CN111067133B - Preparation method of vinous low-temperature non-combustion reconstituted tobacco - Google Patents
Preparation method of vinous low-temperature non-combustion reconstituted tobacco Download PDFInfo
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- CN111067133B CN111067133B CN201911349936.4A CN201911349936A CN111067133B CN 111067133 B CN111067133 B CN 111067133B CN 201911349936 A CN201911349936 A CN 201911349936A CN 111067133 B CN111067133 B CN 111067133B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
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Abstract
The invention discloses a preparation method of vinous low-temperature non-combustion reconstituted tobacco, which comprises the following steps: mixing the solid residues extracted from the vinasse, the solid residues extracted from the tobacco, wood pulp fibers and fillers for pulping to prepare a sheet base; mixing the vinasse extracting solution, the tobacco extracting solution, the atomizing agent, the adhesive, the spice and the solvent to prepare a coating liquid; and coating the prepared coating liquid on the prepared film base, and drying to obtain the vinous low-temperature non-combustion reconstituted tobacco. The vinasse is used as the raw material, vinasse is kept to the maximum extent, vinasse aroma substances contained in the vinasse are kept, the atomization effect is good, the surface is not adhered, the processing resistance is good, smoke can be uniformly released during smoking, and the vinasse low-temperature non-combustion reconstituted tobacco prepared by the preparation method is good in taste and good in sensory effect during smoking.
Description
Technical Field
The invention relates to the field of cigarette production, in particular to a preparation method of vinous low-temperature non-combustion reconstituted tobacco.
Background
The low-temperature non-combustion cigarette refers to a novel tobacco product which heats tobacco leaves through a special heating source to provide tobacco flavor substances and nicotine feeling for consumers, and is not a mode of combusting tobacco substances. Compared with the traditional cigarette, the low-temperature non-combustion cigarette can ensure that the tobacco substances are just heated to a degree of giving off the flavor under the condition of not igniting the tobacco leaves. Generally, when a traditional cigarette is smoked, the temperature can reach 600 ℃ to 900 ℃, a plurality of harmful substances can be generated, and the heating temperature of the low-temperature non-burning cigarette is below 500 ℃, so that the harmful substances can be obviously reduced.
The reconstituted tobacco is a reprocessed tobacco product, and has strong controllability of physical characteristics and related chemical components. The research focus of the existing low-temperature non-burning cigarettes mainly focuses on the development of smoking sets, particularly heaters, and the research on the low-temperature non-burning tobacco leaves with novel characteristic fragrance is less.
Therefore, how to provide the low-temperature non-combustion reconstituted tobacco with novel characteristic fragrance becomes a technical problem which needs to be solved urgently in the field.
Disclosure of Invention
The invention aims to provide a novel technical scheme of a preparation method of vinous low-temperature non-combustion reconstituted tobacco with novel characteristic fragrance and low-temperature non-combustion reconstituted tobacco.
According to the first aspect of the invention, a preparation method of vinous low-temperature non-combustion reconstituted tobacco is provided.
The preparation method of the vinous low-temperature non-burning reconstituted tobacco comprises the following steps:
(1) mixing and pulping the distillers 'grains extracted solid residue, the tobacco extracted solid residue, the wood pulp fiber and the filler according to the mass ratio of the distillers' grains to the tobacco before extraction to the wood pulp fiber and the filler of (30-60) to (30-50) to (0-20) to (0-30) to prepare a sheet base;
(2) mixing the vinasse extracting solution, the tobacco extracting solution, the atomizing agent, the adhesive, the spice and the solvent according to the mass ratio of (10-30) to (0-20) to prepare a coating liquid;
(3) and (3) coating the coating liquid prepared in the step (2) on the film base prepared in the step (1), and drying to obtain the vinous low-temperature non-combustion reconstituted tobacco.
Optionally, the distiller's grains before extraction in the step (1) are one or more of sorghum distiller's grains, corn distiller's grains, rice distiller's grains, soybean distiller's grains and potato distiller's grains.
