WO2022138263A1 - Method for manufacturing tobacco rod part for non-combustion heating-type flavor inhalation article - Google Patents

Method for manufacturing tobacco rod part for non-combustion heating-type flavor inhalation article Download PDF

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Publication number
WO2022138263A1
WO2022138263A1 PCT/JP2021/045741 JP2021045741W WO2022138263A1 WO 2022138263 A1 WO2022138263 A1 WO 2022138263A1 JP 2021045741 W JP2021045741 W JP 2021045741W WO 2022138263 A1 WO2022138263 A1 WO 2022138263A1
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Prior art keywords
tobacco
sheet
tobacco sheet
filling
reconstituted
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PCT/JP2021/045741
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French (fr)
Japanese (ja)
Inventor
真樹 六川
大輔 南條
俊介 相澤
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日本たばこ産業株式会社
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Priority to JP2022572158A priority Critical patent/JPWO2022138263A1/ja
Priority to EP21910412.2A priority patent/EP4268622A1/en
Publication of WO2022138263A1 publication Critical patent/WO2022138263A1/en

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24CMACHINES FOR MAKING CIGARS OR CIGARETTES
    • A24C5/00Making cigarettes; Making tipping materials for, or attaching filters or mouthpieces to, cigars or cigarettes
    • A24C5/01Making cigarettes for simulated smoking devices

Definitions

  • the present invention relates to a method for manufacturing a tobacco rod portion for a non-combustion heating type flavor suction article.
  • a non-combustion heating type flavor suction article has been developed as an alternative to the conventional combustion type flavor suction article.
  • a reconstituted tobacco sheet containing a relatively large amount of aerosol-forming substrate is used for the article.
  • Patent Documents 1 and 2 propose a method of discharging the reconstructed tobacco sheet from a bobbin and directly filling the reconstructed tobacco sheet in a wrapper to manufacture a tobacco rod portion.
  • the method described in the patent document can efficiently produce a tobacco rod portion, but the inventors have the idea that the quality can be further improved by performing a specific treatment before filling the wrapper with the tobacco filling. Got In view of such circumstances, it is an object of the present invention to provide a tobacco rod portion for a non-combustion heating type flavor suction article with improved quality.
  • Aspect 1 Step 1 which dries the tobacco filling after humidification Step 2, to prepare a tobacco rod portion in which the tobacco filler obtained in step 1 is filled in a tubular wrapper.
  • Aspect 2 The production method according to aspect 1, wherein the tobacco filler contains an aerosol-forming substrate and a reconstituted tobacco sheet.
  • Aspect 3 The production method according to aspect 2, further comprising a step of cutting the tobacco filling into a strand shape.
  • Aspect 4 The tobacco filling contains the reconstituted tobacco sheet A and the reconstructed tobacco sheet B.
  • the step 1 comprises humidifying and then mixing each reconstituted tobacco sheet to dry the mixture, or humidifying and then drying each reconstituted tobacco sheet and then mixing.
  • Aspect 5 The tobacco filling contains the reconstituted tobacco sheet A and lamina.
  • the step 1 comprises humidifying and then mixing the reconstituted tobacco sheet A and lamina to dry the mixture, or humidifying and then drying the reconstituted tobacco sheet A and lamina, respectively.
  • Aspect 6 The production method according to any one of aspects 1 to 5, further comprising the step of mixing the non-tobacco material with the tobacco filling.
  • Aspect 7 The production method according to any one of aspects 1 to 6, further comprising a step of adding an additive to the tobacco filling.
  • Aspect 8 The production method according to aspect 4 or 6, further comprising a step of adding an additive to either or both of the reconstituted tobacco sheet A and the reconstituted tobacco sheet B.
  • Aspect 9 The production method according to aspect 5 or 6, further comprising a step of adding an additive to either or both of the reconstituted tobacco sheet and the lamina.
  • Aspect 10 The production method according to any one of aspects 7 to 9, further comprising a step of measuring the components of the tobacco filling and adjusting the type or amount of the additive based on the measurement result.
  • Aspect 11 The components of the reconstituted tobacco sheet A were measured and Determine the type of reconstituted tobacco sheet B or lamina based on the measurement results, The production method according to aspect 4 or 5.
  • Aspect 12 The components of the reconstituted tobacco sheet A were measured and Based on the measurement results To determine the type or amount of additive to be added to the reconstituted tobacco sheet B, or the type or amount of additive to be added to lamina.
  • Aspect 13 The production method according to any one of aspects 1 to 3, 6 or 7, wherein the humidification is performed so that the water content in the tobacco filling is 15 to 25% by weight.
  • Aspect 14 The production method according to any one of aspects 4 to 12, wherein humidification is performed so that the water content in the reconstructed tobacco sheet is 15 to 25% by weight.
  • Aspect 15 The production method according to any one of aspects 1 to 14, wherein the drying is carried out by an air flow drying method or an annual drying method.
  • Aspect 16 The production method according to any one of aspects 4 to 15, wherein the reconstructed tobacco sheet is a papermaking sheet, a cast sheet, or an extruded sheet.
  • X to Y includes X and Y which are fractional values thereof.
  • the production method of the present invention includes a step 1 of humidifying and then drying the tobacco filling, and a step 2 of preparing a tobacco rod portion in which the tobacco filling obtained in the step 1 is filled in a tubular wrapper.
  • 1. Process 1 (1) Tobacco filling
  • the tobacco filling is a material that is filled in a wrapper and used for smoking.
  • known tobacco fillers can be used in the present invention, it is preferable to include a tobacco sheet from the viewpoint of ease of production.
  • the tobacco sheet is a sheet-shaped tobacco material, and in the present invention, a reconstructed tobacco sheet is preferable.
  • the term "tobacco sheet” means a sheet-like tobacco material or a material derived from the sheet-like tobacco material (eg, a cut piece).
  • the reconstituted tobacco sheet is a tobacco sheet containing a reconstituted product (reconstructed tobacco or reconstituted tobacco granules) composed of fine powder of a plant belonging to the genus Tobacco.
  • the tobacco sheet may be a papermaking sheet manufactured by a papermaking method, a cast sheet manufactured by a casting method, or an extrusion sheet manufactured by an extrusion method.
  • the papermaking method is a method in which a mixture containing a tobacco raw material and a liquid medium such as water is made into paper and dried to produce a sheet.
  • the mixture usually contains pulp or fibrous tobacco material.
  • the casting method is a method in which a mixture containing a tobacco raw material and a liquid medium such as water is developed (cast) on a substrate and dried to produce a sheet.
  • the extrusion method is a method for producing a sheet by extruding a mixture containing a tobacco raw material and a liquid medium such as water from a die such as a T die.
  • the tobacco filling may contain an aerosol-forming substrate.
  • the aerosol-forming substrate is a material that is vaporized and cooled by heating to form an aerosol, or is atomized to produce an aerosol.
  • Known aerosol-forming substrates can be used, and examples thereof include polyhydric alcohols such as glycerin and propylene glycol (PG), triethylcitrate (TEC), triacetin and the like having a boiling point of more than 100 ° C. Can be mentioned.
  • the amount of the aerosol-forming substrate in the tobacco filling is preferably 1 to 40% by weight, more preferably 5 to 30% by weight, still more preferably, by dry weight (weight excluding mixed water, the same applies hereinafter). It is 5 to 20% by weight. If the amount of the aerosol-forming substrate exceeds the upper limit, it may be difficult to manufacture the tobacco filling, and if it is less than the lower limit, the amount of smoke sensation may decrease.
  • the sheet-fed form When using a reconstructed tobacco sheet, it is preferable to release the sheet-fed form and supply it quantitatively to step 1. Release means to loosen the reconstructed tobacco sheet (in the form of a single leaf) that is laminated and agglomerated into one sheet.
  • the size is not limited, but in one embodiment, the single-leaf reconstructed tobacco sheet is a columnar body, and its cross section is a quadrangle having a side of 3 to 10 cm.
  • a packaging container having a shape and size that is easy to handle.
  • An example of a packaging container is the C-48 box, which is known among cigarette manufacturers.
  • the C-48 box is made of cardboard and measures approximately 115 x 70 x 75 cm.
  • the single-wafer regenerated tobacco sheet can be directly filled in the C-48 box, but may be packed in a plastic bag and then housed in the C-48 box in order to suppress quality changes during transportation. ..
  • the C-48 box is filled with about 100 to 200 kg of a reconstructed tobacco sheet in a single-wafer form.
  • Another aspect is a method of transporting a recycled tobacco sheet in a bobbin shape.
  • a vertically continuous sheet having a width of 10 to 100 cm can be wound around a core to form a bobbin shape.
  • the regenerated tobacco sheet transported in the bobbin shape is used in the present invention, it is necessary to cut the reconstructed tobacco sheet to a predetermined size using a shredder or the like before the reconstructed tobacco sheet is subjected to the step 1.
  • Humidification Humidification can be performed using a known device, but in the present invention, it is preferable to use a cylinder type device from the viewpoint of efficiency.
  • the device includes a water supply device, a heating device, an exhaust device, and a rotating device that rotates around the central axis of the cylinder.
  • Humidification is carried out by supplying water from the water supply device to the tobacco filling.
  • the humidification conditions are adjusted so that the water content of the tobacco filling after humidification is about 15 to 25% by weight.
  • the temperature of the inner wall of the cylinder can be set to 50 to 70 ° C.
  • the flow rate of air in the cylinder can be set to 0.05 to 0.15 m / sec
  • the residence time of the tobacco filling can be set to about 3 to 6 minutes.
  • the size of the cylinder is not limited, but in one embodiment, the diameter is about 2 to 4 m and the length is about 5 to 10 m.
  • Humidification is more preferably carried out by ventilating the inside of the cylinder. When the tobacco filling is heated, some of the low boiling point content components such as ammonia are volatilized and discharged to the outside of the cylinder by exhaust gas, thereby reducing the negative taste and aroma during use.
  • Drying By drying, the tobacco filling can be put into a state suitable for storage. Drying can be performed by a known method, but in the present invention, it is preferable to adopt an air flow drying method or an annual drying method from the viewpoint of efficiency.
  • the former is a method in which a heated air flow (preferably superheated steam) and a tobacco filling are brought into contact with each other in a pipe to perform drying. Examples of such a device include those described in International Publication 2013/052490.
  • this method it is also possible to give a characteristic flavor character to the tobacco filling.
  • the moisture in the tobacco filling is dried in a short time, so that the dried tobacco filling can be inflated compared to before drying, and the shape of the dried tobacco filling is curled.
  • the bulkiness of the tobacco filling increases.
  • the amount of oxygen in the atmosphere when heated in the drying step can be reduced, and the chemical change of the unwanted tobacco filling caused by oxygen is suppressed. can.
  • the latter is a method of heating and drying the tobacco filling in a cylinder type device. With this method, it is also possible to remove highly volatile components contained in the tobacco filling. Since this method requires a longer time to dry than the air flow drying method, it is preferable in that fine moisture control can be performed and accurate finish of outlet moisture can be achieved.
  • FIG. 1 shows the first embodiment.
  • a reconstructed tobacco sheet in a single-wafer form is prepared and released.
  • the water content of the reconstituted tobacco sheet at this stage is preferably 5 to 15% by weight.
  • the aerosol-forming substrate is added before or after release.
  • the amount of the aerosol-forming substrate in the sheet is preferably 5 to 30% by weight.
  • Foreign matter is removed from the released reconstituted tobacco sheet. It is also possible to use a blend silo to mix the reconstituted tobacco sheets to homogenize the quality.
  • Humidification humidify the reconstituted tobacco sheet.
  • the equipment used for humidification and the humidification conditions are as described above. At this time, the water content of the reconstituted tobacco sheet is adjusted to 15 to 25% by weight. Further, in this step, unfavorable components derived from the tobacco raw material (components that give an astringent taste, etc.) are removed.
  • additives are added to the reconstituted tobacco sheet after humidification.
  • the additive is a material other than a raw material such as a reconstructed tobacco sheet and an aerosol-forming base material.
  • Additives include tobacco powder; fragrances; the aforementioned aerosol-producing substrates; tobacco aroma enhancers such as acids and alkalis; solvents such as ethanol, water, benzyl alcohol and propylene glycol; antioxidants such as polyphenols or vitamins. Be done.
  • the additive can be added by a known method, but it can be carried out by filling a rotating cylinder type device with a reconstructed tobacco sheet and spraying a fragrance or the like.
  • fragrance which is a flavor component
  • the aroma at this stage is suitable for adding a flavor component having a relatively large molecular weight. This is because such a flavor component has a low vapor pressure and a high affinity with water, and therefore, when added to a reconstituted tobacco sheet after humidification, it easily penetrates into the inside of the sheet.
  • the fragrances include the following, which can be used alone or in combination of two or more. Acetanisol, acetophenone, acetylpyrazine, 2-acetylthiazole, alfalfa extract, amyl alcohol, amyl butyrate, trans-annetol, staranis oil, apple juice, peruval balsam oil, honeywort absolute, benzaldehyde, benzoin resinoid, benzyl alcohol, benzoate Lactone benzyl acid, benzyl phenylacetate, benzyl propionate, 2,3-butandione, 2-butanol, butyl butyrate, butyric acid, caramel, cardamon oil, carobu absolute, ⁇ -carotene, carrot juice, L-carboxylic, ⁇ -cariophyllene, cassia Bark oil, cedar wood oil, celery seed oil, chamomile oil, cinnamaldehyde, silicic acid, cinnamy
  • Non-Patent Document 1 TSNAs (Tobacco specific nitrosamines) are contained in the tobacco vapor of the non-combustion heating type flavor suction article.
  • TSNAs tobacco specific nitrosamines
  • the tobacco filling is continuously heated for a long time at the time of use. Therefore, in the tobacco filling of the non-combustion heating type flavor suction article, unintended components may be generated by heating for a long time.
  • an antioxidant By adding an antioxidant, the above reaction can be suppressed and the production of unintended components can be suppressed.
  • an antioxidant known as a food additive can be used.
  • examples include ascorbic acid, erythorbic acid, ascorbic acid, catechin, dihydrocaffeic acid, p-coumaric acid, ferulic acid, 3- (4-hydroxyphenyl) propionic acid, quercetin, esculetin, kenferol, caffeic acid, tocopherol, Examples include dibutylhydroxytoluene (BHT), quinic acid, chlorogenic acid, rutin, scopoletin, and cinnamic acid.
  • the antioxidant is preferably at least one selected from the group consisting of gallic acid and erythorbic acid.
  • the antioxidant is contained in the tobacco filling in an amount of, for example, 0.25 to 10% by weight, preferably 0.25 to 5.0% by weight, more preferably% by weight, based on the tobacco filling.
  • the antioxidant can be added to the tobacco filling by melting or dispersing it in a solvent such as water or ethanol and spraying it.
  • the scented reconstituted tobacco sheet is stamped.
  • the cutting can be performed using a known device, but in the present invention, the reconstructed tobacco sheet is supplied by pressing and supplying the reconstructed tobacco sheet so that its end is parallel to the extending direction of the blade of the knife drum, and the strand is It is preferable to cut it into a shape.
  • the shape of the strand can be about 0.6 to 1.5 mm in width from the viewpoint of ease of filling the wrapper.
  • the length of the strand after cutting is the size of the sheet-fed reconstructed tobacco sheet supplied to the cutting process, and the crushed state of the sheet-fed reconstructed tobacco sheet in each process, during cutting, and cutting.
  • the reconstructed tobacco sheet may be adjusted to 15 to 25% by weight.
  • the strand-shaped reconstructed tobacco sheet is dried.
  • the equipment and drying conditions used for drying are as described above. At this time, the water content of the reconstituted tobacco sheet is adjusted to 8 to 12% by weight. Further, in this step, the bulkiness of the strand-shaped reconstructed tobacco sheet is improved.
  • a solid additive carrying a filler or a fragrance is added to the strand-shaped reconstructed tobacco sheet.
  • the filler include strand-shaped paper, strand-shaped calcium carbonate sheet, granular porous polysaccharide beads, and the like. From the viewpoint of enhancing the mixing property, it is preferable that the material to be added has a shape close to that of the strand. For example, adding a perfume-carrying polysaccharide sheet as a solid additive carrying a perfume has an advantage that the taste and aroma at the time of use of a non-combustion heating type flavor suction article can be enhanced.
  • the perfume-supporting sheet to be mixed with the tobacco filler is based on the thickening polysaccharide disclosed in Japanese Patents 5941988, 5934799, 5514953, and 541574. It is preferable in terms of the balance of fragrance release performance during use.
  • the shape of the fragrance-supporting polysaccharide sheet can be 0.5 to 1.5 mm in width, 2 to 4 mm in length, and about 70 ⁇ m in thickness.
  • the mixing method is not limited, and a method of merging a conveyor carrying a strand-shaped reconstructed tobacco sheet with a conveyor carrying an engraved fragrance-supporting polysaccharide sheet and mixing the two, or both. Is introduced into a cylinder type mixer and mixed.
  • Incense Incense may be applied again to the reconstructed tobacco sheet having a strand shape after drying.
  • the method of incense and the components used are as described above.
  • the aroma at this stage is suitable for adding a flavor component having a relatively small molecular weight.
  • the tobacco filling can be processed into a flavor-sucking article without drying. Therefore, in this step, a strong scent characteristic should be given to the final product by adding a flavor component that expresses a relatively volatile scent. Can be done.
  • FIG. 2 shows a second embodiment.
  • two lines are used.
  • the reconstructed tobacco sheet A is prepared by carrying out 1) to 3) of the first embodiment.
  • 1) to 3) of the first embodiment are carried out to prepare the reconstructed tobacco sheet B.
  • the reconstituted tobacco sheets A and B are composed of different components.
  • the incense may be applied to both the reconstituted tobacco sheets A and B, may be applied to one of them, or may not be applied to both of them.
  • the reconstituted tobacco sheets A and B are mixed.
  • the mixing ratio is appropriately adjusted so that the desired flavor can be achieved.
  • the mixing efficiency can be improved, and the mixed product can be subjected to processes such as cutting and drying, so that the product can be made more uniform.
  • the mixture of the reconstituted tobacco sheets A and B is subjected to a cutting, drying, mixing with a non-tobacco material, and aromatling process, and the obtained product is first stored. These steps are as described in the first embodiments 4) to 8).
  • This aspect is suitable for manufacturing brands with different flavor characteristics.
