CN110747538A - Preparation method of antioxidant antistatic ATY oil - Google Patents
Preparation method of antioxidant antistatic ATY oil Download PDFInfo
- Publication number
- CN110747538A CN110747538A CN201911143394.5A CN201911143394A CN110747538A CN 110747538 A CN110747538 A CN 110747538A CN 201911143394 A CN201911143394 A CN 201911143394A CN 110747538 A CN110747538 A CN 110747538A
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- Prior art keywords
- agent
- antioxidant
- antistatic
- aty
- oil
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/262—Sulfated compounds thiosulfates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/44—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen containing nitrogen and phosphorus
- D06M13/453—Phosphates or phosphites containing nitrogen atoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a preparation method of an antioxidant antistatic ATY oil agent, which comprises the following steps of preparing raw materials, wherein the raw materials comprise a mother agent, a surfactant, an antistatic agent, an antioxidant, an emulsifier, a softener, a lubricant and deionized water; heating deionized water to 40-46 ℃, adding a mother agent, and stirring and mixing for 10-15 minutes after the mother agent is added to obtain a primary oil agent; and sequentially adding a surfactant, an antistatic agent, an antioxidant, an emulsifier, a softening agent and a lubricant into the obtained primary oil agent, and continuously stirring for 30-45 minutes to obtain the ATY oil agent. The preparation method disclosed by the invention is simple in preparation process, convenient to operate and implement, and good in antistatic property and oxidation resistance, and further beneficial to popularization and application.
Description
Technical Field
The invention relates to the technical field of oil preparation, in particular to a preparation method of an antioxidant antistatic ATY oil.
Background
In the production and processing of the textile industry, the oil is an indispensable auxiliary agent, and the problems of mutual friction of fibers and static electricity and oxidation generated in the friction process of mechanical equipment cannot be solved in the using process of the existing oil, so that great troubles and inconvenience are brought to the production and processing of the fibers. Therefore, a preparation method of the antioxidant antistatic ATY oil agent is provided.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a preparation method of an antioxidant antistatic ATY oil agent.
In order to achieve the purpose, the invention adopts the following technical scheme:
the preparation method of the antioxidant antistatic ATY oil agent comprises the following steps:
s1, preparing raw materials: the raw materials comprise mother agent, surfactant, antistatic agent, antioxidant, emulsifier, softening agent, lubricant and deionized water;
s2, heating deionized water to 40-46 ℃, adding a mother agent, and stirring and mixing for 10-15 minutes after the mother agent is added to obtain a primary oil agent;
s3, sequentially adding a surfactant, an antistatic agent, an antioxidant, an emulsifier, a softening agent and a lubricant into the primary oil agent obtained in the step S2, and continuously stirring for 30-45 minutes to obtain an ATY oil agent.
Preferably, in the processes of step S2 and step S3, the weight percentages of the deionized water, the mother agent, the surfactant, the antistatic agent, the antioxidant, the emulsifier, the softener and the lubricant are 50-60%: 20-30%: 3-6%: 2-5%: 1-2%: 1-2%: 2 to 4 percent; 5 to 7 percent.
Preferably, the mother agent in step S1 is a modified POO polyether.
Preferably, the surfactant in step S1 is alkyl polyoxyethylene ether phosphate.
Preferably, the antistatic agent in step S1 is alkyl phosphate diethanolammonium.
Preferably, the antioxidant in step S1 is nonylphenol.
Preferably, the emulsifier in step S1 is sodium lauryl sulfate.
Preferably, the softening agent in step S1 is fatty acid polyoxyethylene ester.
Preferably, the lubricant in step S1 is an octylphenol POE ether.
The preparation method of the antioxidant antistatic ATY oil agent provided by the invention has the beneficial effects that: the oil agent prepared by the scheme contains the surfactant, the antistatic agent, the antioxidant, the emulsifier, the softener and the lubricant, so that the oil agent has good antistatic property and oxidation resistance, and also has the advantages of smoothness, softening property and softness, so that the ATY oil agent is favorable for being used in the fiber production and processing processes in the textile industry, the preparation process is simple, and the ATY oil agent is convenient to operate and implement and further favorable for popularization and application.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The preparation method of the antioxidant antistatic ATY oil agent comprises the following steps:
s1, preparing raw materials: the raw materials comprise mother agent, surfactant, antistatic agent, antioxidant, emulsifier, softening agent, lubricant and deionized water;
s2, heating deionized water to 40-46 ℃, adding a mother agent, and stirring and mixing for 10-15 minutes after the mother agent is added to obtain a primary oil agent;
s3, sequentially adding a surfactant, an antistatic agent, an antioxidant, an emulsifier, a softening agent and a lubricant into the primary oil agent obtained in the step S2, and continuously stirring for 30-45 minutes to obtain an ATY oil agent.
