CN110934782A - Moisturizing and hand-protecting cream containing deep seawater and preparation method thereof - Google Patents

Moisturizing and hand-protecting cream containing deep seawater and preparation method thereof Download PDF

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CN110934782A
CN110934782A CN201911330474.1A CN201911330474A CN110934782A CN 110934782 A CN110934782 A CN 110934782A CN 201911330474 A CN201911330474 A CN 201911330474A CN 110934782 A CN110934782 A CN 110934782A
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raw material
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deep seawater
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glycerol
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张应贤
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Guangzhou Lakel Stem Cell Research Institute
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Guangzhou Lakel Stem Cell Research Institute
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9717Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/678Tocopherol, i.e. vitamin E
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    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K2800/30Characterized by the absence of a particular group of ingredients
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82Preparation or application process involves sonication or ultrasonication

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Abstract

The invention discloses moisturizing and hand-protecting cream containing deep seawater and a preparation method thereof, and relates to the technical field of skin care products. The feed comprises the following raw materials in parts by weight: 0.5% of hydrolyzed red algae extract, 0.5% of deep seawater, 0.2% of shea butter extract, 0.3% of tocopherol acetate, 3% of cetostearyl alcohol, 0.5% of cetostearyl polyether, 4% of polydimethylsiloxane, 12% of shea butter, 1% of petrolatum, 1% of glyceryl stearate, 1% of PEG-100 stearate, 0.5% of squalane, 1% of sunflower seed oil, 0.1% of xanthan gum, 6% of glycerol, 0.1% of methyl hydroxybenzoate, 0.1% of propyl hydroxybenzoate, 0.2% of polyacrylamide, 0.2% of C13-14 isoparaffin, 70.3% of laureth, 1% of starch octenyl aluminum succinate, 0.3% of panthenol, 0.3% of phenoxyethanol, 0.3% of ethylhexyl glycerol, 0.5% of PEG/PPG/polybutylene glycol-8/5/3 glycerol, 0.05% of sodium dilaurylamido-glutamine lysine, 0.5% of lecithin, 0.1 percent of urea and 64.45 percent of deionized water. The moistening and preventing hand cream containing deep seawater has the effects of promoting blood circulation for removing blood stasis, moistening skin and keeping moisture.

Description

Moisturizing and hand-protecting cream containing deep seawater and preparation method thereof
Technical Field
The invention relates to the technical field of skin care products, in particular to moisturizing and anti-hand cream containing deep seawater and a preparation method thereof.
Background
The hand cream is a skin care product which can heal and smooth skin cracks and dryness and can effectively prevent and treat rough and dry hands, hands of people in labor are in contact with various substances in the nature, so the skin on the hands is most easily damaged, the hands are often in contact with water and detergent, the back of the hands has few sebaceous glands, oil and water are required to be supplemented frequently, otherwise the skin becomes rough and dry, various hand skin problems such as dryness, itching, agnail, desquamation, cracking and the like occur, therefore, no matter in winter and summer, the hand cream is very important to be carried with, can moisten and protect the hands in time, particularly after washing hands, after housework and before leaving a door, white-collar office workers often work against a computer in an air-conditioning office building, because the humidity in an air-conditioning room is low, and the hands are dry due to the addition of some radiation of the computer, outdoor workers suffer from stimulation and damage of wind sand and ultraviolet rays to the skin, hand aging phenomena such as skin darkness, fine wrinkles and obvious chap are all said to be the second face, and along with the improvement of living standard, hand protection is also a part of body skin care, and people pay more attention to hand maintenance.
The hand cream in the prior art has the advantages of unsatisfactory effect, short moisturizing action time, poor bacteriostatic ability and almost no effect of repairing hand wounds in the using process, so that the hand cream has an unsatisfactory hand skin protecting effect, and the hand cream containing deep seawater is widely used by people, wherein the deep seawater is seawater in a deep sea part which is more than 200 meters below sea level. In such depths, photosynthesis can not be carried out, water quality is stable and clean, the decomposition speed of organic matters is far higher than the synthesis speed of the organic matters, so that most of trace element mineral matters such as calcium, zinc, selenium and sodium serving as fertilizers are preserved, and the organic matters have the characteristics of low temperature, rich mineral matters and the like, so that the nutrition of the organic matters is very rich, conditions are provided for utilizing deep seawater, and meanwhile, the deep seawater is water which is hardly polluted and has few germs, so that the hand skin is conveniently protected.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides moisturizing and hand-protecting cream containing deep seawater and a preparation method thereof, and aims to solve the problems in the background art.
In order to achieve the purpose, the invention provides the following technical scheme: the moisturizing and hand-protecting cream containing deep seawater comprises the following raw materials in parts by weight: 0.2 to 0.6 percent of hydrolyzed red algae extract, 0.3 to 0.5 percent of deep seawater, 0.1 to 0.2 percent of shea butter extract, 0.1 to 0.3 percent of tocopherol acetate, 1 to 3 percent of cetearyl alcohol, 0.1 to 0.5 percent of ceteareth-250.1, 2 to 4 percent of polydimethylsiloxane, 8 to 12 percent of shea butter, 0.5 to 1 percent of petrolatum, 0.4 to 1 percent of glycerol stearate, 0.6 to 1 percent of PEG-100 stearate, 0.2 to 0.5 percent of squalane, 0.8 to 1.5 percent of sunflower seed oil, 0.05 to 0.15 percent of xanthan gum, 3 to 6 percent of glycerol, 0.05 to 0.1 percent of methyl hydroxybenzoate, 0.05 to 0.1 percent of propyl hydroxybenzoate, 0.05 to 0.2 percent of polyacrylamide, 0.05 to 0.2 percent of C13 to 14 isoparaffin, 0.1 to 0.3 percent of laureth-70.1, and 0.5 to 1 percent of aluminum octenyl succinate, 0.05-0.3% of panthenol, 0.15-0.3% of phenoxyethanol, 0.1-0.3% of ethylhexyl glycerol, 0.2-0.5% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol, 0.01-0.05% of sodium di (lauramide glutamine) lysine, 0.3-0.5% of lecithin, 0.05-0.15% of urea and 100% of deionized water.