  • the base material common to these brands is the reconstructed tobacco sheet A
  • another brand can be efficiently manufactured by appropriately using the reconstructed tobacco sheet B which is a sub-raw material at the time of brand switching.
  • the quality is stabilized by mixing the reconstructed tobacco sheet B designed to supplement the component. Mixtures of reconstituted tobacco sheets can also be produced.
  • Examples of the types of tobacco used as the material for reconstituted tobacco include yellow species, Burley species, Orient species, and native species in Nicotiana rustica, which can be used alone or in combination. Usually, these blend ratios are changed to achieve the desired taste and aroma.
  • the ratio of yellow type and orient type is increased as the constituent tobacco types (the total amount of both is preferably more than 50% by weight of the total amount of tobacco).
  • Sheet A was prepared (more preferably 80% by weight or more), and the proportion of Burley or native species was increased as the constituent tobacco types (the total amount of both is preferably more than 30% by weight of the total amount of tobacco).
  • More preferably 80% by weight or more) Prepare the sheet B.
  • cigarettes having strong taste and aroma characteristics even in a small amount.
  • tobacco having strong taste and aroma characteristics even in a small amount.
  • cigarettes include cigarettes called Peric, Latakia, and Dark Fire Cured. These varieties are the same as the yellow, Burley, Orient, or Native varieties described above, but are smoked or fermented under forced high temperature and high moisture after harvesting at leaf tobacco farmers. Specially treated tobacco, such as fermented tobacco such as pellic and dark fire cure, or smoked tobacco such as latakia, is slightly blended to give it a unique flavor characteristic. Express. When a reconstructed tobacco sheet containing pellic, latakia, dark fire cure, etc.
  • the total blending amount of peric, latakia and dark fire cure is preferably 1.0% by weight or more and less than 10.0% by weight, more preferably 1.0% by weight or more and less than 5.0% by weight of the total amount of tobacco. Is.
  • FIG. 3 shows a third embodiment.
  • two lines are used.
  • 1) to 5) of the first embodiment are carried out to prepare a strand-shaped reconstructed tobacco sheet A.
  • 1) to 5) of the first embodiment are carried out to prepare a strand-shaped reconstituted tobacco sheet B.
  • the reconstituted tobacco sheets A and B are composed of different components.
  • the incense may be applied to both the reconstituted tobacco sheets A and B, or may be applied to one of them.
  • the strand-shaped reconstituted tobacco sheets A and B are mixed.
  • the mixing ratio is appropriately adjusted so that the desired flavor can be achieved.
  • the mixture is subjected to a mixing and incense step with a non-tobacco material, and the obtained product is first stored. These steps are as described in the first embodiments 6) and 7).
  • This aspect is suitable for producing a brand having different flavor characteristics as in the second aspect.
  • the base material common to these brands is the reconstructed tobacco sheet A
  • another brand can be efficiently manufactured by appropriately using the reconstructed tobacco sheet B which is a sub-raw material at the time of brand switching.
  • the quality is stabilized by mixing the reconstructed tobacco sheet B designed to supplement the component.
  • the reconstituted tobacco sheet A can also be manufactured.
  • the reconstructed tobacco sheets A and B are subjected to cutting and drying, respectively, so that the conditions can be set according to the individual characteristics. For example, when the fragrance added to the reconstituted tobacco sheet A and the fragrance added to the reconstructed tobacco sheet B are different, the optimum drying conditions differ depending on the fragrance, but in this embodiment, there is an advantage that conditions suitable for the fragrance can be selected. There is.
  • FIG. 4 shows a fourth embodiment.
  • two lines are used.
  • the reconstructed tobacco sheet A is processed by carrying out 1) to 3) of the first embodiment.
  • lamina is processed.
  • Lamina is a deboned leaf obtained by removing the middle bone from tobacco leaves.
  • FIG. 4 shows a form in which two types of laminas are used, but one or more types of laminas can be used. At this time, it is preferable that Lamina A and B are composed of different components.
  • the steps up to the scenting step of lamina can be carried out in the same manner as in 1) to 3) of the first embodiment.
  • Lamina A and B are mixed, and the mixture is further humidified.
  • Humidification can be carried out in the same manner as in 2) of the first embodiment.
  • the humidified mixture is further mixed with the aromatized reconstituted tobacco sheet A, which is then subjected to a cutting, drying, mixing with non-tobacco material and aromatizing steps, and the obtained product is first stored. .. These steps are as described in the first embodiments 4) to 8).
  • the incense may be applied to one or more of the reconstituted tobacco sheets A, Lamina A, and Lamina B, or may be applied to all of them.
  • the effect described in the second aspect can be obtained. Further, if a lamina having a higher swelling property than that of the tobacco sheet is mixed, the filling amount for achieving the same winding hardness can be reduced as compared with the case where the tobacco rod portion is formed only by the tobacco sheet.
  • FIG. 5 shows a fifth embodiment.
  • two lines are used.
  • 1) to 5) of the first embodiment are carried out to prepare a strand-shaped reconstructed tobacco sheet A.
  • a mixture of lamina A and B is prepared in the same manner as in 1) to 3) of the first embodiment, and this is further applied to 2), 3), 5 of the first embodiment.
  • the strand-shaped reconstituted tobacco sheet A and the strand-shaped lamina mixture are mixed.
  • the mixing ratio is appropriately adjusted so that the desired flavor can be achieved.
  • the mixture is subjected to a mixing and incense step with a non-tobacco material, and the obtained product is first stored.
  • the incense may be applied to one or more of the reconstituted tobacco sheets A, Lamina A, and Lamina B, or may be applied to all of them.
  • the effect described in the third aspect can be obtained. Further, as described in the fourth aspect, the filling amount can be reduced.
  • the production method of the present invention may further include a step of measuring the components of the tobacco filling and adjusting the addition amount of the additive based on the measurement result. At this time, it is preferable to convey the measurement result to the controller so that the information can be transmitted from the controller to the additive addition device. In particular, it is preferable to measure the nitrite of the tobacco filling and determine the amount of the antioxidant added based on this. If the amount of the antioxidant added is excessive, the cost will increase or the flavor will be impaired. Therefore, by determining the appropriate amount, it is possible to provide a user-friendly product without causing such a problem.
  • (6) Preparation of Reconstructed Tobacco Sheet The following describes a preferred embodiment for preparing the reconstructed tobacco sheet.
  • As the tobacco plant material yellow species, Burley species, Orient species, or native species in Nicotiana tabacum can be used alone or in combination.
  • the plant site may be any one or combination of flowers, leaves, veins, stems, or roots.
  • Tobacco plant material is roughly crushed to a size of about 1 to 40 mm or less and used for extraction with water.
  • the extraction temperature is preferably 30 to 90 ° C., and the extraction time is preferably 10 to 45 minutes.
  • the mixture that has undergone the extraction step is subjected to a separation operation by centrifugation or using a wire mesh, and is separated into an extract and a residue.
  • the extract is concentrated under reduced pressure under a temperature condition of 40 to 70 ° C. so that the ratio of the extract to water is 40 to 55% by weight.
  • An aerosol-forming substrate such as glycerin is mixed with the concentrated solution.
  • After mixing the residue with the coarsely ground wood pulp it is treated with a refiner to make the fibers fluffy, and then further ground to make the size uniform.
  • a mixture of the residue and wood pulp is suspended in a large amount of water, supplied in a fixed amount on a mesh wire used in a paper manufacturing process, dehydrated and dried to obtain a sheet.
  • the concentrate is sprayed onto the sheet. After spraying, dry again.
  • the sheet may be bobbin-wound, or may be shredded, cut into 3 to 10 cm squares, and stored in a container.
  • (Raw material composition) Yellow lamina / scrap (meat) 50-70% by weight Burley Lamina 0-50% by weight Yellow middle bone (leaf vein) 0-50% by weight Burley middle bone 0-35% by weight Wood pulp 7-12% by weight Glycerin 10-20% by weight Moisture 7-12% by weight (component) Nicotine 0.8-3.0% by weight (dry base) Reducing sugar 5.0-20.0% by weight (dry base) (Physical characteristics) Simple 0.8mm width Bulkiness after cutting 250-400cm 3 / 100g Swellability after watering, chopping to 0.8 mm width, and air-drying 300-450 cm 3/100 g
  • As the tobacco plant material yellow, Burley, Orient, or native species in Nicotiana tabacum can be used alone or in combination.
  • the plant site may be any one or combination of flowers, leaves, veins, stems, or roots.
  • Tobacco plant material is crushed to a size of 100 ⁇ m or less and mixed with aerosol-forming base materials such as water, pulp and glycerin, gums, modified celluloses, thickening polysaccharides, binders such as modified starch, and fragrances.
  • aerosol-forming base materials such as water, pulp and glycerin, gums, modified celluloses, thickening polysaccharides, binders such as modified starch, and fragrances.
  • the water content of the slurry is preferably 50% by volume or more.
  • the slurry is developed into a thin sheet on the substrate and dried in a dryer until the water content reaches about 7-14% by weight.
  • the sheet may be bobbin-wound, or may be shredded, cut into 3 to 10 cm squares, and stored in a container.
  • the raw material composition of the reconstructed tobacco sheet by the casting method and an example of the components are shown below.
  • (Raw material composition) Yellow lamina (meat) 60-95% by weight Burley Lamina 0-20% by weight Yellow middle bone (leaf vein) 0 to 20% by weight Burley middle bone 0% by weight Wood pulp 3-5% by weight Glycerin 10-20% by weight Guar gum 2-10% by weight Moisture 7-14% (component) Nicotine 1.5-5.0% by weight (dry base) Reducing sugar 5-20% by weight (dry base)
  • Aerosol-producing base materials such as water, pulp and glycerin, gums, modified cellulose, thickening polysaccharides, and binders such as modified starch are obtained by crushing tobacco plant material to a size of 300 ⁇ m or less. And mix with fragrances to prepare the kneaded product. After that, the kneaded product is placed in an extruder having a die having a predetermined thickness and a predetermined width at the outlet, and the sheet-shaped kneaded product is dried from the extruder on a drying drum or a drying conveyor. Push it out to the part. Dry in the dry part until the moisture value reaches about 7 to 14% by weight. Finally, the sheet may be bobbin-wound, or may be shredded, cut into 3 to 10 cm squares, and stored in a container.
  • Aerosol-producing base materials such as water, pulp and glycerin, gums, modified cellulose, thickening polysaccharides, and binders such as modified starch are obtained by crushing
  • (Raw material composition) Yellow lamina (meat) 60-95% by weight Burley Lamina 0-20% by weight Yellow middle bone (leaf vein) 0 to 20% by weight Burley middle bone 0% by weight Wood pulp 3-5% by weight Glycerin 10-20% by weight Hydroxypropyl cellulose 2-10% by weight Moisture 7-14% (component) Nicotine 1.5-5.0% by weight (dry base) Reducing sugar 5-20% by weight (dry base)
  • a tobacco rod portion in which the tobacco filler obtained in step 1 is filled in a tubular wrapper is prepared.
  • a tobacco rod portion can be manufactured by preparing paper as a wrapper and wrapping the tobacco filler with the paper.
  • the tobacco rod portion can be manufactured by preparing a tubular wrapper and filling the inside thereof with a tobacco filler.
  • the cross-sectional shape of the tubular wrapper is not limited and can be circular, elliptical, or polygonal.
  • the tobacco filling obtained by the production method of the present invention has particularly excellent swelling property.
  • the swelling property is a volume per unit weight when a mass of tobacco filling (preferably chopped) is compressed with a constant force, and is also an index of bulk density. Specifically, it is calculated by the following formula from the height of the tobacco carved cylinder obtained after applying a load of 11.4 kg in a measuring cylinder having a diameter of 95 mm in which the sample is placed for 5 seconds.
  • FP (A ⁇ h5) / W [cm 3 / 100g]
  • FP Bulkiness
  • A Cross-sectional area of the tobacco carved cylinder
  • W Weight of the tobacco carved h5: Height of the tobacco carved cylinder at the end of the load
  • the tobacco rod part of the flavor suction article is mainly manufactured by wrapping the tobacco filling with a columnar paper wrapper.
  • the tobacco rod part tends to be preferred by users if it is hard to some extent.
  • it is conceivable to increase the filling amount of the tobacco filling but increasing the filling amount causes an increase in cost.
  • a highly bulging tobacco filler can provide a tobacco rod portion with the required hardness with a smaller filling amount.
  • Non-combustion heating type flavor suction article Smoking articles include flavor suction articles in which the user tastes the flavor by suction, and smokeless tobacco (smokeless smoking article) in which the user tastes the flavor by directly including the product in the nasal cavity and oral cavity.
  • the flavor suction article can be roughly classified into a combustion type smoking article typified by a conventional cigarette and a non-combustion type smoking article.
  • the tobacco rod portion of the present invention is used for non-combustion heating type flavor suction articles used by heating among non-combustion type smoking articles.
  • the non-combustion heating type flavor suction article may be heated by a heating device separate from the article, or may be heated by a heating device integrated with the article.
  • the non-combustion heating type flavor suction article and the heating device are collectively referred to as a "non-combustion heating type smoking system".
  • An example of a non-combustion heating type smoking system will be described below with reference to FIGS. 6 and 7.
  • FIG. 6 is a schematic cross-sectional view showing an example of a non-combustion heating type smoking system, and shows a state before inserting the heater 12 into the tobacco rod portion 20A of the non-combustion heating type flavor suction article 20. At the time of use, the heater 12 is inserted into the tobacco rod portion 20A.
  • FIG. 7 is a cross-sectional view of the non-combustion heating type flavor suction article 20.
  • the non-combustion heating type smoking system includes a non-combustion heating type flavor suction article 20 and a heating device 10 for heating the tobacco rod portion 20A from the inside.
  • the non-combustion heating type smoking system is not limited to the configuration shown in FIG.
  • the heating device 10 shown in FIG. 6 includes a body 11 and a heater 12.
  • the body 11 may include a battery unit and a control unit.
  • the heater 12 can be a heater due to electric resistance, and is inserted into the tobacco rod portion 20A to heat the tobacco rod portion 20A.
  • the figure shows a mode in which the tobacco rod portion 20A is heated from the inside.
  • the aspect of the non-combustion heating type flavor suction article 20 is not limited to this, and in another aspect, the tobacco rod portion 20A is heated from the outside.
  • the heating temperature by the heating device 10 is not particularly limited, but is preferably 400 ° C. or lower, more preferably 50 to 400 ° C., and even more preferably 150 to 350 ° C.
  • the heating temperature refers to the temperature of the heater 12 of the heating device 10.
  • the non-combustion heating type flavor suction article 20 (hereinafter, simply referred to as “flavor suction article 20”) has a cylindrical shape.
  • the circumference of the flavor suction article 20 is preferably 16 mm to 27 mm, more preferably 20 mm to 26 mm, and even more preferably 21 mm to 25 mm.
  • the total length (horizontal length) of the flavor suction article 20 is not particularly limited, but is preferably 40 mm to 90 mm, more preferably 50 mm to 75 mm, and even more preferably 50 mm to 60 mm.
  • the flavor suction article 20 is composed of a tobacco rod portion 20A, a filter portion 20C constituting a mouthpiece, and a connecting portion 20B connecting these.
  • the tobacco rod portion 20A has a columnar shape, and its total length (length in the axial direction) is preferably, for example, 5 to 100 mm, more preferably 10 to 50 mm, and more preferably 10 to 25 mm. More preferred.
  • the shape of the cross section of the tobacco rod portion 20A is not particularly limited, but may be, for example, a circular shape, an elliptical shape, a polygonal shape, or the like.
  • the tobacco rod portion 20A has a tobacco filling 21 and a wrapper 22 wrapped around the tobacco filling 21. Further, the wrapper 22 may be a tobacco sheet made of the tobacco filler of the present invention.
  • the filter unit 20C has a cylindrical shape.
  • the filter unit 20C has a rod-shaped first segment 25 filled with cellulose acetate acetate fiber and a rod-shaped second segment 26 also filled with cellulose acetate acetate fiber.
  • the first segment 25 is located on the tobacco rod portion 20A side.
  • the first segment 25 may have a hollow portion.
  • the second segment 26 is located on the mouthpiece side.
  • the second segment 26 is solid.
  • the first segment 25 is composed of a first packed layer (cellulose acetate acetate fiber) 25a and an inner plug wrapper 25b wound around the first packed layer 25a.
  • the second segment 26 is composed of a second packed layer (cellulose acetate acetate fiber) 26a and an inner plug wrapper 26b wound around the second packed layer 26a.
  • the first segment 25 and the second segment 26 are connected by an outer plug wrapper 27.
  • the outer plug wrapper 27 is adhered to the first segment 25 and the second segment 26 with a vinyl acetate emulsion-based
  • the length of the filter portion 20C is, for example, 10 to 30 mm
  • the length of the connecting portion 20B is, for example, 10 to 30 mm
  • the length of the first segment 25 is, for example, 5 to 15 mm
  • the length of the second segment 26 is, for example, 5 to 15 mm. can do.
  • the length of each of these individual segments is an example, and can be appropriately changed depending on the manufacturing aptitude, the required quality, the length of the tobacco rod portion 20A, and the like.
  • the first segment 25 (center hole segment) is composed of a first packed layer 25a having one or more hollow portions and an inner plug wrapper 25b covering the first packed layer 25a.
  • the first segment 25 has a function of increasing the strength of the second segment 26.
  • the first packed layer 25a of the first segment 25 is filled with, for example, cellulose acetate fibers at a high density.
  • a plasticizer containing triacetin is added to the cellulose acetate fiber in an amount of, for example, 6 to 20% by weight based on the weight of the cellulose acetate and cured.
  • the hollow portion of the first segment 25 has, for example, an inner diameter of ⁇ 1.0 to ⁇ 5.0 mm.
  • the first packed layer 25a of the first segment 25 may be composed of, for example, a relatively high fiber filling density, or may be equivalent to the fiber filling density of the second packed layer 26a of the second segment 26 described later. May be good. Therefore, at the time of suction, air or aerosol flows only in the hollow portion, and almost no air or aerosol flows in the first packed bed 25a.
  • the length of the second segment 26 can be shortened and the first segment 25 can be lengthened by that amount.
  • Replacing the shortened second segment 26 with the first segment 25 is effective for increasing the delivery amount of the aerosol component. Since the first packed layer 25a of the first segment 25 is a fiber packed layer, the feeling of touch from the outside during use does not cause a sense of discomfort to the user.
  • the second segment 26 is composed of a second packed layer 26a and an inner plug wrapper 26b that covers the second packed layer 26a.
