CN111135213A - Processing and preparation method of Xiaojin pills - Google Patents
Processing and preparation method of Xiaojin pills Download PDFInfo
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- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
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- A61K36/32—Burseraceae (Frankincense family)
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- A61K36/328—Commiphora, e.g. mecca myrrh or balm of Gilead
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- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/42—Cucurbitaceae (Cucumber family)
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
- A61K36/714—Aconitum (monkshood)
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- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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Abstract
The invention discloses a processing and preparation method of Xiaojin pills, which comprises the following steps: preparing the following raw materials by weight: 20-30g of artificial musk, 155g of cochinchina momordica seed, 145-155g of prepared kusnezoff monkshood root, 145g of liquidambar formosana maxim, 145g of prepared frankincense, 65-75g of prepared myrrh, 140g of trogopterus dung fried with vinegar, 65-75g of Chinese angelica, 145g of earthworm, 135-12 g of fragrant ink; sterilizing; vacuum drying; sieving with a sieve of 150-; soaking in clear water; heating 50-70g of honey to boil for 5-15min, and then filtering to remove impurities to obtain refined honey; mixing and making into pill; drying at 50-70 deg.C by a drier, screening the pill with particle size of 3-4mm to obtain small golden pill, and quality-testing and packaging. The method has the advantages of excellent content uniformity of the Xiaojin pills, simple operation, better mixing uniformity, contribution to improving the quality uniformity of the Chinese medicinal preparation, simple process route and easy realization.
Description
Technical Field
The invention belongs to the field of pharmacy, and particularly relates to a processing and preparation method of Xiaojin pills.
Background
The Xiaojin pill is collected and carried by Chinese pharmacopoeia (2010 edition), consists of ten medicinal materials such as musk, cochinchina momordica seed, prepared kusnezoff monkshood root, sweetgum resin, frankincense, myrrh, trogopterus dung, Chinese angelica, earthworm, Chinese ink and the like, has the effects of eliminating stagnation, reducing swelling, removing blood stasis and relieving pain, is widely used for clinically treating diseases such as early carbuncle on the yin, multiple abscess, goiter, scrofula, mammary nodule and the like, and is a first-choice Chinese patent medicine for clinically treating breast diseases at present. In the traditional production process of the Xiaojin pill, due to the properties, dosage proportions and other reasons of the medicinal materials, the powder mixing uniformity of the Xiaojin pill is poor, the quality uniformity is difficult to ensure, and further the problems of uneven color, obvious odor difference, large batch difference and the like of the Xiaojin pill product generally exist.
Disclosure of Invention
The invention aims to overcome the problems in the prior art and provides a processing and preparation method of Xiaojin pills.
In order to achieve the technical purpose and achieve the technical effect, the invention is realized by the following technical scheme:
a processing and preparation method of Xiaojin pills comprises the following steps: (ii) a
The method comprises the following steps: preparing the following raw materials by weight: 20-30g of artificial musk, 155g of cochinchina momordica seed, 145-155g of prepared kusnezoff monkshood root, 145g of liquidambar formosana maxim, 145g of prepared frankincense, 65-75g of prepared myrrh, 140g of trogopterus dung fried with vinegar, 65-75g of Chinese angelica, 145g of earthworm, 135-12 g of fragrant ink;
step two: putting all raw materials into a sterilization chamber for sterilization treatment, continuously and uniformly inputting high-pressure steam into the sterilization chamber, wherein the duration time of the high-pressure steam is 60-80min, and the temperature is controlled at 120-;
step three: after the steam input is finished, the sterilization chamber is pumped to vacuum for drying, the drying temperature is controlled at 180 ℃, and the drying time is 1-2 hours;
step four: crushing the dried raw materials by a crusher, and sieving the crushed raw materials by a sieve of 150-200 meshes to obtain raw material mixed powder;
step five: then putting the mixed powder of the raw materials into clear water for soaking, concentrating for three times, and decocting for one hour each time to obtain a raw material mixture;
step six: heating 50-70g of honey to boil for 5-15min, and then filtering to remove impurities to obtain refined honey;
step seven: finally, mixing the raw material mixture, the refined honey and 80g of starch, adding 5-10g of clear water, stirring to form paste, and feeding the paste into a medicine refining machine to prepare pills;
step eight: drying at 50-70 deg.C by a drier, screening the pill with particle size of 3-4mm to obtain small golden pill, and quality-testing and packaging.
