CN110812317A - Skin care product with effects of moisturizing epidermis and resisting wrinkles of skin and preparation method thereof - Google Patents
Skin care product with effects of moisturizing epidermis and resisting wrinkles of skin and preparation method thereof Download PDFInfo
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- CN110812317A CN110812317A CN201911328019.8A CN201911328019A CN110812317A CN 110812317 A CN110812317 A CN 110812317A CN 201911328019 A CN201911328019 A CN 201911328019A CN 110812317 A CN110812317 A CN 110812317A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention provides a skin care product with the effects of moisturizing epidermis and resisting wrinkles on skin, which is prepared by uniformly mixing tuna bone zymolyte, a saccharomyces cerevisiae extract, 1, 3-butanediol, hydrogenated polyisobutene, glycerol tri (ethyl hexanoate), cetostearyl alcohol, macadamia nut oil, tremella polysaccharide, polydimethylsiloxane, glycerol stearate citrate, cyclopenta dimethyl siloxane, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, vitamin E, glycerol caprylate, acrylate/C10-30 alkyl acrylate cross-linked copolymer, triethanolamine, disodium ethylene diamine tetraacetate and deionized water. The invention uses cheap raw materials to obtain extracts of various moisture-keeping and oxidation-resisting components through enzymolysis, and can provide continuous good effects of keeping moisture of epidermis and resisting wrinkle of skin.
Description
Technical Field
The invention relates to the technical field of skin care cosmetics, in particular to a skin care product with the effects of moisturizing epidermis and resisting wrinkles on the skin and a preparation method thereof.
Background
In the prior art, various plant extracts, small molecular compounds and synthetic molecular peptides are added into the formula of the traditional skin care cosmetic to obtain the skin care cosmetic with the effects of moisturizing epidermis and resisting wrinkles on skin. When the skin care cosmetic is applied to the surface of the skin by a user, the cosmetic promotes the growth of skin cells and maintains the youthful state of the skin to obtain the effects of moisturizing the epidermis and preventing wrinkles on the skin. However, various plant extracts, small molecular compounds and synthetic molecular peptides which are added conventionally generally have the problems of complex preparation process, scarce raw materials and higher cost.
Disclosure of Invention
In order to solve the problems, the invention provides a skin care product with the effects of moisturizing epidermis and resisting wrinkles on the skin.
The purpose of the invention is realized by adopting the following technical scheme:
a skin care product with skin moisturizing and anti-wrinkle effects comprises tuna bone zymolyte and Saccharomyces cerevisiae extract;
preferably, the skin care product with the effects of moisturizing epidermis and resisting wrinkles on skin comprises the following components in percentage by weight: 0.1-4 parts of tuna bone zymolyte, 0.05-6 parts of saccharomyces cerevisiae extract, 8-12 parts of 1, 3-butanediol, 6-8 parts of hydrogenated polyisobutene, 4-6 parts of glycerol, 3-5 parts of glycerol tri (ethyl hexanoate), 2-4 parts of cetostearyl alcohol, 1-4 parts of macadamia nut oil, 0.05-2 parts of tremella polysaccharide, 1-3 parts of polydimethylsiloxane, 1-2 parts of glycerol stearate citrate, 1-2 parts of cyclopenta dimethyl siloxane, 1-2 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 0-0.5 part of vitamin E, 0.3-0.5 part of glycerol caprylate, 0.05-0.2 part of acrylate/C10-30 alkyl acrylate cross-linked copolymer, and 0.1-0.2 part of triethanolamine, 0.01-0.05 part of disodium ethylene diamine tetraacetate and 50-70 parts of deionized water, which are uniformly mixed;
