CN110742301A - Method for preparing microporous tobacco powder by complex enzyme method - Google Patents
Method for preparing microporous tobacco powder by complex enzyme method Download PDFInfo
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- CN110742301A CN110742301A CN201911126843.5A CN201911126843A CN110742301A CN 110742301 A CN110742301 A CN 110742301A CN 201911126843 A CN201911126843 A CN 201911126843A CN 110742301 A CN110742301 A CN 110742301A
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- tobacco
- powder
- complex enzyme
- microporous
- solution
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 90
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 90
- 239000000843 powder Substances 0.000 title claims abstract description 58
- 238000000034 method Methods 0.000 title claims abstract description 39
- 108090000790 Enzymes Proteins 0.000 title claims abstract description 38
- 102000004190 Enzymes Human genes 0.000 title claims abstract description 38
- 239000002994 raw material Substances 0.000 claims abstract description 32
- 239000000243 solution Substances 0.000 claims abstract description 28
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000007974 sodium acetate buffer Substances 0.000 claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 claims abstract description 10
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 239000011259 mixed solution Substances 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 9
- 238000000967 suction filtration Methods 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 7
- 238000005406 washing Methods 0.000 claims abstract description 7
- 229940088598 enzyme Drugs 0.000 claims description 34
- 108010059892 Cellulase Proteins 0.000 claims description 8
- 102000004139 alpha-Amylases Human genes 0.000 claims description 8
- 108090000637 alpha-Amylases Proteins 0.000 claims description 8
- 229940024171 alpha-amylase Drugs 0.000 claims description 8
- 229940106157 cellulase Drugs 0.000 claims description 8
- 125000003118 aryl group Chemical group 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 239000000428 dust Substances 0.000 claims 1
- 238000006911 enzymatic reaction Methods 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 abstract description 10
- 235000013599 spices Nutrition 0.000 abstract description 10
- 238000002156 mixing Methods 0.000 abstract description 8
- 230000000391 smoking effect Effects 0.000 abstract description 7
- 238000001179 sorption measurement Methods 0.000 abstract description 2
- 238000010521 absorption reaction Methods 0.000 description 16
- 238000005303 weighing Methods 0.000 description 11
- 239000003921 oil Substances 0.000 description 8
- 235000019198 oils Nutrition 0.000 description 8
- 239000000725 suspension Substances 0.000 description 8
- 239000000779 smoke Substances 0.000 description 7
- 238000002485 combustion reaction Methods 0.000 description 5
- 239000012153 distilled water Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 108010073178 Glucan 1,4-alpha-Glucosidase Proteins 0.000 description 4
- 102100022624 Glucoamylase Human genes 0.000 description 4
- 239000008399 tap water Substances 0.000 description 4
- 235000020679 tap water Nutrition 0.000 description 4
- 238000009736 wetting Methods 0.000 description 4
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 239000004006 olive oil Substances 0.000 description 3
- 235000008390 olive oil Nutrition 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000005903 acid hydrolysis reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F47/00—Smokers' requisites not otherwise provided for
Abstract
The invention discloses a method for preparing microporous tobacco powder by a complex enzyme method. The method comprises the following steps: preparing a tobacco raw material; crushing the tobacco raw materials into powder, adding water to soak the tobacco raw material powder according to the mass ratio of the tobacco raw materials to the water of 1:5-1:10, adjusting the pH value by using a sodium acetate buffer solution, and finally heating and stirring the mixed solution; adding the complex enzyme solution into the mixed solution to perform enzymolysis reaction; and after the enzymolysis reaction is finished, carrying out suction filtration, washing and drying on the mixed solution to obtain the microporous tobacco powder. The tobacco powder can be made into sheets to be applied to low-temperature cigarettes, the adsorption performance of the tobacco powder on the atomizing agent and the essence and spice for the cigarettes is enhanced by treating the tobacco powder with the complex enzyme, the blending space of the atomizing agent and the essence and spice is expanded, the smoking taste added by a single tobacco sheet is improved, and the smoking taste of the low-temperature cigarettes is improved.