  • the second segment 26 (filter segment) is filled with cellulose acetate fibers at a general density and has the filtering performance of a general aerosol component.
  • the filtration performance for filtering the aerosol (mainstream smoke) emitted from the tobacco rod portion 20A may be different between the first segment 25 and the second segment 26. At least one of the first segment 25 and the second segment 26 may contain a fragrance.
  • the structure of the filter unit 20C is arbitrary, and may be a structure having a plurality of segments as described above, or may be composed of a single segment. Further, the filter unit 20C may be composed of one segment. In this case, the filter unit 20C may be composed of either the first segment or the second segment.
  • the connecting portion 20B has a cylindrical shape.
  • the connecting portion 20B has a paper tube 23 formed in a cylindrical shape by, for example, thick paper.
  • the connecting portion 20B may be filled with a cooling member for cooling the aerosol.
  • the cooling member include a sheet of a polymer such as polylactic acid, and the sheet can be folded and filled.
  • a support portion for suppressing the position of the tobacco rod portion 20A from fluctuating may be provided between the tobacco rod portion 20A and the connecting portion 20B.
  • the support portion can be made of a known material such as a center hole filter such as the first segment 25.
  • the wrapper 28 is wound in a cylindrical shape on the outside of the tobacco rod portion 20A, the connecting portion 20B, and the filter portion 20C, and these are integrally connected.
  • a vinyl acetate emulsion-based adhesive is applied to one surface (inner surface) of the wrapper 28 on the entire surface or substantially the entire surface except the vicinity of the ventilation hole portion 24.
  • the plurality of ventilation holes 24 are formed by laser processing from the outside after the tobacco rod portion 20A, the connecting portion 20B, and the filter portion 20C are integrated by the wrapper 28.
  • the ventilation hole portion 24 has two or more through holes so as to penetrate the connecting portion 20B in the thickness direction.
  • the two or more through holes are formed so as to be arranged radially when viewed from the extension line of the central axis of the flavor suction article 20.
  • the ventilation hole portion 24 is provided in the connecting portion 20B, but may be provided in the filter portion 20C.
  • the two or more through holes of the ventilation hole portion 24 are provided side by side in a row at regular intervals on one ring, but at regular intervals on the two rings.
  • the vent holes 24 in one row or two rows may be provided side by side in two rows, or the ventilation holes 24 in one row or two rows may be provided side by side in a discontinuous or irregular manner.
  • the swellability is a numerical value calculated from the height of a tobacco-engraved cylinder obtained after applying a load of 11.4 kg for 5 seconds in a measuring cylinder having a diameter of 95 mm in which a sample is placed. In other words, it represents the volume per unit weight when the block of ticks is compressed with a constant force.
  • FP (A ⁇ h5) / W [cm 3 / 100g]
  • FP Bulkiness
  • A Cross-sectional area of the tobacco carved cylinder
  • W Weight of the tobacco carved h5: Height of the tobacco carved cylinder at the end of the load
  • Example 1 ⁇ Humidification>
  • the reconstructed tobacco sheet (name: sheet 1) is placed in a cylinder-type container (inner diameter 0.9 m, length 2.0 m) equipped with a water supply device, a heating device, and a rotating device, and steam is added to humidify the sheet.
  • the product temperature of the reconstructed tobacco sheet at this time was about 50 to 70 ° C.
  • exhaust was performed from the cylinder.
  • the moisture content of the reconstituted tobacco sheet after humidification was 18.0% by weight.
  • the humidified tobacco sheet was cut using a cutting machine (manufactured by Hauni, named KT2L) with a cutting width of 0.8 mm.
  • the length of the engraving after cutting varied, but was in the range of approximately 5.0 mm to 30.0 mm.
  • the water content was 18.0% by weight.
  • Example 2 The reconstructed tobacco sheet was stamped by the same method as in Example 1 except that the type of the reconstructed tobacco sheet was changed to sheet 2, and the bulkiness was evaluated. The results are shown below. Moisture: 13.2 [% by weight] Bulkiness: 371 [cm 3 / 100g] The above results are summarized in the table below.
  • Both types of the reconstructed tobacco sheet produced by the method of the present invention had higher swelling property than the reconstructed tobacco sheet produced in the comparative example. Since the value of swelling property is strongly influenced by the shape of tobacco at the time of measuring swelling property, in this example, all the shapes of tobacco carvings are the same. In addition, since the water content during tobacco cutting also affects the swelling property, in this example, the water content of the tobacco cutting is made to be the same as much as possible. As an empirical formula (empirical formula), there is a correction formula that corrects the moisture content of tobacco in terms of bulkiness, but in this example, the difference in water content at each level is small, and it was judged that the water content correction is unnecessary.
  • an empirical formula empirical formula

Abstract

This method for manufacturing a tobacco rod part for a non-combustion heating-type flavor inhalation article comprises: step 1 for humidifying a tobacco filling material, followed by drying; and step 2 for preparing a tobacco rod part in which the tobacco filling material obtained in step 1 is filled in a cylindrical wrapper.

Description

非燃焼加熱型香味吸引物品用たばこロッド部の製造方法Manufacturing method of tobacco rod part for non-combustion heating type flavor suction goods
 本発明は非燃焼加熱型香味吸引物品用たばこロッド部の製造方法に関する。 The present invention relates to a method for manufacturing a tobacco rod portion for a non-combustion heating type flavor suction article.
 従来型の燃焼型香味吸引物品の代替として、非燃焼加熱型香味吸引物品が開発されている。当該物品には、比較的多量のエアロゾル生成基材を含有する再構成たばこシートが用いられる。例えば特許文献1、2には、前記再構成たばこシートをボビンから排出し、これを直接ラッパー内に充填してたばこロッド部を製造する方法が提案されている。 A non-combustion heating type flavor suction article has been developed as an alternative to the conventional combustion type flavor suction article. A reconstituted tobacco sheet containing a relatively large amount of aerosol-forming substrate is used for the article. For example, Patent Documents 1 and 2 propose a method of discharging the reconstructed tobacco sheet from a bobbin and directly filling the reconstructed tobacco sheet in a wrapper to manufacture a tobacco rod portion.
特許第6017546号Patent No. 6017546 特許第6307661号Patent No. 6307661
 前記特許文献に記載の方法は効率よくたばこロッド部を製造できるが、発明者らはたばこ充填物をラッパーに充填する前に特定の処理を行なえば、より品質を向上させることができるとの着想を得た。かかる事情を鑑み、本発明は品質を向上させた非燃焼加熱型香味吸引物品用たばこロッド部を提供することを課題とする。 The method described in the patent document can efficiently produce a tobacco rod portion, but the inventors have the idea that the quality can be further improved by performing a specific treatment before filling the wrapper with the tobacco filling. Got In view of such circumstances, it is an object of the present invention to provide a tobacco rod portion for a non-combustion heating type flavor suction article with improved quality.
 前記課題は、以下の本発明によって解決される。
態様1
 たばこ充填物を加湿後に乾燥する工程1、
 工程1で得たたばこ充填物が筒状ラッパー内に充填されたたばこロッド部を調製する工程2、
を備える非燃焼加熱型香味吸引物品用たばこロッド部の製造方法。
態様2
 前記たばこ充填物が、エアロゾル生成基材と再構成たばこシートとを含有する、態様1に記載の製造方法。
態様3
 前記たばこ充填物をストランド形状に裁断する工程をさらに備える、態様2に記載の製造方法。
態様4
 前記たばこ充填物が、再構成たばこシートAと再構成たばこシートBとを含有し、
 前記工程1が、それぞれの再構成たばこシートを加湿後に混合して当該混合物を乾燥する、またはそれぞれの再構成たばこシートを加湿し次いで乾燥した後に混合することを含む、
態様1~3のいずれかに記載の製造方法。
態様5
 前記たばこ充填物が、再構成たばこシートAとラミナとを含有し、
 前記工程1が、再構成たばこシートAとラミナをそれぞれ加湿後に混合して当該混合物を乾燥する、または再構成たばこシートAとラミナをそれぞれ加湿し次いで乾燥した後に混合することを含む、
態様1~3のいずれかに記載の製造方法。
態様6
 前記たばこ充填物に非たばこ材料を混合する工程をさらに含む、態様1~5のいずれかに記載の製造方法。
態様7
 前記たばこ充填物に添加剤を加える工程をさらに含む、態様1~6のいずれかに記載の製造方法。
態様8
 前記再構成たばこシートAと再構成たばこシートBのいずれか一方もしくは両方に添加剤を加える工程をさらに備える、態様4または6に記載の製造方法。
態様9
 前記再構成たばこシートとラミナのいずれか一方もしくは両方に添加剤を加える工程をさらに備える、態様5または6に記載の製造方法。
態様10
 前記たばこ充填物の成分を測定し、測定結果を基に前記添加剤の種類または添加量を調整する工程をさらに含む、態様7~9のいずれかに記載の製造方法。
態様11
 前記再構成たばこシートAの成分を測定し、
 測定結果に基づいて、再構成たばこシートBまたはラミナの種類を決定する、
 態様4または5に記載の製造方法。
態様12
 前記再構成たばこシートAの成分を測定し、
 測定結果に基づいて、
 再構成たばこシートBに添加する添加剤の種類または量、あるいは
 ラミナに添加する添加剤の種類または量を決定する、
 態様7に記載の製造方法。
態様13
 前記たばこ充填物中の水分量を15~25重量%とするように加湿を行う、態様1~3、6、または7のいずれかに記載の製造方法。
態様14
 前記再構成たばこシート中の水分量を15~25重量%とするように加湿を行う、態様4~12のいずれかに記載の製造方法。
態様15
 前記乾燥を、気流乾燥方式またはアニュラー乾燥方式で実施する、態様1~14のいずれかに記載の製造方法。
態様16
 前記再構成たばこシートが、抄造シート、キャストシート、または押出シートである、態様4~15のいずれかに記載の製造方法。
The above problems are solved by the following invention.
Aspect 1
Step 1, which dries the tobacco filling after humidification
Step 2, to prepare a tobacco rod portion in which the tobacco filler obtained in step 1 is filled in a tubular wrapper.
A method for manufacturing a tobacco rod portion for a non-combustion heating type flavor suction article.
Aspect 2
The production method according to aspect 1, wherein the tobacco filler contains an aerosol-forming substrate and a reconstituted tobacco sheet.
Aspect 3
The production method according to aspect 2, further comprising a step of cutting the tobacco filling into a strand shape.
Aspect 4
The tobacco filling contains the reconstituted tobacco sheet A and the reconstructed tobacco sheet B.
The step 1 comprises humidifying and then mixing each reconstituted tobacco sheet to dry the mixture, or humidifying and then drying each reconstituted tobacco sheet and then mixing.
The production method according to any one of aspects 1 to 3.
Aspect 5
The tobacco filling contains the reconstituted tobacco sheet A and lamina.
The step 1 comprises humidifying and then mixing the reconstituted tobacco sheet A and lamina to dry the mixture, or humidifying and then drying the reconstituted tobacco sheet A and lamina, respectively.
The production method according to any one of aspects 1 to 3.
Aspect 6
The production method according to any one of aspects 1 to 5, further comprising the step of mixing the non-tobacco material with the tobacco filling.
Aspect 7
The production method according to any one of aspects 1 to 6, further comprising a step of adding an additive to the tobacco filling.
Aspect 8
The production method according to aspect 4 or 6, further comprising a step of adding an additive to either or both of the reconstituted tobacco sheet A and the reconstituted tobacco sheet B.
Aspect 9
The production method according to aspect 5 or 6, further comprising a step of adding an additive to either or both of the reconstituted tobacco sheet and the lamina.
Aspect 10
The production method according to any one of aspects 7 to 9, further comprising a step of measuring the components of the tobacco filling and adjusting the type or amount of the additive based on the measurement result.
Aspect 11
The components of the reconstituted tobacco sheet A were measured and
Determine the type of reconstituted tobacco sheet B or lamina based on the measurement results,
The production method according to aspect 4 or 5.
Aspect 12
The components of the reconstituted tobacco sheet A were measured and
Based on the measurement results
To determine the type or amount of additive to be added to the reconstituted tobacco sheet B, or the type or amount of additive to be added to lamina.
The manufacturing method according to aspect 7.
Aspect 13
The production method according to any one of aspects 1 to 3, 6 or 7, wherein the humidification is performed so that the water content in the tobacco filling is 15 to 25% by weight.
Aspect 14
The production method according to any one of aspects 4 to 12, wherein humidification is performed so that the water content in the reconstructed tobacco sheet is 15 to 25% by weight.
Aspect 15
The production method according to any one of aspects 1 to 14, wherein the drying is carried out by an air flow drying method or an annual drying method.
Aspect 16
The production method according to any one of aspects 4 to 15, wherein the reconstructed tobacco sheet is a papermaking sheet, a cast sheet, or an extruded sheet.
 本発明によって品質を向上させた非燃焼加熱型香味吸引物品用のたばこロッド部を提供することができる。 According to the present invention, it is possible to provide a tobacco rod portion for a non-combustion heating type flavor suction article whose quality has been improved.
第1の実施形態の概念図Conceptual diagram of the first embodiment 第2の実施形態の概念図Conceptual diagram of the second embodiment 第3の実施形態の概念図Conceptual diagram of the third embodiment 第4の実施形態の概念図Conceptual diagram of the fourth embodiment 第5の実施形態の概念図Conceptual diagram of the fifth embodiment 非燃焼加熱型喫煙システムの一例を示す断面模式図Schematic cross-sectional view showing an example of a non-combustion heating type smoking system 非燃焼加熱型香味吸引物品の一例を示す断面模式図Schematic cross-sectional view showing an example of a non-combustion heating type flavor suction article
発明を実施する形態Embodiment of the invention
 以下、本発明を詳細に説明する。本発明において「X~Y」はその端値であるXおよびYを含む。
 本発明の製造方法はたばこ充填物を加湿後に乾燥する工程1、および工程1で得たたばこ充填物が筒状ラッパー内に充填されたたばこロッド部を調製する工程2を備える。
1.工程1
(1)たばこ充填物
 たばこ充填物とは、ラッパー内に充填されて喫煙に供される材料である。本発明においては公知のたばこ充填物を使用できるが、製造のし易さという観点からたばこシートを含むことが好ましい。たばこシートとは、シート状のたばこ材料であり、本発明においては再構成たばこシートが好ましい。一態様において「たばこシート」という文言は、シート状のたばこ材料、または当該シート状のたばこ材料に由来する材料(例えば裁刻物)を意味する。再構成たばこシートとは、タバコ属植物の細粉からなる再構成物(再構成たばこまたは再構成たばこ顆粒)を含むたばこシートである。当該たばこシートは抄造法で製造される抄造シート、キャスト法で製造されるキャストシート、または押出法で製造される押出シートであってよい。
Hereinafter, the present invention will be described in detail. In the present invention, "X to Y" includes X and Y which are fractional values thereof.
The production method of the present invention includes a step 1 of humidifying and then drying the tobacco filling, and a step 2 of preparing a tobacco rod portion in which the tobacco filling obtained in the step 1 is filled in a tubular wrapper.
1. 1. Process 1
(1) Tobacco filling The tobacco filling is a material that is filled in a wrapper and used for smoking. Although known tobacco fillers can be used in the present invention, it is preferable to include a tobacco sheet from the viewpoint of ease of production. The tobacco sheet is a sheet-shaped tobacco material, and in the present invention, a reconstructed tobacco sheet is preferable. In one aspect, the term "tobacco sheet" means a sheet-like tobacco material or a material derived from the sheet-like tobacco material (eg, a cut piece). The reconstituted tobacco sheet is a tobacco sheet containing a reconstituted product (reconstructed tobacco or reconstituted tobacco granules) composed of fine powder of a plant belonging to the genus Tobacco. The tobacco sheet may be a papermaking sheet manufactured by a papermaking method, a cast sheet manufactured by a casting method, or an extrusion sheet manufactured by an extrusion method.
 抄造法は、たばこ原料と水等の液体媒体とを含む混合物を抄紙し、乾燥してシートを製造する方法である。混合物は、通常、パルプまたは繊維化されたたばこ原料を含む。キャスト法は、たばこ原料と水等の液体媒体とを含む混合物を、基材の上に展開(キャストして)、乾燥してシートを製造する方法である。押出法は、たばこ原料と水等の液体媒体とを含む混合物をTダイなどのダイから押出してシートを製造する方法である。 The papermaking method is a method in which a mixture containing a tobacco raw material and a liquid medium such as water is made into paper and dried to produce a sheet. The mixture usually contains pulp or fibrous tobacco material. The casting method is a method in which a mixture containing a tobacco raw material and a liquid medium such as water is developed (cast) on a substrate and dried to produce a sheet. The extrusion method is a method for producing a sheet by extruding a mixture containing a tobacco raw material and a liquid medium such as water from a die such as a T die.
 たばこ充填物はエアロゾル生成基材を含んでいてもよい。エアロゾル生成基材とは、加熱により気化し冷却されてエアロゾルを生成するあるいは霧化によってエアロゾルを生成する材料である。エアロゾル生成基材としては公知のものを用いることができるが、その例としてはグリセリン、プロピレングリコール(PG)等の多価アルコール、トリエチルシトレート(TEC)、トリアセチン等の沸点が100℃を超えるものが挙げられる。たばこ充填物におけるエアロゾル生成基材の量は、乾燥重量(混入している水を除いた重量、以下同様)で、好ましくは1~40重量%、より好ましくは5~30重量%、さらに好ましくは5~20重量%である。エアロゾル生成基材の量が上限値を超えるとたばこ充填物の製造が困難となるおそれがあり、下限値未満であると煙感量が低下するおそれがある。 The tobacco filling may contain an aerosol-forming substrate. The aerosol-forming substrate is a material that is vaporized and cooled by heating to form an aerosol, or is atomized to produce an aerosol. Known aerosol-forming substrates can be used, and examples thereof include polyhydric alcohols such as glycerin and propylene glycol (PG), triethylcitrate (TEC), triacetin and the like having a boiling point of more than 100 ° C. Can be mentioned. The amount of the aerosol-forming substrate in the tobacco filling is preferably 1 to 40% by weight, more preferably 5 to 30% by weight, still more preferably, by dry weight (weight excluding mixed water, the same applies hereinafter). It is 5 to 20% by weight. If the amount of the aerosol-forming substrate exceeds the upper limit, it may be difficult to manufacture the tobacco filling, and if it is less than the lower limit, the amount of smoke sensation may decrease.