A preparation method of moistening and hand-protecting cream containing deep seawater comprises the following steps:
s1, preparing a first raw material: weighing the required tocopherol acetate, cetostearyl alcohol, polydimethylsiloxane, shea butter, petrolatum, glyceryl stearate, PEG-100 stearate, squalane, sunflower seed oil, lecithin and cetostearyl polyether-25 according to the proportion, and adding the mixture into a first beaker for later use;
s2, preparation of a first raw material: heating the raw material in the beaker I in the step S1, uniformly stirring the raw material to completely and uniformly disperse the raw material in the beaker I to obtain the required raw material I, and keeping the temperature for later use;
s3, standby two of raw materials: weighing required xanthan gum, urea, glycerol, methyl hydroxybenzoate, propyl hydroxybenzoate and deionized water in proportion, and adding into the beaker II for later use;
s4, preparation of a raw material II: uniformly dispersing the raw material in the beaker II in the step S3 by using ultrasonic waves, heating to completely dissolve the raw material to obtain the required raw material II, and keeping the temperature for later use;
s5, ultrasonic emulsification: adding the raw material I obtained in the step S2 into a beaker III, sequentially adding polyacrylamide, C13-14 isoparaffin and laureth-7 into the beaker III, adding the raw material II obtained in the step S4 into the beaker III, starting an ultrasonic micronizer for emulsification, emulsifying until the mixture is completely uniform to obtain a raw material III, and cooling for later use;
s6, adding raw materials: cooling the raw material III obtained in the step S5, and adding aluminum starch octenyl succinate, sodium bis (lauramide glutamine) lysine, phenoxyethanol, ethylhexyl glycerol, PEG/PPG/polybutylene glycol-8/5/3 glycerol and panthenol in sequence while stirring to uniformly stir for later use;
s7, aging: adding the hydrolyzed red algae extract, the deep seawater and the shea butter extract into the raw material III in the step S6 in sequence, stirring and adding, and performing ultrasonic emulsification for 0.5 min;
s8, packaging: and (5) packaging the emulsified liquid in the step S5 in vacuum to obtain the required moistening and hand-protecting cream.
Further optimizing the technical scheme, the heating temperature in the step S2 is 70-75 ℃, and the heating temperature in the step S4 is 70-75 ℃.
Further optimizing the technical scheme, in the step S5, an ultrasonic micronizer is adopted for emulsification and homogenization, the ultrasonic condition is 22-25KHz, the power is 650-800 ℃, and the ultrasonic temperature is set to 65-72 ℃.
Further optimizing the technical scheme, the emulsifying time in the step S5 is 1-3min, and the temperature of the raw material III in the step S6 is reduced to 40-45 ℃.
Further optimizing the technical scheme, the deep seawater in the step S7 is taken from the sea level of 550-700 m, and is firstly filtered by a fiber filtering system and an ultrafiltration system in sequence and then prepared by a vacuum concentration system.
Advantageous effects
Compared with the prior art, the invention provides the moisturizing and hand-protecting cream containing deep seawater and the preparation method thereof, and the moisturizing and hand-protecting cream has the following beneficial effects:
1. the moisturizing and anti-hand cream containing deep seawater and the preparation method thereof have the advantages that the hand cream has a moisturizing function by the aid of the glycerin, the hand cream prepared by mixing has the effects of promoting blood circulation to remove blood stasis, resisting bacteria, whitening, moisturizing and moisturizing, meanwhile, the raw materials are emulsified by the aid of an ultrasonic micronizer, particle dispersion reaction is performed on each component by means of the characteristics of good self-directivity, strong penetration capacity, short distance and strong amplitude of ultrasonic waves, the emulsifying effect is better, the penetration of active substances is stronger, skin irritation is smaller, the excellent oxidation resistance biochemical performance of vitamin E is matched, the rough and aging phenomenon of hands is effectively improved after long-term use, each skin of the hands is moistened, the hands are wrapped lightly, the hands are moisturized deeply, chapping is prevented, the skin color is brightened, and natural gloss is developed.
2. The deep seawater in the hand cream is rich in mineral substances, can increase the capacity of skin to absorb nutrition and moisture, is matched with components such as hydrolyzed red algae extract, shea butter fruit resin extract and the like, so that the prepared hand cream is soft in skin feel, synergizes synergistically, permeates into skin, helps skin to absorb rapidly, enables the moisturizing components to permeate sufficiently, can repair skin and moisturize hands well, can form a protective film on the surface of the skin, prevents moisture evaporation, helps to strengthen and recover the moisture retention state of the skin, has a good sun protection effect on the hand skin, and can be used for centralized repair and care of hands, moisturize but not greasy, moisturize permanently and guide the hand to soft young hand skin. The capsule essence has the advantages that the activity of active ingredients in the capsule essence is well maintained, and no preservative is added in the capsule essence, so that the risk of skin sensitivity is reduced.