In the processes of the step S2 and the step S3, the weight percentage of the deionized water, the mother agent, the surfactant, the antistatic agent, the antioxidant, the emulsifier, the softener and the lubricant is 50-60%: 20-30%: 3-6%: 2-5%: 1-2%: 1-2%: 2 to 4 percent; 5 to 7 percent.
The mother agent in step S1 is a modified POO polyether.
The surfactant in step S1 is alkyl polyoxyethylene ether phosphate.
The antistatic agent in step S1 is alkyl phosphate diethanolammonium.
The antioxidant in step S1 is nonylphenol.
The emulsifier in step S1 is sodium lauryl sulfate.
The softening agent in step S1 is fatty acid polyoxyethylene ester.
The lubricant in step S1 is octyl phenol POE ether.
Example 1:
the preparation method of the antioxidant antistatic ATY oil agent comprises the following steps
S1, preparing raw materials: the raw materials comprise modified POO polyether, alkyl polyoxyethylene ether phosphate, alkyl phosphate diethanolammonium, nonylphenol, sodium dodecyl sulfate, fatty acid polyoxyethylene ester, octyl phenol POE ether and deionized water;
s2, heating deionized water to 40 ℃, adding the modified POO polyether, and stirring and mixing for 10 minutes after the mother agent is added to obtain a primary oil agent;
s3, adding alkyl polyoxyethylene ether phosphate, alkyl phosphate diethanolammonium, nonylphenol, sodium dodecyl sulfate, fatty acid polyoxyethylene ester and octyl phenol POE ether into the primary oil agent obtained in the step S2 in sequence, and continuously stirring for 30 minutes to obtain the ATY oil agent.
In the processes performed in steps S2 and S3, the weight percentages of the deionized water, the modified POO polyether, the alkyl polyoxyethylene ether phosphate, the alkyl phosphate diethanolammonium, the nonylphenol, the sodium lauryl sulfate, the fatty acid polyoxyethylene ester, and the octylphenol POE ether are 50%: 30%: 3%: 5%: 2%: 1%: 4 percent; 5 percent.
Example 2:
the preparation method of the antioxidant antistatic ATY oil agent comprises the following steps
S1, preparing raw materials: the raw materials comprise modified POO polyether, alkyl polyoxyethylene ether phosphate, alkyl phosphate diethanolammonium, nonylphenol, sodium dodecyl sulfate, fatty acid polyoxyethylene ester, octyl phenol POE ether and deionized water;
s2, heating deionized water to 43 ℃, adding the modified POO polyether, and stirring and mixing for 13 minutes after the mother agent is added to obtain a primary oil agent;
s3, adding alkyl polyoxyethylene ether phosphate, alkyl phosphate diethanolammonium, nonylphenol, sodium dodecyl sulfate, fatty acid polyoxyethylene ester and octyl phenol POE ether into the primary oil agent obtained in the step S2 in sequence, and continuously stirring for 38 minutes to obtain the ATY oil agent.
In the processes performed in steps S2 and S3, the weight percentages of the deionized water, the modified POO polyether, the alkyl polyoxyethylene ether phosphate, the alkyl phosphate diethanolammonium, the nonylphenol, the sodium lauryl sulfate, the fatty acid polyoxyethylene ester, and the octylphenol POE ether are 55%: 25%: 4.5%: 3.5%: 1.5%: 1.5%: 3 percent; 6 percent.
Example 3:
the preparation method of the antioxidant antistatic ATY oil agent comprises the following steps
S1, preparing raw materials: the raw materials comprise modified POO polyether, alkyl polyoxyethylene ether phosphate, alkyl phosphate diethanolammonium, nonylphenol, sodium dodecyl sulfate, fatty acid polyoxyethylene ester, octyl phenol POE ether and deionized water;
s2, heating deionized water to 46 ℃, adding the modified POO polyether, and stirring and mixing for 15 minutes after the mother agent is added to obtain a primary oil agent;
s3, adding alkyl polyoxyethylene ether phosphate, alkyl phosphate diethanolammonium, nonylphenol, sodium dodecyl sulfate, fatty acid polyoxyethylene ester and octyl phenol POE ether into the primary oil agent obtained in the step S2 in sequence, and continuously stirring for 45 minutes to obtain the ATY oil agent.
In the processes performed in steps S2 and S3, the weight percentages of the deionized water, the modified POO polyether, the alkyl polyoxyethylene ether phosphate, the alkyl phosphate diethanolammonium, the nonylphenol, the sodium lauryl sulfate, the fatty acid polyoxyethylene ester, and the octylphenol POE ether are 60%: 20%: 6%: 2%: 1%: 2%: 2 percent; 7 percent.