 再構成たばこシートを用いる場合は、枚葉形態であるものを解除して、工程1に定量的に供給することが好ましい。解除とは、積層されて塊状になっている(枚葉形態にある)再構成たばこシートを1枚のシートにほぐすことをいう。そのサイズは限定されないが、一態様において枚葉形態の再構成たばこシートは、柱状体であり、その断面は1辺が3~10cmの四角形である。 When using a reconstructed tobacco sheet, it is preferable to release the sheet-fed form and supply it quantitatively to step 1. Release means to loosen the reconstructed tobacco sheet (in the form of a single leaf) that is laminated and agglomerated into one sheet. The size is not limited, but in one embodiment, the single-leaf reconstructed tobacco sheet is a columnar body, and its cross section is a quadrangle having a side of 3 to 10 cm.
 枚葉形態の再生たばこシートを輸送する際は、取り扱いやすい形状およびサイズの梱包容器内に充填されることが好ましい。梱包容器の一例として、たばこ製造業者の間で知られているC-48ボックスが挙げられる。C-48ボックスは段ボール製であり、約115×70×75cmのサイズである。枚葉形態の再生たばこシートをC-48ボックスに直接充填することもできるが、輸送中の品質変化を抑制するために、プラスチック製の袋に充填した後にC-48ボックスに収容してもよい。本願実施形態によれば、C-48ボックス中に100~200kg程度の枚葉形態の再構成たばこシートが充填される。 When transporting a single-leaf regenerated tobacco sheet, it is preferable to fill it in a packaging container having a shape and size that is easy to handle. An example of a packaging container is the C-48 box, which is known among cigarette manufacturers. The C-48 box is made of cardboard and measures approximately 115 x 70 x 75 cm. The single-wafer regenerated tobacco sheet can be directly filled in the C-48 box, but may be packed in a plastic bag and then housed in the C-48 box in order to suppress quality changes during transportation. .. According to the embodiment of the present application, the C-48 box is filled with about 100 to 200 kg of a reconstructed tobacco sheet in a single-wafer form.
 別の態様として、再生たばこシートをボビン形状で輸送する方法が挙げられる。再構成シート製造工程において、幅10~100cmの縦方向に連なるシートをコアに巻きつけてボビン形状とすることができる。ボビン形状で輸送された再生たばこシートを本発明に用いる場合は、再構成たばこシートを工程1に供する前に、シュレッダー等を用いて所定の大きさに再構成たばこシートをカットする必要がある。 Another aspect is a method of transporting a recycled tobacco sheet in a bobbin shape. In the reconstructed sheet manufacturing process, a vertically continuous sheet having a width of 10 to 100 cm can be wound around a core to form a bobbin shape. When the regenerated tobacco sheet transported in the bobbin shape is used in the present invention, it is necessary to cut the reconstructed tobacco sheet to a predetermined size using a shredder or the like before the reconstructed tobacco sheet is subjected to the step 1.
(2)加湿
 加湿は公知の装置を用いて行うことができるが、本発明においては効率性の観点から、シリンダ型装置を用いることが好ましい。当該装置は、給水装置、加熱装置、排気装置を備え、シリンダの中心軸を中心として回転させる回転装置を備える。加湿は、給水装置からたばこ充填物に水を供給することで実施される。加湿条件は、加湿後のたばこ充填物の水分量が15~25重量%程度となるように調整される。一態様において、シリンダの内壁温度を50~70℃、シリンダ内の空気の流速を0.05~0.15m/秒、たばこ充填物の滞在時間を3~6分程度とすることができる。シリンダの寸法は限定されないが、一態様において直径は2~4m、長さは5~10m程度である。加湿は、シリンダ内を通気して実施することがより好ましい。たばこ充填物が加熱されることで、アンモニア等の沸点の低い内容成分の一部が揮発し、排気によりシリンダ外に排出されることで、使用時のネガティブな味および香りが軽減される。
(2) Humidification Humidification can be performed using a known device, but in the present invention, it is preferable to use a cylinder type device from the viewpoint of efficiency. The device includes a water supply device, a heating device, an exhaust device, and a rotating device that rotates around the central axis of the cylinder. Humidification is carried out by supplying water from the water supply device to the tobacco filling. The humidification conditions are adjusted so that the water content of the tobacco filling after humidification is about 15 to 25% by weight. In one embodiment, the temperature of the inner wall of the cylinder can be set to 50 to 70 ° C., the flow rate of air in the cylinder can be set to 0.05 to 0.15 m / sec, and the residence time of the tobacco filling can be set to about 3 to 6 minutes. The size of the cylinder is not limited, but in one embodiment, the diameter is about 2 to 4 m and the length is about 5 to 10 m. Humidification is more preferably carried out by ventilating the inside of the cylinder. When the tobacco filling is heated, some of the low boiling point content components such as ammonia are volatilized and discharged to the outside of the cylinder by exhaust gas, thereby reducing the negative taste and aroma during use.
(3)乾燥
 乾燥により、たばこ充填物を保存に適した状態とできる。乾燥は公知の方法で行うことができるが、本発明においては効率性の観点から、気流乾燥方式またはアニュラー乾燥方式を採用することが好ましい。前者は加熱された気流(好ましくは過熱水蒸気)とたばこ充填物とを管内で接触させて乾燥を行う方式である。このような装置としては国際公開2013/052490に記載されたものが挙げられる。この方式ではたばこ充填物に特徴的な香味キャラクターを付与することもできる。この方式では短時間でたばこ充填物中の水分を乾燥させるので、乾燥後のたばこ充填物を乾燥前と比して膨らませることができるし、乾燥後のたばこ充填物の形状がカールされた形状となるため、たばこ充填物の膨嵩性が増大する。また、大量の過熱水蒸気の雰囲気下にて短時間で乾燥されるため、乾燥工程で加熱される際の雰囲気中の酸素量を低減できるので酸素に起因する望まないたばこ充填物の化学変化を抑制できる。
(3) Drying By drying, the tobacco filling can be put into a state suitable for storage. Drying can be performed by a known method, but in the present invention, it is preferable to adopt an air flow drying method or an annual drying method from the viewpoint of efficiency. The former is a method in which a heated air flow (preferably superheated steam) and a tobacco filling are brought into contact with each other in a pipe to perform drying. Examples of such a device include those described in International Publication 2013/052490. In this method, it is also possible to give a characteristic flavor character to the tobacco filling. In this method, the moisture in the tobacco filling is dried in a short time, so that the dried tobacco filling can be inflated compared to before drying, and the shape of the dried tobacco filling is curled. Therefore, the bulkiness of the tobacco filling increases. In addition, since it is dried in a short time under the atmosphere of a large amount of superheated steam, the amount of oxygen in the atmosphere when heated in the drying step can be reduced, and the chemical change of the unwanted tobacco filling caused by oxygen is suppressed. can.
 後者は、シリンダ型装置内でたばこ充填物を加熱して乾燥させる方式である。この方式であると、たばこ充填物に含まれている揮発性の高い成分を除去することもできる。本方式は、気流乾燥方式と比較して乾燥に長時間を要するため、きめ細かい水分管理が行なうことができ、出口水分の正確な仕上がりを達成できる点で好ましい。 The latter is a method of heating and drying the tobacco filling in a cylinder type device. With this method, it is also possible to remove highly volatile components contained in the tobacco filling. Since this method requires a longer time to dry than the air flow drying method, it is preferable in that fine moisture control can be performed and accurate finish of outlet moisture can be achieved.
(4)実施態様
 以下、好ましい実施態様を挙げて工程1を説明する。
(4-1)第1の実施形態
 1)準備
 図1は第1の実施形態を示す。本実施態様によれば、枚葉形態の再構成たばこシートを準備して、これを解除する。この段階での再構成たばこシートの水分量は、好ましくは5~15重量%である。解除前または解除後にエアロゾル生成基材を添加する。当該シートにおけるエアロゾル生成基材の量は、好ましくは5~30重量%である。解除された再構成たばこシートからは異物が除去される。また、ブレンドサイロを用いて再構成たばこシートを混合し、品質を均質化することもできる。
(4) Embodiment Hereinafter, step 1 will be described with reference to preferred embodiments.
(4-1) First Embodiment 1) Preparation Figure 1 shows the first embodiment. According to this embodiment, a reconstructed tobacco sheet in a single-wafer form is prepared and released. The water content of the reconstituted tobacco sheet at this stage is preferably 5 to 15% by weight. The aerosol-forming substrate is added before or after release. The amount of the aerosol-forming substrate in the sheet is preferably 5 to 30% by weight. Foreign matter is removed from the released reconstituted tobacco sheet. It is also possible to use a blend silo to mix the reconstituted tobacco sheets to homogenize the quality.
 2)加湿
 次いで再構成たばこシートを加湿する。加湿に用いる装置および加湿条件は前述のとおりである。この際、再構成たばこシートの水分量は15~25重量%に調製される。また、この工程で、たばこ原料由来の好ましくない成分(エグ味を与える成分等)が除去される。
2) Humidification Next, humidify the reconstituted tobacco sheet. The equipment used for humidification and the humidification conditions are as described above. At this time, the water content of the reconstituted tobacco sheet is adjusted to 15 to 25% by weight. Further, in this step, unfavorable components derived from the tobacco raw material (components that give an astringent taste, etc.) are removed.
 3)添加剤の添加(加香)
 この工程では、加湿後の再構成たばこシートに添加剤を加える。添加剤とは、再構成たばこシート等の原料とエアロゾル生成基材以外の材料である。添加剤としては、たばこ粉;香料;前述のエアロゾル生成基材;酸やアルカリ等のたばこ香増強剤;エタノール、水、ベンジルアルコール、プロピレングリコール等の溶媒;ポリフェノールまたはビタミンなどの抗酸化剤が挙げられる。添加剤の添加は公知の方法で実施できるが、回転するシリンダ型装置に再構成たばこシートを充填し、香料等を噴霧することで実施できる。中でも、香味成分であるたばこ粉または香料を添加することを特に加香といい、本態様では加香を行うことが好ましい。この段階での加香は、分子量が比較的大きい香味成分を添加する場合に好適である。このような香味成分は蒸気圧が低く、水との親和性が高いため、加湿後の再構成たばこシートに加えると、シートの内部まで浸透しやすいからである。
3) Addition of additives (incense)
In this step, additives are added to the reconstituted tobacco sheet after humidification. The additive is a material other than a raw material such as a reconstructed tobacco sheet and an aerosol-forming base material. Additives include tobacco powder; fragrances; the aforementioned aerosol-producing substrates; tobacco aroma enhancers such as acids and alkalis; solvents such as ethanol, water, benzyl alcohol and propylene glycol; antioxidants such as polyphenols or vitamins. Be done. The additive can be added by a known method, but it can be carried out by filling a rotating cylinder type device with a reconstructed tobacco sheet and spraying a fragrance or the like. Above all, the addition of tobacco powder or fragrance, which is a flavor component, is particularly referred to as fragrance, and in this embodiment, it is preferable to perform fragrance. The aroma at this stage is suitable for adding a flavor component having a relatively large molecular weight. This is because such a flavor component has a low vapor pressure and a high affinity with water, and therefore, when added to a reconstituted tobacco sheet after humidification, it easily penetrates into the inside of the sheet.
 香料としては、以下のものが挙げられ、これらは単独または複数の組み合わせで使用できる。
 アセトアニソール、アセトフェノン、アセチルピラジン、2-アセチルチアゾール、アルファルファエキストラクト、アミルアルコール、酪酸アミル、トランス-アネトール、スターアニス油、リンゴ果汁、ペルーバルサム油、ミツロウアブソリュート、ベンズアルデヒド、ベンゾインレジノイド、ベンジルアルコール、安息香酸ベンジル、フェニル酢酸ベンジル、プロピオン酸ベンジル、2,3-ブタンジオン、2-ブタノール、酪酸ブチル、酪酸、カラメル、カルダモン油、キャロブアブソリュート、β-カロテン、ニンジンジュース、L-カルボン、β-カリオフィレン、カシア樹皮油、シダーウッド油、セロリーシード油、カモミール油、シンナムアルデヒド、ケイ皮酸、シンナミルアルコール、ケイ皮酸シンナミル、シトロネラ油、DL-シトロネロール、クラリセージエキストラクト、ココア、コーヒー、コニャック油、コリアンダー油、クミンアルデヒド、ダバナ油、δ-デカラクトン、γ-デカラクトン、デカン酸、ディルハーブ油、3,4-ジメチル-1,2-シクロペンタンジオン、4,5-ジメチル-3-ヒドロキシ-2,5-ジヒドロフラン-2-オン、3,7-ジメチル-6-オクテン酸、2,3-ジメチルピラジン、2,5-ジメチルピラジン、2,6-ジメチルピラジン、2-メチル酪酸エチル、酢酸エチル、酪酸エチル、ヘキサン酸エチル、イソ吉草酸エチル、乳酸エチル、ラウリン酸エチル、レブリン酸エチル、エチルマルトール、オクタン酸エチル、オレイン酸エチル、パルミチン酸エチル、フェニル酢酸エチル、プロピオン酸エチル、ステアリン酸エチル、吉草酸エチル、エチルバニリン、エチルバニリングルコシド、2-エチル-3,(5または6)-ジメチルピラジン、5-エチル-3-ヒドロキシ-4-メチル-2(5H)-フラノン、2-エチル-3-メチルピラジン、ユーカリプトール、フェネグリークアブソリュート、ジェネアブソリュート、リンドウ根インフュージョン、ゲラニオール、酢酸ゲラニル、ブドウ果汁、グアヤコール、グァバエキストラクト、γ-ヘプタラクトン、γ-ヘキサラクトン、ヘキサン酸、シス-3-ヘキセン-1-オール、酢酸ヘキシル、ヘキシルアルコール、フェニル酢酸ヘキシル、ハチミツ、4-ヒドロキシ-3-ペンテン酸ラクトン、4-ヒドロキシ-4-(3-ヒドロキシ-1-ブテニル)-3,5,5-トリメチル-2-シクロヘキセン-1-オン、4-(パラ-ヒドロキシフェニル)-2-ブタノン、4-ヒドロキシウンデカン酸ナトリウム、インモルテルアブソリュート、β-イオノン、酢酸イソアミル、酪酸イソアミル、フェニル酢酸イソアミル、酢酸イソブチル、フェニル酢酸イソブチル、ジャスミンアブソリュート、コーラナッツティンクチャー、ラブダナム油、レモンテルペンレス油、カンゾウエキストラクト、リナロール、酢酸リナリル、ロベージ根油、マルトール、メープルシロップ、メンソール、メントン、酢酸L-メンチル、パラメトキシベンズアルデヒド、メチル-2-ピロリルケトン、アントラニル酸メチル、フェニル酢酸メチル、サリチル酸メチル、4’-メチルアセトフェノン、メチルシクロペンテノロン、3-メチル吉草酸、ミモザアブソリュート、トウミツ、ミリスチン酸、ネロール、ネロリドール、γ-ノナラクトン、ナツメグ油、δ-オクタラクトン、オクタナール、オクタン酸、オレンジフラワー油、オレンジ油、オリス根油、パルミチン酸、ω-ペンタデカラクトン、ペパーミント油、プチグレインパラグアイ油、フェネチルアルコール、フェニル酢酸フェネチル、フェニル酢酸、ピペロナール、プラムエキストラクト、プロペニルグアエトール、酢酸プロピル、3-プロピリデンフタリド、プルーン果汁、ピルビン酸、レーズンエキストラクト、ローズ油、ラム酒、セージ油、サンダルウッド油、スペアミント油、スチラックスアブソリュート、マリーゴールド油、ティーディスティレート、α-テルピネオール、酢酸テルピニル、5,6,7,8-テトラヒドロキノキサリン、1,5,5,9-テトラメチル-13-オキサシクロ(8.3.0.0(4.9))トリデカン、2,3,5,6-テトラメチルピラジン、タイム油、トマトエキストラクト、2-トリデカノン、クエン酸トリエチル、4-(2,6,6-トリメチル-1-シクロヘキセニル)2-ブテン-4-オン、2,6,6-トリメチル-2-シクロヘキセン-1,4-ジオン、4-(2,6,6-トリメチル-1,3-シクロヘキサジエニル)2-ブテン-4-オン、2,3,5-トリメチルピラジン、γ-ウンデカラクトン、γ-バレロラクトン、バニラエキストラクト、バニリン、ベラトルアルデヒド、バイオレットリーフアブソリュート、N-エチル-p-メンタン-3-カルボアミド(WS-3)、エチル-2-(p-メンタン-3-カルボキサミド)アセテート(WS-5)、糖(スクロース、フルクトース等)、ココア粉、キャロブ粉、コリアンダー粉、リコリス粉、オレンジピール粉、ローズピップ粉、カモミールフラワー(flower)粉、レモンバーベナ粉、ペパーミント粉、リーフ粉、スペアミント粉、紅茶粉、天然植物性香料(例えば、ジャスミン油、レモン油、ベチバー油、ロベージ油)、エステル類(例えば、酢酸メンチル、プロピオン酸イソアミル、等)、アルコール類(例えば、フェニルエチルアルコール、シス-6-ノネン-1-オール、等)。
The fragrances include the following, which can be used alone or in combination of two or more.
