CN110897968A - Alliin moisturizing lotion and preparation method thereof - Google Patents
Alliin moisturizing lotion and preparation method thereof Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses alliin moisturizing lotion and a preparation method thereof, wherein the alliin moisturizing lotion comprises the following components in parts by weight: 70-80 parts of alliin rose juice, 8-20 parts of plant extract composition, 8-10 parts of plant protein composition, 5-10 parts of 1-3 butanediol, 0.01-1 part of polypeptide composition and 1-2 parts of hyaluronic acid; the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the alliin concentration is 0.3-1%; according to the invention, the alliin rose juice is used as a substrate, the anti-aging effect of alliin is fully utilized, the essence can obtain a good anti-oxidation effect, and the anti-oxidation and anti-aging effects are further achieved; alliin is colorless and tasteless, is easily soluble in water, and has stable components; the moisturizing lotion prepared by using alliin as a main component has the effects of effectively improving skin, strongly resisting oxidation, blackening and aging, preventing sun, preventing melanin deposition, removing stains and whitening.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to alliin moisturizing lotion.
Background
Alliin (alliin) (alliin, S-Allyl-L-cysteine sulfoxide, S-Allyl-L- (+) -cysteine and amino acids of Sacs) is one of the main bioactive substances in garlic, and accounts for 0.6-2% of the dry weight of garlic.
The unique non-protein sulfur-containing amino acid in the garlic accounts for 0.6 to 2 percent of the dry weight of the garlic. It is very soluble in water, and insoluble in absolute ethanol, chloroform, acetone, ether and benzene, and can be crystallized with diluted acetone and ethanol to obtain white needle cluster crystal. Modern medicine shows that: alliin has various pharmacological effects of resisting tumor, synergistically lowering blood pressure, resisting bacteria and virus, eliminating free radicals, protecting liver, resisting diabetes and the like. Is a unique sulfur-containing compound in garlic.
Modern medical research proves that garlic sulfur-containing amino acid represented by alliin has unique pharmacological activity. Has obvious effects of reducing blood fat, improving body immunity, sterilizing, inhibiting bacteria, resisting cold, resisting aging, promoting blood circulation, preventing cancer and resisting cancer and the like after being taken for a long time. The bactericide has the effects of inhibiting and killing various pathogenic bacteria harmful to human beings, is natural phytoncide, and has obvious bacteriostatic and bactericidal effects on pathogenic staphylococcus, pyococcus, dysentery bacillus, escherichia coli, typhoid bacillus, tubercle bacillus, diphtheria bacillus, carbon maggot bacillus, bacillus subtilis, paratyphoid bacillus, meningitis, diplococcus, vibrio cholerae, streptococcus, staphylococcus albus, schoenophyton and the like; the traditional Chinese medicine composition has treatment and prevention values on various bacterial, fungal and protozoal infections, has great effects on research and development of biological medicines, and is called as one of the greatest magical discoveries in the field of natural food and medicines in the twenty-first century by the world medical community. Alliin, a polar monomer in garlic, has attracted much attention of various national scholars in recent years.
Garlic, also known as garlic, is the underground bulb of garlic (Allium sativum L.) of Allium of Liliaceae, and is a long-standing plant used as both medicine and food. Alliin, also known as allicin, is mainly present in the cells of garlic bulbs and is colorless and odorless. Alliin is unstable in nature and is rapidly converted into Allicin (Allicin) under the action of Allinase and water at normal temperature to produce acetone and ammonia. Wherein the allicin will be further decomposed into various sulfur-containing compounds. Animal experiments prove that alliin has the effects of resisting thrombus, killing fungi and the like. The current methods for preparing alliin mainly comprise two methods: one is an extraction method, which is generally obtained by a method of firstly freezing at low temperature, then centrifuging, and separating and purifying through a column. The method has the advantages that the product has full-natural property, but has the disadvantages of low alliin content in garlic, high separation cost and low efficiency.
