CN110934794B - Shampoo special for industrial enterprises - Google Patents
Shampoo special for industrial enterprises Download PDFInfo
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- CN110934794B CN110934794B CN201911307880.6A CN201911307880A CN110934794B CN 110934794 B CN110934794 B CN 110934794B CN 201911307880 A CN201911307880 A CN 201911307880A CN 110934794 B CN110934794 B CN 110934794B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B11/00—Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use
- B05B11/01—Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use characterised by the means producing the flow
- B05B11/10—Pump arrangements for transferring the contents from the container to a pump chamber by a sucking effect and forcing the contents out through the dispensing nozzle
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B11/00—Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use
- B05B11/01—Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use characterised by the means producing the flow
- B05B11/10—Pump arrangements for transferring the contents from the container to a pump chamber by a sucking effect and forcing the contents out through the dispensing nozzle
- B05B11/1042—Components or details
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B11/00—Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use
- B05B11/01—Single-unit hand-held apparatus in which flow of contents is produced by the muscular force of the operator at the moment of use characterised by the means producing the flow
- B05B11/10—Pump arrangements for transferring the contents from the container to a pump chamber by a sucking effect and forcing the contents out through the dispensing nozzle
- B05B11/1081—Arrangements for pumping several liquids or other fluent materials from several containers, e.g. for mixing them at the moment of pumping
Abstract
The invention belongs to the technical field of shampoo, in particular to special shampoo for industrial enterprises; 20 parts of sodium dodecyl sulfate, 20 parts of disodium lauroamphodipropionate, 8 parts of sandalwood oil, 2 parts of ammonium xylene sulfonate, 1 part of hyaluronic acid, 20 parts of a natural surfactant and 19 parts of a mixed solvent; the natural surfactant is low-concentration tea saponin concentrated solution; the mixed solvent is prepared by mixing the extract of the alpine edelweiss and menthol; hyaluronic acid acts on the epidermis of the skin to form chemical hydrogen bonds with the surface of the skin, so that the loss of the nutrient components of the epidermis of the skin is prevented, and the skin is protected; tea saponin is an excellent natural surfactant, and can effectively remove impurities such as tar, wax, dust and the like on hair; meanwhile, the extractive solution of the Hibiscus alpinus in the mixed solvent can play a role in skin care essence on the scalp, activate the activity of skin cells, improve the metabolism capability and self-repairing capability of the cells, and prevent the phenomenon that the tea saponin enters the scalp to cause damage to hair roots.
Description
Technical Field
The invention belongs to the technical field of shampoo, and particularly relates to special shampoo for industrial enterprises.
Background
In daily life of people, hair washing is also an important thing for people, and the hair washing is black and bright, so that the color value can be improved, and convenience can be brought to people.
Shampoos, also known as shampoos, shampoos or shampoos, have the main function of cleansing the hair and scalp and provide the basis for the styling of the hair. The purpose of shampooing is to remove dust from the hair and scalp and to wash away excess oil. When shampooing hair, the hair swells when it absorbs water, becomes wet and soft, and the protective oil is washed off, which leads to the damage of hair scales. In order to solve the problem of hair damage, the traditional shampoo adopts a mode of adding silicone oil into the shampoo.
The existing shampoo has different cleaning effects on hair due to different internal components; especially, the shampoo for industrial and mining enterprises, because miners stay in the mine for a long time, a large amount of pollutants such as tar, dust and the like in the mine can be accumulated on the hair of the miners, and when the miners wear the shampoo for a long time, the corrosion of the tar, the wax and the dust can cause the scalp to generate red swelling or eczema, thereby affecting the safe work of the miners; meanwhile, tar and dust on the hair can be adhered to the hair, so that miners are difficult to clean.
Disclosure of Invention
In order to make up for the defects of the prior art, the special shampoo for industrial enterprises is mainly used for solving the problems that the existing shampoo for industrial and mining enterprises is in a mine for a long time, a large amount of pollutants such as tar, dust and the like are contained in the mine and can be greatly accumulated on the hair of the miners, and when a spacious worker wears a safety helmet for a long time, the corrosion of the tar, the wax and the dust can cause the red swelling or the eczema of the scalp, thereby affecting the safety work of the miners; meanwhile, tar and dust on the hair can be adhered to the hair, so that miners are difficult to clean.
The technical scheme adopted by the invention for solving the technical problems is as follows: the shampoo special for industrial enterprises, provided by the invention, comprises the following raw materials in parts by weight: 20 parts of sodium dodecyl sulfate, 20 parts of disodium lauroamphodipropionate, 8 parts of sandalwood oil, 2 parts of ammonium xylene sulfonate, 1 part of hyaluronic acid, 20 parts of a natural surfactant, 19 parts of a mixed solvent and the balance of water; the hyaluronic acid acts on the epidermis layer of the skin to form chemical hydrogen bonds with the surface of the skin, so that the loss of the nutrient components of the epidermis layer of the skin is prevented, the skin is protected, and meanwhile, the natural surfactant is prevented from permeating into fur tissues, so that hair roots are prevented from being damaged to a certain extent.