Optionally, the tobacco before extraction in the step (1) is one or more of tobacco stem, tobacco leaf, tobacco powder and ash stick.
Optionally, the wood pulp fiber in the step (1) is one or more of softwood pulp, hardwood pulp and gramineous pulp.
Optionally, the filler in the step (1) is calcium carbonate.
Optionally, the density of the distiller's grains extract and the tobacco extract in the step (2) is 1.10-1.20g/cm3。
Optionally, the atomizing agent in the step (2) is one or more of propylene glycol, glycerol, ethanol and ethyl acetate.
Optionally, the adhesive in the step (2) is one or more of carboxymethyl cellulose, sodium alginate, guar gum and chitosan.
Optionally, the perfume in step (2) is one or more of vanillin, megastigmatrienone, dihydroactinidiolide, beta-ionone, geranyl acetone, benzoic acid, phenylacetic acid, benzyl alcohol, phenethyl alcohol, isovaleric acid, ethyl acetate, ethyl butyrate, ethyl lactate, ethyl caprylate, ethyl heptanoate and ethyl 2-methyl butyrate.
Optionally, the mass percentage of the solvent in the step (2) in the coating liquid is 10% -20%.
The vinasse is used as the raw material, vinasse is kept to the maximum extent, vinasse aroma substances contained in the vinasse are kept, the atomization effect is good, the surface is not adhered, the processing resistance is good, smoke can be uniformly released during smoking, and the vinasse low-temperature non-combustion reconstituted tobacco prepared by the preparation method is good in taste and good in sensory effect during smoking.
Detailed Description
Various exemplary embodiments of the present invention will now be described in detail. It should be noted that: the relative arrangement of the components and steps, the numerical expressions and numerical values set forth in these embodiments do not limit the scope of the present invention unless specifically stated otherwise.
The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses.
Techniques, methods, and apparatus known to those of ordinary skill in the relevant art may not be discussed in detail but are intended to be part of the specification where appropriate.
In all examples shown and discussed herein, any particular value should be construed as merely illustrative, and not limiting. Thus, other examples of the exemplary embodiments may have different values.
The preparation method of the vinous low-temperature non-combustion reconstituted tobacco comprises the following steps:
step (1): mixing the distillers 'grains solid residue, the tobacco solid residue, the wood pulp fiber and the filler according to the mass ratio of the distillers' grains to the tobacco to the wood pulp fiber to the filler before extraction of (30-60) to (30-50) to (0-20) to (0-30) to prepare the sheet base.
The solid residue extracted from distiller's grains is extracted from distiller's grains by leaching, refluxing or Soxhlet extraction. The solid residue obtained by extracting tobacco is extracted by leaching, reflux extraction or Soxhlet extraction. In particular implementation, in order to reduce the cost, the tobacco before extraction can be one or more of tobacco stems, tobacco leaves, tobacco shreds and cigarette ash sticks.
To illustrate the above extraction method more clearly, reference may be made to the following description:
the leaching method comprises the following steps: also known as liquid-solid extraction, employs a volatile organic solvent to transfer certain components of the feedstock into a solvent phase, and then recovers the organic solvent by evaporation, distillation, or the like, to obtain the desired extraction components.
A reflux extraction method: the organic solvent is adopted for heating and extraction, and a reflux heating device is adopted. For small runs, a reflux condenser may be attached to the round bottom flask. Reflux is heated in a water bath and typically kept boiling for about 1 hour. Cooling, filtering, adding solvent into the residue, and performing second and third heating reflux for about half an hour or until the effective components are basically extracted.
Soxhlet extraction: also known as continuous extraction method, Soxhlet extraction method, utilizes the principles of solvent reflux and siphon to make the solid matter be extracted by solvent every time. The solid matter may be ground before extraction to increase the leaching area of the liquid.
In addition, the film base can be prepared by a thick slurry method, a paper-making method or a rolling method.