Alliin is a substance found and extracted from garlic and has a wide range of biological activities: the bactericidal composition has a strong killing effect on common pathogenic bacteria such as staphylococcus aureus, tubercle bacillus, meningococcus and the like, and also has a remarkable curative effect on microbial infectious diseases such as fungal infection, protozoal disease and the like; in addition, the health-care tea also has good effects of reducing blood fat, improving human immunity, resisting aging, resisting and preventing cancers and the like. At present, alliin health care products are mainly used for preventing myocardial infarction, cerebral infarction, blood fat reduction and the like abroad. In view of the excellent curative effect of alliin in preventing and treating cardiovascular and cerebrovascular diseases, the product is expected by the foreign medical health-care community, and is expected to become a new plant medicine product for resisting cardiovascular and cerebrovascular diseases worldwide after the 'ginkgo fever'.
Alliin is currently used only in the fields of medicines and foods, and is not used in the field of cosmetics, and is considered to be applied to the field of cosmetics because of its effect of promoting blood circulation to human skin.
Therefore, the invention applies the alliin to the essence liquid products in the field of cosmetics, so that the alliin can be well applied.
Disclosure of Invention
The invention aims to provide alliin moisturizing water to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
the alliin moisturizing water comprises the following components in parts by weight:
70-80 parts of alliin rose dew, 14-20 parts of plant extract composition, 8-10 parts of vegetable protein composition, 5-10 parts of 1-3 butanediol, 0.005-0.01 part of polypeptide composition, 1-2 parts of hyaluronic acid and 1-2 parts of solubilizer.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%. Allicin is generated by alliin after an alliinase chemical reaction, and the problem is that the alliin is not stable enough, the quality guarantee period of the prepared cosmetic is short, and the product popularization is not facilitated.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3; the soybean protein has rich lysine content, makes up the deficiency of oat protein and zein lysine, and makes the essential amino acid ratio of the mixed protein more approximate to the mode required by human body, thereby improving the nutritive value of the plant protein composition.
As a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
In a further embodiment of the present invention, the alliin moisturizer further comprises a skin feel modifier, which is any one of magnesium aspartate, zinc gluconate, copper gluconate, calcium pantothenate or a mixture of at least two of them.
In a further embodiment of the present invention, the skin feel modifier is 2 to 3 parts by weight.
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
Compared with the prior art, the invention has the beneficial effects that:
the moisturizing lotion prepared by using alliin as a main component has the effects of effectively improving skin quality, strongly resisting oxidation, resisting black, resisting aging, preventing sun, preventing melanin deposition, removing stains and whitening. The alliin has the effect of promoting blood circulation on human skin, has strong penetrability, and does not need to be added with chemical penetrant.
According to the invention, the alliin rose juice is used as a substrate, the anti-aging effect of alliin is fully utilized, the essence can obtain a good anti-oxidation effect, and the anti-oxidation and anti-aging effects are further achieved; alliin is colorless and tasteless, is easy to dissolve in water, has stable components, can be used for preparing cosmetics with a shelf life of up to three years, does not have the peculiar garlic smell of allicin, is more convenient to add the smell of other components, and has better cosmetic effect.
The combined plant extract essence composition is prepared by combining a plurality of natural plant essence components including a gentian extract, a lemon extract, a licorice extract, green tea carnitine, a red date extract and rice fermentation liquor, and can achieve good effects of repairing skin, resisting aging and resisting oxidation.
The vegetable protein composition compounded by the soy protein, the oat protein and the corn protein is adopted, the content of lysine in the soy protein in the vegetable protein composition is rich, the defects of the oat protein and the corn protein lysine are overcome, the proportion of essential amino acids of mixed protein is closer to the mode required by a human body, the nutritive value of the vegetable protein composition is improved, and the nutrition required by skin is provided by natural vegetable protein with high nutritive value.