Preferably, the natural surfactant is a low-concentration tea saponin concentrated solution; the mixed solvent is prepared by mixing the extract of the alpine edelweiss and menthol; the tea saponin is an extract in tea leaves, has a structure of triterpenoid saponin, and has strong surface activity, hard water resistance and foaming capacity; the tea saponin has multiple functions of emulsification, decontamination, wetting, dispersion, foaming and the like; the emulsifying capacity of the oil-free hair cleaning agent exceeds that of emulsifying agents such as oleic soap, alkyl sulfonate, polyoxyethylene fatty alcohol ether and the like, and the oil-free hair cleaning agent is an excellent natural surfactant and can effectively remove impurities such as tar, wax, dust and the like on hair; meanwhile, the extract of the leontopodium alpinum in the mixed solvent can play a role of skin care essence on the scalp, is natural and mild, activates the activity of skin cells, improves the metabolism capability and self-repairing capability of the cells, prevents the tea saponin from entering the scalp to cause the phenomenon that hairy roots cause damage, and simultaneously prevents the tea saponin solution from entering the red swelling skin to cause damage to red blood cells; the skin care essence of the edelweiss extracting solution is matched with the penetration enhancer menthol for use, so that the absorption of the skin on the edelweiss extracting solution can be enhanced, the action effect is enhanced, and the absorption rate is improved; meanwhile, the menthol can relieve pain to the scalp, treat red swelling dermatitis caused by erosion of tar or dust on the scalp, and inhibit growth and reproduction of bacteria.
Preferably, the preparation method of the shampoo comprises the following steps:
s1: adding sodium dodecyl sulfate, disodium lauroamphodipropionate, sandalwood oil, ammonium xylene sulfonate and hyaluronic acid into a mixing pot, adding a part of deionized water into the mixing pot, heating to 80 ℃, preserving heat and stirring for 20 minutes until the deionized water is completely dissolved to obtain a solution A; deionized water is pure water from which salts are removed and silicic acid, carbon dioxide and the like are partially removed, so that the phenomenon of caking or paste formation of the raw materials during mixing and stirring is effectively prevented, and the scalp can be moisturized;
s2: placing the dried, ground and crushed tea seed meal particles into a flat-turn leacher, adding ethanol for leaching, and extracting an ethanol saponin mixed solution at the bottom of the flat-turn leacher; putting the mixed solution of the ethanol and the saponin into a long-tube evaporator to recover most of ethanol; filtering impurities and pigments in the solution by using activated carbon, and recovering most of water in the tea saponin by using membrane separation equipment to prepare a tea saponin concentrated solution; the tea saponin can be partially separated and intercepted by adopting a membrane separation technology, and part of water is removed, so that the effective components are concentrated and refined, membrane permeation water can be recycled to a previous extraction process, energy is saved, and emission is reduced; ethanol is adopted for leaching, and after ethanol in the ethanol saponin solution is mostly extracted by distillation, the residual ethanol in the tea saponin can accelerate the dissolving effect of menthol in water;
s3: adding the tea saponin concentrated solution prepared in the step S2 into the solution A prepared in the step S1, stirring until no agglomeration phenomenon exists, emulsifying and concentrating the mixed raw materials through a vacuum emulsifying pot until the maximum temperature is not more than 75 ℃, and stirring until all components are completely dissolved; mixing the low-concentration tea saponin concentrated solution prepared in the step S2 with deionized water in the step S1, wherein the deionized water is pure water for removing salts and partially removing silicic acid, carbon dioxide and the like, so that the phenomenon that saponin in the tea saponin is precipitated due to certain hydrochloric acid contained in the solution is prevented, and the emulsifying and dirt-removing capacity of the tea saponin is further influenced;
s4: soaking fresh or dried Hibiscus alpinus Leontopodium herb in purified water in an extraction tank for 1 h; extracting the extract by using a rotary evaporator at the evaporation temperature of 50 ℃, and then filtering the extract; mixing the formula amount of the alpine edelweiss extract with menthol in advance, and uniformly stirring to prepare a mixed solvent; the extraction of the alpine fire velvet liquid in the alpine fire velvet grass can be effectively improved through the rotary evaporator, and impurities in the alpine fire velvet liquid can be separated from the extracting solution through the action of centrifugal force; the penetration enhancer mint is added, so that the absorption of the skin to the extract of the alpine edelweiss can be promoted, and the effect is enhanced;
s5: filling the mixed emulsion prepared in the step S3 into a shampoo bottle, and simultaneously filling the mixed solution prepared in the step S4 into the shampoo bottle, and simultaneously separately storing the mixed emulsion and the mixed solvent through a partition plate; the mixed emulsion and the mixed solvent are independently stored, so that the phenomenon that a small amount of ethanol solution in the tea saponin is dissolved in menthol in the mixed solvent when the shampoo is kept still is prevented, and the using effect of the mixed solvent is further influenced; meanwhile, the phenomenon that the concentration of the tea saponin is improved due to less ethanol solution in the tea saponin is prevented.