Specifically, the thick paste method is a processing method in which the prepared paste is uniformly spread on a circulating metal belt, and then dried and peeled to prepare a substrate. The papermaking method is a method of making a sheet from the obtained slurry by paper-making. The rolling method is a method for preparing a sheet base by rolling and drying the prepared slurry.
Step (2): mixing the vinasse extracting solution, the tobacco extracting solution, the atomizing agent, the adhesive, the spice and the solvent according to the mass ratio of (10-30) to (0-20) to prepare the coating liquid. The solvent may be an organic solvent or water. The vinasse extracting solution and the tobacco extracting solution refer to products obtained by extracting vinasse and tobacco in the step (1).
And (3): and (3) coating the coating liquid prepared in the step (2) on the film base prepared in the step (1), and drying to obtain the vinous low-temperature non-combustion reconstituted tobacco.
The vinasse is used as the raw material, vinasse is kept to the maximum extent, vinasse aroma substances contained in the vinasse are kept, the atomization effect is good, the surface is not adhered, the processing resistance is good, smoke can be uniformly released during smoking, and the vinasse low-temperature non-combustion reconstituted tobacco prepared by the preparation method is good in taste and good in sensory effect during smoking.
In the preparation method of the vinous low-temperature non-combustion reconstituted tobacco, before extraction in the step (1), vinasse can be white spirit vinasse for preparing wine from five cereals, and specifically can be one or more of sorghum vinasse, corn vinasse, rice vinasse, soybean vinasse and potato vinasse.
In the preparation method of the vinous low-temperature non-combustion reconstituted tobacco disclosed by the invention, the tobacco before extraction in the step (1) is one or more of tobacco stems, tobacco leaves, tobacco shreds and tobacco ash sticks.
In the preparation method of the vinous low-temperature non-combustion reconstituted tobacco disclosed by the disclosure, the wood pulp fiber in the step (1) is one or more of softwood pulp, hardwood pulp and gramineous pulp.
In the preparation method of the vinous low-temperature non-combustion reconstituted tobacco disclosed by the invention, the filler in the step (1) is calcium carbonate.
In the preparation method of the vinous low-temperature non-combustion reconstituted tobacco, the density of the vinasse extracting solution and the tobacco extracting solution in the step (2) is 1.10-1.20g/cm3。
In the preparation method of the vinous low-temperature non-combustion reconstituted tobacco disclosed by the disclosure, the atomizing agent in the step (2) can be polyhydric alcohol and/or polyhydric ester. Specifically, the atomizing agent is one or more of propylene glycol, glycerol, ethanol and ethyl acetate.
In the preparation method of the vinous low-temperature non-combustion reconstituted tobacco disclosed by the invention, the adhesive in the step (2) is one or more of carboxymethyl cellulose, sodium alginate, guar gum and chitosan.
In the preparation method of the vinous low-temperature non-combustion reconstituted tobacco, the spice in the step (2) is one or more of vanillin, megastigmatrienone, dihydroactinidiolide, beta-ionone, geranylacetone, benzoic acid, phenylacetic acid, benzyl alcohol, phenethyl alcohol, isovaleric acid, ethyl acetate, ethyl butyrate, ethyl lactate, ethyl caprylate, ethyl heptanoate and ethyl 2-methylbutanoate. Preferably, the perfume is one or more of viniferous ethyl acetate, ethyl butyrate, ethyl lactate, ethyl octanoate, ethyl heptanoate and ethyl 2-methylbutyrate.
In the preparation method of the vinous low-temperature non-combustion reconstituted tobacco, the mass percentage of the solvent in the step (2) in the coating liquid is 10-20%.
The experimental procedures used in the examples below are conventional unless otherwise specified, the materials and reagents used therein are commercially available, and the equipment used in the experiments are well known to those skilled in the art without otherwise specified.