In summary, the following steps: the oil agent prepared by the invention contains the surfactant, the antistatic agent, the antioxidant, the emulsifier, the softener and the lubricant, so that the oil agent has good antistatic property and oxidation resistance, and also has the advantages of smoothness, softening property and softness, and further the ATY oil agent is beneficial to being used in the fiber production and processing processes in the textile industry, and the preparation process is simple, convenient to operate and implement and further beneficial to being popularized and applied.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (9)
1. The preparation method of the antioxidant antistatic ATY oil agent is characterized by comprising the following steps:
s1, preparing raw materials: the raw materials comprise mother agent, surfactant, antistatic agent, antioxidant, emulsifier, softening agent, lubricant and deionized water;
s2, heating deionized water to 40-46 ℃, adding a mother agent, and stirring and mixing for 10-15 minutes after the mother agent is added to obtain a primary oil agent;
s3, sequentially adding a surfactant, an antistatic agent, an antioxidant, an emulsifier, a softening agent and a lubricant into the primary oil agent obtained in the step S2, and continuously stirring for 30-45 minutes to obtain an ATY oil agent.
2. The method for preparing an antioxidant antistatic ATY oil agent according to claim 1, wherein in the process of steps S2 and S3, the weight percentage of the deionized water, the mother agent, the surfactant, the antistatic agent, the antioxidant, the emulsifier, the softener and the lubricant is 50-60%: 20-30%: 3-6%: 2-5%: 1-2%: 1-2%: 2 to 4 percent; 5 to 7 percent.
3. The method for preparing the antioxidant antistatic ATY oil as claimed in claim 1, wherein the mother agent in step S1 is modified POO polyether.
4. The method for preparing an antioxidant antistatic ATY oil as claimed in claim 1, wherein the surfactant in step S1 is alkyl polyoxyethylene ether phosphate.
5. The method for preparing an antioxidant antistatic ATY oil as claimed in claim 1, wherein the antistatic agent in step S1 is alkyl phosphate diethanolammonium.
6. The method for preparing the antioxidant antistatic ATY oil agent as claimed in claim 1, wherein the antioxidant in step S1 is nonylphenol.
7. The method for preparing the antioxidant antistatic ATY oil as claimed in claim 1, wherein the emulsifier in step S1 is sodium dodecyl sulfate.
8. The method for preparing an antioxidant antistatic ATY oil as claimed in claim 1, wherein the softening agent in step S1 is fatty acid polyoxyethylene ester.
9. The method for preparing the antioxidant antistatic ATY oil as claimed in claim 1, wherein the lubricant in step S1 is octyl phenol POE ether.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911143394.5A CN110747538A (en) | 2019-11-20 | 2019-11-20 | Preparation method of antioxidant antistatic ATY oil |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201911143394.5A CN110747538A (en) | 2019-11-20 | 2019-11-20 | Preparation method of antioxidant antistatic ATY oil |
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| CN110747538A true CN110747538A (en) | 2020-02-04 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104179005A (en) * | 2014-08-15 | 2014-12-03 | 上海中孚特种油品有限公司 | Fiber fully drawn yarn (FDY) spinning oil and preparation method thereof |
| CN105113227A (en) * | 2015-09-21 | 2015-12-02 | 天津工业大学 | Novel nylon industrial yarn oil and method for manufacturing same |
| CN105603730A (en) * | 2016-02-25 | 2016-05-25 | 苏州三和开泰花线织造有限公司 | Oil solution special for environmentally-friendly efficient synthetic fiber and preparation method thereof |
| CN109763335A (en) * | 2019-01-12 | 2019-05-17 | 厦门东纶股份有限公司 | A kind of nylon spinning oil and preparation method thereof |
-
2019
- 2019-11-20 CN CN201911143394.5A patent/CN110747538A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104179005A (en) * | 2014-08-15 | 2014-12-03 | 上海中孚特种油品有限公司 | Fiber fully drawn yarn (FDY) spinning oil and preparation method thereof |
| CN105113227A (en) * | 2015-09-21 | 2015-12-02 | 天津工业大学 | Novel nylon industrial yarn oil and method for manufacturing same |
| CN105603730A (en) * | 2016-02-25 | 2016-05-25 | 苏州三和开泰花线织造有限公司 | Oil solution special for environmentally-friendly efficient synthetic fiber and preparation method thereof |
| CN109763335A (en) * | 2019-01-12 | 2019-05-17 | 厦门东纶股份有限公司 | A kind of nylon spinning oil and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 沈一丁主编: "《轻化工助剂》", 31 July 2004, 中国轻工业出版社 * |
| 邓舜扬: "《化学配方与工艺手册》", 31 January 2003, 上海科学技术文献出版社 * |
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Application publication date: 20200204 |