Preferably, the shampoo bottle in the step S5 includes a bottle body, a bottle cap and a liquid pumping device; the bottle body is provided with a card reader; a partition plate is arranged in the bottle body, and a bottle cap is connected to the upper part of the bottle body through threads; the liquid pumping device comprises a liquid pumping nozzle, a pressing pipe, a pipe seat, a pressing spring, a liquid suction pipe and a liquid distribution pipe; the liquid pumping nozzle is movably arranged on the bottle cap through a pressing pipe, and the pressing pipe is inserted on the pipe seat in a sliding manner; the tube seat is arranged on the bottle cap, and a pressing spring is inserted in the tube seat; the bottom end of the tube seat is connected with a pipette, and the orifice of the pipette is positioned above the separation plate; the liquid suction pipe is connected with a liquid separation pipe, and the lower end of the liquid separation pipe is positioned below the separation plate; a sealing device is arranged in the pipette; the sealing device comprises an extrusion pipe, a mounting disc, a guide pipe, an extrusion bag, a sliding rod, a sealing sliding plate, a limiting spring and a sealing disc; the extrusion pipe is installed at the bottom end of the pressing pipe through an installation disc, and a liquid guide groove is formed in the installation disc; a pneumatic control valve is arranged in the extrusion pipe; the guide pipe is arranged in the sealing device through an installation disc, the top end of the guide pipe is provided with an extrusion bag, and a sliding rod is arranged in the guide pipe in a sliding manner; the top end of the extrusion bag is communicated with the extrusion pipe; the bottom end of the sliding rod is provided with a sealing sliding plate, the bottom end of the sealing sliding plate is provided with a sealing block, and the sealing sliding plate is provided with a liquid guide groove; the sealing disc is positioned at the bottom end of the sealing sliding plate, and a liquid discharge hole is formed in the sealing disc; a limiting spring is arranged between the sealing disc and the sealing sliding plate; the sealing block corresponds to the liquid discharge hole; the bottle body is provided with a control unit, and the control unit is in electric signal connection with the card reader;
when the shampoo bottle works, when a user needs to use shampoo, the user presses the liquid pumping nozzle, the downward movement of the liquid pumping nozzle can drive the pressing pipe to slide downwards in the pipe seat, the pressing pipe can compress the pressing spring, when the user breaks away from and presses the liquid pumping nozzle, the suction force of the pressing pipe can enable mixed emulsion and mixed solvent to enter the liquid suction pipe through the liquid suction pipe and the liquid distribution pipe respectively, meanwhile, when the pressing pipe moves downwards, the pressing pipe can extrude the extrusion bag through the extrusion pipe, gas in the extrusion bag can enter the guide pipe, along with continuous pressing of the liquid pumping nozzle, the mixed emulsion above the partition plate and the mixed solvent below the partition plate can be mixed in the liquid suction pipe and then enter the liquid pumping nozzle through the pressing pipe to be sprayed out, along with continuous entering of the guide pipe of the gas in the extrusion bag, the sealing sliding plate can slide downwards to be contacted with the sealing disc, the sealing block arranged at the bottom end of the sealing sliding plate can block the liquid, thereby limiting the use of the shampoo in the bottle body; through the matching of the liquid pumping device and the sealing device, the liquid pumping device can mix and pump the divided mixed emulsion and the mixed solvent part, so that the mixed emulsion and the mixed solvent are mixed in the liquid suction pipe and the pipe seat, and the phenomenon that the shampoo is deteriorated due to the mixing reaction of local components in the mixed emulsion and the mixed solvent is effectively prevented; meanwhile, the sealing device can be used for quantitatively using the shampoo, so that the shampoo is prevented from being wasted by the malicious use of staff; meanwhile, the phenomenon that the tea saponin damages the scalp of a user due to excessive use of the tea saponin in the mixed emulsion when the shampoo is used is prevented; when the next user uses shampoo, the user can attach the employee card to the card reader, the card reader controls the air control valve to be opened through the control unit, and the restoring force of the limiting spring can enable the sealing sliding plate to drive the sliding rod to move upwards so that the sealing block and the liquid guide groove are separated from sealing.
Preferably, an elastic liquid guide film is arranged between the sealing disc and the sealing sliding plate and is fixedly arranged on the limiting spring; the during operation, when spacing spring compress down, the elasticity drain membrane that sets up on the spacing spring can improve the mixed intensive mixing effect of mixed emulsion and mixed solvent in the imbibition pipe, prevents that mixed emulsion and mixed solvent can not abundant effectual mixture, and then reduces the abundant clearance effect of silicon oil, the dust that the shampoo bonded on to the user's hair.
Preferably, the pipe orifice of the liquid distribution pipe is positioned above the sealing disc, the elastic membrane is thermally pressed on the sealing disc, and one third of the excircle of the elastic membrane is thermally pressed on the sealing disc; the method comprises the following steps of; the thickness of the sealing sliding plate and the sealing disc is larger than the diameter of the pipe orifice of the liquid distribution pipe; when the device works, when the pressing pipe presses downwards, the elastic membrane is tightly attached to the sealing disk by the driving force of gas in the liquid suction pipe, so that the phenomenon that the mixed solvent pumped in through the liquid distribution pipe enters the mixed emulsion through the liquid suction pipe due to the downward pressing force of the pressing pipe is prevented, and the separation effect of the mixed solvent and the mixed emulsion is further influenced; when sealed slide and sealed dish were laminated simultaneously, the thickness of sealed slide and sealed dish can block up branch liquid pipe, prevents to divide the suction of liquid pipe to lead to dividing the phenomenon that the mixed solvent in the liquid pipe was taken out.
