CN110862696A - Damp-proof Buddha incense and processing technology thereof - Google Patents

Damp-proof Buddha incense and processing technology thereof Download PDF

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CN110862696A
CN110862696A CN201911058941.XA CN201911058941A CN110862696A CN 110862696 A CN110862696 A CN 110862696A CN 201911058941 A CN201911058941 A CN 201911058941A CN 110862696 A CN110862696 A CN 110862696A
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essential oil
parts
processing residues
buddha incense
oil processing
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李开祥
曾祥艳
李军集
梁文汇
曾广宇
韦晓娟
陈金艳
彭锋
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Guangxi Zhuang Autonomous Region Forestry Research Institute
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Guangxi Zhuang Autonomous Region Forestry Research Institute
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L91/00Compositions of oils, fats or waxes; Compositions of derivatives thereof
    • AHUMAN NECESSITIES
    • A47FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
    • A47GHOUSEHOLD OR TABLE EQUIPMENT
    • A47G33/00Religious or ritual equipment in dwelling or for general use
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L1/00Compositions of cellulose, modified cellulose or cellulose derivatives
    • C08L1/02Cellulose; Modified cellulose
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/14Polymer mixtures characterised by other features containing polymeric additives characterised by shape
    • C08L2205/16Fibres; Fibrils
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/14Polymer mixtures characterised by other features containing polymeric additives characterised by shape
    • C08L2205/18Spheres

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  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
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  • Oil, Petroleum & Natural Gas (AREA)
  • Dispersion Chemistry (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a damp-proof Buddha incense and a processing technology thereof, belonging to the technical field of Buddha incense processing, wherein 50-55 parts of cinnamomum camphora essential oil processing residues, 40-45 parts of cajeput essential oil processing residues, 30-35 parts of Baeckea frutescens essential oil processing residues, 20-25 parts of citronella essential oil processing residues, 1.0-1.5 parts of nano essential oil microcapsule powder, 25-30 parts of bamboo chips, 2-4 parts of auxiliary materials and 3-6 parts of binders are added; wherein the auxiliary materials are any one of graphite powder, turpentine and white carbon black or the combination of any proportion of the graphite powder, the turpentine and the white carbon black. The invention also provides a processing technology of the moisture-proof Buddha incense, and the nanometer microcapsule technology is adopted to stably add the aromatic alcohol essential oil into the Buddha incense, so that the moisture resistance of the Buddha incense is improved, the obtained Buddha incense wet water is still combustible, the smoke gas amount and ash amount of the Buddha incense are reduced, the reutilization of waste resources can be realized, and energy is saved.

Description

Damp-proof Buddha incense and processing technology thereof
Technical Field
The invention belongs to the technical field of Buddha incense processing, and particularly relates to a moisture-proof Buddha incense and a processing technology thereof.
Background
The Buddha incense is a general name of Buddhism incense, which is often used in religious activities or places related to health preservation, and the traditional Buddha incense is generally made of incense medicines, wood powder, a binder and an additive. With the continuous development of economy and social progress, the Buddha incense is not only used in religious activities, but also widely used in refreshing, deodorizing, home health preserving, ceramic temperament and other aspects.
With the development of microcapsule technology, the nano microcapsule technology is receiving more and more attention, the microcapsule technology means that a certain target object is continuously coated by various natural or synthetic high molecular compounds without any damage to the original chemical properties of the target object, then the function of the target object is gradually presented outside again through some external stimulation or slow release action, or the function of protecting a core material is played by depending on the shielding action of a capsule wall, the diameter of the microcapsule is generally 1-500 μm, the thickness of the wall is 0.5-150 μm, and the ultra-microcapsule with the particle size below 1 μm is developed. On the basis of microcapsule technology, the nano microcapsule particles have tiny particles, are easy to disperse, can further improve the stability of products, prevent mutual interference among various components, and have good slow release effect, so the nano microcapsule particles are widely researched in a plurality of fields.