Description
Technical Field
The invention belongs to the technical field of tobacco, and particularly relates to a method for preparing microporous tobacco powder by a complex enzyme method.
Background
With the rise of global smoking control and the increase of human attention on health, the number and proportion of smokers are continuously reduced in recent years. In order to adapt to development, low-temperature cigarettes become the key development direction of the tobacco industry.
The low temperature cigarette does not produce smoke by combustion, and can remarkably reduce known harmful smoke components generated by combustion and thermal degradation of tobacco in the traditional cigarette.
For example, chinese patent CN103549657A discloses a heating type low temperature cigarette, wherein the low temperature heat source is composed of a vacuum heat pipe and a combustion chamber, the combustion chamber is used for generating heat, the heat pipe is used for conducting heat, the heat absorbing section of the heat pipe is placed in the combustion chamber, the heat releasing section of the heat pipe is wrapped by tobacco shreds or filled with tobacco shreds, and the heating type low temperature cigarette can completely replace the traditional cigarette. The heat source device is efficient, safe and low in cost, and can meet the requirements of various cigarette consumers after being combined with low-temperature cigarettes.
At present, the main filler of the low-temperature cigarette is reconstituted tobacco, and the reconstituted tobacco is adopted for improving the capacity of tobacco leaves to the atomizing agent due to the limited capacity of tobacco shreds to the atomizing agent. The existing low-temperature cigarette has single tobacco shred smoking taste and limited essence and spice loading, and can not prepare low-temperature cigarettes with different flavors to meet the requirements of different consumers.
Disclosure of Invention
The invention aims to provide a method for preparing microporous tobacco powder by a complex enzyme method. The tobacco powder can be made into sheets to be applied to low-temperature cigarettes, the adsorption performance of the tobacco powder on the atomizing agent and the essence and spice for the cigarettes is enhanced by treating the tobacco powder with the complex enzyme, the blending space of the atomizing agent and the essence and spice is expanded, the smoking taste added by a single tobacco sheet is improved, and the smoking taste of the low-temperature cigarettes is improved.
In order to achieve the purpose, the invention adopts the following technical scheme:
a method for preparing microporous tobacco powder by a complex enzyme method comprises the following steps:
(1) preparing a tobacco raw material;
(2) crushing the tobacco raw materials into powder, adding water to soak the tobacco raw material powder according to the mass ratio of the tobacco raw materials to the water of 1:5-1:10, adjusting the pH value by using a sodium acetate buffer solution, and finally heating and stirring the mixed solution;
(3) adding the complex enzyme solution into the mixed solution in the step (2) to perform enzymolysis reaction;
(4) and (4) after the enzymolysis reaction in the step (3) is finished, carrying out suction filtration, washing and drying on the mixed solution to obtain the microporous tobacco powder.
Further, the tobacco raw material comprises one or more of flue-cured tobacco leaves, aromatic tobacco leaves, sun-cured tobacco leaves, tobacco stems and tobacco powder.
Further, the pH value of the step (2) is adjusted to 6-7 by sodium acetate buffer solution.
Further, the heating temperature in the step (2) is 35-40 ℃, and the heating time is 30-45 min.
Further, the complex enzyme in the step (3) consists of cellulase, saccharifying enzyme and α -amylase, and preferably, the mass ratio of the cellulase to the saccharifying enzyme to the α -amylase is 0.5-2:0.5-2: 1.
Further, the complex enzyme solution in the step (3) is prepared by dissolving the complex enzyme in a sodium acetate buffer solution; preferably, the concentration of the complex enzyme solution is 1 g/ml.
Further, the enzymolysis reaction time in the step (3) is 12-24 h.