Drawings
Fig. 1 is a flow chart of a moisturizing and hand-protecting cream containing deep seawater and a preparation method thereof.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows: referring to fig. 1, the invention discloses a moisturizing and hand-protecting cream containing deep seawater, which comprises the following raw materials in parts by weight: 0.5% of hydrolyzed red algae extract, 0.5% of deep seawater, 0.2% of shea butter extract, 0.3% of tocopherol acetate, 3% of cetostearyl alcohol, 0.5% of cetostearyl polyether, 4% of polydimethylsiloxane, 12% of shea butter, 1% of petrolatum, 1% of glyceryl stearate, 1% of PEG-100 stearate, 0.5% of squalane, 1% of sunflower seed oil, 0.1% of xanthan gum, 6% of glycerol, 0.1% of methyl hydroxybenzoate, 0.1% of propyl hydroxybenzoate, 0.2% of polyacrylamide, 0.2% of C13-14 isoparaffin, 70.3% of laureth, 1% of starch octenyl aluminum succinate, 0.3% of panthenol, 0.3% of phenoxyethanol, 0.3% of ethylhexyl glycerol, 0.5% of PEG/PPG/polybutylene glycol-8/5/3 glycerol, 0.05% of sodium dilaurylamido-glutamine lysine, 0.5% of lecithin, 0.1 percent of urea and 64.45 percent of deionized water.
A preparation method of moistening and hand-protecting cream containing deep seawater comprises the following steps:
s1, preparing a first raw material: weighing the required tocopherol acetate, cetostearyl alcohol, polydimethylsiloxane, shea butter, petrolatum, glyceryl stearate, PEG-100 stearate, squalane, sunflower seed oil, lecithin and cetostearyl polyether-25 according to the proportion, and adding the mixture into a first beaker for later use;
s2, preparation of a first raw material: heating the raw material in the beaker I in the step S1, uniformly stirring the raw material to completely and uniformly disperse the raw material in the beaker I to obtain the required raw material I, and keeping the temperature for later use;
s3, standby two of raw materials: weighing required xanthan gum, urea, glycerol, methyl hydroxybenzoate, propyl hydroxybenzoate and deionized water in proportion, and adding into the beaker II for later use;
s4, preparation of a raw material II: uniformly dispersing the raw material in the beaker II in the step S3 by using ultrasonic waves, heating to completely dissolve the raw material to obtain the required raw material II, and keeping the temperature for later use;
s5, ultrasonic emulsification: adding the raw material I obtained in the step S2 into a beaker III, sequentially adding polyacrylamide, C13-14 isoparaffin and laureth-7 into the beaker III, adding the raw material II obtained in the step S4 into the beaker III, starting an ultrasonic micronizer for emulsification, emulsifying until the mixture is completely uniform to obtain a raw material III, and cooling for later use;
s6, adding raw materials: cooling the raw material III obtained in the step S5, and adding aluminum starch octenyl succinate, sodium bis (lauramide glutamine) lysine, phenoxyethanol, ethylhexyl glycerol, PEG/PPG/polybutylene glycol-8/5/3 glycerol and panthenol in sequence while stirring to uniformly stir for later use;
s7, aging: adding the hydrolyzed red algae extract, the deep seawater and the shea butter extract into the raw material III in the step S6 in sequence, stirring and adding, and performing ultrasonic emulsification for 0.5 min;
s8, packaging: and (5) packaging the emulsified liquid in the step S5 in vacuum to obtain the required moistening and hand-protecting cream.
As a specific optimization scheme of this embodiment, the heating temperature in step S2 is 71 ℃, and the heating temperature in step S4 is 71 ℃.
As a specific optimization scheme of this embodiment, in the step S5, an ultrasonic micronizer is used for emulsification and homogenization, the ultrasonic condition is 22-25KHz, the power is 650-800, and the ultrasonic temperature is set to 65-72 ℃.
As a specific optimization scheme of this embodiment, the time for emulsification in step S5 is 1min, and the temperature for cooling the raw material three in step S6 is 40 ℃.
As a specific optimization scheme of this embodiment, the deep seawater in step S7 is taken from the sea level of 550-700 m, and is filtered by a fiber filtration system and an ultrafiltration system in sequence, and then is obtained by a vacuum concentration system.
Example two: referring to fig. 1, the invention discloses a moisturizing and hand-protecting cream containing deep seawater, which comprises the following raw materials in parts by weight: 0.2% of hydrolyzed red algae extract, 0.3% of deep seawater, 0.1% of shea butter extract, 0.1% of tocopheryl acetate, 1% of cetostearyl alcohol, 0.1% of ceteareth-250.1%, 2% of polydimethylsiloxane, 8% of shea butter, 0.5% of petrolatum, 0.4% of glyceryl stearate, 0.6% of PEG-100 stearate, 0.2% of squalane, 0.8% of sunflower seed oil, 0.1% of xanthan gum, 3% of glycerol, 0.05% of methyl hydroxybenzoate, 0.05% of propylparaben, 0.05% of polyacrylamide, 0.05% of C13-14 isoparaffin, 70.1% of laureth-1%, 0.5% of starch octenyl succinic acid aluminum, 0.05% of panthenol, 0.15% of phenoxyethanol, 0.1% of ethylhexylglycerin, 0.2% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerin, 0.01% of sodium dilauramide glutamine), 0.3% of lecithin, 0.05 percent of urea and 79.99 percent of deionized water.