The invention has the following beneficial effects:
1. the natural surfactant and the mixed solvent are matched for use, the natural surfactant adopts tea saponin which is an extract in tea leaves, the structure is triterpenoid saponin, and the triterpenoid saponin has strong surface activity, high hard water resistance and high foaming capacity; the tea saponin has multiple functions of emulsification, decontamination, wetting, dispersion, foaming and the like; the emulsifying capacity of the oil-free hair cleaning agent exceeds that of emulsifying agents such as oleic soap, alkyl sulfonate, polyoxyethylene fatty alcohol ether and the like, and the oil-free hair cleaning agent is an excellent natural surfactant and can effectively remove impurities such as tar, wax, dust and the like on hair; meanwhile, the extract of the Hibiscus alpinus in the mixed solvent can play a role of skin care essence on the scalp, is natural and mild, activates the activity of skin cells, improves the metabolism capability and self-repairing capability of the cells, prevents the tea saponin from entering the scalp to cause the phenomenon of injury of hair roots, and prevents the tea saponin solution from entering the red swelling skin to cause injury to red blood cells.
2. According to the invention, the skin care essence of the edelweiss extracting solution is matched with the penetration enhancer menthol for use, so that the absorption of the skin on the edelweiss extracting solution can be enhanced, the action effect is enhanced, and the absorption rate is improved; meanwhile, the menthol can relieve pain to the scalp, treat red swelling dermatitis caused by erosion of tar or dust on the scalp, and inhibit growth and reproduction of bacteria.
3. According to the invention, through the matching of the liquid pumping device and the sealing device, the liquid pumping device can mix and pump out the divided mixed emulsion and the mixed solvent, so that the mixed emulsion and the mixed solvent are mixed in the liquid suction pipe and the pipe seat, and the phenomenon of shampoo deterioration caused by mixing reaction of local components in the mixed emulsion and the mixed solvent is effectively prevented; meanwhile, the sealing device can be used for quantitatively using the shampoo, so that the shampoo is prevented from being wasted by the malicious use of staff; meanwhile, the phenomenon that the tea saponin damages the scalp of a user due to excessive use of the tea saponin in the mixed emulsion when the shampoo is used is prevented.
Drawings
The invention will be further explained with reference to the drawings.
FIG. 1 is a process flow diagram of a shampoo of the invention;
FIG. 2 is a perspective view of a shampoo bottle of the invention;
FIG. 3 is a cross-sectional view of a shampoo bottle of the invention;
FIG. 4 is an enlarged view of a portion of the invention at A in FIG. 3;
in the figure: the bottle body 1, the bottle cap 2, the liquid pumping device 3, the liquid pumping nozzle 31, the pressing tube 32, the tube seat 33, the pressing spring 34, the liquid suction tube 341, the liquid distribution tube 35, the sealing device 4, the extruding tube 41, the mounting disc 42, the liquid guide groove 421, the guide tube 43, the extruding bag 44, the sealing sliding plate 46, the limiting spring 47, the sealing disc 48, the sealing block 49, the elastic liquid guide film 5, the elastic film 6 and the partition plate 7.
Detailed Description
The shampoo for industrial use according to an embodiment of the present invention will be described below with reference to fig. 1 to 4.
As shown in fig. 1-4, the shampoo special for industrial enterprises, provided by the invention, comprises the following raw materials in parts by weight: 20 parts of sodium dodecyl sulfate, 20 parts of disodium lauroamphodipropionate, 8 parts of sandalwood oil, 2 parts of ammonium xylene sulfonate, 1 part of hyaluronic acid, 20 parts of a natural surfactant, 19 parts of a mixed solvent and the balance of water; the hyaluronic acid acts on the epidermis layer of the skin to form chemical hydrogen bonds with the surface of the skin, so that the loss of the nutrient components of the epidermis layer of the skin is prevented, the skin is protected, and meanwhile, the natural surfactant is prevented from permeating into fur tissues, so that hair roots are prevented from being damaged to a certain extent.
As an embodiment of the present invention, the natural surfactant is a concentrated solution of low-concentration tea saponin; the mixed solvent is prepared by mixing the extract of the alpine edelweiss and menthol; the tea saponin is an extract in tea leaves, has a structure of triterpenoid saponin, and has strong surface activity, hard water resistance and foaming capacity; the tea saponin has multiple functions of emulsification, decontamination, wetting, dispersion, foaming and the like; the emulsifying capacity of the oil-free hair cleaning agent exceeds that of emulsifying agents such as oleic soap, alkyl sulfonate, polyoxyethylene fatty alcohol ether and the like, and the oil-free hair cleaning agent is an excellent natural surfactant and can effectively remove impurities such as tar, wax, dust and the like on hair; meanwhile, the extract of the leontopodium alpinum in the mixed solvent can play a role of skin care essence on the scalp, is natural and mild, activates the activity of skin cells, improves the metabolism capability and self-repairing capability of the cells, prevents the tea saponin from entering the scalp to cause the phenomenon that hairy roots cause damage, and simultaneously prevents the tea saponin solution from entering the red swelling skin to cause damage to red blood cells; the skin care essence of the edelweiss extracting solution is matched with the penetration enhancer menthol for use, so that the absorption of the skin on the edelweiss extracting solution can be enhanced, the action effect is enhanced, and the absorption rate is improved; meanwhile, the menthol can relieve pain to the scalp, treat red swelling dermatitis caused by erosion of tar or dust on the scalp, and inhibit growth and reproduction of bacteria.