In addition, the invention also provides application of the microporous tobacco powder, and the microporous tobacco powder is pressed into a sheet and is used for low-temperature cigarettes.
The invention has the beneficial effects that:
(1) compared with physical methods such as ultrasonic wave, spraying, mechanical impact and the like and chemical acid hydrolysis and the like, the method for preparing the microporous tobacco powder by adopting a biological means has the advantages of relatively simple and mild process and better pore-forming uniformity.
(2) The water absorption and oil absorption of the microporous tobacco powder are scientifically tested, so that a large amount of atomizing agent and essence perfume can be loaded, and the requirements of low-temperature cigarettes are met.
(3) By changing the formula of the tobacco raw material and the formula of the essence and the spice, the low-temperature cigarettes with different flavors can be developed, and the requirements of different consumers are met.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions of the embodiments of the present invention will be clearly and completely described below. It is to be understood that the embodiments described are only a few embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the described embodiments of the invention without any inventive step, are within the scope of protection of the invention.
Unless defined otherwise, technical or scientific terms used herein shall have the ordinary meaning as understood by one of ordinary skill in the art to which this invention belongs.
Example 1
A method for preparing microporous tobacco powder by a complex enzyme method comprises the following steps:
(1) taking flue-cured tobacco leaves as raw materials, crushing the tobacco raw materials into powder by using a crusher, accurately weighing 1kg of tobacco raw material powder, putting the tobacco raw material powder into a flask, adding tap water according to the material-to-liquid ratio of 1:10 for wetting, slowly adding the raw material powder, adjusting the pH value (6-7), putting the flask into a constant-temperature water bath kettle at a certain temperature (35-40 ℃) for preheating for 30min, and stirring by using an electric stirrer.
(2) Accurately weighing 10g of complex enzyme comprising cellulase, glucoamylase and α -amylase, uniformly mixing according to the weight ratio of 2:2:1, preparing an enzyme solution by using 10ml of sodium acetate buffer solution, transferring the enzyme solution into a flask, and stopping the reaction after 12 hours of enzymolysis.
(3) And (4) carrying out suction filtration on the suspension in the flask, washing the suspension with distilled water, and drying to obtain microporous tobacco powder.
Example 2
A method for preparing microporous tobacco powder by a complex enzyme method comprises the following steps:
(1) the method comprises the steps of taking flue-cured tobacco leaves as raw materials, crushing the tobacco raw materials into powder by using a crusher, accurately weighing 1kg of tobacco raw material powder, putting the tobacco raw material powder into a flask, adding tap water according to the material-to-liquid ratio of 1:10 for wetting, slowly adding sodium acetate buffer solution, adjusting the pH value (6-7), putting the flask into a constant-temperature water bath kettle at a certain temperature (35-40 ℃) for preheating for 30min, and stirring by using an electric stirrer.
(2) Accurately weighing 10g of complex enzyme comprising cellulase, glucoamylase and α -amylase according to the weight ratio of 2:1:2, uniformly mixing, preparing an enzyme solution by using 10ml of sodium acetate buffer solution, transferring into a flask, and stopping reaction after 12 hours of enzymolysis.
(3) And (4) carrying out suction filtration on the suspension in the flask, washing the suspension with distilled water, and drying to obtain microporous tobacco powder.
Example 3
A method for preparing microporous tobacco powder by a complex enzyme method comprises the following steps:
(1) the method comprises the steps of taking flue-cured tobacco leaves as raw materials, crushing the tobacco raw materials into powder by using a crusher, accurately weighing 1kg of tobacco raw material powder, putting the tobacco raw material powder into a flask, adding tap water according to the material-to-liquid ratio of 1:8 for wetting, slowly adding sodium acetate buffer solution, adjusting the PH value (6-7), putting the flask into a constant-temperature water bath kettle at a certain temperature (35-40 ℃) for preheating for 30min, and stirring by using an electric stirrer.