Further, the medicine is prepared in the first step according to the following raw materials by weight: 25g of artificial musk, 150g of semen momordicae, 150g of prepared kusnezoff monkshood root, 140g of resina liquidambaris, 65g of prepared frankincense, 70g of prepared myrrh, 135g of trogopterus dung fried with vinegar, 70g of Chinese angelica with wine, 140g of earthworm and 11g of fragrant ink.
Further, the density of the finished product of the small golden pills is 0.4-0.5g/cm 3.
The invention has the beneficial effects that:
the method has the advantages of excellent content uniformity of the Xiaojin pills, simple operation, better mixing uniformity, contribution to improving the quality uniformity of the Chinese medicinal preparation, simple process route and easy realization.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
a processing and preparation method of Xiaojin pills comprises the following steps: (ii) a
The method comprises the following steps: preparing the following raw materials by weight: 25g of artificial musk, 150g of semen momordicae, 150g of prepared kusnezoff monkshood root, 140g of resina liquidambaris, 65g of prepared frankincense, 70g of prepared myrrh, 135g of trogopterus dung fried with vinegar, 70g of Chinese angelica, 140g of earthworm and 11g of fragrant ink;
step two: putting all raw materials into a sterilization chamber for sterilization treatment, continuously and uniformly inputting high-pressure steam into the sterilization chamber, wherein the duration of the high-pressure steam is 70min, and the temperature is controlled at 125 ℃;
step three: after the steam input is finished, the sterilization chamber is vacuumized to be dried, the drying temperature is controlled to be 165 ℃, and the drying time is 1.5 hours;
step four: crushing the dried raw materials by a crusher, and sieving the crushed raw materials by a 175-mesh sieve to obtain raw material mixed powder;
step five: then putting the mixed powder of the raw materials into clear water for soaking, concentrating for three times, and decocting for one hour each time to obtain a raw material mixture;
step six: heating 60g of honey to boil for 10min, and then filtering to remove impurities to obtain refined honey;
step seven: finally, mixing the raw material mixture, the refined honey and 80g of starch, adding 7g of clear water, stirring to form paste, and feeding the paste into a medicine refining machine to prepare pills;
step eight: drying at 60 deg.C by a drier, and screening pellets with particle size of 3.5mm to obtain small gold pill product with density of 0.45g/cm3And performing quality inspection and packaging.
Example 2:
a processing and preparation method of Xiaojin pills comprises the following steps: (ii) a
The method comprises the following steps: preparing the following raw materials by weight: 20g of artificial musk, 145g of semen momordicae, 145g of prepared kusnezoff monkshood root, 135g of sweetgum resin, 60g of prepared frankincense, 65g of prepared myrrh, 130g of trogopterus dung fried with vinegar, 65g of wine-treated Chinese angelica, 135g of earthworm and 10g of fragrant ink;
step two: putting all raw materials into a sterilization chamber for sterilization treatment, continuously and uniformly inputting high-pressure steam into the sterilization chamber, wherein the duration of the high-pressure steam is 60min, and the temperature is controlled at 120 ℃;
step three: after the steam input is finished, the sterilization chamber is vacuumized to be dried, the drying temperature is controlled at 150 ℃, and the drying time is 1 hour;
step four: crushing the dried raw materials by a crusher, and sieving the crushed raw materials by a 150-mesh sieve to obtain raw material mixed powder;
step five: then putting the mixed powder of the raw materials into clear water for soaking, concentrating for three times, and decocting for one hour each time to obtain a raw material mixture;
step six: heating 50g of honey to boil for 5min, and then filtering to remove impurities to obtain refined honey;
step seven: finally, mixing the raw material mixture, the refined honey and 80g of starch, adding 5g of clear water, stirring to form paste, and feeding the paste into a medicine refining machine to prepare pills;
step eight: drying at 50 deg.C by a drier, and screening pellets with particle size of 3mm to obtain small gold pill product with density of 0.4g/cm3And performing quality inspection and packaging.