Example 1
(1) Preparing raw materials: 2000g of rice wine lees, 2000g of tobacco (wherein the tobacco stalks are 800g, and the tobacco shreds are 1200g), 500g of softwood pulp and 500g of calcium carbonate;
(2) raw material extraction: extracting with 50% ethanol at a mass concentration of 8:1 and 10:1 respectively for 2 times under reflux for 30 min; then performing solid-liquid separation, and concentrating the extractive solution to density of 1.10g/cm3Obtaining rice wine lees extract and tobacco extract;
(3) preparing a coating liquid: mixing and uniformly stirring 20% of prepared rice wine lees extract, 30% of tobacco extract, 20% of glycerol, 0.5% of vanillin, 0.5% of megastigmatrienone, 1% of dihydroactinidiolide, 1% of beta-ionone, 0.4% of geranylacetone, 0.6% of phenethyl alcohol, 6% of tree moss extract and 20% of water according to mass percentage to obtain a coating liquid;
(4) preparing a film base: respectively defibering the rice wine lees extraction solid residue and the tobacco extraction solid residue by adopting a papermaking method, mixing the defibered solid residue with softwood pulp, pulping, mixing with calcium carbonate, and performing net-surfing molding to prepare a sheet base;
(5) and (3) preparing a finished product: and coating the prepared coating liquid on a film base, and drying to obtain the vinous low-temperature non-combustion reconstituted tobacco S1.
The vinous low-temperature non-combustion reconstituted tobacco S1 can be directly filled in low-temperature cigarette smoking set as smoking material. When the wine is smoked, the smoking speed is high, the whole body is heated uniformly, the smoke amount is large, and a smoker can feel fresh wine fragrance well.
Example 2
(1) Preparing raw materials: 1000g of rice wine lees and 1000g of tobacco leaves;
(2) raw material extraction: extracting with 50% ethanol at a mass ratio of 6:1 and 8:1 for 30minTaking for 2 times; then performing solid-liquid separation, and concentrating the extractive solution to density of 1.20g/cm3Obtaining rice wine lees extract and tobacco leaf extract;
(3) preparing a coating liquid: mixing 20% of prepared rice wine lees extract, 20% of tobacco leaf extract, 30% of propylene glycol, 27% of carboxymethyl cellulose, 0.5% of ethyl acetate, 0.5% of ethyl lactate, 0.5% of megastigmatrienone, 0.5% of dihydroactinidiolide and 1% of vanillin according to the mass percentage, and uniformly stirring to obtain a coating liquid;
(4) preparing a film base: preparing the solid residue extracted from the rice wine lees and the solid residue extracted from the tobacco leaves into a film base by adopting a thick slurry method;
(5) and (3) preparing a finished product: and coating the prepared coating liquid on a film base, and drying to obtain the vinous low-temperature non-combustion reconstituted tobacco S2.
The vinous low-temperature non-combustion reconstituted tobacco S2 can be directly filled in a special low-temperature cigarette smoking set to be used as a smoking material. When the wine is smoked, the smoking speed is high, the whole body is heated uniformly, the smoke amount is moderate, and a smoker can feel the fragrance of the wine well.
Example 3
(1) Preparing raw materials: 800g of rice wine lees, 1000g of tobacco (wherein 600g of tobacco powder, 200g of cigarette ash rod and 200g of tobacco stem) and 200g of hemp pulp;
(2) raw material extraction: the extractant of the rice wine lees is 50% ethanol, and the mass ratio of the extractant to the rice wine lees is 8: 1; the extracting agent of the tobacco is water, and the mass ratio of the water to the tobacco is 9: 1; reflux extracting for 30min for 2 times; then performing solid-liquid separation, and concentrating the extractive solution to density of 1.10g/cm3Obtaining rice wine lees extract and tobacco extract;
(3) preparing a coating liquid: mixing 10% of rice wine lees extract, 30% of tobacco extract, 10% of propylene glycol, 20% of glycerol, 10% of carboxymethyl cellulose, 10% of guar gum and 10% of water according to the mass percentage, and uniformly stirring to obtain a coating liquid;
(4) preparing a film base: preparing the solid residues extracted from the rice wine lees, the solid residues extracted from the tobacco and the hemp pulp into a sheet base by adopting a rolling method;
(5) and (3) preparing a finished product: and coating the prepared coating liquid on a film base, and drying to obtain the vinous low-temperature non-combustion reconstituted tobacco S3.