(2) Accurately weighing 8g of complex enzyme comprising cellulase, glucoamylase and α -amylase according to the weight ratio of 1:2:2, uniformly mixing, preparing an enzyme solution by using 10ml of sodium acetate buffer solution, transferring into a flask, and stopping reaction after 24 times of enzymolysis.
(3) And (4) carrying out suction filtration on the suspension in the flask, washing the suspension with distilled water, and drying to obtain microporous tobacco powder.
Example 4
A method for preparing microporous tobacco powder by a complex enzyme method comprises the following steps:
(1) the method comprises the steps of taking flue-cured tobacco leaves as raw materials, crushing the tobacco raw materials into powder by using a crusher, accurately weighing 1kg of tobacco raw material powder, putting the tobacco raw material powder into a flask, adding tap water according to the material-to-liquid ratio of 1:10 for wetting, slowly adding sodium acetate buffer solution, adjusting the pH value (6-7), putting the flask into a constant-temperature water bath kettle at a certain temperature (35-40 ℃) for preheating for 30min, and stirring by using an electric stirrer.
(2) Accurately weighing 8g of complex enzyme comprising cellulase, glucoamylase and α -amylase according to the weight ratio of 1:1: 1, uniformly mixing, preparing an enzyme solution by using 10ml of sodium acetate buffer solution, transferring into a flask, and stopping reaction after enzymolysis for 24 hours.
(3) And (4) carrying out suction filtration on the suspension in the flask, washing the suspension with distilled water, and drying to obtain microporous tobacco powder.
The tobacco powders of examples 1 to 4 were pressed into sheets, and the water absorption and oil absorption of the sheets were tested, and the water absorption and oil absorption were measured as follows:
method for measuring Water absorption:
accurately weighing the microporous smoke powder with the mass of M1, placing the microporous smoke powder into a 250ml beaker, adding 100ml of distilled water, mixing and stirring for 30min at normal temperature, performing suction filtration by using a sand core funnel until no liquid drops exist, taking out the microporous smoke powder, weighing, wherein the mass is M2, and calculating the water absorption rate according to the weight difference between the front weight and the rear weight.
Water absorption (%) = (M2-M1)/M1X 100
The method for measuring the oil absorption rate comprises the following steps: accurately weighing microporous smoke powder with the mass of M3, placing the microporous smoke powder into a 250ml beaker, adding olive oil with the volume of V1, mixing and stirring for 30min at normal temperature, centrifuging for 15min at 4000r/min by adopting a centrifuge, taking out the upper layer olive oil, measuring the volume of the upper layer olive oil to be V2, and calculating the oil absorption rate according to the volume difference between the front and the back.
Oil absorption (mL/g) = (V1-V2)/M3
Table 1 shows the water absorption and oil absorption of examples 1-4 and control 1, wherein control 1 was prepared by preparing tobacco powder according to the same formulation without an enzymatic step and then pressing into tobacco sheets.
TABLE 1 Water absorption and oil absorption of examples 1-4 and control 1
Table 2 shows the evaluation of the effects of examples 1 to 4 and control 1 on low-temperature cigarettes.
Table 2 evaluation of effects of examples 1 to 4 and control 1 on low-temperature cigarettes
As can be seen from tables 1 and 2, the capacity of the tobacco shreds for the atomizing agent can be improved, the smoking taste of the low-temperature cigarette can be improved, auxiliary material components such as the fogging agent and the essence and spice can be effectively loaded as far as possible, the tobacco leaves are used as raw materials, the compound enzyme treatment is carried out, the microporous tobacco powder is obtained, a large amount of essence and spice can be loaded in micropores, and the low-temperature cigarette slice prepared from the tobacco powder can be loaded with a large amount of the atomizing agent, the essence and the spice and the like. And the low-temperature cigarettes with different flavors can be prepared by changing the formulas of the tobacco leaves and the essence spices, so that the requirements of different consumers are met.