A preparation method of moistening and hand-protecting cream containing deep seawater comprises the following steps:
s1, preparing a first raw material: weighing the required tocopherol acetate, cetostearyl alcohol, polydimethylsiloxane, shea butter, petrolatum, glyceryl stearate, PEG-100 stearate, squalane, sunflower seed oil, lecithin and cetostearyl polyether-25 according to the proportion, and adding the mixture into a first beaker for later use;
s2, preparation of a first raw material: heating the raw material in the beaker I in the step S1, uniformly stirring the raw material to completely and uniformly disperse the raw material in the beaker I to obtain the required raw material I, and keeping the temperature for later use;
s3, standby two of raw materials: weighing required xanthan gum, urea, glycerol, methyl hydroxybenzoate, propyl hydroxybenzoate and deionized water in proportion, and adding into the beaker II for later use;
s4, preparation of a raw material II: uniformly dispersing the raw material in the beaker II in the step S3 by using ultrasonic waves, heating to completely dissolve the raw material to obtain the required raw material II, and keeping the temperature for later use;
s5, ultrasonic emulsification: adding the raw material I obtained in the step S2 into a beaker III, sequentially adding polyacrylamide, C13-14 isoparaffin and laureth-7 into the beaker III, adding the raw material II obtained in the step S4 into the beaker III, starting an ultrasonic micronizer for emulsification, emulsifying until the mixture is completely uniform to obtain a raw material III, and cooling for later use;
s6, adding raw materials: cooling the raw material III obtained in the step S5, and adding aluminum starch octenyl succinate, sodium bis (lauramide glutamine) lysine, phenoxyethanol, ethylhexyl glycerol, PEG/PPG/polybutylene glycol-8/5/3 glycerol and panthenol in sequence while stirring to uniformly stir for later use;
s7, aging: adding the hydrolyzed red algae extract, the deep seawater and the shea butter extract into the raw material III in the step S6 in sequence, stirring and adding, and performing ultrasonic emulsification for 0.5 min;
s8, packaging: and (5) packaging the emulsified liquid in the step S5 in vacuum to obtain the required moistening and hand-protecting cream.
As a specific optimization scheme of this embodiment, the temperature heated in step S2 is 72 ℃, and the temperature heated in step S4 is 72 ℃.
As a specific optimization scheme of this embodiment, in the step S5, an ultrasonic micronizer is used for emulsification and homogenization, the ultrasonic condition is 22-25KHz, the power is 650-800, and the ultrasonic temperature is set to 65-72 ℃.
As a specific optimization scheme of this embodiment, the time for emulsification in step S5 is 2min, and the temperature for reducing the temperature of the raw material three in step S6 is 42 ℃.
As a specific optimization scheme of this embodiment, the deep seawater in step S7 is taken from the sea level of 550-700 m, and is filtered by a fiber filtration system and an ultrafiltration system in sequence, and then is obtained by a vacuum concentration system.
Example three: referring to fig. 1, the invention discloses a moisturizing and hand-protecting cream containing deep seawater, which comprises the following raw materials in parts by weight: 0.6% of hydrolyzed red algae extract, 0.5% of deep seawater, 0.2% of shea butter extract, 0.3% of tocopherol acetate, 3% of cetostearyl alcohol, 0.5% of cetostearyl polyether, 4% of polydimethylsiloxane, 12% of shea butter, 1% of petrolatum, 1% of glyceryl stearate, 1% of PEG-100 stearate, 0.5% of squalane, 1.5% of sunflower seed oil, 0.15% of xanthan gum, 6% of glycerol, 0.1% of methyl hydroxybenzoate, 0.1% of propyl hydroxybenzoate, 0.2% of polyacrylamide, 0.2% of C13-14 isoparaffin, 70.3% of laureth, 1% of aluminum starch octenyl succinate, 0.3% of panthenol, 0.3% of phenoxyethanol, 0.3% of ethylhexylglycerol, 0.5% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol, 0.05% of sodium dilauramidoglutamine lysine, 0.5% of lecithin, 0.15 percent of urea and 63.75 percent of deionized water.
A preparation method of moistening and hand-protecting cream containing deep seawater comprises the following steps:
s1, preparing a first raw material: weighing the required tocopherol acetate, cetostearyl alcohol, polydimethylsiloxane, shea butter, petrolatum, glyceryl stearate, PEG-100 stearate, squalane, sunflower seed oil, lecithin and cetostearyl polyether-25 according to the proportion, and adding the mixture into a first beaker for later use;
s2, preparation of a first raw material: heating the raw material in the beaker I in the step S1, uniformly stirring the raw material to completely and uniformly disperse the raw material in the beaker I to obtain the required raw material I, and keeping the temperature for later use;
s3, standby two of raw materials: weighing required xanthan gum, urea, glycerol, methyl hydroxybenzoate, propyl hydroxybenzoate and deionized water in proportion, and adding into the beaker II for later use;
s4, preparation of a raw material II: uniformly dispersing the raw material in the beaker II in the step S3 by using ultrasonic waves, heating to completely dissolve the raw material to obtain the required raw material II, and keeping the temperature for later use;
s5, ultrasonic emulsification: adding the raw material I obtained in the step S2 into a beaker III, sequentially adding polyacrylamide, C13-14 isoparaffin and laureth-7 into the beaker III, adding the raw material II obtained in the step S4 into the beaker III, starting an ultrasonic micronizer for emulsification, emulsifying until the mixture is completely uniform to obtain a raw material III, and cooling for later use;
s6, adding raw materials: cooling the raw material III obtained in the step S5, and adding aluminum starch octenyl succinate, sodium bis (lauramide glutamine) lysine, phenoxyethanol, ethylhexyl glycerol, PEG/PPG/polybutylene glycol-8/5/3 glycerol and panthenol in sequence while stirring to uniformly stir for later use;
s7, aging: adding the hydrolyzed red algae extract, the deep seawater and the shea butter extract into the raw material III in the step S6 in sequence, stirring and adding, and performing ultrasonic emulsification for 0.5 min;
s8, packaging: and (5) packaging the emulsified liquid in the step S5 in vacuum to obtain the required moistening and hand-protecting cream.