The vinous low-temperature non-combustion reconstituted tobacco S3 can be directly filled in a special low-temperature cigarette smoking set to be used as a smoking material. When the wine is smoked, the smoking speed is high, the whole body is heated uniformly, the smoke amount is moderate, and a smoker can feel strong wine fragrance well.
Example 4
(1) Preparing raw materials: 950g of corn vinasse, 800g of tobacco (600 g of tobacco powder and 200g of tobacco stem), 200g of hemp pulp and 50g of calcium carbonate;
(2) raw material extraction: extracting corn vinasse by an extraction method, wherein an extracting agent adopts 50% ethanol by mass, the mass ratio of the extracting agent to the corn vinasse is 8:1, extracting for 30min, and extracting for 1 time; extracting tobacco by reflux extraction method with water at a mass ratio of 10:1 for 2 times for 30 min; then performing solid-liquid separation, and concentrating the extractive solution to density of 1.10g/cm3Obtaining corn vinasse extracting solution and tobacco extracting solution;
(3) preparing a coating liquid: mixing 20% of corn vinasse extracting solution, 20% of tobacco extracting solution, 20% of glycerol, 5% of propylene glycol, 10% of sodium alginate, 5% of guar gum and 20% of water according to mass percentage, and uniformly stirring to obtain a coating liquid;
(4) preparing a film base: respectively defibrating the solid residue extracted from the corn distillers' grains and the solid residue extracted from the tobacco by adopting a thick slurry method, mixing the defibered solid residue with hemp pulp and calcium carbonate, and then preparing a sheet base;
(5) and (3) preparing a finished product: and coating the prepared coating liquid on a film base, and drying to obtain the vinous low-temperature non-combustion reconstituted tobacco S4.
The vinous low-temperature non-combustion reconstituted tobacco S4 can be directly filled in a special low-temperature cigarette smoking set to be used as a smoking material. When the wine is smoked, the smoking speed is high, the whole body is heated uniformly, the smoke amount is moderate, and a smoker can well feel the special fruity bouquet.
Example 5
(1) Preparing raw materials: 600g of corn vinasse, 1000g of tobacco (wherein 400g of tobacco leaf, 400g of tobacco stem and 200g of ash stick), and 200g of hardwood pulp;
(2) raw material extraction: extracting corn vinasse by a Soxhlet extraction method, wherein an extracting agent adopts 50% ethanol by mass, the mass ratio of the extracting agent to the corn vinasse is 6:1, and extracting for 1 time; extracting tobacco by extraction method with water at a mass ratio of water to tobacco of 8:1 for 30min for 2 times; then performing solid-liquid separation, and concentrating the extractive solution to density of 1.15g/cm3Obtaining corn vinasse extracting solution and tobacco extracting solution;
(3) preparing a coating liquid: mixing and uniformly stirring 15% of prepared corn vinasse extracting solution, 30% of tobacco extracting solution, 10% of glycerol, 10% of propylene glycol, 5% of ethylene glycol, 15% of carboxymethyl cellulose, 5% of chitosan and 10% of water according to the mass percentage to obtain a coating liquid;
(4) preparing a film base: preparing the solid residues of corn vinasse extraction, the solid residues of tobacco extraction and broad-leaved wood pulp into a sheet base by adopting a rolling method;
(5) and (3) preparing a finished product: and coating the prepared coating liquid on a film base, and drying to obtain the vinous low-temperature non-combustion reconstituted tobacco S5.