Detailed Description
The present application is described in further detail below, and it should be noted that the following detailed description is provided for illustrative purposes only, and is not intended to limit the scope of the present application, which is defined by the appended claims.
Example one
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose liquid 70, plant extract composition 14, plant protein composition 8, 1-3 butanediol 5, polypeptide composition 0.005, hyaluronic acid 1, and solubilizer 1.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
The polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
The solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-butanol polyether-26, polysorbate-20 or a mixture of at least two of the above.
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
Example two
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose liquid 72, plant extract composition 15, plant protein composition 8.2, 1-3 butanediol 6, polypeptide composition 0.006, hyaluronic acid 1.2, and solubilizer 1.1.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
EXAMPLE III
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose dew 75, plant extract composition 16, plant protein composition 8.5, 1-3 butanediol 6, polypeptide composition 0.006, hyaluronic acid 1.2, and solubilizer 1.3.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
Example four
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose dew 76, plant extract composition 16, plant protein composition 8.5, 1-3 butanediol 6, polypeptide composition 0.007, hyaluronic acid 1.6, and solubilizer 1.5.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
EXAMPLE five
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose dew 78, plant extract composition 18, plant protein composition 9.5, 1-3 butanediol 9.5, polypeptide composition 0.008, hyaluronic acid 1.7, and solubilizer 1.8.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
EXAMPLE six
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose dew 79, plant extract composition 19, plant protein composition 9, 1-3 butanediol 9, polypeptide composition 0.008, hyaluronic acid 2, and solubilizer 2.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
EXAMPLE seven
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose liquid 80, plant extract composition 20, vegetable protein composition 10, 1-3 butanediol 10, polypeptide composition 0.009, hyaluronic acid 2, and solubilizer 2.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
Example eight
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose liquid 80, plant extract composition 20, plant protein composition 10, 1-3 butanediol 10, polypeptide composition 0.01, hyaluronic acid 2, and solubilizer 2.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
Example nine
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose dew 78, plant extract composition 18, plant protein composition 9.5, 1-3 butanediol 9.5, polypeptide composition 0.008, hyaluronic acid 1.7, solubilizer 1.8, and skin feeling regulator 2.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
As a further embodiment of the invention, the skin feel modifier is any one of magnesium aspartate, zinc gluconate, copper gluconate, calcium pantothenate or a mixture of at least two of them
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid, a skin feeling regulator and a solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
Example ten
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose liquor 78, plant extract composition 18, plant protein composition 9.5, 1-3 butanediol 9.5, polypeptide composition 0.008, hyaluronic acid 1.7, solubilizer 1.8, and skin feeling regulator 2.5.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
As a further embodiment of the invention, the skin feel modifier is any one of magnesium aspartate, zinc gluconate, copper gluconate, calcium pantothenate or a mixture of at least two of them
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid, a skin feeling regulator and a solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
EXAMPLE eleven
The alliin moisturizing water comprises the following components in parts by weight:
alliin rose dew 78, plant extract composition 18, plant protein composition 9.5, 1-3 butanediol 9.5, polypeptide composition 0.008, hyaluronic acid 1.7, solubilizer 1.8, and skin feeling regulator 3.
As a further scheme of the invention, the alliin rose juice is prepared by dissolving alliin in red rose juice, wherein the concentration of alliin is 0.3-1%.
As a further aspect of the present invention, the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2-3;
as a further aspect of the present invention, the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
As a further scheme of the invention, the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the mixture ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
As a further embodiment of the present invention, the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20, or a mixture of at least two thereof.
As a further embodiment of the invention, the skin feel modifier is any one of magnesium aspartate, zinc gluconate, copper gluconate, calcium pantothenate or a mixture of at least two of them
The preparation method of the alliin moisturizing lotion comprises the following steps:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid, a skin feeling regulator and a solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
Results of the experiment
The products of examples one to eight were used as samples for experiments and tests, and the experimental results were as follows:
wherein the average value of the water loss (%) in the control area in the water loss test was 40%.
