CN111039599B - 一种耐磨抗冲击环氧砂浆修补材料及其制备方法 - Google Patents
一种耐磨抗冲击环氧砂浆修补材料及其制备方法 Download PDFInfo
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- CN111039599B CN111039599B CN201911334931.4A CN201911334931A CN111039599B CN 111039599 B CN111039599 B CN 111039599B CN 201911334931 A CN201911334931 A CN 201911334931A CN 111039599 B CN111039599 B CN 111039599B
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- copper powder
- epoxy resin
- graphene oxide
- nano copper
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- 239000004570 mortar (masonry) Substances 0.000 title claims abstract description 18
- 239000000463 material Substances 0.000 title claims abstract description 14
- 239000004593 Epoxy Substances 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 230000008439 repair process Effects 0.000 title claims abstract description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 62
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 52
- 229910021389 graphene Inorganic materials 0.000 claims abstract description 52
- 239000003822 epoxy resin Substances 0.000 claims abstract description 50
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 50
- 229920005989 resin Polymers 0.000 claims abstract description 41
- 239000011347 resin Substances 0.000 claims abstract description 41
- 239000004793 Polystyrene Substances 0.000 claims abstract description 38
- 229920002223 polystyrene Polymers 0.000 claims abstract description 38
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000004576 sand Substances 0.000 claims abstract description 29
- 238000003756 stirring Methods 0.000 claims abstract description 22
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 19
- 239000010703 silicon Substances 0.000 claims abstract description 19
- 239000003208 petroleum Substances 0.000 claims abstract description 16
- 150000003505 terpenes Chemical class 0.000 claims abstract description 16
- 235000007586 terpenes Nutrition 0.000 claims abstract description 16
- 239000005543 nano-size silicon particle Substances 0.000 claims abstract description 15
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 15
- 238000010438 heat treatment Methods 0.000 claims abstract description 10
- 238000001816 cooling Methods 0.000 claims abstract description 8
- 238000001132 ultrasonic dispersion Methods 0.000 claims abstract description 6
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 31
- 239000004200 microcrystalline wax Substances 0.000 claims description 17
- 235000019808 microcrystalline wax Nutrition 0.000 claims description 17
- 238000002156 mixing Methods 0.000 claims description 15
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 11
- 239000012948 isocyanate Substances 0.000 claims description 11
- 150000002513 isocyanates Chemical class 0.000 claims description 11
- 229920001690 polydopamine Polymers 0.000 claims description 10
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 6
- 239000011229 interlayer Substances 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 239000004566 building material Substances 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 21
- 230000000052 comparative effect Effects 0.000 description 14
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 13
- 239000000203 mixture Substances 0.000 description 13
- 239000002131 composite material Substances 0.000 description 7
- 238000001723 curing Methods 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 239000011248 coating agent Substances 0.000 description 6
- 238000000576 coating method Methods 0.000 description 6
- VYFYYTLLBUKUHU-UHFFFAOYSA-N dopamine Chemical compound NCCC1=CC=C(O)C(O)=C1 VYFYYTLLBUKUHU-UHFFFAOYSA-N 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 239000010410 layer Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 239000004567 concrete Substances 0.000 description 4
- KOBKUSXTVUSJEU-UHFFFAOYSA-N copper;prop-2-enoic acid Chemical compound [Cu].OC(=O)C=C KOBKUSXTVUSJEU-UHFFFAOYSA-N 0.000 description 4
- 239000008367 deionised water Substances 0.000 description 4
- 229910021641 deionized water Inorganic materials 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 4
- 230000003993 interaction Effects 0.000 description 4
- -1 nano copper powder compound Chemical class 0.000 description 4
- 239000011858 nanopowder Substances 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- 238000001694 spray drying Methods 0.000 description 4
- 229960003638 dopamine Drugs 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000002344 surface layer Substances 0.000 description 3
- 238000005299 abrasion Methods 0.000 description 2
- 239000004568 cement Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 239000002105 nanoparticle Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- RZVHIXYEVGDQDX-UHFFFAOYSA-N 9,10-anthraquinone Chemical group C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 RZVHIXYEVGDQDX-UHFFFAOYSA-N 0.000 description 1