As a specific optimization scheme of this embodiment, the temperature heated in step S2 is 73 ℃, and the temperature heated in step S4 is 73 ℃.
As a specific optimization scheme of this embodiment, in the step S5, an ultrasonic micronizer is used for emulsification and homogenization, the ultrasonic condition is 22-25KHz, the power is 650-800, and the ultrasonic temperature is set to 65-72 ℃.
As a specific optimization scheme of this embodiment, the time for emulsification in step S5 is 2.5min, and the temperature for reducing the temperature of the raw material three in step S6 is 43 ℃.
As a specific optimization scheme of this embodiment, the deep seawater in step S7 is taken from the sea level of 550-700 m, and is filtered by a fiber filtration system and an ultrafiltration system in sequence, and then is obtained by a vacuum concentration system.
Example four: referring to fig. 1, the invention discloses a moisturizing and hand-protecting cream containing deep seawater, which comprises the following raw materials in parts by weight: 0.4% of hydrolyzed red algae extract, 0.4% of deep seawater, 0.15% of shea butter extract, 0.2% of tocopherol acetate, 2% of cetostearyl alcohol, 0.4% of cetostearyl polyether, 3% of polydimethylsiloxane, 10% of shea butter, 0.8% of petrolatum, 0.8% of glyceryl stearate, 0.8% of PEG-100 stearate, 0.35% of squalane, 1% of sunflower seed oil, 0.08% of xanthan gum, 5% of glycerol, 0.08% of methyl hydroxybenzoate, 0.05% of propyl hydroxybenzoate, 0.1% of polyacrylamide, 0.1% of C13-14 isoparaffin, 70.2% of laureth, 0.6% of starch octenyl aluminum succinate, 0.2% of panthenol, 0.2% of phenoxyethanol, 0.25% of ethylhexylglycerol, 0.35% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol, 0.03% of sodium dilauramide glutamine lysine, 0.4% of lecithin, 0.1 percent of urea and 71.96 percent of deionized water.
A preparation method of moistening and hand-protecting cream containing deep seawater comprises the following steps:
s1, preparing a first raw material: weighing the required tocopherol acetate, cetostearyl alcohol, polydimethylsiloxane, shea butter, petrolatum, glyceryl stearate, PEG-100 stearate, squalane, sunflower seed oil, lecithin and cetostearyl polyether-25 according to the proportion, and adding the mixture into a first beaker for later use;
s2, preparation of a first raw material: preparation of a first raw material: heating the raw material in the beaker I in the step S1, uniformly stirring the raw material to completely and uniformly disperse the raw material in the beaker I to obtain the required raw material I, and keeping the temperature for later use;
s3, standby two of raw materials: weighing required xanthan gum, urea, glycerol, methyl hydroxybenzoate, propyl hydroxybenzoate and deionized water in proportion, and adding into the beaker II for later use;
s4, preparation of a raw material II: uniformly dispersing the raw material in the beaker II in the step S3 by using ultrasonic waves, heating to completely dissolve the raw material to obtain the required raw material II, and keeping the temperature for later use;
s5, ultrasonic emulsification: adding the raw material I obtained in the step S2 into a beaker III, sequentially adding polyacrylamide, C13-14 isoparaffin and laureth-7 into the beaker III, adding the raw material II obtained in the step S4 into the beaker III, starting an ultrasonic micronizer for emulsification, emulsifying until the mixture is completely uniform to obtain a raw material III, and cooling for later use;
s6, adding raw materials: cooling the raw material III obtained in the step S5, and adding aluminum starch octenyl succinate, sodium bis (lauramide glutamine) lysine, phenoxyethanol, ethylhexyl glycerol, PEG/PPG/polybutylene glycol-8/5/3 glycerol and panthenol in sequence while stirring to uniformly stir for later use;
s7, aging: adding the hydrolyzed red algae extract, the deep seawater and the shea butter extract into the raw material III in the step S6 in sequence, stirring and adding, and performing ultrasonic emulsification for 0.5 min;
s8, packaging: and (5) packaging the emulsified liquid in the step S5 in vacuum to obtain the required moistening and hand-protecting cream.
As a specific optimization scheme of this embodiment, the heating temperature in step S2 is 74 ℃, and the heating temperature in step S4 is 74 ℃.
As a specific optimization scheme of this embodiment, in the step S5, an ultrasonic micronizer is used for emulsification and homogenization, the ultrasonic condition is 22-25KHz, the power is 650-800, and the ultrasonic temperature is set to 65-72 ℃.
As a specific optimization scheme of this embodiment, the time for emulsification in step S5 is 2.8min, and the temperature for reducing the temperature of the raw material three in step S6 is 44 ℃.
As a specific optimization scheme of this embodiment, the deep seawater in step S7 is taken from the sea level of 550-700 m, and is filtered by a fiber filtration system and an ultrafiltration system in sequence, and then is obtained by a vacuum concentration system.