It should be noted that, the components in the sampling are specifically defined as follows:
the alliin concentration of the alliin rose juice is 0.3%;
the plant extract composition comprises the following components in parts by weight:
gentian extract 2, lemon extract 1, licorice extract 1, green tea carnitine 1, red date extract 1, rice fermentation liquid 2 and seaweed extract 1;
polypeptide composition hexapeptide-8: snake venom peptide-3 ═ 1: 1;
the solubilizer is PEG-40 hydrogenated castor oil;
no skin feel modifier is included.
The above experimental results were obtained by the following experimental methods:
experimental method for determining antioxidant activity of essence by DPPH (denaturing high pH) method
Antioxidant is any substance that is present at low concentrations to effectively inhibit the oxidation reaction of free radicals, either by acting directly on the free radicals or by indirectly consuming substances that readily form free radicals, preventing further reactions from occurring.
The current research methods for free radical scavengers mainly belong to 2 types, one type is an in vitro model, and the other type is an in vivo model, wherein the DPPH method is the most common method in the in vitro model.
DPPH is also called 1, 1-diphenyl-2-trinitrophenylhydrazine, is a very stable free radical with a nitrogen center, and the stability of DPPH mainly comes from the steric hindrance of 3 benzene rings with resonance stabilization effect, so that unpaired electrons on the nitrogen atom in the middle cannot play the role of electron pairing. Its absolute ethyl alcohol solution is purple, and has maximum absorption at wavelength of 517nm, and its absorbance and concentration are in linear relation. . When a radical scavenger is added thereto, DPPH may be combined with or substituted for the radical scavenger, whereby the radical scavenging ability can be evaluated by decreasing the number of radicals, decreasing the absorbance, and decreasing the color of the solution. Namely, the antioxidant capacity was calculated by measuring the DPPH-removing effect of the sample at a wavelength of 517 nm.
Experimental materials: DPPH (1, 1-diphenyl-2-trinitrophenylhydrazine); absolute ethyl alcohol;
an experimental instrument: spectrophotometer
Preparation of DPPH stock solution
Accurately weighing 3.5mg of DPPH reagent, dissolving with absolute ethyl alcohol, quantitatively transferring into a 10mL volumetric flask, fixing the volume to a scale with the absolute ethyl alcohol, taking 2mL to 100mL volumetric flask, shaking up to obtain DPPH stock solution with the concentration of 0.0178mmol/L, and placing in a refrigerator for storage.
Measurement of two, DPPH and clearance
Adding 4.0mL of the LDPPH solution and the essence into a 10mL colorimetric tube in sequence, adding absolute ethyl alcohol to the scale, immediately mixing, measuring a light absorption value (A) at a wavelength of 517nm by using a 1cm cuvette, marking the light absorption value as Ai, then measuring the light absorption value after storing in a greenhouse in a dark place for 30min, marking the light absorption value as Aj, and marking the light absorption value as Ac in a contrast test by using an ethanol solution only added with DPPH. The radical clearance (K) was calculated as follows:
K(％)＝[1-(Ai-Aj)/Ac]*100％
the test was repeated three times, and the average value was taken as the final result.
Medicine preparation: DPPH (1, 1-diphenyl-2-trinitrophenylhydrazine);
the manufacturer: shanghai such as Ji Biotech development Inc. or Beijing Nuo Bo Laide technology Inc.;
and (4) quotation: 380 yuan/bottle; 500 yuan/bottle;
specification: 1 g/bottle;
the content is as follows: 99 percent;
the producing area: imported from Japan.