At present, most of the Buddha incense in the market is chemical incense, a large amount of additives such as chemical adhesives, chemical flame retardants, stone powder and the like are added, the weight is increased, the incense cannot be completely combusted, the ash content is large, and in addition, the Buddha incense can generate various pollutants and toxic smoke in the combustion process; the traditional Buddha incense is extinguished when being wetted in the combustion process, so that the Buddha incense is difficult to combust when rains or air humidity is high, in addition, the traditional Buddha incense is exposed to the air for a long time, the originally added oil components can be oxidized, denatured or volatilized and lost, so that the original efficacy of the traditional Buddha incense is lost, even the traditional Buddha incense generates harmful substances through denaturation, therefore, the research on the moistureproof Buddha incense with stable property, difficult loss of aroma and less ash content is urgent, and the application of the nano microcapsule technology to the field of Buddha incense becomes one of the key points in the current research.
Disclosure of Invention
Aiming at the problems, the invention provides the damp-proof Buddha incense and the processing technology thereof, the nanometer microcapsule technology is adopted, the aromatic alcohol essential oil is stably added into the Buddha incense, the stability of the Buddha incense can be improved, the fragrance lasts for a long time, and the essential oil is not easy to be oxidized.
Therefore, the scheme provided by the invention is as follows:
the damp-proof Buddha incense comprises the following raw materials in parts by weight: 50-55 parts of camphor essential oil processing residues, 40-45 parts of cajeput essential oil processing residues, 30-35 parts of baeckea frutescens essential oil processing residues, 20-25 parts of citronella essential oil processing residues, 1.0-1.5 parts of nano essential oil microcapsule powder, 25-30 parts of bamboo dust, 2-4 parts of auxiliary materials and 3-6 parts of binding agents; wherein the auxiliary materials are any one of graphite powder, turpentine and white carbon black or the combination of any proportion of the graphite powder, the turpentine and the white carbon black.
Preferably, the auxiliary materials are a composition of graphite powder, turpentine and white carbon black according to the mass ratio of 1-2:10-15: 2-4.
Furthermore, the volatile oil content of the camphor essential oil processing residues, the cajeput essential oil processing residues, the baeckea essential oil processing residues and the citronella essential oil processing residues is 2-3%.
Further, the binder is any one of sodium starch phosphate, carboxymethyl cellulose and seaweed gel or a composition thereof.
Preferably, the binder is a composition of sodium starch phosphate, carboxymethyl cellulose and seaweed gel according to a mass ratio of 4-7:1-3: 2-5.
Further, the preparation method of the nanometer essential oil microcapsule powder comprises the following steps:
(1) mixing polycyanoacrylate and polylactic acid at 30-35 deg.C, stirring, sequentially adding polystyrene and ethanol, and stirring at 8000-;
(2) adding plant essential oil into the wall material, stirring and emulsifying, mixing and stirring for 10-15min, and then homogenizing under high pressure for 20-25min to obtain an emulsion;
(3) heating the emulsion at 45-50 ℃ for 3-5 hours under the protection of nitrogen to initiate polymerization reaction, and then drying to obtain the nano essential oil microcapsule powder.
Further, in the step (1), the mass ratio of the polycyanoacrylate to the polylactic acid is 1: 10-15.
Further, in the step (1), the amount of the polystyrene is 0.5-1.5% of the mass of the polylactic acid; the dosage of the ethanol is 1.2-2.5% of the mass of the polylactic acid.
Further, in the step (2), the plant essential oil is any one of spearmint essential oil, tea tree essential oil, mint essential oil and agilawood essential oil; the mass ratio of the plant essential oil to the wall material is 1: 18-20.