Example 3:
a processing and preparation method of Xiaojin pills comprises the following steps: (ii) a
The method comprises the following steps: preparing the following raw materials by weight: 30g of artificial musk, 155g of semen momordicae, 155g of prepared kusnezoff monkshood root, 145g of resina liquidambaris, 70g of prepared frankincense, 75g of prepared myrrh, 140g of trogopterus dung fried with vinegar, 75g of Chinese angelica with wine, 145g of earthworm and 12g of fragrant ink;
step two: putting all raw materials into a sterilization chamber for sterilization treatment, continuously and uniformly inputting high-pressure steam into the sterilization chamber, wherein the duration of the high-pressure steam is 80min, and the temperature is controlled at 130 ℃;
step three: after the steam input is finished, the sterilization chamber is vacuumized to be dried, the drying temperature is controlled at 180 ℃, and the drying time is 2 hours;
step four: crushing the dried raw materials by a crusher, and sieving the crushed raw materials by a 200-mesh sieve to obtain raw material mixed powder;
step five: then putting the mixed powder of the raw materials into clear water for soaking, concentrating for three times, and decocting for one hour each time to obtain a raw material mixture;
step six: heating 70g of honey to boil for 15min, and then filtering to remove impurities to obtain refined honey;
step seven: finally, mixing the raw material mixture, the refined honey and 80g of starch, adding 10g of clear water, stirring to form paste, and feeding the paste into a medicine refining machine to prepare pills;
step eight: drying at 70 deg.C by a drier, and screening pellets with particle size of 4mm to obtain small gold pill product with density of 0.5g/cm3And performing quality inspection and packaging.
In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed.
Claims (3)
1. A processing and preparation method of Xiaojin pills is characterized in that: the processing and preparation method comprises the following steps: (ii) a
The method comprises the following steps: preparing the following raw materials by weight: 20-30g of artificial musk, 155g of cochinchina momordica seed, 145-155g of prepared kusnezoff monkshood root, 145g of liquidambar formosana maxim, 145g of prepared frankincense, 65-75g of prepared myrrh, 140g of trogopterus dung fried with vinegar, 65-75g of Chinese angelica, 145g of earthworm, 135-12 g of fragrant ink;
step two: putting all raw materials into a sterilization chamber for sterilization treatment, continuously and uniformly inputting high-pressure steam into the sterilization chamber, wherein the duration time of the high-pressure steam is 60-80min, and the temperature is controlled at 120-;
step three: after the steam input is finished, the sterilization chamber is pumped to vacuum for drying, the drying temperature is controlled at 180 ℃, and the drying time is 1-2 hours;
step four: crushing the dried raw materials by a crusher, and sieving the crushed raw materials by a sieve of 150-200 meshes to obtain raw material mixed powder;
step five: then putting the mixed powder of the raw materials into clear water for soaking, concentrating for three times, and decocting for one hour each time to obtain a raw material mixture;
step six: heating 50-70g of honey to boil for 5-15min, and then filtering to remove impurities to obtain refined honey;
step seven: finally, mixing the raw material mixture, the refined honey and 80g of starch, adding 5-10g of clear water, stirring to form paste, and feeding the paste into a medicine refining machine to prepare pills;
step eight: drying at 50-70 deg.C by a drier, screening the pill with particle size of 3-4mm to obtain small golden pill, and quality-testing and packaging.
2. The processing and preparation method of the Xiaojin pills according to claim 1, which is characterized in that: preparing the following raw materials in the first step by weight: 25g of artificial musk, 150g of semen momordicae, 150g of prepared kusnezoff monkshood root, 140g of resina liquidambaris, 65g of prepared frankincense, 70g of prepared myrrh, 135g of trogopterus dung fried with vinegar, 70g of Chinese angelica with wine, 140g of earthworm and 11g of fragrant ink.
3. The processing and preparation method of the Xiaojin pills according to claim 1, which is characterized in that: the density of the finished product of the Xiaojin pill is 0.4-0.5g/cm3。
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010041968.4A CN111135213A (en) | 2020-01-15 | 2020-01-15 | Processing and preparation method of Xiaojin pills |
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| CN202010041968.4A CN111135213A (en) | 2020-01-15 | 2020-01-15 | Processing and preparation method of Xiaojin pills |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1726969A (en) * | 2005-06-30 | 2006-02-01 | 成都永康制药有限公司 | Small golden pellets and preparation method |
| CN104306474A (en) * | 2014-10-29 | 2015-01-28 | 成都中医药大学 | Process for preparing xiaojin pill |
| CN105168407A (en) * | 2015-09-01 | 2015-12-23 | 成都九芝堂金鼎药业有限公司 | Preparation method of Xiaojin pills |
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- 2020-01-15 CN CN202010041968.4A patent/CN111135213A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1726969A (en) * | 2005-06-30 | 2006-02-01 | 成都永康制药有限公司 | Small golden pellets and preparation method |
| CN104306474A (en) * | 2014-10-29 | 2015-01-28 | 成都中医药大学 | Process for preparing xiaojin pill |
| CN105168407A (en) * | 2015-09-01 | 2015-12-23 | 成都九芝堂金鼎药业有限公司 | Preparation method of Xiaojin pills |
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