The vinous low-temperature non-combustion reconstituted tobacco S5 can be directly filled in a special low-temperature cigarette smoking set to be used as a smoking material. When the wine is smoked, the smoking speed is high, the whole body is heated uniformly, the smoke amount is moderate, and a smoker can feel the fragrance of the wine well.
Although some specific embodiments of the present invention have been described in detail by way of examples, it should be understood by those skilled in the art that the above examples are for illustrative purposes only and are not intended to limit the scope of the present invention. It will be appreciated by those skilled in the art that modifications may be made to the above embodiments without departing from the scope and spirit of the invention. The scope of the invention is defined by the appended claims.
Claims (10)
1. The preparation method of the vinous low-temperature non-combustion reconstituted tobacco is characterized by comprising the following steps of:
(1) mixing and pulping the distillers 'grains extracted solid residue, the tobacco extracted solid residue, the wood pulp fiber and the filler according to the mass ratio of the distillers' grains to the tobacco before extraction to the wood pulp fiber and the filler of (30-60) to (30-50) to (0-20) to (0-30) to prepare a sheet base;
(2) mixing the vinasse extracting solution, the tobacco extracting solution, the atomizing agent, the adhesive, the spice and the solvent according to the mass ratio of (10-30) to (0-20) to prepare a coating liquid;
(3) and (3) coating the coating liquid prepared in the step (2) on the film base prepared in the step (1), and drying to obtain the vinous low-temperature non-combustion reconstituted tobacco.
2. The method for preparing the vintage type low-temperature non-combustion reconstituted tobacco according to claim 1, wherein the vinasse before extraction in the step (1) is one or more of sorghum vinasse, corn vinasse, rice vinasse, soybean vinasse and potato vinasse.
3. The method for preparing vintage type low temperature non-combustion reconstituted tobacco according to claim 1, wherein the tobacco before extraction in the step (1) is one or more of tobacco stem, tobacco leaf, tobacco powder and cigarette ash rod.
4. The method for preparing the vinous low-temperature non-combustion reconstituted tobacco according to claim 1, wherein the wood pulp fiber in the step (1) is one or more of softwood pulp, hardwood pulp and gramineous pulp.
5. The method for preparing the vinous low-temperature non-combustion reconstituted tobacco according to claim 1, wherein the filler in the step (1) is calcium carbonate.
6. The method for preparing vinous low-temperature non-combustion reconstituted tobacco according to claim 1, wherein the densities of the vinasse extracting solution and the tobacco extracting solution in the step (2) are 1.10-1.20g/cm3。
7. The method for preparing the vinous low-temperature non-combustion reconstituted tobacco according to claim 1, wherein the atomizing agent in the step (2) is one or more of propylene glycol, glycerol, ethanol and ethyl acetate.
8. The preparation method of the vinous low-temperature non-combustion reconstituted tobacco according to claim 1, wherein the adhesive in the step (2) is one or more of carboxymethyl cellulose, sodium alginate, guar gum and chitosan.
9. The method for preparing the vinous low-temperature non-combustion reconstituted tobacco according to claim 1, wherein the spices in the step (2) are one or more of vanillin, megastigmatrienone, dihydroactinidiolide, beta-ionone, geranylacetone, benzoic acid, phenylacetic acid, benzyl alcohol, phenethyl alcohol, isovaleric acid, ethyl acetate, ethyl butyrate, ethyl lactate, ethyl caprylate, ethyl heptanoate and ethyl 2-methylbutyrate.
10. The preparation method of the vinous low-temperature non-combustion reconstituted tobacco according to claim 1, wherein the solvent in the step (2) accounts for 10-20% of the coating liquid in percentage by mass.
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| CN114176246B (en) * | 2021-12-07 | 2022-12-16 | 云南恒罡科技有限公司 | White spirit flavor type heating non-combustion fuming particle and preparation method and application thereof |
| CN114223924A (en) * | 2021-12-17 | 2022-03-25 | 云南巴菰生物科技股份有限公司 | Production method of low-temperature heating non-combustion herbaceous product |
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