further preferably, the skin care product with the effects of moisturizing epidermis and resisting wrinkles on skin comprises the following components in percentage by weight: 3.2 parts of tuna bone zymolyte, 4.8 parts of saccharomyces cerevisiae extract, 10 parts of 1, 3-butanediol, 7 parts of hydrogenated polyisobutene, 5 parts of glycerol, 4 parts of glycerol tri (ethyl hexanoate), 3 parts of cetostearyl alcohol, 3 parts of macadamia nut oil, 1.5 parts of tremella polysaccharide, 2 parts of polydimethylsiloxane, 1.2 parts of glycerol stearate citrate, 1.5 parts of cyclopenta polydimethylsiloxane, 1.5 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 0.2 part of vitamin E, 0.4 part of glyceryl caprylate, 0.1 part of acrylate/C10-30 alkyl acrylate cross-linked copolymer, 0.12 part of triethanolamine, 0.04 part of disodium ethylene diamine tetraacetate and 65 parts of deionized water;
preferably, the preparation method of the tuna bone zymolyte comprises the following steps: washing the head and/or bone of tuna, adding the tuna head and/or bone into a sodium carbonate solution with the temperature of 60-80 ℃ and the concentration of 1mol/L for deodorization treatment, soaking for 10-30min, filtering out and washing aggregate, adding distilled water with the mass of 8-10 times, pulping by a pulping machine to obtain a feed liquid, adjusting the pH to 8-9, stirring and homogenizing, raising the temperature of the feed liquid to 55-60 ℃, adding 0.7-1.0% of complex enzyme for enzymolysis, wherein the complex enzyme consists of neutral protease and alkaline protease according to the mass ratio of 1:2-2.3, the enzyme activity is 10 ten thousand units, the enzymolysis time is 3.5-4.5h, filtering out residues after the enzymolysis is finished, heating the enzymolysis liquid to 90 ℃, preserving the temperature for 5-10min for enzyme deactivation, cooling to the room temperature, adding polyvinylpyrrolidone with the mass of 0.05-0.1% of the enzymolysis liquid and active carbon with the mass of 0.1-0.2% of the enzymolysis liquid, adjusting pH of the solution to 4.8-5.0 with acetic acid solution, stirring, standing for 8-12 hr, filtering to obtain clear solution, and concentrating under reduced pressure at 55-60 deg.C and vacuum degree of 0.09-0.10Mpa for 30-60min to obtain tuna bone zymolyte;
preferably, the preparation method of the saccharomyces cerevisiae extract comprises the steps of filtering crude impurities of inactivated waste fruit wine and/or beer yeast mud, washing with water, adjusting the concentration of yeast slurry to be 200-300g/L, adding sodium hydroxide and sodium chloride, respectively adjusting the final concentration to be 10-20g/L, stirring at normal temperature for 2-3h, adjusting the pH of a solution to be 6-7 by hydrochloric acid, heating the slurry to 50-55 ℃ after desalting, respectively adding β -mannase and β -glucanase which are 0.05-0.1% of the mass of the yeast master batch, carrying out electrodialysis for 1-2h, and carrying out enzyme deactivation, concentration and spray drying to obtain the saccharomyces cerevisiae extract.
The invention has the beneficial effects that:
(1) tuna heads and bones are marine fish processing wastes, are mainly processed into fish meal, organic fertilizer, leaf fertilizer and the like at present, and have a single utilization mode; the collagen polypeptide can be obtained by enzymolysis, but the fishy smell and the odor are difficult to be completely removed; the invention uses the tuna heads and bones with wide sources and low price as raw materials, and carries out deodorization treatment, namely, the tuna heads and the bones are soaked in hot alkali before enzymolysis for deodorization, and active carbon deodorization is carried out after enzymolysis, so that the enzymolysis polypeptide extract without peculiar smell is obtained, and the invention has good moisture retention and oxidation resistance effects, simple process and no pollutant discharge, and achieves the aim of clean production.
(2) The saccharomyces cerevisiae is a byproduct in the brewing industry, is mostly prepared into crude protein feed through simple processing, contains rich protein, vitamins, mineral substances and various physiological active substances, and the cell wall also contains rich zymosan, but the cell wall of the saccharomyces cerevisiae is difficult to break, so that the active ingredients are difficult to release.