As an embodiment of the present invention, the shampoo is prepared by a method comprising the steps of:
s1: adding sodium dodecyl sulfate, disodium lauroamphodipropionate, sandalwood oil, ammonium xylene sulfonate and hyaluronic acid into a mixing pot, adding a part of deionized water into the mixing pot, heating to 80 ℃, preserving heat and stirring for 20 minutes until the deionized water is completely dissolved to obtain a solution A; deionized water is pure water from which salts are removed and silicic acid, carbon dioxide and the like are partially removed, so that the phenomenon of caking or paste formation of the raw materials during mixing and stirring is effectively prevented, and the scalp can be moisturized;
s2: placing the dried, ground and crushed tea seed meal particles into a flat-turn leacher, adding ethanol for leaching, and extracting an ethanol saponin mixed solution at the bottom of the flat-turn leacher; putting the mixed solution of the ethanol and the saponin into a long-tube evaporator to recover most of ethanol; filtering impurities and pigments in the solution by using activated carbon, and recovering most of water in the tea saponin by using membrane separation equipment to prepare a tea saponin concentrated solution; the tea saponin can be partially separated and intercepted by adopting a membrane separation technology, and part of water is removed, so that the effective components are concentrated and refined, membrane permeation water can be recycled to a previous extraction process, energy is saved, and emission is reduced; ethanol is adopted for leaching, and after ethanol in the ethanol saponin solution is mostly extracted by distillation, the residual ethanol in the tea saponin can accelerate the dissolving effect of menthol in water;
s3: adding the tea saponin concentrated solution prepared in the step S2 into the solution A prepared in the step S1, stirring until no agglomeration phenomenon exists, emulsifying and concentrating the mixed raw materials through a vacuum emulsifying pot until the maximum temperature is not more than 75 ℃, and stirring until all components are completely dissolved; mixing the low-concentration tea saponin concentrated solution prepared in the step S2 with deionized water in the step S1, wherein the deionized water is pure water for removing salts and partially removing silicic acid, carbon dioxide and the like, so that the phenomenon that saponin in the tea saponin is precipitated due to certain hydrochloric acid contained in the solution is prevented, and the emulsifying and dirt-removing capacity of the tea saponin is further influenced;
s4: soaking fresh or dried Hibiscus alpinus Leontopodium herb in purified water in an extraction tank for 1 h; extracting the extract by using a rotary evaporator at the evaporation temperature of 50 ℃, and then filtering the extract; mixing the formula amount of the alpine edelweiss extract with menthol in advance, and uniformly stirring to prepare a mixed solvent; the extraction of the alpine fire velvet liquid in the alpine fire velvet grass can be effectively improved through the rotary evaporator, and impurities in the alpine fire velvet liquid can be separated from the extracting solution through the action of centrifugal force; the penetration enhancer mint is added, so that the absorption of the skin to the extract of the alpine edelweiss can be promoted, and the effect is enhanced;
s5: filling the mixed emulsion prepared in the step S3 into a shampoo bottle, and simultaneously filling the mixed solution prepared in the step S4 into the shampoo bottle, and simultaneously separately storing the mixed emulsion and the mixed solvent through a partition 7; the mixed emulsion and the mixed solvent are independently stored, so that the phenomenon that a small amount of ethanol solution in the tea saponin is dissolved in menthol in the mixed solvent when the shampoo is kept still is prevented, and the using effect of the mixed solvent is further influenced; meanwhile, the phenomenon that the concentration of the tea saponin is improved due to less ethanol solution in the tea saponin is prevented.
As an embodiment of the present invention, wherein the shampoo bottle in the step S5 includes a bottle body 1, a bottle cap 2, and a liquid extracting device 3; the bottle body 1 is provided with a card reader; a partition plate 7 is arranged in the bottle body 1, and a bottle cap 2 is connected to the upper part of the bottle body 1 through threads; the liquid pumping device 3 comprises a liquid pumping nozzle 31, a pressing pipe 32, a pipe seat 33, a pressing spring 34, a liquid suction pipe 341 and a liquid distribution pipe 35; the liquid pumping nozzle 31 is movably arranged on the bottle cap 2 through a pressing pipe 32, and the pressing pipe 32 is inserted on a pipe seat 33 in a sliding way; the tube seat 33 is arranged on the bottle cap 2, and a pressing spring 34 is inserted in the tube seat 33; the bottom end of the pipe seat 33 is connected with a pipette 341, and the nozzle of the pipette 341 is positioned above the separation plate 7; the liquid-distributing pipe 35 is connected to the liquid-sucking pipe 341, and the lower end of the liquid-distributing pipe 35 is positioned below the partition plate 7; a sealing device 4 is arranged in the pipette 341; the sealing device 4 comprises a squeezing pipe 41, a mounting disc 42, a guide pipe 43, a squeezing bag 44, a sliding rod, a sealing sliding plate 46, a limiting spring 47 and a sealing disc 48; the extrusion pipe 41 is installed at the bottom end of the pressing pipe 32 through an installation disc 42, and a liquid guide groove 