Table 1 recipe table for each example
Figure BDA0002329427140000111
Figure BDA0002329427140000121
Figure BDA0002329427140000131
Example five: referring to fig. 1, the invention discloses a moisturizing and hand-protecting cream containing deep seawater, which comprises the following raw materials in parts by weight: 0.3% of hydrolyzed red algae extract, 0.3% of deep seawater, 0.13% of shea butter extract, 0.15% of tocopherol acetate, 1.5% of cetearyl alcohol, 0.250.2% of ceteareth, 2.5% of polydimethylsiloxane, 11% of shea butter, 0.6% of petrolatum, 0.6% of glyceryl stearate, 0.5% of PEG-100 stearate, 0.3% of squalane, 0.9% of sunflower seed oil, 0.07% of xanthan gum, 4% of glycerol, 0.06% of methyl hydroxybenzoate, 0.07% of propyl hydroxybenzoate, 0.15% of polyacrylamide, 0.15% of C13-14 isoparaffin, 0.15% of laureth-70.15%, 0.7% of starch octenyl succinic acid aluminum salt, 0.1% of panthenol, 0.25% of phenoxyethanol, 0.15% of ethylhexyl glycerol, 0.15% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol, 0.25% of sodium dilauramide glutamine), 0.02% of lecithin, 0.35% of lecithin, 0.08 percent of urea and 82.88 percent of deionized water.
A preparation method of moistening and hand-protecting cream containing deep seawater comprises the following steps:
s1, preparing a first raw material: weighing the required tocopherol acetate, cetostearyl alcohol, polydimethylsiloxane, shea butter, petrolatum, glyceryl stearate, PEG-100 stearate, squalane, sunflower seed oil, lecithin and cetostearyl polyether-25 according to the proportion, and adding the mixture into a first beaker for later use;
s2, preparation of a first raw material: preparation of a first raw material: heating the raw material in the beaker I in the step S1, uniformly stirring the raw material to completely and uniformly disperse the raw material in the beaker I to obtain the required raw material I, and keeping the temperature for later use;
s3, standby two of raw materials: weighing required xanthan gum, urea, glycerol, methyl hydroxybenzoate, propyl hydroxybenzoate and deionized water in proportion, and adding into the beaker II for later use;
s4, preparation of a raw material II: uniformly dispersing the raw material in the beaker II in the step S3 by using ultrasonic waves, heating to completely dissolve the raw material to obtain the required raw material II, and keeping the temperature for later use;
s5, ultrasonic emulsification: adding the raw material I obtained in the step S2 into a beaker III, sequentially adding polyacrylamide, C13-14 isoparaffin and laureth-7 into the beaker III, adding the raw material II obtained in the step S4 into the beaker III, starting an ultrasonic micronizer for emulsification, emulsifying until the mixture is completely uniform to obtain a raw material III, and cooling for later use;
s6, adding raw materials: cooling the raw material III obtained in the step S5, and adding aluminum starch octenyl succinate, sodium bis (lauramide glutamine) lysine, phenoxyethanol, ethylhexyl glycerol, PEG/PPG/polybutylene glycol-8/5/3 glycerol and panthenol in sequence while stirring to uniformly stir for later use;
s7, aging: adding the hydrolyzed red algae extract, the deep seawater and the shea butter extract into the raw material III in the step S6 in sequence, stirring and adding, and performing ultrasonic emulsification for 0.5 min;
s8, packaging: and (5) packaging the emulsified liquid in the step S5 in vacuum to obtain the required moistening and hand-protecting cream.
As a specific optimization scheme of this embodiment, the constant temperature in step S2 is 75 ℃, and the heating temperature in step S4 is 75 ℃.
As a specific optimization scheme of this embodiment, in the step S5, an ultrasonic micronizer is used for emulsification and homogenization, the ultrasonic condition is 22-25KHz, the power is 650-800, and the ultrasonic temperature is set to 65-72 ℃.
As a specific optimization scheme of this embodiment, the time for emulsification in step S5 is 3min, and the temperature for cooling the raw material three in step S6 is up to 45 ℃.
As a specific optimization scheme of this embodiment, the deep seawater in step S7 is taken from the sea level of 550-700 m, and is filtered by a fiber filtration system and an ultrafiltration system in sequence, and then is obtained by a vacuum concentration system.
Example six: referring to fig. 1, the invention discloses a moisturizing and hand-protecting cream containing deep seawater, which comprises the following raw materials in parts by weight: 0.45% of hydrolyzed red algae extract, 0.35% of deep seawater, 0.18% of shea butter extract, 0.25% of tocopherol acetate, 2.5% of cetostearyl alcohol, 0.3% of ceteareth-250.3%, 3.5% of polydimethylsiloxane, 9% of shea butter, 0.7% of petrolatum, 0.7% of glyceryl stearate, 0.7% of PEG-100 stearate, 0.4% of squalane, 1.2% of sunflower seed oil, 0.12% of xanthan gum, 4.5% of glycerol, 0.07% of methyl hydroxybenzoate, 0.08% of propylhydroxybenzoate, 0.17% of polyacrylamide, 0.17% of C13-14 isopropyl, 0.17% of laureth-70.25%, 0.8% of starch octenyl paraffinosuccinate, 0.25% of panthenol, 0.28% of phenoxyethanol, 0.28% of ethylhexyl glycerol, 0.28% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol, 0.4% of sodium dilauramide glutamine lysine, 0.04% of lecithin, 0.45% of lecithin, 0.13 percent of urea and 89.66 percent of deionized water.