The invention provides a processing technology of the moisture-proof Buddha incense, which specifically comprises the following steps:
1) removing dust particles and impurities contained in the bamboo scraps by using an electrostatic dust removal device to obtain dust-free bamboo scraps; mixing the dust-free bamboo chips with the camphor essential oil processing residues, the cajeput essential oil processing residues, the baeckea essential oil processing residues and the citronella essential oil processing residues, crushing and sieving the mixture to obtain a base material, and uniformly mixing the base material and water according to a mass ratio of 1:0.85-0.95 to obtain a mixed material;
2) drying the mixed material in an environment of 50-60 ℃ for 5-8 hours, taking out, and crushing the mixed material in a crusher until the mixed material passes through a standard sieve of 100-160 meshes to obtain a basic spice;
3) and mixing the nano essential oil microcapsule powder, the binder and the auxiliary materials into the basic spice, uniformly mixing, pressing and molding the mixture, and drying to obtain the damp-proof Buddha incense.
Further, in step 3), the adhesive should pass through a 160-mesh standard sieve of 100-.
The polycyanoacrylate, the polylactic acid, the polystyrene, the ethanol, the auxiliary materials and the binder used in the invention are purchased from chemical reagent companies at home and abroad and are directly used without being continuously purified.
The invention adds nano essential oil microcapsule powder into the Buddha incense, takes plant essential oil as a core material, takes polycyanoacrylate and polylactic acid as a composite wall material, and prepares nano essential oil microcapsule emulsion through high-pressure homogeneous emulsification. Overcomes the problems of short retention time and poor durability of the natural essential oil in the prior Buddha incense, has the advantages of no toxicity, safety and environmental protection, and has wide application value.
The invention has the following beneficial effects:
1. the invention effectively utilizes camphor tree essential oil processing residues, cajeput essential oil processing residues, baeckea frutescens essential oil processing residues and citronella essential oil processing residues, and the residues are solid residues left after extracting essential oil from camphor tree leaves, cajeput, baeckea frutescens and citronella grass, the residues are rich in various plant essential oil and cellulose components, and the residues contain a small amount of essential oil which is difficult to volatilize and not easy to lose after long-term storage, and have bacteriostatic and bactericidal effects, so that the resource recycling is realized, the production cost can be reduced, and the mite killing and bactericidal effects are facilitated.
2. The raw materials used in the invention are matched with each other and are buckled with each other in a ring-to-ring manner, particularly, the binding agent consisting of sodium starch phosphate, carboxymethyl cellulose and seaweed gel is used, the binding agent is combined with the processing residues of various essential oils to improve the hydrophobicity among the components in the Buddha incense and ensure that the wet water of the Buddha incense is still combustible, and the auxiliary materials consisting of graphite powder, turpentine and white carbon black are combined, so that the Buddha incense product has less ash, the ash is not easy to disperse, falls in a segment shape, has no sparks and is safe to use and does not generate toxic smoke.
3. The invention has simple production process, recycles various wastes, is beneficial to protecting ecological environment, reduces production cost, avoids secondary pollution to the surrounding environment and is suitable for large-scale production.
Detailed Description
The invention is further described with reference to the following examples:
example 1
The damp-proof Buddha incense comprises the following raw materials in parts by weight: 50 parts of camphor essential oil processing residues, 40 parts of cajeput essential oil processing residues, 30 parts of baeckea frutescens essential oil processing residues, 20 parts of citronella essential oil processing residues, 1.0 part of nano essential oil microcapsule powder, 25 parts of bamboo dust, 2 parts of auxiliary materials and 3 parts of binders; wherein the auxiliary material is graphite powder; the binder is sodium starch phosphate;
the preparation method of the nanometer essential oil microcapsule powder comprises the following steps:
(1) mixing polycyanoacrylate and polylactic acid at 30 ℃, uniformly stirring, sequentially adding polystyrene and ethanol, and stirring at 8000rpm for 30 minutes to obtain a wall material; the mass ratio of the polycyanoacrylate to the polylactic acid is 1: 10; the using amount of the polystyrene is 0.5 percent of the mass of the polylactic acid; the dosage of the ethanol is 1.2 percent of the mass of the polylactic acid.