421 is formed in the installation disc 42; a pneumatic control valve is arranged in the extrusion pipe 41; the guide tube 43 is installed in the sealing device 4 through the installation disc 42, the top end of the guide tube 43 is provided with the extrusion bag 44, and the guide tube 43 is internally provided with a sliding rod in a sliding manner; the top end of the extrusion bladder 44 is communicated with the extrusion tube 41; a sealing sliding plate 46 is arranged at the bottom end of the sliding rod, a sealing block 49 is arranged at the bottom end of the sealing sliding plate 46, and a liquid guide groove 421 is formed in the sealing sliding plate 46; the sealing disc 48 is positioned at the bottom end of the sealing sliding plate 46, and a liquid discharge hole is formed in the sealing disc 48; a limiting spring 47 is arranged between the sealing disc 48 and the sealing sliding plate 46; the sealing block 49 corresponds to the liquid discharge hole; the bottle body 1 is provided with a control unit, and the control unit is in electric signal connection with the card reader;
when the shampoo bottle works, when a user needs to use shampoo, the user presses the liquid pumping nozzle 31, the downward movement of the liquid pumping nozzle 31 can drive the pressing pipe 32 to slide downwards in the pipe seat 33, meanwhile, the pressing pipe 32 can compress the pressing spring 34, when the user breaks away from pressing the liquid pumping nozzle 31, the suction force of the pressing pipe 32 can enable mixed emulsion and mixed solvent to enter the liquid pumping pipe 341 through the liquid pumping pipe 341 and the liquid distributing pipe 35 respectively, meanwhile, when the pressing pipe 32 moves downwards, the pressing bag 44 can be pressed through the pressing pipe 41, gas in the pressing bag 44 can enter the guide pipe 43, along with continuous pressing of the liquid pumping nozzle 31, the mixed emulsion above the separation plate 7 and the mixed solvent below the separation plate can be mixed in the liquid pumping pipe 341 and then enter the liquid pumping nozzle 31 through the pressing pipe 32 to be sprayed out, along with continuous entering of the gas in the pressing bag 44, the sealing sliding plate 46 can slide downwards to be contacted with the sealing disc 48, the sealing block 49 arranged at the bottom end of the sealing slide plate 46 blocks the liquid discharge hole, so that the shampoo in the bottle body 1 can be used in a limited amount; through the matching of the liquid extracting device 3 and the sealing device 4, the liquid extracting device 3 can mix and extract the divided mixed emulsion and the mixed solvent, so that the mixed emulsion and the mixed solvent are mixed in the liquid suction pipe 341 and the pipe seat 33, and the phenomenon that the shampoo is deteriorated due to the mixing reaction of local components in the mixed emulsion and the mixed solvent is effectively prevented; meanwhile, the sealing device 4 can be used for quantitatively using the shampoo, so that the shampoo waste phenomenon caused by malicious use of the shampoo by staff is prevented; meanwhile, the phenomenon that the tea saponin damages the scalp of a user due to excessive use of the tea saponin in the mixed emulsion when the shampoo is used is prevented; when the next user uses shampoo, the user can attach the employee card to the card reader, the card reader controls the air control valve to be opened through the control unit, the restoring force of the limiting spring 47 can enable the sealing sliding plate 46 to drive the sliding rod to move upwards, and then the sealing block 49 is separated from the liquid guide groove 421 for sealing.
In one embodiment of the present invention, an elastic liquid guiding film 5 is disposed between the sealing disc 48 and the sealing sliding plate 46, and the elastic liquid guiding film 5 is fixedly disposed on the limiting spring 47; in operation, when spacing spring 47 compresses down, the last elasticity of setting of spacing spring 47 leads liquid film 5 can improve the mixed emulsion and the intensive mixing effect of mixed solvent in pipette 341, prevents that mixed emulsion and mixed solvent can not abundant effectual mixture, and then reduces the abundant clearance effect of the silicon oil of shampoo to bonding on the user's hair, dust.
As an embodiment of the present invention, the orifice of the liquid distribution pipe 35 is located above the sealing disc 48, and the elastic membrane 6 is thermally compressed on the sealing disc 48, and one third of the outer circle of the elastic membrane 6 is thermally compressed on the sealing disc 48; the thickness of the seal sliding plate 46 and the seal disc 48 is larger than the diameter of the nozzle of the liquid distribution pipe 35; in operation, when the pressing pipe 32 presses downwards, the elastic membrane 6 is tightly attached to the sealing disk 48 by the driving force of the gas in the liquid suction pipe 341, so as to prevent the phenomenon that the mixed solvent pumped in through the liquid distribution pipe 35 enters the mixed emulsion through the liquid suction pipe 341 due to the downward pressing force of the pressing pipe 32, and further influence the separation effect of the mixed solvent and the mixed emulsion; meanwhile, when the sealing slide plate 46 and the sealing disc 48 are attached, the liquid distribution pipe 35 can be blocked by the thicknesses of the sealing slide plate 46 and the sealing disc 48, and the phenomenon that the mixed solvent in the liquid distribution pipe 35 is drawn out due to the suction force of the liquid distribution pipe 35 is prevented.