Detailed Description
The invention is further described with reference to the following examples.
Example 1
A skin care product with effects of moisturizing epidermis and resisting wrinkle of skin comprises the following components in percentage by weight: 3.2 parts of tuna bone zymolyte, 4.8 parts of saccharomyces cerevisiae extract, 10 parts of 1, 3-butanediol, 7 parts of hydrogenated polyisobutene, 5 parts of glycerol, 4 parts of glycerol tri (ethyl hexanoate), 3 parts of cetostearyl alcohol, 3 parts of macadamia nut oil, 1.5 parts of tremella polysaccharide, 2 parts of polydimethylsiloxane, 1.2 parts of glycerol stearic acid citrate, 1.5 parts of cyclopenta polydimethylsiloxane, 1.5 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 0.2 part of vitamin E, 0.4 part of glyceryl caprylate, 0.1 part of acrylate/C10-30 alkyl acrylate cross-linked copolymer, 0.12 part of triethanolamine, 0.04 part of ethylene diamine tetraacetic acid disodium and 65 parts of deionized water, which are uniformly mixed;
example 2
On the basis of the embodiment 1, the preparation method of the tuna bone zymolyte comprises the following steps: washing the head and/or bones of tuna, adding the tuna into a sodium carbonate solution with the temperature of 70 ℃ and the concentration of 1mol/L for deodorization treatment, soaking for 20min, filtering and washing aggregates, adding distilled water with the mass of 10 times, pulping by a pulping machine to obtain a feed liquid, adjusting the pH to 8-9, stirring and homogenizing, raising the temperature of the feed liquid to 55-60 ℃, adding 1.0% of complex enzyme for enzymolysis, wherein the complex enzyme is prepared by mixing neutral protease and alkaline protease according to the mass ratio of 1:2, the enzyme activity is 10 ten thousand units, the enzymolysis time is 4.5 hours, residues are filtered out after the enzymolysis is finished, the enzymolysis liquid is heated to 90 ℃, the temperature is kept for 5-10 minutes to inactivate the enzyme, the temperature is cooled to the room temperature, polyvinylpyrrolidone with the mass of 0.1 percent of the enzymolysis liquid and active carbon with the mass of 0.2 percent of the enzymolysis liquid are added, the pH value of the acetic acid solution is adjusted to 4.8-5.0, the mixture is stirred and then stands for 8-12 hours, clear liquid is filtered out, and the mixture is decompressed and concentrated for 30-60 minutes at the temperature of 55-60 ℃ and the vacuum degree of 0.09-0.10Mpa to obtain the tuna bone zymoly.
Example 3
A skin care product with effects of moisturizing epidermis and resisting wrinkle of skin comprises the following components in percentage by weight: 2.8 parts of tuna bone zymolyte, 6 parts of saccharomyces cerevisiae extract, 8 parts of 1, 3-butanediol, 6 parts of hydrogenated polyisobutene, 4 parts of glycerol, 5 parts of glycerol tri (ethyl hexanoate), 4 parts of cetostearyl alcohol, 2 parts of macadamia nut oil, 1 part of tremella polysaccharide, 2 parts of polydimethylsiloxane, 1 part of glycerol stearate citrate, 1.5 parts of cyclopenta polydimethylsiloxane, 1 part of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 0.4 part of glycerol caprylate, 0.2 part of acrylate/C10-30 alkyl acrylate cross-linked copolymer, 0.1 part of triethanolamine, 0.05 part of disodium ethylene diamine tetraacetate and 60 parts of deionized water, and the components are uniformly mixed;
the preparation method of the tuna bone zymolyte comprises the following steps: washing the head and/or bone of tuna, adding the tuna head and/or bone into a sodium carbonate solution with the temperature of 80 ℃ and the concentration of 1mol/L for deodorization treatment, soaking for 30min, filtering out and washing aggregate, adding distilled water with the mass of 8 times, pulping by a pulping machine to obtain a feed liquid, adjusting the pH to 8-9, stirring and homogenizing, heating the feed liquid to 55-60 ℃, adding 0.8% of a complex enzyme for enzymolysis, wherein the complex enzyme consists of neutral protease and alkaline protease according to the mass ratio of 1:2.3, performing enzyme activity of 10 ten thousand units, performing enzymolysis for 4h, filtering out residues after the enzymolysis is finished, heating the enzymolysis liquid to 90 ℃, performing heat preservation for 5-10min for enzyme deactivation, cooling to room temperature, adding polyvinylpyrrolidone with the mass of 0.06% of the enzymolysis liquid and active carbon with the mass of 0.12% of the enzymolysis liquid, adjusting the pH of the solution to 4.8-5.0 by an acetic acid solution, stirring, standing for 8-, concentrating under reduced pressure at 55-60 deg.C and 0.09-0.10Mpa for 30-60min to obtain tuna bone zymolyte.