(2) Adding plant essential oil into the wall material, stirring and emulsifying, mixing and stirring for 10min, and then homogenizing under high pressure for 20min to obtain an emulsion; the plant essential oil is spearmint essential oil; the mass ratio of the plant essential oil to the wall material is 1: 18;
(3) heating the emulsion at 45 ℃ for 3 hours under the protection of nitrogen to initiate polymerization reaction, and then drying to obtain the nano essential oil microcapsule powder.
The processing technology of the moisture-proof Buddha incense comprises the following steps:
1) removing dust particles and impurities contained in the bamboo scraps by using an electrostatic dust removal device to obtain dust-free bamboo scraps; mixing the dust-free bamboo chips with the camphor essential oil processing residues, the cajeput essential oil processing residues, the baeckea essential oil processing residues and the citronella essential oil processing residues, crushing and sieving the mixture to obtain a base material, and uniformly mixing the base material and water according to a mass ratio of 1:0.85 to obtain a mixed material;
2) drying the mixed material in an environment of 50 ℃ for 5 hours, taking out, and crushing in a crusher until the mixed material passes through a standard sieve of 100 meshes to obtain a basic spice;
3) mixing the nano essential oil microcapsule powder, the binder and the auxiliary materials into the basic spice, uniformly mixing, pressing and molding the mixture, and drying the mixture to obtain the damp-proof Buddha incense; the adhesive should pass through a 100 mesh standard screen.
Example 2
The damp-proof Buddha incense comprises the following raw materials in parts by weight: 55 parts of camphor essential oil processing residues, 45 parts of cajeput essential oil processing residues, 35 parts of baeckea frutescens essential oil processing residues, 25 parts of citronella essential oil processing residues, 1.5 parts of nano essential oil microcapsule powder, 30 parts of bamboo dust, 4 parts of auxiliary materials and 6 parts of bonding agents; wherein the auxiliary material is white carbon black; the binder is seaweed glue;
the preparation method of the nanometer essential oil microcapsule powder comprises the following steps:
(1) mixing polycyanoacrylate and polylactic acid, uniformly stirring at the temperature of 35 ℃, sequentially adding polystyrene and ethanol, and stirring at the rotating speed of 10000rpm for 35 minutes to obtain a wall material; the mass ratio of the polycyanoacrylate to the polylactic acid is 1: 15; the using amount of the polystyrene is 1.5 percent of the mass of the polylactic acid; the dosage of the ethanol is 2.5 percent of the mass of the polylactic acid.
(2) Adding plant essential oil into the wall material, stirring and emulsifying, mixing and stirring for 15min, and then homogenizing under high pressure for 25min to obtain an emulsion; the plant essential oil is tea tree essential oil; the mass ratio of the plant essential oil to the wall material is 1: 20;
(3) heating the emulsion at 50 ℃ for 5 hours under the protection of nitrogen to initiate polymerization reaction, and then drying to obtain the nano essential oil microcapsule powder.
The processing technology of the moisture-proof Buddha incense comprises the following steps:
1) removing dust particles and impurities contained in the bamboo scraps by using an electrostatic dust removal device to obtain dust-free bamboo scraps; mixing the dust-free bamboo chips with the camphor essential oil processing residues, the cajeput essential oil processing residues, the baeckea essential oil processing residues and the citronella essential oil processing residues, crushing and sieving the mixture to obtain a base material, and uniformly mixing the base material and water according to a mass ratio of 1:0.95 to obtain a mixed material;
2) drying the mixed material in an environment at 60 ℃ for 8 hours, taking out, and crushing in a crusher until the mixed material passes through a 160-mesh standard sieve to obtain a basic spice;
3) mixing the nano essential oil microcapsule powder, the binder and the auxiliary materials into the basic spice, uniformly mixing, pressing and molding the mixture, and drying the mixture to obtain the damp-proof Buddha incense; the adhesive should pass through a 160 mesh standard screen.