Acetanisol, acetophenone, acetylpyrazine, 2-acetylthiazole, alfalfa extract, amyl alcohol, amyl butyrate, trans-annetol, staranis oil, apple juice, peruval balsam oil, honeywort absolute, benzaldehyde, benzoin resinoid, benzyl alcohol, benzoate Lactone benzyl acid, benzyl phenylacetate, benzyl propionate, 2,3-butandione, 2-butanol, butyl butyrate, butyric acid, caramel, cardamon oil, carobu absolute, β-carotene, carrot juice, L-carboxylic, β-cariophyllene, cassia Bark oil, cedar wood oil, celery seed oil, chamomile oil, cinnamaldehyde, silicic acid, cinnamyl alcohol, cinnamyl silicate oil, citronella oil, DL-citronellol, clarisage extract, cocoa, coffee, cognac oil, coriander oil, Cuminaldehyde, davana oil, δ-decalactone, γ-decalactone, decanoic acid, dill herb oil, 3,4-dimethyl-1,2-cyclopentandione, 4,5-dimethyl-3-hydroxy-2,5-dihydro Fran-2-one, 3,7-dimethyl-6-octenoic acid, 2,3-dimethylpyrazine, 2,5-dimethylpyrazine, 2,6-dimethylpyrazine, ethyl 2-methylbutyrate, ethyl acetate, ethyl butyrate, Ethyl hexaneate, ethyl isovalerate, ethyl lactate, ethyl laurate, ethyl levulinate, ethyl maltor, ethyl octanate, ethyl oleate, ethyl palmitate, ethyl phenylacetate, ethyl propionate, ethyl stearate, ethyl valerate , Ethylvaniline, ethylvaniline glucoside, 2-ethyl-3, (5 or 6) -dimethylpyrazine, 5-ethyl-3-hydroxy-4-methyl-2 (5H) -furanone, 2-ethyl-3-methylpyrazine , Eucalyptor, Pheneglique Absolute, Gene Absolute, Lindow Root Infusion, Geraniol, Geranyl Acetate, Grape Juice, Guayacol, Guava Extract, γ-Heptalactone, γ-Hexalactone, Hexanoic Acid, Sis-3-Hexen-1 -Ol, hexyl acetate, hexyl alcohol, phenylacetate hexyl, honey, 4-hydroxy-3-pentenoic acid lactone, 4-hydroxy-4- (3-hydroxy-1-butenyl) -3,5,5-trimethyl-2 -Cyclo Hexen-1-one, 4- (para-hydroxyphenyl) -2-butanone, sodium 4-hydroxyundecanoate, immortel absolute, β-ionone, isoamyl acetate, isoamyl butyrate, isoamyl phenylacetate, isobutyl acetate, phenylacetic acid Isobutyl, jasmine absolute, cola nut tincture, labdanum oil, lemon terpenless oil, kanzo extract, linalol, linaryl acetate, lobage root oil, maltol, maple syrup, menthol, menthon, L-mentyl acetate, paramethoxybenzaldehyde, methyl -2-Pyrrolyl ketone, Methyl anthranilate, Methyl phenylacetate, Methyl salicylate, 4'-Methylacetophenone, Methylcyclopentenolone, 3-Methylvaleric acid, Mimosa absolute, Toumitsu, Myristic acid, Nerol, Nerolidel, γ-Nonalactone, Natsumegu oil, δ-octalactone, octanal, octanoic acid, orange flower oil, orange oil, orris root oil, palmitic acid, ω-pentadecalactone, peppermint oil, petitgrain paraguay oil, phenethyl alcohol, phenylacetate phenethyl, phenylacetic acid , Piperonal, Plum Extract, Propenylguaetol, propyl Acetate, 3-Propyridenphthalide, Prune Juice, Pyruvate, Rasen Extract, Rose Oil, Lamb Liquor, Sage Oil, Sandalwood Oil, Sparemint Oil, Stilax Absolute, marigold oil, tea distillate, α-terpineol, terpinyl acetate, 5,6,7,8-tetrahydroquinoxaline, 1,5,5,9-tetramethyl-13-oxacyclo (8.3.0.0) (4.9)) Tridecane, 2,3,5,6-tetramethylpyrazine, thyme oil, tomato extract, 2-toridecanone, triethyl citrate, 4- (2,6,6-trimethyl-1-cyclohexenyl) ) 2-Buten-4-one, 2,6,6-trimethyl-2-cyclohexene-1,4-dione, 4- (2,6,6-trimethyl-1,3-cyclohexadienyl) 2-buten- 4-one, 2,3,5-trimethylpyrazine, γ-undecalactone, γ-valerolactone, vanilla extract, vanillin, veratoraldehyde, violet leaf absolute, N-ethyl-p-menthan-3-carbamide ( WS-3), ethyl-2- (p-mentor) N-3-Carboxamide) Acetate (WS-5), sugar (sucrose, fructose, etc.), cocoa powder, carob powder, coriander powder, licorice powder, orange peel powder, rose pip powder, chamomile flower powder, lemon verbena Powder, peppermint powder, leaf powder, sparemint powder, black tea powder, natural vegetable fragrances (eg jasmine oil, lemon oil, vetiver oil, lobage oil), esters (eg mentyl acetate, isoamyl propionate, etc.), alcohol Kinds (eg, phenylethyl alcohol, cis-6-nonen-1-ol, etc.).
 また、添加剤として抗酸化剤を添加することも好ましい。非燃焼加熱型香味吸引物品のたばこベイパー中にはTSNAs(Tobacco specific ニトロソアミン)が含まれていることが報告されている(非特許文献1)。非燃焼加熱型香味吸引物品においては、使用時にたばこ充填物が長時間継続して加熱される。このため、非燃焼加熱型香味吸引物品のたばこ充填物中では、長時間の加熱により、意図しない成分が生成される可能性がある。抗酸化剤を添加することによって前記の反応を抑制し、意図しない成分の生成を抑えることができる。 It is also preferable to add an antioxidant as an additive. It has been reported that TSNAs (Tobacco specific nitrosamines) are contained in the tobacco vapor of the non-combustion heating type flavor suction article (Non-Patent Document 1). In the non-combustion heating type flavor suction article, the tobacco filling is continuously heated for a long time at the time of use. Therefore, in the tobacco filling of the non-combustion heating type flavor suction article, unintended components may be generated by heating for a long time. By adding an antioxidant, the above reaction can be suppressed and the production of unintended components can be suppressed.
 抗酸化剤としては、例えば食品添加物として公知である抗酸化剤を使用することができる。例としては、没食子酸、エリソルビン酸、アスコルビン酸、カテキン、ジヒドロカフェ酸、p-クマル酸、フェルラ酸、3-(4-ヒドロキシフェニル)プロピオン酸、ケルセチン、エスクレチン、ケンフェロール、カフェ酸、トコフェロール、ジブチルヒドロキシトルエン(BHT)、キナ酸、クロロゲン酸、ルチン、スコポレチン、およびケイ皮酸が挙げられる。抗酸化剤は、好ましくは、没食子酸およびエリソルビン酸からなる群より選ばれる少なくとも1つである。抗酸化剤は、たばこ充填物に対して、例えば0.25~10重量%、好ましくは0.25~5.0重量%、より好ましくは重量%の量で、たばこ充填物に含まれる。抗酸化剤は、水やエタノール等の溶媒に溶融もしくは分散させてスプレーすること等によってたばこ充填物に添加することができる。 As the antioxidant, for example, an antioxidant known as a food additive can be used. Examples include ascorbic acid, erythorbic acid, ascorbic acid, catechin, dihydrocaffeic acid, p-coumaric acid, ferulic acid, 3- (4-hydroxyphenyl) propionic acid, quercetin, esculetin, kenferol, caffeic acid, tocopherol, Examples include dibutylhydroxytoluene (BHT), quinic acid, chlorogenic acid, rutin, scopoletin, and cinnamic acid. The antioxidant is preferably at least one selected from the group consisting of gallic acid and erythorbic acid. The antioxidant is contained in the tobacco filling in an amount of, for example, 0.25 to 10% by weight, preferably 0.25 to 5.0% by weight, more preferably% by weight, based on the tobacco filling. The antioxidant can be added to the tobacco filling by melting or dispersing it in a solvent such as water or ethanol and spraying it.
 4)裁刻
 本工程では、加香された再構成たばこシートを裁刻する。裁刻は公知の装置を用いて実施できるが、本発明においては、再構成たばこシートを、その端部がナイフドラムの刃の延びる方向に平行になるように、かつ押圧して供給し、ストランド状に切断することが好ましい。ストランドの形状は、ラッパーへの充填のし易さ等の観点から、幅0.6~1.5mm程度とすることができる。裁刻後のストランドの長さは裁刻工程に供給される枚葉形状の再構成たばこシートのサイズ、および、各工程における枚葉形状の再構成たばこシートの破砕状態や裁刻中、裁刻後のストランドの破砕状態によって決定されるが、ラッパーへの充填のしやすさから、約5~40mm程度とすることが好ましい。再構成たばこシートの裁刻機への供給は、メタリングチューブを用いて行うことが好ましい。本工程では、裁断を効率よく行うために、裁刻工程に供給する再構成たばこシートの水分量を15~25重量%に調整してもよい。
4) Stamping In this process, the scented reconstituted tobacco sheet is stamped. The cutting can be performed using a known device, but in the present invention, the reconstructed tobacco sheet is supplied by pressing and supplying the reconstructed tobacco sheet so that its end is parallel to the extending direction of the blade of the knife drum, and the strand is It is preferable to cut it into a shape. The shape of the strand can be about 0.6 to 1.5 mm in width from the viewpoint of ease of filling the wrapper. The length of the strand after cutting is the size of the sheet-fed reconstructed tobacco sheet supplied to the cutting process, and the crushed state of the sheet-fed reconstructed tobacco sheet in each process, during cutting, and cutting. Although it is determined by the crushed state of the subsequent strand, it is preferably about 5 to 40 mm from the viewpoint of ease of filling in the wrapper. It is preferable to supply the reconstructed tobacco sheet to the cutting machine using a metering tube. In this step, in order to efficiently perform cutting, the water content of the reconstructed tobacco sheet supplied to the cutting step may be adjusted to 15 to 25% by weight.
 5)乾燥
 本工程では、ストランド形状の再構成たばこシートを乾燥する。乾燥に用いる装置および乾燥条件は前述のとおりである。この際、再構成たばこシートの水分量は8~12重量%に調製される。また、この工程で、ストランド形状の再構成たばこシートの膨嵩性が向上する。
5) Drying In this step, the strand-shaped reconstructed tobacco sheet is dried. The equipment and drying conditions used for drying are as described above. At this time, the water content of the reconstituted tobacco sheet is adjusted to 8 to 12% by weight. Further, in this step, the bulkiness of the strand-shaped reconstructed tobacco sheet is improved.
 6)非たばこ材料の混合
 本工程では、ストランド形状の再構成たばこシートに、充填剤や香料が担持された固体添加剤を添加する。充填剤としては、ストランド形状の紙や、ストランド形状の炭酸カルシウムシート等や、顆粒状の多孔性多糖類ビーズ等が挙げられる。混合性を高める観点から、添加される材料は前記ストランドと近い形状を有することが好ましい。例えば香料が担持された固体添加剤として香料担持多糖類シートを添加すると、非燃焼加熱型香味吸引物品の使用時の味香りを増強できるといった利点がある。たばこ充填材と混合する香料担持シートは、特許5941988、特許第5934799、特許第5514953、および特許第5481574に開示されている、増粘多糖類を基材としたものが保管時の保香性能と使用時の香料リリース性能のバランスの面で好ましい。香料担持多糖類シートの形状は幅0.5~1.5mm、長さ2~4mm、厚さ70μm程度とすることができる。混合の方法は限定されず、ストランド形状の再構成たばこシートが搬送されているコンベアに、裁刻された香料担持多糖類シートが搬送されているコンベアを合流させて両者を混合する方法や、両者をシリンダ型の混合器に導入して混合する方法等が挙げられる。
6) Mixing of non-tobacco materials In this step, a solid additive carrying a filler or a fragrance is added to the strand-shaped reconstructed tobacco sheet. Examples of the filler include strand-shaped paper, strand-shaped calcium carbonate sheet, granular porous polysaccharide beads, and the like. From the viewpoint of enhancing the mixing property, it is preferable that the material to be added has a shape close to that of the strand. For example, adding a perfume-carrying polysaccharide sheet as a solid additive carrying a perfume has an advantage that the taste and aroma at the time of use of a non-combustion heating type flavor suction article can be enhanced. The perfume-supporting sheet to be mixed with the tobacco filler is based on the thickening polysaccharide disclosed in Japanese Patents 5941988, 5934799, 5514953, and 541574. It is preferable in terms of the balance of fragrance release performance during use. The shape of the fragrance-supporting polysaccharide sheet can be 0.5 to 1.5 mm in width, 2 to 4 mm in length, and about 70 μm in thickness. The mixing method is not limited, and a method of merging a conveyor carrying a strand-shaped reconstructed tobacco sheet with a conveyor carrying an engraved fragrance-supporting polysaccharide sheet and mixing the two, or both. Is introduced into a cylinder type mixer and mixed.
 7)加香
 乾燥後のストランド形状の再構成たばこシートに再度、加香を施してもよい。加香の方法および用いる成分については前述のとおりである。この段階での加香は、分子量が比較的小さい香味成分を添加する場合に好適である。本工程以降はたばこ充填物を乾燥することなく香味吸引物品に加工できるため、本工程においては比較的揮発しやすい香りを発現する香味成分を添加することで最終製品に強い香り特徴を付与することができる。
7) Incense Incense may be applied again to the reconstructed tobacco sheet having a strand shape after drying. The method of incense and the components used are as described above. The aroma at this stage is suitable for adding a flavor component having a relatively small molecular weight. After this step, the tobacco filling can be processed into a flavor-sucking article without drying. Therefore, in this step, a strong scent characteristic should be given to the final product by adding a flavor component that expresses a relatively volatile scent. Can be done.
 8)1次貯蔵
 このようにして得たストランドを貯蔵する。貯蔵されたたばこ充填物(ストランド)は工程2に供される。
8) Primary storage The strands thus obtained are stored. The stored tobacco filler (strand) is subjected to step 2.
(4-2)第2の実施形態
 図2は、第2の実施形態を示す。本実施形態では2つのラインを用いる。一方のラインにおいて、第1の実施形態の1)~3)を実施して再構成たばこシートAを調製する。同様に、他方のラインにおいて、第1の実施形態の1)~3)を実施して再構成たばこシートBを調製する。この際、再構成たばこシートAとBは、異なる成分で構成されていることが好ましい。また、加香は、再構成たばこシートAとBの双方に対して実施されてもよいし、一方に対して実施されてもよいし、双方に実施されなくてもよい。
(4-2) Second Embodiment FIG. 2 shows a second embodiment. In this embodiment, two lines are used. In one line, the reconstructed tobacco sheet A is prepared by carrying out 1) to 3) of the first embodiment. Similarly, in the other line, 1) to 3) of the first embodiment are carried out to prepare the reconstructed tobacco sheet B. At this time, it is preferable that the reconstituted tobacco sheets A and B are composed of different components. Further, the incense may be applied to both the reconstituted tobacco sheets A and B, may be applied to one of them, or may not be applied to both of them.
 次いで、再構成たばこシートAとBを混合する。混合比率は所望の香味を達成できるように適宜調製される。この時点で両者を混合することで、混合効率を高めることができ、さらに混合したものを裁刻および乾燥等の工程に供することができるので製品をより均一にすることができる。 Next, the reconstituted tobacco sheets A and B are mixed. The mixing ratio is appropriately adjusted so that the desired flavor can be achieved. By mixing the two at this point, the mixing efficiency can be improved, and the mixed product can be subjected to processes such as cutting and drying, so that the product can be made more uniform.
 続いて、再構成たばこシートAとBの混合物を、裁刻、乾燥、非たばこ材料との混合、加香工程に供し、得たものを1次貯蔵する。これらの工程は、第1の実施形態4)~8)で説明したとおりである。 Subsequently, the mixture of the reconstituted tobacco sheets A and B is subjected to a cutting, drying, mixing with a non-tobacco material, and aromatling process, and the obtained product is first stored. These steps are as described in the first embodiments 4) to 8).
 この態様は、香味の特徴が異なる銘柄を製造する際に好適である。例えば、これらの銘柄に共通するベース材料を再構成たばこシートAとするとき、銘柄切替えの際にサブ原料である再構成たばこシートBを適宜用いれば、効率よく別の銘柄を製造できる。また、再構成たばこシートAの製造中に当該シートAを分析して不足している成分があれば、これを補うように設計された再構成たばこシートBを混合することで、品質が安定した再構成たばこシートの混合品を製造することもできる。 This aspect is suitable for manufacturing brands with different flavor characteristics. For example, when the base material common to these brands is the reconstructed tobacco sheet A, another brand can be efficiently manufactured by appropriately using the reconstructed tobacco sheet B which is a sub-raw material at the time of brand switching. In addition, if there is a missing component in the analysis of the reconstituted tobacco sheet A during the production of the reconstructed tobacco sheet A, the quality is stabilized by mixing the reconstructed tobacco sheet B designed to supplement the component. Mixtures of reconstituted tobacco sheets can also be produced.
 再構成たばこの材料となるたばこの種類についてはニコチアナタバカムの中の黄色種、バーレー種、オリエント種、または在来種が挙げられ、これらは単独あるいは混合して使用することができる。通常、これらのブレンド比率を変えて目的とする味香りを達成する。シートAとシートBとを配合する設計思想としては、例えば、まず構成するたばこ種類として黄色種とオリエント種の割合を多くした(両者の合計量が全たばこの量の好ましくは、50重量%超、より好ましくは80重量%以上である)シートAを準備し、構成するたばこ種類としてバーレー種または在来種の割合を多くした(両者の合計量が全たばこの量の好ましくは30重量%超、より好ましくは80重量%以上である)シートBを準備する。目的とする味香に応じて、シートAとシートBとの配合割合を決定することで、準備するシート種類は2種類でありながら、多数のバリエーションを有する香味吸引物品を製造することができる。 Examples of the types of tobacco used as the material for reconstituted tobacco include yellow species, Burley species, Orient species, and native species in Nicotiana rustica, which can be used alone or in combination. Usually, these blend ratios are changed to achieve the desired taste and aroma. As a design concept for blending sheet A and sheet B, for example, the ratio of yellow type and orient type is increased as the constituent tobacco types (the total amount of both is preferably more than 50% by weight of the total amount of tobacco). Sheet A was prepared (more preferably 80% by weight or more), and the proportion of Burley or native species was increased as the constituent tobacco types (the total amount of both is preferably more than 30% by weight of the total amount of tobacco). , More preferably 80% by weight or more) Prepare the sheet B. By determining the blending ratio of the sheet A and the sheet B according to the desired taste and aroma, it is possible to produce a flavor suction article having a large number of variations while preparing two types of sheets.