The specific working process of the shampoo is as follows:
when the shampoo bottle works, when a user needs to use shampoo, the user presses the liquid pumping nozzle 31, the downward movement of the liquid pumping nozzle 31 can drive the pressing pipe 32 to slide downwards in the pipe seat 33, meanwhile, the pressing pipe 32 can compress the pressing spring 34, when the user breaks away from pressing the liquid pumping nozzle 31, the suction force of the pressing pipe 32 can enable mixed emulsion and mixed solvent to enter the liquid pumping pipe 341 through the liquid pumping pipe 341 and the liquid distributing pipe 35 respectively, meanwhile, when the pressing pipe 32 moves downwards, the pressing bag 44 can be pressed through the pressing pipe 41, gas in the pressing bag 44 can enter the guide pipe 43, along with continuous pressing of the liquid pumping nozzle 31, the mixed emulsion above the separation plate 7 and the mixed solvent below the separation plate can be mixed in the liquid pumping pipe 341 and then enter the liquid pumping nozzle 31 through the pressing pipe 32 to be sprayed out, along with continuous entering of the gas in the pressing bag 44, the sealing sliding plate 46 can slide downwards to be contacted with the sealing disc 48, the liquid discharge hole is blocked by a sealing block 49 provided at the bottom end of the sealing slide plate 46, and the shampoo in the bottle body 1 is used in a limited amount.
In order to verify the efficacy of the shampoo and the existing shampoo in industrial enterprises, the related applicants of the invention carry out the following experimental operations of experimental examples: selecting tar and dust accumulated on hair from coal mine enterprises, wherein general workers with red and swollen scalp count 400 persons, randomly dividing the persons into 4 groups, one group, two groups, three groups and four groups, wherein each group comprises 100 persons, continuously using the shampoo provided by the invention and the conventional shampoo for one month and once every 3 days, and performing experiments on the improvement of the tar and dust accumulated on hair and the red and swollen scalp;
experiment group one:
adding sufficient water into 20 parts of sodium dodecyl sulfate, 20 parts of disodium lauroyl amphodipropionate, 8 parts of sandalwood oil, 2 parts of ammonium xylene sulfonate, 1 part of hyaluronic acid and 20 parts of natural surfactant, preparing the shampoo raw material into a shampoo emulsion by the preparation method of the shampoo, and placing the prepared emulsion into a spacious worker in a washing room for use;
experiment group two:
adding sufficient water into 20 parts of sodium dodecyl sulfate, 20 parts of disodium lauroyl amphoteric dipropionate, 8 parts of sandalwood oil, 2 parts of ammonium xylene sulfonate, 1 part of hyaluronic acid and 19 parts of mixed solvent, preparing the shampoo raw material into shampoo emulsion by the preparation method of the shampoo, and placing the prepared emulsion into a spacious worker in a washing room for use;
experiment group three:
adding sufficient water into 20 parts of sodium dodecyl sulfate, 20 parts of disodium lauroyl amphodipropionate, 8 parts of sandalwood oil, 2 parts of ammonium xylene sulfonate, 1 part of hyaluronic acid, 20 parts of natural surfactant and 19 parts of mixed solvent, preparing the shampoo raw material into shampoo emulsion by the preparation method of the shampoo, and placing the prepared emulsion into a gargle worker for use;
control group:
taking 20 parts of sodium dodecyl sulfate, 20 parts of disodium lauroyl amphoteric dipropionate, 8 parts of sandalwood oil, 2 parts of ammonium xylene sulfonate, 1 part of hyaluronic acid and sufficient water as raw materials, preparing the shampoo raw materials into a shampoo emulsion by the preparation method of the shampoo, and placing the prepared emulsion into a spacious worker in a washing room for use;
experimental tables
The experimental table shows that through comparison between a control group and an experimental group, through the matching use of the added natural surfactant and the mixed solvent, the natural surfactant adopts tea saponin which is an extract in tea leaves, the structure is triterpenoid saponin, and the triterpenoid saponin has strong surface activity, hard water resistance and foaming capacity; the tea saponin has multiple functions of emulsification, decontamination, wetting, dispersion, foaming and the like; the skin care essence of the edelweiss extracting solution is matched with the penetration enhancer menthol for use, so that the absorption of the skin on the edelweiss extracting solution can be enhanced, the action effect is enhanced, and the absorption rate is improved; meanwhile, the menthol can relieve pain to the scalp and treat red dermatitis caused by erosion of tar or dust on the scalp; compared with the experimental group I and the experimental group II, only one natural surfactant or mixed solvent is added, so that the function of slightly clearing and treating tar, dust or red swelling parts can be achieved, hyaluronic acid in the raw materials cannot promote the single natural surfactant or mixed solvent, and the using effect of the shampoo is difficult to improve.
While the invention has been described with reference to specific embodiments, it will be understood by those skilled in the art that various changes may be made and equivalents may be substituted without departing from the scope of the invention. In addition, many modifications may be made to adapt a particular situation or material to the teachings of the invention without departing from its scope. Therefore, it is intended that the invention not be limited to the particular embodiment disclosed, but that the invention will include all embodiments falling within the scope of the appended claims.
In the description of the present invention, it is to be understood that the terms "center", "front", "rear", "vertical", "horizontal", "top", "bottom", "inner", "outer", etc., indicate orientations or positional relationships based on those shown in the drawings, and are used only for convenience in describing the present invention and for simplicity in description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore, should not be taken as limiting the scope of the present invention.