Example 3
The damp-proof Buddha incense comprises the following raw materials in parts by weight: 52 parts of camphor essential oil processing residues, 42 parts of cajeput essential oil processing residues, 32 parts of baeckea frutescens essential oil processing residues, 22 parts of citronella essential oil processing residues, 1.2 parts of nano essential oil microcapsule powder, 27 parts of bamboo dust, 3 parts of auxiliary materials and 4 parts of bonding agents; wherein the auxiliary materials are a composition of graphite powder, turpentine and white carbon black according to a mass ratio of 1:10: 2; the binder is a composition of sodium starch phosphate, carboxymethyl cellulose and seaweed gel in a mass ratio of 4:1: 2;
the preparation method of the nanometer essential oil microcapsule powder comprises the following steps:
(1) mixing polycyanoacrylate and polylactic acid, uniformly stirring at the temperature of 32 ℃, sequentially adding polystyrene and ethanol, and stirring at the rotating speed of 9000rpm for 32 minutes to obtain a wall material; the mass ratio of the polycyanoacrylate to the polylactic acid is 1: 12; the using amount of the polystyrene is 0.8 percent of the mass of the polylactic acid; the dosage of the ethanol is 1.8 percent of the mass of the polylactic acid.
(2) Adding plant essential oil into the wall material, stirring and emulsifying, mixing and stirring for 12min, and then homogenizing under high pressure for 22min to obtain an emulsion; the plant essential oil is mint essential oil; the mass ratio of the plant essential oil to the wall material is 1: 19;
(3) heating the emulsion at 47 ℃ for 4 hours under the protection of nitrogen to initiate polymerization reaction, and then drying to obtain the nano essential oil microcapsule powder.
The processing technology of the moisture-proof Buddha incense comprises the following steps:
1) removing dust particles and impurities contained in the bamboo scraps by using an electrostatic dust removal device to obtain dust-free bamboo scraps; mixing the dust-free bamboo chips with the camphor essential oil processing residues, the cajeput essential oil processing residues, the baeckea essential oil processing residues and the citronella essential oil processing residues, crushing and sieving the mixture to obtain a base material, and uniformly mixing the base material and water according to a mass ratio of 1:0.87 to obtain a mixed material;
2) drying the mixed material in an environment of 55 ℃ for 6 hours, taking out, and crushing in a crusher until the mixed material passes through a standard sieve of 120 meshes to obtain a basic spice;
3) mixing the nano essential oil microcapsule powder, the binder and the auxiliary materials into the basic spice, uniformly mixing, pressing and molding the mixture, and drying the mixture to obtain the damp-proof Buddha incense; the adhesive should pass through a 120 mesh standard screen.
Example 4
The damp-proof Buddha incense comprises the following raw materials in parts by weight: 54 parts of camphor essential oil processing residues, 43 parts of cajeput essential oil processing residues, 33 parts of baeckea frutescens essential oil processing residues, 24 parts of citronella essential oil processing residues, 1.3 parts of nano essential oil microcapsule powder, 29 parts of bamboo dust, 3 parts of auxiliary materials and 5 parts of bonding agents; wherein the auxiliary materials are a composition of graphite powder, turpentine and white carbon black according to a mass ratio of 2:15: 4; the binder is a composition of sodium starch phosphate, carboxymethyl cellulose and seaweed gel in a mass ratio of 7:3: 5;
the preparation method of the nanometer essential oil microcapsule powder comprises the following steps:
(1) mixing polycyanoacrylate and polylactic acid, uniformly stirring at the temperature of 33 ℃, sequentially adding polystyrene and ethanol, and stirring at the rotating speed of 8500rpm for 33 minutes to obtain a wall material; the mass ratio of the polycyanoacrylate to the polylactic acid is 1: 14; the using amount of the polystyrene is 1.2 percent of the mass of the polylactic acid; the dosage of the ethanol is 2.0 percent of the mass of the polylactic acid.