 また、種類によって発現する香味が変わる前記4種類のたばこの他に、少量でも強い味香り特徴を有する種類のたばこが存在する。このようなたばことして、ペリック、ラタキア、ダークファイアーキュアードと呼ばれるたばこが挙げられる。これらの品種は前述の黄色種、バーレー種、オリエント種、または在来種と同じであるが、葉たばこ農家で収穫後に、燻製処理や強制的な高温高水分下での発酵処理が施される。ペリックやダークファイアーキュアード等の発酵処理がなされたたばこ、あるいはラタキヤ等の燻製処理がなされたたばこの様に、特別な処理を施されたたばこは少々ブレンドされることで特異的な香味特徴を発現する。シートBとしてペリックやラタキアやダークファイアーキュアード等が配合された再構成たばこシートを用いると、銘柄特徴のバリエーションを拡大することができる。ペリック、ラタキアおよびダークファイアーキュアードの合計の配合量は、全たばこの量の好ましくは1.0重量%以上10.0重量%未満、より好ましくは1.0重量%以上5.0重量%未満である。 In addition to the above-mentioned four types of tobacco whose flavor changes depending on the type, there are types of tobacco having strong taste and aroma characteristics even in a small amount. Examples of such cigarettes include cigarettes called Peric, Latakia, and Dark Fire Cured. These varieties are the same as the yellow, Burley, Orient, or Native varieties described above, but are smoked or fermented under forced high temperature and high moisture after harvesting at leaf tobacco farmers. Specially treated tobacco, such as fermented tobacco such as pellic and dark fire cure, or smoked tobacco such as latakia, is slightly blended to give it a unique flavor characteristic. Express. When a reconstructed tobacco sheet containing pellic, latakia, dark fire cure, etc. is used as the sheet B, the variation of brand characteristics can be expanded. The total blending amount of peric, latakia and dark fire cure is preferably 1.0% by weight or more and less than 10.0% by weight, more preferably 1.0% by weight or more and less than 5.0% by weight of the total amount of tobacco. Is.
(4-3)第3の実施形態
 図3は、第3の実施形態を示す。本実施形態では2つのラインを用いる。一方のラインにおいて、第1の実施形態の1)~5)を実施してストランド状の再構成たばこシートAを調製する。同様に、他方のラインにおいて、第1の実施形態の1)~5)を実施してストランド状の再構成たばこシートBを調製する。この際、再構成たばこシートAとBは、異なる成分で構成されていることが好ましい。また、加香は、再構成たばこシートAとBの双方に対して実施されてもよいし、一方に対して実施されてもよい。
(4-3) Third Embodiment FIG. 3 shows a third embodiment. In this embodiment, two lines are used. In one line, 1) to 5) of the first embodiment are carried out to prepare a strand-shaped reconstructed tobacco sheet A. Similarly, in the other line, 1) to 5) of the first embodiment are carried out to prepare a strand-shaped reconstituted tobacco sheet B. At this time, it is preferable that the reconstituted tobacco sheets A and B are composed of different components. Further, the incense may be applied to both the reconstituted tobacco sheets A and B, or may be applied to one of them.
 次いで、ストランド状の再構成たばこシートAとBを混合する。混合比率は所望の香味を達成できるように適宜調製される。 Next, the strand-shaped reconstituted tobacco sheets A and B are mixed. The mixing ratio is appropriately adjusted so that the desired flavor can be achieved.
 続いて、前記混合物を、非たばこ材料との混合、加香工程に供し、得たものを1次貯蔵する。これらの工程は、第1の実施形態6)および7)で説明したとおりである。 Subsequently, the mixture is subjected to a mixing and incense step with a non-tobacco material, and the obtained product is first stored. These steps are as described in the first embodiments 6) and 7).
 この態様は、第2の態様と同様に香味の特徴が異なる銘柄を製造する際に好適である。例えば、これらの銘柄に共通するベース材料を再構成たばこシートAとするとき、銘柄切替えの際にサブ原料である再構成たばこシートBを適宜用いれば、効率よく別の銘柄を製造できる。また、再構成たばこシートAの製造中に当該シートAを分析して不足している成分があれば、これを補うように設計された再構成たばこシートBを混合することで、品質が安定した再構成たばこシートAを製造することもできる。さらに、本態様では再構成たばこシートAとBとを、それぞれ裁刻および乾燥に供するので、個々の特性に合わせた条件設定が可能である。例えば、再構成たばこシートAに添加された香料と、再構成たばこシートBに添加された香料が異なる場合、香料によって最適乾燥条件も異なるが、本態様では香料に適した条件を選択できるという利点がある。 This aspect is suitable for producing a brand having different flavor characteristics as in the second aspect. For example, when the base material common to these brands is the reconstructed tobacco sheet A, another brand can be efficiently manufactured by appropriately using the reconstructed tobacco sheet B which is a sub-raw material at the time of brand switching. In addition, if there is a missing component in the analysis of the reconstituted tobacco sheet A during the production of the reconstructed tobacco sheet A, the quality is stabilized by mixing the reconstructed tobacco sheet B designed to supplement the component. The reconstituted tobacco sheet A can also be manufactured. Further, in this embodiment, the reconstructed tobacco sheets A and B are subjected to cutting and drying, respectively, so that the conditions can be set according to the individual characteristics. For example, when the fragrance added to the reconstituted tobacco sheet A and the fragrance added to the reconstructed tobacco sheet B are different, the optimum drying conditions differ depending on the fragrance, but in this embodiment, there is an advantage that conditions suitable for the fragrance can be selected. There is.
(4-4)第4の実施形態
 図4は、第4の実施形態を示す。本実施形態では2つのラインを用いる。一方のラインにおいて、第1の実施形態の1)~3)を実施して再構成たばこシートAを加工する。同様に、他方のラインにおいて、ラミナを加工する。ラミナとはタバコ葉から中骨を除去して得られる除骨葉である。図4には2種類のラミナを使用する形態を示したが、ラミナは1種類以上を用いることができる。この際、ラミナAとBは、異なる成分で構成されていることが好ましい。ラミナの加香工程までは、第1の実施形態の1)~3)と同様にして実施できる。
(4-4) Fourth Embodiment FIG. 4 shows a fourth embodiment. In this embodiment, two lines are used. In one line, the reconstructed tobacco sheet A is processed by carrying out 1) to 3) of the first embodiment. Similarly, in the other line, lamina is processed. Lamina is a deboned leaf obtained by removing the middle bone from tobacco leaves. FIG. 4 shows a form in which two types of laminas are used, but one or more types of laminas can be used. At this time, it is preferable that Lamina A and B are composed of different components. The steps up to the scenting step of lamina can be carried out in the same manner as in 1) to 3) of the first embodiment.
 次いでラミナAとBを混合して、さらに混合物を加湿する。加湿は第1の実施形態の2)と同様にして実施できる。この加湿された混合物を加香された再構成たばこシートAとさらに混合し、続いてこれを裁刻、乾燥、非たばこ材料との混合、加香工程に供し、得たものを1次貯蔵する。これらの工程は、第1の実施形態4)~8)で説明したとおりである。また、加香は、再構成たばこシートA、ラミナA、ラミナBの1以上に対してして実施されてもよいし、すべてに対して実施されてもよい。 Next, Lamina A and B are mixed, and the mixture is further humidified. Humidification can be carried out in the same manner as in 2) of the first embodiment. The humidified mixture is further mixed with the aromatized reconstituted tobacco sheet A, which is then subjected to a cutting, drying, mixing with non-tobacco material and aromatizing steps, and the obtained product is first stored. .. These steps are as described in the first embodiments 4) to 8). Further, the incense may be applied to one or more of the reconstituted tobacco sheets A, Lamina A, and Lamina B, or may be applied to all of them.
 本態様は、第2の態様で説明した効果が得られる。さらに、たばこシートよりも膨嵩性が高いラミナを混合すれば、たばこシートのみでたばこロッド部を形成する場合に比べて同じ巻き硬さを達成するための充填量を低減させることもできる。 In this aspect, the effect described in the second aspect can be obtained. Further, if a lamina having a higher swelling property than that of the tobacco sheet is mixed, the filling amount for achieving the same winding hardness can be reduced as compared with the case where the tobacco rod portion is formed only by the tobacco sheet.
(4-5)第5の実施形態
 図5は、第5の実施形態を示す。本実施形態では2つのラインを用いる。一方のラインにおいて、第1の実施形態の1)~5)を実施してストランド状の再構成たばこシートAを調製する。同様に、他方のラインにおいて、第1の実施形態の1)~3)と同様にしてラミナAとBの混合物を調製し、さらにこれを、第1の実施形態の2)、3)、5)と同様にして加湿、裁刻、乾燥に供する。
(4-5) Fifth Embodiment FIG. 5 shows a fifth embodiment. In this embodiment, two lines are used. In one line, 1) to 5) of the first embodiment are carried out to prepare a strand-shaped reconstructed tobacco sheet A. Similarly, in the other line, a mixture of lamina A and B is prepared in the same manner as in 1) to 3) of the first embodiment, and this is further applied to 2), 3), 5 of the first embodiment. ), Humidify, cut and dry.
 次いで、ストランド状の再構成たばこシートAとストランド状のラミナ混合物とを、混合する。混合比率は所望の香味を達成できるように適宜調製される。 Next, the strand-shaped reconstituted tobacco sheet A and the strand-shaped lamina mixture are mixed. The mixing ratio is appropriately adjusted so that the desired flavor can be achieved.
 続いて、前記混合物を、非たばこ材料との混合、加香工程に供し、得たものを1次貯蔵する。これらの工程は、第1の実施形態6)および7)で説明したとおりである。また、加香は、再構成たばこシートA、ラミナA、ラミナBの1以上に対してして実施されてもよいし、すべてに対して実施されてもよい。 Subsequently, the mixture is subjected to a mixing and incense step with a non-tobacco material, and the obtained product is first stored. These steps are as described in the first embodiments 6) and 7). Further, the incense may be applied to one or more of the reconstituted tobacco sheets A, Lamina A, and Lamina B, or may be applied to all of them.
 本態様は、第3の態様で説明した効果が得られる。さらに、第4の態様で説明したとおり、充填量を低減させることもできる。 In this aspect, the effect described in the third aspect can be obtained. Further, as described in the fourth aspect, the filling amount can be reduced.
(5)他の工程
 本発明の製造方法は、前記たばこ充填物の成分を測定し、測定結果を基に前記添加剤の添加量を調整する工程をさらに備えていてもよい。この際、測定結果を制御機へ伝え、制御機から添加剤の添加装置に情報が伝わるようにすることが好ましい。特に、たばこ充填物の亜硝酸塩を測定し、これに基づいて抗酸化剤の添加量を決定することが好ましい。抗酸化剤の添加量が過剰であるとコストアップまたは香味を損なうこととなるので、適量を決定することでこのような不具合を生じさせることなくユーザーにやさしい製品を提供できる。
(5) Other Steps The production method of the present invention may further include a step of measuring the components of the tobacco filling and adjusting the addition amount of the additive based on the measurement result. At this time, it is preferable to convey the measurement result to the controller so that the information can be transmitted from the controller to the additive addition device. In particular, it is preferable to measure the nitrite of the tobacco filling and determine the amount of the antioxidant added based on this. If the amount of the antioxidant added is excessive, the cost will increase or the flavor will be impaired. Therefore, by determining the appropriate amount, it is possible to provide a user-friendly product without causing such a problem.
(6)再構成たばこシートの調製
 以下に、再構成たばこシートの調製にかかる好ましい態様を説明する。
(6-1)抄造法
 タバコ植物材料としては、ニコチアナタバカムの中の黄色種、バーレー種、オリエント種、または在来種を単独あるいは混合して使用することができる。植物の部位は花、葉、葉脈、茎、または根のいずれか一種または組合せであってよい。
(6) Preparation of Reconstructed Tobacco Sheet The following describes a preferred embodiment for preparing the reconstructed tobacco sheet.
(6-1) Papermaking method As the tobacco plant material, yellow species, Burley species, Orient species, or native species in Nicotiana tabacum can be used alone or in combination. The plant site may be any one or combination of flowers, leaves, veins, stems, or roots.
 タバコ植物材料を1~40mm以下程度の大きさに粗粉砕して、水での抽出に供する。抽出温度は好ましくは30~90℃であり、抽出時間は好ましくは10~45分である。 Tobacco plant material is roughly crushed to a size of about 1 to 40 mm or less and used for extraction with water. The extraction temperature is preferably 30 to 90 ° C., and the extraction time is preferably 10 to 45 minutes.
 次いで、抽出工程を経た混合物を、遠心分離によるまたは金網メッシュを用いた分離操作に供し、抽出液と残渣に分離する。抽出液を40~70℃の温度条件下で減圧濃縮し、水に対する抽出物の割合が40~55重量%となるようにする。当該濃縮液に、グリセリン等のエアロゾル生成基材を混合する。残渣と粗粉砕された木材パルプと混合した後に調成機(refiner)で処理して繊維を毛羽立たせ、さらに粉砕して大きさを均一にする。残渣と木材パルプとの混合物を大量の水中に懸濁し、紙製造プロセスで用いられるメッシュワイヤー上に定量で供給し、脱水および乾燥して、シートを得る。当該シートに前記濃縮液をスプレー噴霧する。スプレー噴霧後に再度乾燥を行なう。最終的にシートはボビン巻き上げされてもよく、シュレッダーで処理して3~10cm角に裁断されて容器に収納されてもよい。 Next, the mixture that has undergone the extraction step is subjected to a separation operation by centrifugation or using a wire mesh, and is separated into an extract and a residue. The extract is concentrated under reduced pressure under a temperature condition of 40 to 70 ° C. so that the ratio of the extract to water is 40 to 55% by weight. An aerosol-forming substrate such as glycerin is mixed with the concentrated solution. After mixing the residue with the coarsely ground wood pulp, it is treated with a refiner to make the fibers fluffy, and then further ground to make the size uniform. A mixture of the residue and wood pulp is suspended in a large amount of water, supplied in a fixed amount on a mesh wire used in a paper manufacturing process, dehydrated and dried to obtain a sheet. The concentrate is sprayed onto the sheet. After spraying, dry again. Finally, the sheet may be bobbin-wound, or may be shredded, cut into 3 to 10 cm squares, and stored in a container.
 以下に、抄造法による再構成たばこシートの原料構成、成分、および、物性の一例を示す。
(原料構成)
 黄色ラミナ/スクラップ(葉肉) 50~70重量%
 バーレーラミナ 0~50重量%
 黄色中骨(葉脈)  0~50重量%
 バーレー中骨 0~35重量%
 木材パルプ 7~12重量%
 グリセリン 10~20重量%
 水分 7~12重量%
(成分)
 ニコチン 0.8~3.0重量%(ドライベース)
 還元糖 5.0~20.0重量%(ドライベース)
(物性)
 単純0.8mm幅裁刻後の膨嵩性   250~400cm/100g
 加水し、0.8mm幅に裁刻し、気流乾燥した後の膨嵩性  300~450cm/100g
The following is an example of the raw material composition, components, and physical properties of the reconstructed tobacco sheet by the papermaking method.
(Raw material composition)
Yellow lamina / scrap (meat) 50-70% by weight
Burley Lamina 0-50% by weight
Yellow middle bone (leaf vein) 0-50% by weight
Burley middle bone 0-35% by weight
Wood pulp 7-12% by weight
Glycerin 10-20% by weight
Moisture 7-12% by weight
(component)
Nicotine 0.8-3.0% by weight (dry base)
Reducing sugar 5.0-20.0% by weight (dry base)
(Physical characteristics)
Simple 0.8mm width Bulkiness after cutting 250-400cm 3 / 100g
Swellability after watering, chopping to 0.8 mm width, and air-drying 300-450 cm 3/100 g
(6-2)キャスト法
 タバコ植物材料としては、ニコチアナタバカムの中の黄色、バーレー種、オリエント種、または在来種を単独あるいは混合して使用することができる。植物の部位は花、葉、葉脈、茎、または根のいずれか一種または組合せであってよい。
(6-2) Casting method As the tobacco plant material, yellow, Burley, Orient, or native species in Nicotiana tabacum can be used alone or in combination. The plant site may be any one or combination of flowers, leaves, veins, stems, or roots.
 タバコ植物材料を100μm以下の大きさに粉砕し、水、パルプ、グリセリン等のエアロゾル生成基材、ガム類、修飾セルロース、増粘多糖類、および修飾でんぷん等のバインダー、および香料類と混合してスラリーを調製する。スラリーの水分割合は50体積%以上であることが好ましい。その後、スラリーを基材上に薄くシート状に展開し、乾燥機で7~14重量%程度の水分値になるまで乾燥する。最終的にシートはボビン巻き上げされてもよく、シュレッダーで処理して3~10cm角に裁断されて容器に収納されてもよい。 Tobacco plant material is crushed to a size of 100 μm or less and mixed with aerosol-forming base materials such as water, pulp and glycerin, gums, modified celluloses, thickening polysaccharides, binders such as modified starch, and fragrances. Prepare the slurry. The water content of the slurry is preferably 50% by volume or more. Then, the slurry is developed into a thin sheet on the substrate and dried in a dryer until the water content reaches about 7-14% by weight. Finally, the sheet may be bobbin-wound, or may be shredded, cut into 3 to 10 cm squares, and stored in a container.
 以下に、キャスト法による再構成たばこシートの原料構成、および、成分の一例を示す。
(原料構成)
 黄色ラミナ(葉肉) 60~95重量%
 バーレーラミナ 0~20重量%
 黄色中骨(葉脈)  0~20重量%
 バーレー中骨 0重量%
 木材パルプ 3~5重量%
 グリセリン 10~20重量%
 グアガム 2~10重量%
 水分 7~14%
 (成分)
 ニコチン 1.5~5.0重量%(ドライベース)
 還元糖 5~20重量%(ドライベース)
The raw material composition of the reconstructed tobacco sheet by the casting method and an example of the components are shown below.
(Raw material composition)
Yellow lamina (meat) 60-95% by weight
Burley Lamina 0-20% by weight
Yellow middle bone (leaf vein) 0 to 20% by weight
Burley middle bone 0% by weight
Wood pulp 3-5% by weight
Glycerin 10-20% by weight
Guar gum 2-10% by weight
Moisture 7-14%
(component)
Nicotine 1.5-5.0% by weight (dry base)
Reducing sugar 5-20% by weight (dry base)
(6-3)押出法
 タバコ植物材料を300μm以下の大きさに粉砕し、水、パルプ、グリセリン等のエアロゾル生成基材、ガム類、修飾セルロース、増粘多糖類、および修飾でんぷん等のバインダー、および香料類と混合して混錬り物を調製する。その後、出口部に所定厚さ所定幅の開孔を有するダイを配置した押出機内に混錬り物を入れて、押出機からシート状の混錬り物を乾燥ドラムもしくは乾燥コンベア上等の乾燥部に押し出す。乾燥部で7~14重量%程度の水分値になるまで乾燥する。最終的にシートはボビン巻き上げされてもよく、シュレッダーで処理して3~10cm角に裁断されて容器に収納されてもよい。
(6-3) Extrusion method Aerosol-producing base materials such as water, pulp and glycerin, gums, modified cellulose, thickening polysaccharides, and binders such as modified starch are obtained by crushing tobacco plant material to a size of 300 μm or less. And mix with fragrances to prepare the kneaded product. After that, the kneaded product is placed in an extruder having a die having a predetermined thickness and a predetermined width at the outlet, and the sheet-shaped kneaded product is dried from the extruder on a drying drum or a drying conveyor. Push it out to the part. Dry in the dry part until the moisture value reaches about 7 to 14% by weight. Finally, the sheet may be bobbin-wound, or may be shredded, cut into 3 to 10 cm squares, and stored in a container.