A preparation method of moistening and hand-protecting cream containing deep seawater comprises the following steps:
s1, preparing a first raw material: weighing the required tocopherol acetate, cetostearyl alcohol, polydimethylsiloxane, shea butter, petrolatum, glyceryl stearate, PEG-100 stearate, squalane, sunflower seed oil, lecithin and cetostearyl polyether-25 according to the proportion, and adding the mixture into a first beaker for later use;
s2, preparation of a first raw material: heating the raw material in the beaker I in the step S1, uniformly stirring the raw material to completely and uniformly disperse the raw material in the beaker I to obtain the required raw material I, and keeping the temperature for later use;
s3, standby two of raw materials: weighing required xanthan gum, urea, glycerol, methyl hydroxybenzoate, propyl hydroxybenzoate and deionized water in proportion, and adding into the beaker II for later use;
s4, preparation of a raw material II: uniformly dispersing the raw material in the beaker II in the step S3 by using ultrasonic waves, heating to completely dissolve the raw material to obtain the required raw material II, and keeping the temperature for later use;
s5, ultrasonic emulsification: adding the raw material I obtained in the step S2 into a beaker III, sequentially adding polyacrylamide, C13-14 isoparaffin and laureth-7 into the beaker III, adding the raw material II obtained in the step S4 into the beaker III, starting an ultrasonic micronizer for emulsification, emulsifying until the mixture is completely uniform to obtain a raw material III, and cooling for later use;
s6, adding raw materials: cooling the raw material III obtained in the step S5, and adding aluminum starch octenyl succinate, sodium bis (lauramide glutamine) lysine, phenoxyethanol, ethylhexyl glycerol, PEG/PPG/polybutylene glycol-8/5/3 glycerol and panthenol in sequence while stirring to uniformly stir for later use;
s7, aging: adding the hydrolyzed red algae extract, the deep seawater and the shea butter extract into the raw material III in the step S6 in sequence, stirring and adding, and performing ultrasonic emulsification for 0.5 min;
s8, packaging: and (5) packaging the emulsified liquid in the step S5 in vacuum to obtain the required moistening and hand-protecting cream.
As a specific optimization scheme of this embodiment, the heating temperature in step S2 is 70 ℃, and the heating temperature in step S4 is 72 ℃.
As a specific optimization scheme of this embodiment, in the step S5, an ultrasonic micronizer is used for emulsification and homogenization, the ultrasonic condition is 22-25KHz, the power is 650-800, and the ultrasonic temperature is set to 65-72 ℃.
As a specific optimization scheme of this embodiment, the time for emulsification in step S5 is 1.5min, and the temperature for reducing the temperature of the raw material three in step S6 is 43 ℃.
As a specific optimization scheme of this embodiment, the deep seawater in step S7 is taken from the sea level of 550-700 m, and is filtered by a fiber filtration system and an ultrafiltration system in sequence, and then is obtained by a vacuum concentration system.
Experimental example: examples 1-4 were prepared using the preparation provided in example 6.
Comparative example 1 differs from example 1 in that 0.65% of hydrolyzed red algae extract, 0.55% of deep seawater, and 0.25% of fruit fat extract of Butyrospermum PARKII (Butyrrhiza PARKII) were added.
Comparative example 2 differs from example 1 in that 0.15% of hydrolyzed red algae extract, 0.25% of deep seawater, and 0.05% of fruit fat extract of Butyrospermum PARKII (Butyrrhiza PARKII) were added.
Comparative example 3 differs from example 1 in that 0.5% of hydrolyzed red algae extract and 0.2% of shea butter extract (Butyrospermum PARKII) were added.
Comparative example 4 is different from example 1 in that it is prepared by the preparation method of example 5.
Comparative example 5 differs from example 1 in that no hydrolyzed red algae extract, deep seawater, shea butter extract were added.
A control group was a commercially available shea butter hand cream.
And (4) judging the standard: sensory evaluation 30 subjects in each group were selected, bean-size hand cream was uniformly applied on the hands, the palm was massaged with the palm to generate heat, the back of the hand was massaged spirally, and the skin was left for 1 minute and scored.
Table 2: sensory evaluation table for each experimental group
Figure BDA0002329427140000171
Measuring the moisture content of the epidermis/upper dermis
30 subjects were selected for each group, the moisture content of the hand skin before and after 5 minutes of application of the hand cream was measured, 3 times of data were measured before and after the same test site, and the average value was taken for comparative evaluation.
Table 3: moisture content of each group of epidermis layer/upper dermis layer
Figure BDA0002329427140000181
And (4) judging the standard: through comparison of six embodiments, the best effect is the first embodiment, and therefore, the first embodiment is selected as the best embodiment, and the specific change of the amount also belongs to the protection scope of the technical scheme.