(2) Adding plant essential oil into the wall material, stirring and emulsifying, mixing and stirring for 14min, and then homogenizing under high pressure for 24min to obtain an emulsion; the plant essential oil is agilawood essential oil; the mass ratio of the plant essential oil to the wall material is 1: 19;
(3) heating the emulsion at 48 ℃ for 4.5 hours under the protection of nitrogen to initiate polymerization reaction, and then drying to obtain the nano essential oil microcapsule powder.
The processing technology of the moisture-proof Buddha incense comprises the following steps:
1) removing dust particles and impurities contained in the bamboo scraps by using an electrostatic dust removal device to obtain dust-free bamboo scraps; mixing the dust-free bamboo chips with the camphor essential oil processing residues, the cajeput essential oil processing residues, the baeckea essential oil processing residues and the citronella essential oil processing residues, crushing and sieving the mixture to obtain a base material, and uniformly mixing the base material and water according to a mass ratio of 1:0.92 to obtain a mixed material;
2) drying the mixed material in an environment at 58 ℃ for 7 hours, taking out, and crushing in a crusher until the mixed material passes through a standard sieve of 140 meshes to obtain a basic spice;
3) mixing the nano essential oil microcapsule powder, the binder and the auxiliary materials into the basic spice, uniformly mixing, pressing and molding the mixture, and drying the mixture to obtain the damp-proof Buddha incense; the adhesive should pass through a 140 mesh standard screen.
Example 5
The damp-proof Buddha incense comprises the following raw materials in parts by weight: 53 parts of camphor essential oil processing residues, 44 parts of cajeput essential oil processing residues, 33 parts of baeckea frutescens essential oil processing residues, 24 parts of citronella essential oil processing residues, 1.3 parts of nano essential oil microcapsule powder, 28 parts of bamboo dust, 3 parts of auxiliary materials and 5 parts of bonding agents; wherein the auxiliary materials are a composition of graphite powder, turpentine and white carbon black according to a mass ratio of 1.5:12: 3; the binder is a composition of sodium starch phosphate, carboxymethyl cellulose and seaweed gel in a mass ratio of 6:2: 3;
the preparation method of the nanometer essential oil microcapsule powder comprises the following steps:
(1) mixing polycyanoacrylate and polylactic acid, uniformly stirring at the temperature of 33 ℃, sequentially adding polystyrene and ethanol, and stirring at the rotating speed of 9500rpm for 33 minutes to obtain a wall material; the mass ratio of the polycyanoacrylate to the polylactic acid is 1: 14; the using amount of the polystyrene is 1.2 percent of the mass of the polylactic acid; the dosage of the ethanol is 2.2 percent of the mass of the polylactic acid.
(2) Adding plant essential oil into the wall material, stirring and emulsifying, mixing and stirring for 14min, and then homogenizing under high pressure for 24min to obtain an emulsion; the plant essential oil is agilawood essential oil; the mass ratio of the plant essential oil to the wall material is 1: 19;
(3) heating the emulsion at 48 ℃ for 4.5 hours under the protection of nitrogen to initiate polymerization reaction, and then drying to obtain the nano essential oil microcapsule powder.
The processing technology of the moisture-proof Buddha incense comprises the following steps:
1) removing dust particles and impurities contained in the bamboo scraps by using an electrostatic dust removal device to obtain dust-free bamboo scraps; mixing the dust-free bamboo chips with the camphor essential oil processing residues, the cajeput essential oil processing residues, the baeckea essential oil processing residues and the citronella essential oil processing residues, crushing and sieving the mixture to obtain a base material, and uniformly mixing the base material and water according to a mass ratio of 1:0.93 to obtain a mixed material;
2) drying the mixed material in an environment of 56 ℃ for 6 hours, taking out, and crushing the mixed material in a crusher until the mixed material passes through a standard sieve of 140 meshes to obtain a basic spice;
3) mixing the nano essential oil microcapsule powder, the binder and the auxiliary materials into the basic spice, uniformly mixing, pressing and molding the mixture, and drying the mixture to obtain the damp-proof Buddha incense; the adhesive should pass through a 140 mesh standard screen.