 以下に、押出法による再構成たばこシートの原料構成および成分の一例を示す。
(原料構成)
 黄色ラミナ(葉肉) 60~95重量%
 バーレーラミナ 0~20重量%
 黄色中骨(葉脈)  0~20重量%
 バーレー中骨 0重量%
 木材パルプ 3~5重量%
 グリセリン 10~20重量%
 ヒドロキシプロピルセルロース 2~10重量%
 水分 7~14%
(成分)
 ニコチン 1.5~5.0重量%(ドライベース)
 還元糖 5~20重量%(ドライベース)
The following is an example of the raw material composition and components of the reconstituted tobacco sheet by the extrusion method.
(Raw material composition)
Yellow lamina (meat) 60-95% by weight
Burley Lamina 0-20% by weight
Yellow middle bone (leaf vein) 0 to 20% by weight
Burley middle bone 0% by weight
Wood pulp 3-5% by weight
Glycerin 10-20% by weight
Hydroxypropyl cellulose 2-10% by weight
Moisture 7-14%
(component)
Nicotine 1.5-5.0% by weight (dry base)
Reducing sugar 5-20% by weight (dry base)
2.工程2
 本工程は、工程1で得たたばこ充填物が筒状ラッパー内に充填されたたばこロッド部を調製する。例えば、ラッパーとして紙を準備し、たばこ充填物を当該紙で巻装することでたばこロッド部を製造できる。あるいは、筒状のラッパーを準備し、その内部にたばこ充填物を充填することによってもたばこロッド部を製造できる。筒状ラッパーの断面形状は限定されず、円、楕円、または多角形とすることができる。
2. 2. Step 2
In this step, a tobacco rod portion in which the tobacco filler obtained in step 1 is filled in a tubular wrapper is prepared. For example, a tobacco rod portion can be manufactured by preparing paper as a wrapper and wrapping the tobacco filler with the paper. Alternatively, the tobacco rod portion can be manufactured by preparing a tubular wrapper and filling the inside thereof with a tobacco filler. The cross-sectional shape of the tubular wrapper is not limited and can be circular, elliptical, or polygonal.
3.特性
 本発明の製造方法で得られるたばこ充填物は特に優れた膨嵩性を有する。膨嵩性とは、たばこ充填物(好ましくは刻)のかたまりを一定の力で圧縮したときの単位重量当たりの体積であり、嵩密度の指標でもある。具体的には、試料を投入した直径95mmの測定シリンダ内に11.4kgの負荷を5秒間かけた後に求められるたばこ刻円柱の高さから下記式で計算される。
   FP=(A×h5)/W [cm/100g]
FP :膨嵩性
A  :たばこ刻円柱の断面積
W  :たばこ刻の重量
h5 :負荷終了時のたばこ刻円柱の高さ
3. 3. Characteristics The tobacco filling obtained by the production method of the present invention has particularly excellent swelling property. The swelling property is a volume per unit weight when a mass of tobacco filling (preferably chopped) is compressed with a constant force, and is also an index of bulk density. Specifically, it is calculated by the following formula from the height of the tobacco carved cylinder obtained after applying a load of 11.4 kg in a measuring cylinder having a diameter of 95 mm in which the sample is placed for 5 seconds.
FP = (A × h5) / W [cm 3 / 100g]
FP: Bulkiness A: Cross-sectional area of the tobacco carved cylinder W: Weight of the tobacco carved h5: Height of the tobacco carved cylinder at the end of the load
 香味吸引物品(または喫煙物品)のたばこロッド部は主に円柱状の紙製のラッパーでたばこ充填物を巻装して製造される。一般的にたばこロッド部はある程度硬い方がユーザーに好まれる傾向がある。たばこロッド部を硬くするにはたばこ充填物の充填量を増やすことが考えられるが、充填量の増大はコストアップを引き起こす。しかし、膨嵩性が大きいたばこ充填物は、より少ない充填量で必要な硬さを有するたばこロッド部を提供できる。 The tobacco rod part of the flavor suction article (or smoking article) is mainly manufactured by wrapping the tobacco filling with a columnar paper wrapper. Generally, the tobacco rod part tends to be preferred by users if it is hard to some extent. To make the tobacco rod part harder, it is conceivable to increase the filling amount of the tobacco filling, but increasing the filling amount causes an increase in cost. However, a highly bulging tobacco filler can provide a tobacco rod portion with the required hardness with a smaller filling amount.
3.非燃焼加熱型香味吸引物品
 喫煙物品としては、ユーザーが吸引により香味を味わう香味吸引物品や、ユーザーが鼻腔や口腔に直接製品を含んで香味を味わう無煙たばこ(無煙喫煙物品)が挙げられる。香味吸引物品は、従来のシガレットを代表とする燃焼型喫煙物品と非燃焼型喫煙物品とに大別できる。本発明のたばこロッド部は、非燃焼型喫煙物品のうち、加熱して使用される非燃焼加熱型香味吸引物品に用いられる。
3. 3. Non-combustion heating type flavor suction article Smoking articles include flavor suction articles in which the user tastes the flavor by suction, and smokeless tobacco (smokeless smoking article) in which the user tastes the flavor by directly including the product in the nasal cavity and oral cavity. The flavor suction article can be roughly classified into a combustion type smoking article typified by a conventional cigarette and a non-combustion type smoking article. The tobacco rod portion of the present invention is used for non-combustion heating type flavor suction articles used by heating among non-combustion type smoking articles.
 非燃焼加熱型香味吸引物品は、当該物品と別体型の加熱装置により加熱されてもよいし、当該物品と一体型の加熱装置により加熱されてもよい。前者の香味吸引物品(別体型)において、非燃焼加熱型香味吸引物品と加熱装置とをまとめて、「非燃焼加熱型喫煙システム」とも称する。以下に非燃焼加熱型喫煙システムの一例を、図6および図7を参照して説明する。 The non-combustion heating type flavor suction article may be heated by a heating device separate from the article, or may be heated by a heating device integrated with the article. In the former flavor suction article (separate type), the non-combustion heating type flavor suction article and the heating device are collectively referred to as a "non-combustion heating type smoking system". An example of a non-combustion heating type smoking system will be described below with reference to FIGS. 6 and 7.
 図6は、非燃焼加熱型喫煙システムの一例を示す断面模式図であり、非燃焼加熱型香味吸引物品20のたばこロッド部20A内に、ヒータ12を挿入する前の状態を示す。使用時には、たばこロッド部20A内に、ヒータ12が挿入される。図7は、非燃焼加熱型香味吸引物品20の断面図である。 FIG. 6 is a schematic cross-sectional view showing an example of a non-combustion heating type smoking system, and shows a state before inserting the heater 12 into the tobacco rod portion 20A of the non-combustion heating type flavor suction article 20. At the time of use, the heater 12 is inserted into the tobacco rod portion 20A. FIG. 7 is a cross-sectional view of the non-combustion heating type flavor suction article 20.
 図6に示すとおり、非燃焼加熱型喫煙システムは、非燃焼加熱型香味吸引物品20と、たばこロッド部20Aを内側から加熱する加熱装置10とを備える。ただし非燃焼加熱型喫煙システムは、図6の構成に限定されない。 As shown in FIG. 6, the non-combustion heating type smoking system includes a non-combustion heating type flavor suction article 20 and a heating device 10 for heating the tobacco rod portion 20A from the inside. However, the non-combustion heating type smoking system is not limited to the configuration shown in FIG.
 図6に示される加熱装置10は、ボディ11と、ヒータ12とを備える。図示していないが、ボディ11は電池ユニットと制御ユニットを備えていてもよい。ヒータ12は電気抵抗によるヒータであることができ、たばこロッド部20A内に挿入されて、たばこロッド部20Aを加熱する。 The heating device 10 shown in FIG. 6 includes a body 11 and a heater 12. Although not shown, the body 11 may include a battery unit and a control unit. The heater 12 can be a heater due to electric resistance, and is inserted into the tobacco rod portion 20A to heat the tobacco rod portion 20A.
 図には、たばこロッド部20Aが内側から加熱される態様を示す。しかしながら、非燃焼加熱型香味吸引物品20の態様はこれに限定されず、別態様においてたばこロッド部20Aは外側から加熱される。 The figure shows a mode in which the tobacco rod portion 20A is heated from the inside. However, the aspect of the non-combustion heating type flavor suction article 20 is not limited to this, and in another aspect, the tobacco rod portion 20A is heated from the outside.
 加熱装置10による加熱温度は特に限定されないが、400℃以下であることが好ましく、50~400℃であることがより好ましく、150~350℃であることがさらに好ましい。加熱温度とは加熱装置10のヒータ12の温度を指す。 The heating temperature by the heating device 10 is not particularly limited, but is preferably 400 ° C. or lower, more preferably 50 to 400 ° C., and even more preferably 150 to 350 ° C. The heating temperature refers to the temperature of the heater 12 of the heating device 10.
 図7に示すとおり、非燃焼加熱型香味吸引物品20(以下、単に「香味吸引物品20」と称する)は、円柱形状を有する。香味吸引物品20の円周の長さは、16mm~27mmであることが好ましく、20mm~26mmであることがより好ましく、21mm~25mmであることがさらに好ましい。香味吸引物品20の全長(水平方向の長さ)は特に限定されないが、40mm~90mmであることが好ましく、50mm~75mmであることがより好ましく、50mm~60mmであることがさらに好ましい。 As shown in FIG. 7, the non-combustion heating type flavor suction article 20 (hereinafter, simply referred to as “flavor suction article 20”) has a cylindrical shape. The circumference of the flavor suction article 20 is preferably 16 mm to 27 mm, more preferably 20 mm to 26 mm, and even more preferably 21 mm to 25 mm. The total length (horizontal length) of the flavor suction article 20 is not particularly limited, but is preferably 40 mm to 90 mm, more preferably 50 mm to 75 mm, and even more preferably 50 mm to 60 mm.
 香味吸引物品20は、たばこロッド部20Aと、吸口を構成するフィルター部20Cと、これらを連結する連結部20Bとから構成される。 The flavor suction article 20 is composed of a tobacco rod portion 20A, a filter portion 20C constituting a mouthpiece, and a connecting portion 20B connecting these.
 たばこロッド部20Aは、円柱状であり、その全長(軸方向の長さ)は、例えば、5~100mmであることが好ましく、10~50mmであることがより好ましく、10~25mmであることがさらに好ましい。たばこロッド部20Aの断面の形状は特に限定されないが、例えば円形、楕円形、多角形等とすることができる。 The tobacco rod portion 20A has a columnar shape, and its total length (length in the axial direction) is preferably, for example, 5 to 100 mm, more preferably 10 to 50 mm, and more preferably 10 to 25 mm. More preferred. The shape of the cross section of the tobacco rod portion 20A is not particularly limited, but may be, for example, a circular shape, an elliptical shape, a polygonal shape, or the like.
 たばこロッド部20Aは、たばこ充填物21と、その周囲に巻かれたラッパー22とを有する。また、ラッパー22は、本発明のたばこ充填物からなるたばこシートであってもよい。 The tobacco rod portion 20A has a tobacco filling 21 and a wrapper 22 wrapped around the tobacco filling 21. Further, the wrapper 22 may be a tobacco sheet made of the tobacco filler of the present invention.
 フィルター部20Cは、円柱形をなしている。フィルター部20Cは、酢酸セルロースアセテート繊維が充填されて構成されたロッド状の第1セグメント25と、同じく酢酸セルロースアセテート繊維が充填されて構成されたロッド状の第2セグメント26とを有する。第1セグメント25は、たばこロッド部20A側に位置している。第1セグメント25は、中空部を有していてもよい。第2セグメント26は、吸口側に位置している。第2セグメント26は、中実である。第1セグメント25は、第1充填層(酢酸セルロースアセテート繊維)25aと、第1充填層25aの周囲に巻かれたインナープラグラッパー25bとにより構成される。第2セグメント26は、第2充填層(酢酸セルロースアセテート繊維)26aと、第2充填層26aの周囲に巻かれたインナープラグラッパー26bとにより構成される。第1セグメント25および第2セグメント26は、アウタープラグラッパー27によって連結されている。アウタープラグラッパー27は、酢酸ビニルエマルジョン系接着剤等によって第1セグメント25および第2セグメント26に接着されている。 The filter unit 20C has a cylindrical shape. The filter unit 20C has a rod-shaped first segment 25 filled with cellulose acetate acetate fiber and a rod-shaped second segment 26 also filled with cellulose acetate acetate fiber. The first segment 25 is located on the tobacco rod portion 20A side. The first segment 25 may have a hollow portion. The second segment 26 is located on the mouthpiece side. The second segment 26 is solid. The first segment 25 is composed of a first packed layer (cellulose acetate acetate fiber) 25a and an inner plug wrapper 25b wound around the first packed layer 25a. The second segment 26 is composed of a second packed layer (cellulose acetate acetate fiber) 26a and an inner plug wrapper 26b wound around the second packed layer 26a. The first segment 25 and the second segment 26 are connected by an outer plug wrapper 27. The outer plug wrapper 27 is adhered to the first segment 25 and the second segment 26 with a vinyl acetate emulsion-based adhesive or the like.
 フィルター部20Cの長さを例えば10~30mm、連結部20Bの長さを例えば10~30mm、第1セグメント25の長さを例えば5~15mm、第2セグメント26の長さを例えば5~15mmとすることができる。これら個々のセグメントの長さは、一例であり、製造適性、要求品質、たばこロッド部20Aの長さ等に応じて、適宜変更できる。 The length of the filter portion 20C is, for example, 10 to 30 mm, the length of the connecting portion 20B is, for example, 10 to 30 mm, the length of the first segment 25 is, for example, 5 to 15 mm, and the length of the second segment 26 is, for example, 5 to 15 mm. can do. The length of each of these individual segments is an example, and can be appropriately changed depending on the manufacturing aptitude, the required quality, the length of the tobacco rod portion 20A, and the like.
 例えば、第1セグメント25(センターホールセグメント)は、1つまたは複数の中空部を有する第1充填層25aと、第1充填層25aを覆うインナープラグラッパー25bとで構成される。第1セグメント25は、第2セグメント26の強度を高める機能を有する。第1セグメント25の第1充填層25aは、例えば酢酸セルロース繊維が高密度で充填されている。この酢酸セルロース繊維には、トリアセチンを含む可塑剤が酢酸セルロースの重量に対して、例えば6~20重量%添加されて硬化されている。第1セグメント25の中空部は、例えば内径φ1.0~φ5.0mmである。 For example, the first segment 25 (center hole segment) is composed of a first packed layer 25a having one or more hollow portions and an inner plug wrapper 25b covering the first packed layer 25a. The first segment 25 has a function of increasing the strength of the second segment 26. The first packed layer 25a of the first segment 25 is filled with, for example, cellulose acetate fibers at a high density. A plasticizer containing triacetin is added to the cellulose acetate fiber in an amount of, for example, 6 to 20% by weight based on the weight of the cellulose acetate and cured. The hollow portion of the first segment 25 has, for example, an inner diameter of φ1.0 to φ5.0 mm.
 第1セグメント25の第1充填層25aは、例えば、比較的に高い繊維充填密度で構成されてもよく、あるいは後述する第2セグメント26の第2充填層26aの繊維充填密度と同等であってもよい。このため、吸引時には、空気やエアロゾルが中空部のみを流れることになり、第1充填層25aには空気やエアロゾルがほとんど流れない。例えば、第2セグメント26において、エアロゾル成分の濾過による減少を少なくしたい場合には、例えば第2セグメント26の長さを短くして、その分だけ第1セグメント25を長くすることもできる。 The first packed layer 25a of the first segment 25 may be composed of, for example, a relatively high fiber filling density, or may be equivalent to the fiber filling density of the second packed layer 26a of the second segment 26 described later. May be good. Therefore, at the time of suction, air or aerosol flows only in the hollow portion, and almost no air or aerosol flows in the first packed bed 25a. For example, in the second segment 26, when it is desired to reduce the decrease due to the filtration of the aerosol component, for example, the length of the second segment 26 can be shortened and the first segment 25 can be lengthened by that amount.
 短縮した第2セグメント26を第1セグメント25で置き換えることは、エアロゾル成分のデリバリー量を増大させるために有効である。第1セグメント25の第1充填層25aが繊維充填層であることから、使用時の外側からの触り心地は、使用者に違和感を生じさせることがない。 Replacing the shortened second segment 26 with the first segment 25 is effective for increasing the delivery amount of the aerosol component. Since the first packed layer 25a of the first segment 25 is a fiber packed layer, the feeling of touch from the outside during use does not cause a sense of discomfort to the user.
 第2セグメント26は、第2充填層26aと、第2充填層26aを覆うインナープラグラッパー26bとで構成される。第2セグメント26(フィルターセグメント)は、酢酸セルロース繊維が一般的な密度で充填されており、一般的なエアロゾル成分の濾過性能を有する。 The second segment 26 is composed of a second packed layer 26a and an inner plug wrapper 26b that covers the second packed layer 26a. The second segment 26 (filter segment) is filled with cellulose acetate fibers at a general density and has the filtering performance of a general aerosol component.
 第1セグメント25と第2セグメント26との間で、たばこロッド部20Aから放出されるエアロゾル(主流煙)をろ過するろ過性能を異ならせてもよい。第1セグメント25および第2セグメント26の少なくとも一方に、香料を含ませてもよい。フィルター部20Cの構造は任意であり、上記のような複数のセグメントを有する構造であってもよいし、単一のセグメントによって構成されていてもよい。またフィルター部20Cは、1つのセグメントで構成されてもよい。この場合、フィルター部20Cは、第1セグメントまたは第2セグメントのいずれで構成されていてもよい。 The filtration performance for filtering the aerosol (mainstream smoke) emitted from the tobacco rod portion 20A may be different between the first segment 25 and the second segment 26. At least one of the first segment 25 and the second segment 26 may contain a fragrance. The structure of the filter unit 20C is arbitrary, and may be a structure having a plurality of segments as described above, or may be composed of a single segment. Further, the filter unit 20C may be composed of one segment. In this case, the filter unit 20C may be composed of either the first segment or the second segment.