Claims (3)
1. The special shampoo for industrial enterprises is characterized in that: comprises the following raw materials in parts by weight: 20 parts of sodium dodecyl sulfate, 20 parts of disodium lauroamphodipropionate, 8 parts of sandalwood oil, 2 parts of ammonium xylene sulfonate, 1 part of hyaluronic acid, 20 parts of a natural surfactant, 19 parts of a mixed solvent and the balance of water;
the natural surfactant is a low-concentration tea saponin concentrated solution; the mixed solvent is prepared by mixing the extract of the alpine edelweiss and menthol;
the preparation method of the shampoo comprises the following steps:
s1: adding sodium dodecyl sulfate, disodium lauroamphodipropionate, sandalwood oil, ammonium xylene sulfonate and hyaluronic acid into a mixing pot, adding a part of deionized water into the mixing pot, heating to 80 ℃, preserving heat and stirring for 20 minutes until the deionized water is completely dissolved to obtain a solution A;
s2: placing the dried, ground and crushed tea seed meal particles into a flat-turn leacher, adding ethanol for leaching, and extracting an ethanol saponin mixed solution at the bottom of the flat-turn leacher; putting the mixed solution of the ethanol and the saponin into a long-tube evaporator to recover most of ethanol;
filtering impurities and pigments in the solution by using activated carbon, and recovering most of water in the tea saponin by using membrane separation equipment to prepare a tea saponin concentrated solution;
s3: adding the tea saponin concentrated solution prepared in the step S2 into the solution A prepared in the step S1, stirring until no agglomeration phenomenon exists, emulsifying and concentrating the mixed raw materials through a vacuum emulsifying pot until the maximum temperature is not more than 75 ℃, and stirring until all components are completely dissolved;
s4: soaking fresh or dried Hibiscus alpinus Leontopodium herb in purified water in an extraction tank for 1 h; extracting the extract by using a rotary evaporator at the evaporation temperature of 50 ℃, and then filtering the extract; mixing the formula amount of the alpine edelweiss extract with menthol in advance, and uniformly stirring to prepare a mixed solvent;
s5: filling the mixed emulsion prepared in the step S3 into a shampoo bottle, simultaneously filling the mixed solution prepared in the step S4 into the shampoo bottle, and simultaneously separately storing the mixed emulsion and the mixed solvent through a partition plate (7);
wherein, the shampoo bottle in the step S5 comprises a bottle body (1), a bottle cap (2) and a liquid pumping device (3); a card reader is arranged on the bottle body (1); a partition plate (7) is arranged in the bottle body (1), and a bottle cap (2) is connected to the upper part of the bottle body (1) in a threaded manner; the liquid pumping device (3) comprises a liquid pumping nozzle (31), a pressing pipe (32), a pipe seat (33), a pressing spring (34), a liquid suction pipe (341) and a liquid distribution pipe (35); the liquid pumping nozzle (31) is movably arranged on the bottle cap (2) through a pressing pipe (32), and the pressing pipe (32) is inserted on the pipe seat (33) in a sliding manner; the tube seat (33) is arranged on the bottle cap (2), and a pressing spring (34) is inserted in the tube seat (33); the bottom end of the pipe seat (33) is connected with a pipette (341), and the pipe orifice of the pipette (341) is positioned above the separation plate (7); a liquid separating pipe (35) is connected to the liquid suction pipe (341), and the lower end of the liquid separating pipe (35) is positioned below the partition plate (7); a sealing device (4) is arranged in the pipette (341); the sealing device (4) comprises an extrusion pipe (41), a mounting disc (42), a guide pipe (43), an extrusion bag (44), a sliding rod, a sealing sliding plate (46), a limiting spring (47) and a sealing disc (48); the extrusion pipe (41) is installed at the bottom end of the pressing pipe (32) through an installation disc (42), and a liquid guide groove (421) is formed in the installation disc (42); a pneumatic control valve is arranged in the extrusion pipe (41); the guide pipe (43) is installed in the sealing device (4) through an installation disc (42), the top end of the guide pipe (43) is provided with a squeezing bag (44), and a sliding rod is arranged in the guide pipe (43) in a sliding manner; the top end of the extrusion bag (44) is communicated with the extrusion pipe (41); a sealing sliding plate (46) is arranged at the bottom end of the sliding rod, a sealing block (49) is arranged at the bottom end of the sealing sliding plate (46), and a liquid guide groove (421) is formed in the sealing sliding plate (46); the sealing disc (48) is positioned at the bottom end of the sealing sliding plate (46), and a liquid discharge hole is formed in the sealing disc (48); a limit spring (47) is arranged between the sealing disc (48) and the sealing sliding plate (46); the sealing block (49) corresponds to the liquid discharge hole; the bottle body (1) is provided with a control unit, and the control unit is in electric signal connection with the card reader.
2. The shampoo special for industrial enterprises according to claim 1, wherein the shampoo comprises the following components in percentage by weight: an elastic liquid guide film (5) is arranged between the sealing disc (48) and the sealing sliding plate (46), and the elastic liquid guide film (5) is fixedly arranged on the limiting spring (47).
3. The shampoo special for industrial enterprises according to claim 2, wherein: the pipe orifice of the liquid distribution pipe (35) is positioned above the sealing disc (48), the elastic membrane (6) is thermally pressed on the sealing disc (48), and one third of the excircle of the elastic membrane (6) is thermally pressed on the sealing disc (48); the thickness of the sealing slide plate (46) and the sealing disc (48) is larger than the diameter of the nozzle of the liquid distribution pipe (35).
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