Comparative example 1
The difference compared to example 5 is that: in comparative example 1, the nano essential oil microcapsule powder was not contained, and the same amount of plant essential oil was used instead.
Comparative example 2
The difference compared to example 5 is that: the binder of comparative example 2 was replaced with an equivalent amount of a single commercially available binder and no adjuvant.
Blank control group: selecting the linear Buddha incense sold in the market.
Comparative experiment:
1. in the experiment, the performance of the examples 1-5 and the comparative examples 1-2 is tested, and a blank control group is added; the volatile oil content of each Buddha incense is detected (after the Buddha incense is placed for 60 days at room temperature), the ash form after combustion and the flammability test after surface wet water are carried out, and the experimental results are shown in table 1.
TABLE 1 results of the experiment
Content of essential oil (%) Combustion pattern Wet water condition
Example 1 3.6 Black linear shape of ash, small amount of ash and less smoke Flammable material
Example 2 3.6 Black linear shape of ash, small amount of ash and less smoke Flammable material
Example 3 3.8 Black linear shape of ash, small amount of ash and less smoke Flammable material
Example 4 3.8 Black linear shape of ash, small amount of ash and less smoke Flammable material
Example 5 3.9 Black linear shape of ash, small amount of ash and less smoke Flammable material
Comparative example 1 2.0 Black linear ashLess amount and smoke Flammable material
Comparative example 2 2.4 Black powder ash, large ash amount, large smoke, Flammable material
Blank control group 1.8 The dust is powder, and the dispersion is serious and the dust is large Non-combustible
As can be seen from Table 1, the indexes of the Buddha incense obtained in the examples 1-5 of the present invention are substantially better than those of the blank control group and the comparative examples 1-2, because the components of the examples of the present invention are combined and matched with each other to promote each other, thereby improving the quality of the Buddha incense.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, and all simple modifications and equivalent variations of the above embodiments according to the technical spirit of the present invention are included in the scope of the present invention.

Claims (9)

1. The damp-proof Buddha incense is characterized by comprising the following raw materials in parts by weight: 50-55 parts of camphor essential oil processing residues, 40-45 parts of cajeput essential oil processing residues, 30-35 parts of baeckea frutescens essential oil processing residues, 20-25 parts of citronella essential oil processing residues, 1.0-1.5 parts of nano essential oil microcapsule powder, 25-30 parts of bamboo dust, 2-4 parts of auxiliary materials and 3-6 parts of binding agents; wherein the auxiliary materials are any one of graphite powder, turpentine and white carbon black or the combination of any proportion of the graphite powder, the turpentine and the white carbon black.
2. The moisture-proof Buddha incense of claim 1, wherein the volatile oil content of the camphor essential oil processing residues, the cajeput essential oil processing residues, the baeckea essential oil processing residues and the citronella essential oil processing residues is 2-3%.
3. The moisture resistant Buddha incense as claimed in claim 1, wherein the binder is any one of sodium starch phosphate, carboxymethyl cellulose, seaweed gel, or a combination thereof.
4. The moisture-proof Buddha incense as claimed in claim 1, wherein the preparation method of the nanometer essential oil microcapsule powder comprises the following steps:
(1) mixing polycyanoacrylate and polylactic acid at 30-35 deg.C, stirring, sequentially adding polystyrene and ethanol, and stirring at 8000-;
(2) adding plant essential oil into the wall material, stirring and emulsifying, mixing and stirring for 10-15min, and then homogenizing under high pressure for 20-25min to obtain an emulsion;
(3) heating the emulsion at 45-50 ℃ for 3-5 hours under the protection of nitrogen to initiate polymerization reaction, and then drying to obtain the nano essential oil microcapsule powder.