Example 4
On the basis of the embodiment 1, the preparation method of the saccharomyces cerevisiae extract comprises the steps of filtering the inactivated waste wine yeast mud to remove impurities such as peel and seeds, washing with water, adjusting the concentration of yeast slurry to 300g/L, adding sodium hydroxide and sodium chloride, respectively adjusting the final concentration to 20g/L, stirring at normal temperature for 2-3h, adjusting the pH of a solution to 6-7 by hydrochloric acid, heating the slurry to 50-55 ℃ after electrodialysis desalination, respectively adding β -mannase and β -glucanase with the mass of 0.1% of the yeast master batch, carrying out enzymolysis for 2h, and carrying out enzyme deactivation, concentration and spray drying to obtain the saccharomyces cerevisiae extract.
Example 5
The preparation method of the saccharomyces cerevisiae extract comprises the steps of filtering the inactivated waste wine yeast paste to remove impurities such as peel and seeds, washing, adjusting the concentration of yeast slurry to 200g/L, adding sodium hydroxide and sodium chloride, respectively adjusting the final concentration to 10g/L, stirring at normal temperature for 2-3h, adjusting the pH of a solution to 6-7 with hydrochloric acid, heating the slurry to 50-55 ℃ after electrodialysis desalination, respectively adding β -mannase and β -glucanase which are 0.05% of the mass of yeast master batch, performing enzymolysis for 1h, and performing enzyme deactivation, concentration and spray drying to obtain the saccharomyces cerevisiae extract.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (6)
1. A skin care product with skin moisturizing and anti-wrinkle effects is characterized by comprising tuna bone zymolyte and saccharomyces cerevisiae extract.
2. The skin care product with the effects of moisturizing epidermis and resisting wrinkles on skin as claimed in claim 1, which is characterized by comprising the following components in percentage by weight: 0.1-4 parts of tuna bone zymolyte, 0.05-6 parts of saccharomyces cerevisiae extract, 8-12 parts of 1, 3-butanediol, 6-8 parts of hydrogenated polyisobutene, 4-6 parts of glycerol, 3-5 parts of glycerol tri (ethyl hexanoate), 2-4 parts of cetostearyl alcohol, 1-4 parts of macadamia nut oil, 0.05-2 parts of tremella polysaccharide, 1-3 parts of polydimethylsiloxane, 1-2 parts of glycerol stearate citrate, 1-2 parts of cyclopenta dimethyl siloxane, 1-2 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 0-0.5 part of vitamin E, 0.3-0.5 part of glycerol caprylate, 0.05-0.2 part of acrylate/C10-30 alkyl acrylate cross-linked copolymer, and 0.1-0.2 part of triethanolamine, 0.01-0.05 part of disodium ethylene diamine tetraacetate and 50-70 parts of deionized water, wherein the skin care product is prepared by uniformly mixing the components.
