited | Novel cosmetics containing pullulan |
| JPH0242011A (en) * | 1988-08-02 | 1990-02-13 | Kobayashi Kose Co Ltd | Film like make-up cosmetic |
| CN102671591A (en) * | 2012-05-26 | 2012-09-19 | 云南恩典科技产业发展有限公司 | Water-encapsulated microcapsule wall material and water-encapsulated microcapsule prepared through same |
| CN109864896A (en) * | 2019-04-02 | 2019-06-11 | 广州果感生物科技有限公司 | A kind of lipstick Combined raincoat object of Anti-fade and preparation method thereof |
-
2020
- 2020-05-06 CN CN202010372771.9A patent/CN111450009B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3972997A (en) * | 1973-10-16 | 1976-08-03 | Sumitomo Chemical Company, Limited | Novel cosmetics containing pullulan |
| JPH0242011A (en) * | 1988-08-02 | 1990-02-13 | Kobayashi Kose Co Ltd | Film like make-up cosmetic |
| CN102671591A (en) * | 2012-05-26 | 2012-09-19 | 云南恩典科技产业发展有限公司 | Water-encapsulated microcapsule wall material and water-encapsulated microcapsule prepared through same |
| CN109864896A (en) * | 2019-04-02 | 2019-06-11 | 广州果感生物科技有限公司 | A kind of lipstick Combined raincoat object of Anti-fade and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 环糊精及其衍生物在中药提取中的应用研究进展;杨建文等;《药物评价研究》;20150430;第38卷(第2期);第208-213页 * |
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