5. The moisture resistant Buddha incense as claimed in claim 4, wherein in step (1), the mass ratio of the polycyanoacrylate to the polylactic acid is 1: 10-15.
6. The moisture-proof Buddha incense as claimed in claim 4, wherein in step (1), the polystyrene is used in an amount of 0.5-1.5% by mass of the polylactic acid; the dosage of the ethanol is 1.2-2.5% of the mass of the polylactic acid.
7. The moisture resistant Buddha incense as claimed in claim 4, wherein in step (2), the plant essential oil is any one of spearmint essential oil, tea tree essential oil, mint essential oil and agilawood essential oil; the mass ratio of the plant essential oil to the wall material is 1: 18-20.
8. The processing technology of the moisture-proof Buddha incense as claimed in any one of claims 1 to 7, which comprises the following steps:
1) removing dust particles and impurities contained in the bamboo scraps by using an electrostatic dust removal device to obtain dust-free bamboo scraps; mixing the dust-free bamboo chips with the camphor essential oil processing residues, the cajeput essential oil processing residues, the baeckea essential oil processing residues and the citronella essential oil processing residues, crushing and sieving the mixture to obtain a base material, and uniformly mixing the base material and water according to a mass ratio of 1:0.85-0.95 to obtain a mixed material;
2) drying the mixed material in an environment of 50-60 ℃ for 5-8 hours, taking out, and crushing the mixed material in a crusher until the mixed material passes through a standard sieve of 100-160 meshes to obtain a basic spice;
3) and mixing the nano essential oil microcapsule powder, the binder and the auxiliary materials into the basic spice, uniformly mixing, pressing and molding the mixture, and drying to obtain the damp-proof Buddha incense.
9. The process for producing moisture-proof Buddha incense as claimed in claim 8, wherein in step 3), the adhesive should pass through a 160-mesh standard sieve of 100 meshes.
CN201911058941.XA 2019-11-01 2019-11-01 Damp-proof Buddha incense and processing technology thereof Pending CN110862696A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113278301A (en) * 2021-05-21 2021-08-20 江西省林业科学院 Degradable container for camphor tree essential oil extraction residues and preparation method and application thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107027823A (en) * 2017-04-24 2017-08-11 陈毅坚 A kind of environment-friendly type Buddhist perfume (or spice) and preparation method thereof
CN107412830A (en) * 2017-06-19 2017-12-01 吉安市高盛生物科技发展有限公司 A kind of kapur and preparation method thereof
CN107969890A (en) * 2017-11-24 2018-05-01 泉州永春达盛香业股份有限公司 A kind of resistance to burning Buddhist perfume (or spice) of high density and preparation method thereof
CN109044069A (en) * 2018-08-09 2018-12-21 广州暨南生物医药研究开发基地有限公司 A kind of wormwood Buddhist perfume (or spice) and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107027823A (en) * 2017-04-24 2017-08-11 陈毅坚 A kind of environment-friendly type Buddhist perfume (or spice) and preparation method thereof
CN107412830A (en) * 2017-06-19 2017-12-01 吉安市高盛生物科技发展有限公司 A kind of kapur and preparation method thereof
CN107969890A (en) * 2017-11-24 2018-05-01 泉州永春达盛香业股份有限公司 A kind of resistance to burning Buddhist perfume (or spice) of high density and preparation method thereof
CN109044069A (en) * 2018-08-09 2018-12-21 广州暨南生物医药研究开发基地有限公司 A kind of wormwood Buddhist perfume (or spice) and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113278301A (en) * 2021-05-21 2021-08-20 江西省林业科学院 Degradable container for camphor tree essential oil extraction residues and preparation method and application thereof

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Application publication date: 20200306