The invention has the beneficial effects that: according to the moistening and anti-hand cream containing deep seawater and the preparation method thereof, the hand cream has a moisturizing function by arranging the glycerin, the hand cream prepared by mixing has the effects of activating blood circulation to dissipate blood stasis, resisting bacteria, whitening, moisturizing and moisturizing, and meanwhile, the raw materials are emulsified by adopting an ultrasonic micro-analyzer, and the characteristics of good self-directivity, strong penetration capacity, short distance and strong amplitude are utilized to carry out particle dispersion reaction on each component, so that the emulsifying effect is better, the penetration of active substances is stronger, the skin irritation is smaller, the excellent oxidation resistance biochemical performance of vitamin E is matched, the rough and aging phenomenon of hands is effectively improved after long-term use, each skin of the hands is moistened, the hands are wrapped with the skin lightly, the hands are deeply moisturized, the hands are prevented from chapping, the skin color is brightened, and the natural gloss is exerted; the deep seawater in the hand cream disclosed by the invention is rich in mineral substances, can increase the capability of skin to absorb nutrition and moisture, and is matched with the components such as the hydrolyzed red algae extract and the shea butter fruit resin extract, so that the prepared hand cream is soft in skin feel, synergistic, capable of permeating into the skin to help the skin to absorb rapidly, and capable of fully permeating the moisturizing components, well repairing the skin and moisturizing the hands, and capable of forming a protective film on the surface of the skin, thereby preventing moisture evaporation, helping to strengthen and restore the skin moisturizing state, having a good sunscreen effect on the hand skin, and feeling the centralized repair of the hands, and being moist but not greasy, lasting and moisturizing and guiding to soft young hand skin. The capsule essence has the advantages that the activity of active ingredients in the capsule essence is well maintained, and no preservative is added in the capsule essence, so that the risk of skin sensitivity is reduced.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. The moisturizing and hand-protecting cream containing deep seawater is characterized by comprising the following raw materials in parts by weight: 0.2 to 0.6 percent of hydrolyzed red algae extract, 0.3 to 0.5 percent of deep seawater, 0.1 to 0.2 percent of shea butter extract, 0.1 to 0.3 percent of tocopherol acetate, 1 to 3 percent of cetearyl alcohol, 0.1 to 0.5 percent of ceteareth-250.1, 2 to 4 percent of polydimethylsiloxane, 8 to 12 percent of shea butter, 0.5 to 1 percent of petrolatum, 0.4 to 1 percent of glycerol stearate, 0.6 to 1 percent of PEG-100 stearate, 0.2 to 0.5 percent of squalane, 0.8 to 1.5 percent of sunflower seed oil, 0.05 to 0.15 percent of xanthan gum, 3 to 6 percent of glycerol, 0.05 to 0.1 percent of methyl hydroxybenzoate, 0.05 to 0.1 percent of propyl hydroxybenzoate, 0.05 to 0.2 percent of polyacrylamide, 0.05 to 0.2 percent of C13 to 14 isoparaffin, 0.1 to 0.3 percent of laureth-70.1, and 0.5 to 1 percent of aluminum octenyl succinate, 0.05-0.3% of panthenol, 0.15-0.3% of phenoxyethanol, 0.1-0.3% of ethylhexyl glycerol, 0.2-0.5% of PEG/PPG/polytetramethylene glycol-8/5/3 glycerol, 0.01-0.05% of sodium di (lauramide glutamine) lysine, 0.3-0.5% of lecithin, 0.05-0.15% of urea and 100% of deionized water.
2. A preparation method of moistening and hand-protecting cream containing deep seawater comprises the following steps:
s1, preparing a first raw material: weighing the required tocopherol acetate, cetostearyl alcohol, polydimethylsiloxane, shea butter, petrolatum, glyceryl stearate, PEG-100 stearate, squalane, sunflower seed oil, lecithin and cetostearyl polyether-25 according to the proportion, and adding the mixture into a first beaker for later use;
s2, preparation of a first raw material: heating the raw material in the beaker I in the step S1, uniformly stirring the raw material to completely and uniformly disperse the raw material in the beaker I to obtain the required raw material I, and keeping the temperature for later use;
s3, standby two of raw materials: weighing required xanthan gum, urea, glycerol, methyl hydroxybenzoate, propyl hydroxybenzoate and deionized water in proportion, and adding into the beaker II for later use;
s4, preparation of a raw material II: uniformly dispersing the raw material in the beaker II in the step S3 by using ultrasonic waves, heating to completely dissolve the raw material to obtain the required raw material II, and keeping the temperature for later use;
s5, ultrasonic emulsification: adding the raw material I obtained in the step S2 into a beaker III, sequentially adding polyacrylamide, C13-14 isoparaffin and laureth-7 into the beaker III, adding the raw material II obtained in the step S4 into the beaker III, starting an ultrasonic micronizer for emulsification, emulsifying until the mixture is completely uniform to obtain a raw material III, and cooling for later use;
s6, adding raw materials: cooling the raw material III obtained in the step S5, and adding aluminum starch octenyl succinate, sodium bis (lauramide glutamine) lysine, phenoxyethanol, ethylhexyl glycerol, PEG/PPG/polybutylene glycol-8/5/3 glycerol and panthenol in sequence while stirring to uniformly stir for later use;
s7, aging: adding the hydrolyzed red algae extract, the deep seawater and the shea butter extract into the raw material III in the step S6 in sequence, stirring and adding, and performing ultrasonic emulsification for 0.5 min;
s8, packaging: and (5) packaging the emulsified liquid in the step S5 in vacuum to obtain the required moistening and hand-protecting cream.
3. The method for preparing the moisturizing and hand-protecting cream containing deep seawater as claimed in claim 2, wherein the heating temperature in the step S2 is 70-75 ℃, and the heating temperature in the step S4 is 70-75 ℃.
4. The method as claimed in claim 2, wherein the step S5 is carried out by emulsifying and homogenizing with an ultrasonic micro-analyzer under the ultrasonic conditions of 22-25KHz and power of 650-800 ℃, and the ultrasonic temperature is set at 65-72 ℃.
5. The method for preparing the moisturizing and anti-hand cream containing deep seawater as claimed in claim 2, wherein the emulsifying time in the step S5 is 1-3min, and the temperature of the raw material III in the step S6 is reduced to 40-45 ℃.
6. The method as claimed in claim 2, wherein the deep seawater in step S7 is obtained from sea level 550-700 m deep seawater, and is obtained by sequentially filtering with a fiber filtering system and an ultra-filtering system, and then passing through a vacuum concentration system.
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