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 229910003471 inorganic composite material Inorganic materials 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 239000010954 inorganic particle Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 125000000962 organic group Chemical group 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 230000005476 size effect Effects 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000012745 toughening agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/30—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Other silicon-containing organic compounds; Boron-organic compounds
- C04B26/32—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Other silicon-containing organic compounds; Boron-organic compounds containing silicon
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
- C04B2201/52—High compression strength concretes, i.e. with a compression strength higher than about 55 N/mm2, e.g. reactive powder concrete [RPC]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/91—Use of waste materials as fillers for mortars or concrete
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Abstract
Description
抗压强度/MPa | 磨耗/mg | |
实施例1 | 95 | 0.022 |
实施例2 | 102 | 0.031 |
实施例3 | 98 | 0.028 |
对比例1 | 80 | 0.35 |
对比例2 | 85 | 0.23 |
对比例3 | 89 | 0.54 |
对比例4 | 78 | 0.36 |
Claims (5)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202011171458.5A CN112408868A (zh) | 2019-12-23 | 2019-12-23 | 耐磨抗冲击环氧砂浆修补材料的制备方法 |
CN202011174499.XA CN112374798B (zh) | 2019-12-23 | 2019-12-23 | 一种耐磨抗冲击环氧砂浆修补材料的制备方法 |
CN201911334931.4A CN111039599B (zh) | 2019-12-23 | 2019-12-23 | 一种耐磨抗冲击环氧砂浆修补材料及其制备方法 |
Applications Claiming Priority (1)
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CN201911334931.4A CN111039599B (zh) | 2019-12-23 | 2019-12-23 | 一种耐磨抗冲击环氧砂浆修补材料及其制备方法 |
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CN202011174499.XA Division CN112374798B (zh) | 2019-12-23 | 2019-12-23 | 一种耐磨抗冲击环氧砂浆修补材料的制备方法 |
CN202011171458.5A Division CN112408868A (zh) | 2019-12-23 | 2019-12-23 | 耐磨抗冲击环氧砂浆修补材料的制备方法 |
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CN111039599A CN111039599A (zh) | 2020-04-21 |
CN111039599B true CN111039599B (zh) | 2020-11-27 |
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CN202011174499.XA Active CN112374798B (zh) | 2019-12-23 | 2019-12-23 | 一种耐磨抗冲击环氧砂浆修补材料的制备方法 |
CN202011171458.5A Withdrawn CN112408868A (zh) | 2019-12-23 | 2019-12-23 | 耐磨抗冲击环氧砂浆修补材料的制备方法 |
CN201911334931.4A Active CN111039599B (zh) | 2019-12-23 | 2019-12-23 | 一种耐磨抗冲击环氧砂浆修补材料及其制备方法 |
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CN202011174499.XA Active CN112374798B (zh) | 2019-12-23 | 2019-12-23 | 一种耐磨抗冲击环氧砂浆修补材料的制备方法 |
CN202011171458.5A Withdrawn CN112408868A (zh) | 2019-12-23 | 2019-12-23 | 耐磨抗冲击环氧砂浆修补材料的制备方法 |
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Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112358233B (zh) * | 2020-12-15 | 2022-07-12 | 中电建十一局工程有限公司 | 一种环氧混凝土及混凝土基面修复加固方法 |
CN112939459B (zh) * | 2021-02-21 | 2022-07-22 | 潮州市祥发陶瓷有限公司 | 一种耐磨耐腐蚀陶瓷釉料及其制备方法和应用 |
CN114196167B (zh) * | 2021-12-31 | 2023-11-24 | 安徽善孚新材料科技股份有限公司 | 一种玻纤复合材料用环氧树脂及其制备方法和应用、玻璃纤维复合材料 |
Family Cites Families (15)
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CN102875057B (zh) * | 2012-08-29 | 2013-12-25 | 江苏博特新材料有限公司 | 一种高强快固环氧砂浆及其制备方法 |
CN104058660B (zh) * | 2014-05-30 | 2016-02-10 | 蚌埠华东石膏有限公司 | 一种速凝高强度混凝土及其制备方法 |
CN104530653B (zh) * | 2014-12-26 | 2016-09-21 | 黑龙江大学 | 一种环氧树脂/石墨烯/纳米铜复合材料的制备方法 |
US10850496B2 (en) * | 2016-02-09 | 2020-12-01 | Global Graphene Group, Inc. | Chemical-free production of graphene-reinforced inorganic matrix composites |
CN106009514B (zh) * | 2016-06-20 | 2019-04-19 | 山东欧铂新材料有限公司 | 一种石墨烯/环氧树脂复合材料的制备方法 |
CN106906028B (zh) * | 2017-03-16 | 2019-07-30 | 深圳市百顺源节能科技有限公司 | 一种石墨烯复合抗磨剂及其制备方法 |
CN107216768B (zh) * | 2017-05-31 | 2019-05-28 | 广州希森美克新材料科技有限公司 | 一种超薄纳米型防腐涂料及其自流平浸涂工艺 |
CN107840605A (zh) * | 2017-11-09 | 2018-03-27 | 安徽艾米伦特建材科技有限公司 | 防裂抹灰砂浆及其制备方法 |
CN108395147A (zh) * | 2018-04-11 | 2018-08-14 | 吉林重通成飞新材料股份公司 | 一种环氧砂浆及地坪涂料 |
CN109021577A (zh) * | 2018-09-30 | 2018-12-18 | 广西驰胜农业科技有限公司 | 一种树脂基道路修补材料 |
CN109534720B (zh) * | 2019-01-16 | 2020-06-23 | 吉林大学 | 一种低线膨胀系数环氧树脂基水泥混凝土道路快速修补材料及其制备方法 |
CN109897165B (zh) * | 2019-03-29 | 2021-09-07 | 中国科学院理化技术研究所 | 一种改性环氧树脂及其制备方法 |
CN110105849A (zh) * | 2019-06-04 | 2019-08-09 | 天津伯仲佳和化工有限公司 | 一种油井管耐磨耐高温粉末涂料 |
CN110357545B (zh) * | 2019-08-16 | 2022-01-07 | 广西理工职业技术学院 | 混凝土基层局部破损快速修补砂浆及其制备方法 |
CN110511803A (zh) * | 2019-08-26 | 2019-11-29 | 泰州学院 | 一种用于钛合金表面具有稳定抗磨减摩功能的纳米复合材料 |
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2019
- 2019-12-23 CN CN202011174499.XA patent/CN112374798B/zh active Active
- 2019-12-23 CN CN202011171458.5A patent/CN112408868A/zh not_active Withdrawn
- 2019-12-23 CN CN201911334931.4A patent/CN111039599B/zh active Active
Also Published As
Publication number | Publication date |
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CN112408868A (zh) | 2021-02-26 |
CN112374798A (zh) | 2021-02-19 |
CN111039599A (zh) | 2020-04-21 |
CN112374798B (zh) | 2023-04-14 |
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