Method for testing moisture loss rate
An experimental instrument: the model is as follows:
percutaneous water loss (TEWL) determinator for AS-VT100RS
1) Subjects were uniformly cleaned of the inside of the forearm by laboratory test personnel. The subject sits still in a laboratory at a temperature of 21 + -1 deg.C, 50 + -5% RH for at least 20 minutes, during which time water and drink cannot be consumed, the forearm is exposed and remains relaxed;
2) selecting and marking two face areas, namely a product area and a comparison area, wherein the area of each area is 2cm multiplied by 2 cm;
3) testing stratum corneum water content basic value of the face area of the subject;
4) using the test sample in the product area according to the product use requirement;
5) the stratum corneum moisture content measurements of the test subject product and control zones were taken 3h later (fan on side to accelerate moisture loss).
Water loss rate (%) (measured value of water content in horny layer-water content basis value of horny layer)/water content basis value of horny layer.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the present invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the spirit of the invention, which falls within the scope of the invention.
Claims (9)
1. The alliin moisturizing lotion is characterized by comprising the following components in parts by weight:
70-80 parts of alliin rose dew, 14-20 parts of plant extract composition, 8-10 parts of vegetable protein composition, 5-10 parts of 1-3 butanediol, 0.005-0.01 part of polypeptide composition, 1-2 parts of hyaluronic acid and 1-2 parts of solubilizer.
2. The alliin moisturizing water as claimed in claim 1, wherein the alliin rose syrup is prepared by dissolving alliin in red rose syrup, wherein the alliin concentration is 0.3-1%.
3. The alliin moisturizer as claimed in claim 1, wherein the vegetable protein composition is a composition of soy protein, oat protein and corn protein, and the ratio of soy protein: oat protein: and (3) corn protein is 5-7: 1-2: 2 to 3.
4. The alliin moisturizing water as claimed in claim 1, wherein the plant extract composition comprises the following components in parts by weight:
2-3 parts of gentian extract, 1-2 parts of lemon extract, 1-3 parts of licorice extract, 1-3 parts of green tea carnitine, 1-3 parts of red date extract, 2-5 parts of rice fermentation liquor and 1-2 parts of seaweed extract.
5. The alliin moisturizing lotion as claimed in claim 1, wherein the polypeptide composition comprises hexapeptide-8 and snake venom peptide-3, and the ratio of the hexapeptide-8: 1-3 of snake venom peptide: 1 to 3.
6. The alliin moisturizing water as claimed in claim 1, wherein the solubilizer is any one of PEG-40 hydrogenated castor oil, PEG-60 hydrogenated castor oil, PPG-26-Butaneth-26, polysorbate-20 or a mixture of at least two thereof.
7. The alliin moisturizer as claimed in claim 1, wherein the alliin moisturizer further comprises a skin feel modifier, and the skin feel modifier is any one of magnesium aspartate, zinc gluconate, copper gluconate, and calcium pantothenate or a mixture of at least two thereof.
8. The alliin moisturizing lotion as claimed in claim 1, wherein the skin feel modifier is 2-3 parts by weight.
9. The method for producing alliin moisturizing water as claimed in any one of claims 1 to 6, comprising the steps of:
firstly, adding alliin rose juice into a magnetic sealed reaction kettle;
secondly, sequentially adding the gentian extract, the lemon extract, the licorice extract, the green tea carnitine, the red date extract and the rice fermentation liquor into a magnetic sealed reaction kettle, and stirring for 10-15 minutes after adding one variety; stirring for 5 hours after the addition is finished, and then standing for 2-3 hours;
thirdly, adding the vegetable protein composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fourthly, adding the polypeptide composition into a magnetic sealing reaction kettle, and stirring for 30 min; then standing for 2-3 hours;
fifthly, adding hyaluronic acid and solubilizer into the magnetic sealing reaction kettle, and stirring for 30 min;
sixthly, adding 1-3 butanediol into the magnetic sealing reaction kettle, and stirring for 10 min;
and seventhly, filling the mixture into a packaging bottle in an aseptic mode to package the mixture to obtain a finished product.
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