3. The skin care product with the effects of moisturizing epidermis and resisting wrinkles on skin as claimed in claim 2, which is characterized by comprising the following components in percentage by weight: 3.2 parts of tuna bone zymolyte, 4.8 parts of saccharomyces cerevisiae extract, 10 parts of 1, 3-butanediol, 7 parts of hydrogenated polyisobutene, 5 parts of glycerol, 4 parts of glycerol tri (ethyl hexanoate), 3 parts of cetostearyl alcohol, 3 parts of macadamia nut oil, 1.5 parts of tremella polysaccharide, 2 parts of polydimethylsiloxane, 1.2 parts of glycerol stearate citrate, 1.5 parts of cyclopenta polydimethylsiloxane, 1.5 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 0.2 part of vitamin E, 0.4 part of glyceryl caprylate, 0.1 part of acrylate/C10-30 alkyl acrylate cross-linked copolymer, 0.12 part of triethanolamine, 0.04 part of ethylene diamine tetraacetic acid disodium and 65 parts of deionized water, wherein the skin care product is prepared by uniformly mixing the components.
4. The skin care product with the effects of moisturizing skin and resisting wrinkles on skin as claimed in claim 1, wherein the preparation method of the tuna bone zymolyte comprises the following steps: washing the head and/or bone of tuna, adding the tuna head and/or bone into a sodium carbonate solution with the temperature of 60-80 ℃ and the concentration of 1mol/L for deodorization treatment, soaking for 10-30min, filtering out and washing aggregate, adding distilled water with the mass of 8-10 times, pulping by a pulping machine to obtain a feed liquid, adjusting the pH to 8-9, stirring and homogenizing, raising the temperature of the feed liquid to 55-60 ℃, adding 0.7-1.0% of complex enzyme for enzymolysis, wherein the complex enzyme consists of neutral protease and alkaline protease according to the mass ratio of 1:2-2.3, the enzyme activity is 10 ten thousand units, the enzymolysis time is 3.5-4.5h, filtering out residues after the enzymolysis is finished, heating the enzymolysis liquid to 90 ℃, preserving the temperature for 5-10min for enzyme deactivation, cooling to the room temperature, adding polyvinylpyrrolidone with the mass of 0.05-0.1% of the enzymolysis liquid and active carbon with the mass of 0.1-0.2% of the enzymolysis liquid, adjusting pH of the solution to 4.8-5.0 with acetic acid solution, stirring, standing for 8-12 hr, filtering to obtain clear solution, and concentrating under reduced pressure at 55-60 deg.C and vacuum degree of 0.09-0.10Mpa for 30-60min to obtain tuna bone zymolyte.
5. The skin care product with the effects of moisturizing epidermis and resisting wrinkles on skin as claimed in claim 1, wherein the preparation method of the saccharomyces cerevisiae extract comprises the steps of filtering crude impurities from inactivated saccharomyces cerevisiae mud, washing with water, adjusting the concentration of yeast slurry to 200-300g/L, adding sodium hydroxide and sodium chloride, respectively adjusting the final concentration to 10-20g/L, stirring at normal temperature for 2-3h, adjusting the pH of a solution to 6-7 with hydrochloric acid, heating the slurry to 50-55 ℃ after electrodialysis desalination, respectively adding β -mannase and β -glucanase with the mass of 0.05-0.1% of the mass of yeast master batch, carrying out enzymolysis for 1-2h, and carrying out enzyme deactivation, concentration and spray drying to obtain the saccharomyces cerevisiae extract.
6. The skin care product with the effects of moisturizing epidermis and resisting wrinkles on skin according to claim 5, wherein the saccharomyces cerevisiae is waste brewer's yeast or waste wine yeast or waste fruit wine yeast.
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| CN201911328019.8A CN110812317A (en) | 2019-12-20 | 2019-12-20 | Skin care product with effects of moisturizing epidermis and resisting wrinkles of skin and preparation method thereof |
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Cited By (1)
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Application publication date: 20200221 |