 連結部20Bは、円筒形をなしている。連結部20Bは、例えば厚紙等によって円筒形に形成された紙管23を有する。連結部20Bには、エアロゾルを冷却するための冷却部材が充填されていてもよい。冷却部材としては、ポリ乳酸等のポリマーのシートが挙げられ、当該シートを折り畳んで充填することができる。さらに、たばこロッド部20Aと連結部20Bの間には、たばこロッド部20Aの位置が変動することを抑制する支持部が設けられていてもよい。支持部は、第1セグメント25のようなセンタホールフィルター等の公知の材料で構成できる。 The connecting portion 20B has a cylindrical shape. The connecting portion 20B has a paper tube 23 formed in a cylindrical shape by, for example, thick paper. The connecting portion 20B may be filled with a cooling member for cooling the aerosol. Examples of the cooling member include a sheet of a polymer such as polylactic acid, and the sheet can be folded and filled. Further, a support portion for suppressing the position of the tobacco rod portion 20A from fluctuating may be provided between the tobacco rod portion 20A and the connecting portion 20B. The support portion can be made of a known material such as a center hole filter such as the first segment 25.
 ラッパー28は、たばこロッド部20A、連結部20B、およびフィルター部20Cの外側に円筒形に巻かれて、これらを一体的に連結している。ラッパー28の一方の面(内面)には、通気孔部24の付近を除く全面または略全面に酢酸ビニルエマルジョン系接着剤が塗布されている。複数の通気孔部24は、ラッパー28によって、たばこロッド部20A、連結部20B、およびフィルター部20Cが一体にされた後に、外側からレーザ加工を施して形成される。 The wrapper 28 is wound in a cylindrical shape on the outside of the tobacco rod portion 20A, the connecting portion 20B, and the filter portion 20C, and these are integrally connected. A vinyl acetate emulsion-based adhesive is applied to one surface (inner surface) of the wrapper 28 on the entire surface or substantially the entire surface except the vicinity of the ventilation hole portion 24. The plurality of ventilation holes 24 are formed by laser processing from the outside after the tobacco rod portion 20A, the connecting portion 20B, and the filter portion 20C are integrated by the wrapper 28.
 通気孔部24は、連結部20Bを厚み方向に貫通するように2以上の貫通孔を有する。2以上の貫通孔は、香味吸引物品20の中心軸の延長線上から見て、放射状に配置するように形成される。本実施形態では、通気孔部24は、連結部20Bに設けられているが、フィルター部20Cに設けられていてもよい。また、本実施形態では、通気孔部24の2以上の貫通孔は、1つの円環上に一定間隔を空けて1列に並んで設けられるが、2つの円環上に一定の間隔を空けて2列に並んで設けられていてもよいし、1列または2列の通気孔部24が不連続または不規則に並んで設けられていてもよい。ユーザーが吸口を咥えて吸引する際に、通気孔部24を介して主流煙中に外気が取り込まれる。ただし、通気孔部24は設けられていなくてもよい。 The ventilation hole portion 24 has two or more through holes so as to penetrate the connecting portion 20B in the thickness direction. The two or more through holes are formed so as to be arranged radially when viewed from the extension line of the central axis of the flavor suction article 20. In the present embodiment, the ventilation hole portion 24 is provided in the connecting portion 20B, but may be provided in the filter portion 20C. Further, in the present embodiment, the two or more through holes of the ventilation hole portion 24 are provided side by side in a row at regular intervals on one ring, but at regular intervals on the two rings. The vent holes 24 in one row or two rows may be provided side by side in two rows, or the ventilation holes 24 in one row or two rows may be provided side by side in a discontinuous or irregular manner. When the user holds the mouthpiece and sucks it, the outside air is taken into the mainstream smoke through the ventilation hole portion 24. However, the ventilation hole portion 24 may not be provided.
[再構成たばこシートの調製]
 抄造法によって、再構成たばこシートを調製した。仕上がり品における各構成成分の比率を表1に、仕上がり品の基本物性を表2に示した。
[Preparation of reconstituted tobacco sheet]
A reconstituted tobacco sheet was prepared by the papermaking method. Table 1 shows the ratio of each component in the finished product, and Table 2 shows the basic physical properties of the finished product.
Figure JPOXMLDOC01-appb-T000001
Figure JPOXMLDOC01-appb-T000001
Figure JPOXMLDOC01-appb-T000002
Figure JPOXMLDOC01-appb-T000002
[膨嵩性測定方法]
 膨嵩性測定は下記の手順で行なった。
<装置>
測定器名称:Factory Densimeter D51  (version 12 Rev 27/03/02)
測定器メーカー:Borgwaldt社製(ドイツ)
<作業環境>
 温度22℃、相対湿度60%
<測定条件>
 たばこコンテナサイズ
 内径:95mm
 容量:約1.5リットル
 ローディングウェイト:11.4kg
 下降速度:約30mm/s
 ローディングの間隔:5秒
 間隔時間:10秒
[Measuring method of bulkiness]
The bulging property was measured by the following procedure.
<Device>
Measuring instrument name: Factory Densimeter D51 (version 12 Rev 27/03/02)
Measuring instrument manufacturer: Borgwaldt (Germany)
<Working environment>
Temperature 22 ° C, relative humidity 60%
<Measurement conditions>
Tobacco container size Inner diameter: 95 mm
Capacity: Approximately 1.5 liters Loading weight: 11.4 kg
Descent speed: Approximately 30 mm / s
Loading interval: 5 seconds Interval time: 10 seconds
<定義>
 膨嵩性とは、試料を投入した直径95mmの測定シリンダ内に11.4kgの負荷を5秒間かけた後に求められるたばこ刻円柱の高さから計算される数値である。つまり、刻のかたまりを一定の力で圧縮したときの刻単位重量当たりの体積を表す。
   FP=(A×h5)/W [cm/100g]
FP :膨嵩性
A  :たばこ刻円柱の断面積
W  :たばこ刻の重量
h5 :負荷終了時のたばこ刻円柱の高さ
<Definition>
The swellability is a numerical value calculated from the height of a tobacco-engraved cylinder obtained after applying a load of 11.4 kg for 5 seconds in a measuring cylinder having a diameter of 95 mm in which a sample is placed. In other words, it represents the volume per unit weight when the block of ticks is compressed with a constant force.
FP = (A × h5) / W [cm 3 / 100g]
FP: Bulkiness A: Cross-sectional area of the tobacco carved cylinder W: Weight of the tobacco carved h5: Height of the tobacco carved cylinder at the end of the load
[比較例1]
 再構成たばこシート(名称:シート1)を、裁刻機(Hauni社製、名称 KT2L)を用いて裁刻幅0.8mm設定で裁刻した。裁刻後の刻の長さは様々ではあったが、およそ、5.0mm~30.0mmの範囲であった。裁刻後の再構成たばこシートの水分測定、ならびに膨嵩性測定を行なった。水分測定は、105℃環境のオーブン内に1時間蔵置した際の重量減少分を水分減少として計算した。
結果を以下に示す。
水分 :13.7[重量%]
膨嵩性:303[cm/100g]
[Comparative Example 1]
The reconstructed tobacco sheet (name: sheet 1) was stamped using a stamping machine (manufactured by Hauni, name KT2L) with a stamping width of 0.8 mm. The length of the engraving after cutting varied, but was in the range of approximately 5.0 mm to 30.0 mm. Moisture measurement and bulkiness measurement of the reconstructed tobacco sheet after stamping were performed. In the water content measurement, the weight loss when stored in an oven at 105 ° C. for 1 hour was calculated as the water content loss.
The results are shown below.
Moisture: 13.7 [% by weight]
Bulkiness: 303 [cm 3 / 100g]
[比較例2]
 再構成たばこシートの種類をシート2に変更した以外は比較例1と同じ方法で裁刻し、膨嵩性を評価した。結果を以下に示す。
結果は下記の通り;
水分 :13.2[重量%]
膨嵩性:342[cm/100g]
[Comparative Example 2]
Except for changing the type of the reconstructed tobacco sheet to sheet 2, stamping was performed in the same manner as in Comparative Example 1 to evaluate the bulkiness. The results are shown below.
The results are as follows;
Moisture: 13.2 [% by weight]
Bulkiness: 342 [cm 3 / 100g]
[実施例1]
<加湿>
 再構成たばこシート(名称:シート1)を、水分供給装置、加熱装置、回転装置を備えたシリンダ型容器(内径0.9m、長さ2.0m)に装入し、水蒸気を添加して加湿を行なった。このときの再構成たばこシートの品温は約50~70℃であった。蒸気と温水を加える際に前記シリンダから排気を行なった。加湿後の再構成たばこシートの水分は、18.0重量%であった。
[Example 1]
<Humidification>
The reconstructed tobacco sheet (name: sheet 1) is placed in a cylinder-type container (inner diameter 0.9 m, length 2.0 m) equipped with a water supply device, a heating device, and a rotating device, and steam is added to humidify the sheet. Was done. The product temperature of the reconstructed tobacco sheet at this time was about 50 to 70 ° C. When steam and hot water were added, exhaust was performed from the cylinder. The moisture content of the reconstituted tobacco sheet after humidification was 18.0% by weight.
<裁刻>
 加湿後のたばこシートを、裁刻機(Hauni社製、名称 KT2L)を用いて裁刻幅0.8mm設定で裁刻した。裁刻後の刻の長さは様々ではあったが、およそ5.0mm~30.0mmの範囲であった。水分は18.0重量%であった。
<Stamping>
The humidified tobacco sheet was cut using a cutting machine (manufactured by Hauni, named KT2L) with a cutting width of 0.8 mm. The length of the engraving after cutting varied, but was in the range of approximately 5.0 mm to 30.0 mm. The water content was 18.0% by weight.
<乾燥>
 裁刻後のたばこシートを、気流乾燥器を用いて乾燥した。気流乾燥器(Garbuio/Dickinson社製、名称 EVA Dryer 400)を使用した。
<Drying>
The tobacco sheet after cutting was dried using an air flow dryer. An airflow dryer (Garbuio / Dickinson, named EVA Dryer 400) was used.
<評価>
 気流乾燥後の再構成たばこシートの水分測定、ならびに膨嵩性測定を行なった。水分測定は、105℃環境のオーブン内に1時間蔵置した際の重量減少分を水分減少として計算した。結果を以下に示す。
水分 :13.3[重量%]
膨嵩性:354[cm/100g]
<Evaluation>
Moisture measurement and bulkiness measurement of the reconstructed tobacco sheet after air flow drying were performed. In the water content measurement, the weight loss when stored in an oven at 105 ° C. for 1 hour was calculated as the water content loss. The results are shown below.
Moisture: 13.3 [% by weight]
Bulkiness: 354 [cm 3 / 100g]
[実施例2]
 再構成たばこシートの種類をシート2に変更した以外は実施例1と同じ方法で裁刻し、膨嵩性を評価した。結果を以下に示す。
水分 :13.2 [重量%]
膨嵩性:371 [cm/100g]
 以上の結果を下表にまとめて示した。
[Example 2]
The reconstructed tobacco sheet was stamped by the same method as in Example 1 except that the type of the reconstructed tobacco sheet was changed to sheet 2, and the bulkiness was evaluated. The results are shown below.
Moisture: 13.2 [% by weight]
Bulkiness: 371 [cm 3 / 100g]
The above results are summarized in the table below.
Figure JPOXMLDOC01-appb-T000003
Figure JPOXMLDOC01-appb-T000003
 本発明の方法で製造した再構成たばこシートは2種類とも、比較例で製造した再構成たばこシートに比べて、高い膨嵩性を有していた。膨嵩性の数値は膨嵩性測定時のたばこの形状の影響を強く受けるので、本例では、たばこ刻の形状はすべて同一とした。また、たばこ刻中の水分も膨嵩性に影響を与えるので、本例ではたばこ刻の水分も極力同一となるようにした。経験式(実験式)として、膨嵩性においてたばこ水分を補正する補正式が存在するが、本例においては各水準の水分差は少なく、水分補正は不要と判断した。 Both types of the reconstructed tobacco sheet produced by the method of the present invention had higher swelling property than the reconstructed tobacco sheet produced in the comparative example. Since the value of swelling property is strongly influenced by the shape of tobacco at the time of measuring swelling property, in this example, all the shapes of tobacco carvings are the same. In addition, since the water content during tobacco cutting also affects the swelling property, in this example, the water content of the tobacco cutting is made to be the same as much as possible. As an empirical formula (empirical formula), there is a correction formula that corrects the moisture content of tobacco in terms of bulkiness, but in this example, the difference in water content at each level is small, and it was judged that the water content correction is unnecessary.

Claims (16)

  1.  たばこ充填物を加湿後に乾燥する工程1、
     工程1で得たたばこ充填物が筒状ラッパー内に充填されたたばこロッド部を調製する工程2、
    を備える非燃焼加熱型香味吸引物品用たばこロッド部の製造方法。
    Step 1, which dries the tobacco filling after humidification
    Step 2, to prepare a tobacco rod portion in which the tobacco filler obtained in step 1 is filled in a tubular wrapper.
    A method for manufacturing a tobacco rod portion for a non-combustion heating type flavor suction article.
  2.  前記たばこ充填物が、エアロゾル生成基材と再構成たばこシートとを含有する、請求項1に記載の製造方法。 The production method according to claim 1, wherein the tobacco filling contains an aerosol-forming substrate and a reconstituted tobacco sheet.
  3.  前記たばこ充填物をストランド形状に裁断する工程をさらに備える、請求項2に記載の製造方法。 The manufacturing method according to claim 2, further comprising a step of cutting the tobacco filling into a strand shape.
  4.  前記たばこ充填物が、再構成たばこシートAと再構成たばこシートBとを含有し、
     前記工程1が、それぞれの再構成たばこシートを加湿後に混合して当該混合物を乾燥する、またはそれぞれの再構成たばこシートを加湿し次いで乾燥した後に混合することを含む、
    請求項1~3のいずれかに記載の製造方法。
    The tobacco filling contains the reconstituted tobacco sheet A and the reconstructed tobacco sheet B.
    The step 1 comprises humidifying and then mixing each reconstituted tobacco sheet to dry the mixture, or humidifying and then drying each reconstituted tobacco sheet and then mixing.
    The manufacturing method according to any one of claims 1 to 3.
  5.  前記たばこ充填物が、再構成たばこシートAとラミナとを含有し、
     前記工程1が、再構成たばこシートAとラミナをそれぞれ加湿後に混合して当該混合物を乾燥する、または再構成たばこシートAとラミナをそれぞれ加湿し次いで乾燥した後に混合することを含む、
    請求項1~3のいずれかに記載の製造方法。
    The tobacco filling contains the reconstituted tobacco sheet A and lamina.
    The step 1 comprises humidifying and then mixing the reconstituted tobacco sheet A and lamina to dry the mixture, or humidifying and then drying the reconstituted tobacco sheet A and lamina, respectively.
    The manufacturing method according to any one of claims 1 to 3.
  6.  前記たばこ充填物に非たばこ材料を混合する工程をさらに含む、請求項1~5のいずれかに記載の製造方法。 The production method according to any one of claims 1 to 5, further comprising a step of mixing a non-tobacco material with the tobacco filling.
  7.  前記たばこ充填物に添加剤を加える工程をさらに含む、請求項1~6のいずれかに記載の製造方法。 The production method according to any one of claims 1 to 6, further comprising a step of adding an additive to the tobacco filling.
  8.  前記再構成たばこシートAと再構成たばこシートBのいずれか一方もしくは両方に添加剤を加える工程をさらに備える、請求項4または6に記載の製造方法。 The production method according to claim 4 or 6, further comprising a step of adding an additive to either or both of the reconstituted tobacco sheet A and the reconstituted tobacco sheet B.
  9.  前記再構成たばこシートとラミナのいずれか一方もしくは両方に添加剤を加える工程をさらに備える、請求項5または6に記載の製造方法。 The production method according to claim 5 or 6, further comprising a step of adding an additive to either or both of the reconstituted tobacco sheet and the lamina.
  10.  前記たばこ充填物の成分を測定し、測定結果を基に前記添加剤の種類または添加量を調整する工程をさらに含む、請求項7~9のいずれかに記載の製造方法。 The production method according to any one of claims 7 to 9, further comprising a step of measuring the components of the tobacco filling and adjusting the type or amount of the additive based on the measurement result.
  11.  前記再構成たばこシートAの成分を測定し、
     測定結果に基づいて、再構成たばこシートBまたはラミナの種類を決定する、
     請求項4または5に記載の製造方法。
    The components of the reconstituted tobacco sheet A were measured and
    Determine the type of reconstituted tobacco sheet B or lamina based on the measurement results,
    The manufacturing method according to claim 4 or 5.
  12.  前記再構成たばこシートAの成分を測定し、
     測定結果に基づいて、
     再構成たばこシートBに添加する添加剤の種類または量、あるいは
     ラミナに添加する添加剤の種類または量を決定する、
     請求項7に記載の製造方法。
    The components of the reconstituted tobacco sheet A were measured and
    Based on the measurement results
    To determine the type or amount of additive to be added to the reconstituted tobacco sheet B, or the type or amount of additive to be added to lamina.
    The manufacturing method according to claim 7.
  13.  前記たばこ充填物中の水分量を15~25重量%とするように加湿を行う、請求項1~3、6、または7のいずれかに記載の製造方法。 The production method according to any one of claims 1 to 3, 6 or 7, wherein humidification is performed so that the water content in the tobacco filling is 15 to 25% by weight.
  14.  前記再構成たばこシート中の水分量を15~25重量%とするように加湿を行う、請求項4~12のいずれかに記載の製造方法。 The production method according to any one of claims 4 to 12, wherein humidification is performed so that the water content in the reconstructed tobacco sheet is 15 to 25% by weight.
  15.  前記乾燥を、気流乾燥方式またはアニュラー乾燥方式で実施する、請求項1~14のいずれかに記載の製造方法。 The manufacturing method according to any one of claims 1 to 14, wherein the drying is carried out by an air flow drying method or an annual drying method.
  16.  前記再構成たばこシートが、抄造シート、キャストシート、または押出シートである、請求項4~15のいずれかに記載の製造方法。 The manufacturing method according to any one of claims 4 to 15, wherein the reconstructed tobacco sheet is a papermaking sheet, a cast sheet, or an extruded sheet.
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