The above description of the embodiments is only intended to facilitate the understanding of the method of the invention and its core ideas. It should be noted that, for those skilled in the art, it is possible to make various improvements and modifications to the present invention without departing from the principle of the present invention, and those improvements and modifications also fall within the scope of the claims of the present invention.
Claims (10)
1. A method for preparing microporous tobacco powder by a complex enzyme method is characterized by comprising the following steps:
(1) preparing a tobacco raw material;
(2) crushing the tobacco raw materials into powder, adding water to soak the tobacco raw material powder according to the mass ratio of the tobacco raw materials to the water of 1:5-1:10, adjusting the pH value by using a sodium acetate buffer solution, and finally heating and stirring the mixed solution;
(3) adding the complex enzyme solution into the mixed solution in the step (2) to perform enzymolysis reaction;
(4) and (4) after the enzymolysis reaction in the step (3) is finished, carrying out suction filtration, washing and drying on the mixed solution to obtain the microporous tobacco powder.
2. The method of claim 1, wherein the tobacco material comprises one or more of flue-cured tobacco leaf, aromatic tobacco leaf, cured tobacco leaf, tobacco stem, tobacco dust.
3. The method according to claim 1, wherein the pH value of the step (2) is adjusted to 6-7 by sodium acetate buffer solution.
4. The method according to claim 1, wherein the heating temperature in the step (2) is 35-40 ℃ and the heating time is 30-45 min.
5. The method as claimed in claim 1, wherein the complex enzyme of step (3) is composed of cellulase, saccharifying enzyme and α -amylase.
6. The method of claim 5, wherein the mass ratio of the cellulase, the saccharifying enzyme and the α -amylase is 0.5-2:0.5-2: 1.
7. The method as claimed in claim 1, wherein the complex enzyme solution of step (3) is prepared by dissolving complex enzyme in sodium acetate buffer solution.
8. The method as claimed in claim 7, wherein the concentration of the complex enzyme solution is 1 g/ml.
9. The method according to claim 1, wherein the time of the enzymatic reaction in step (3) is 12-24 h.
10. Use of a microporous tobacco powder according to any one of claims 1 to 9, compressed into a sheet for use in a low temperature cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911126843.5A CN110742301A (en) | 2019-11-18 | 2019-11-18 | Method for preparing microporous tobacco powder by complex enzyme method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911126843.5A CN110742301A (en) | 2019-11-18 | 2019-11-18 | Method for preparing microporous tobacco powder by complex enzyme method |
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| Publication Number | Publication Date |
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| CN110742301A true CN110742301A (en) | 2020-02-04 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911126843.5A Pending CN110742301A (en) | 2019-11-18 | 2019-11-18 | Method for preparing microporous tobacco powder by complex enzyme method |
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| Country | Link |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101940361A (en) * | 2010-10-11 | 2011-01-12 | 广东中烟工业有限责任公司 | Processing method of waste tobacco |
| CN103989246A (en) * | 2014-05-28 | 2014-08-20 | 广州市澳键丰泽生物科技有限公司 | Aroma-enhancing puffed tobacco stem particles and preparation method and application thereof |
| EP2881002A1 (en) * | 2013-12-06 | 2015-06-10 | Philip Morris Products S.A. | Methods, uses and apparatus for increasing the filling power of tobacco |
| CN107927890A (en) * | 2017-11-23 | 2018-04-20 | 重庆中烟工业有限责任公司 | One kind heats the reconstituted tobacoo and preparation method thereof that do not burn |
| CN108142979A (en) * | 2017-11-27 | 2018-06-12 | 深圳瑞宏邦科技有限公司 | Low temperature cigarette and preparation method thereof |
| CN108713788A (en) * | 2018-06-08 | 2018-10-30 | 湖北中烟工业有限责任公司 | The reconstituted tobacoo and production technology of a kind of high porosity applied to low temperature cigarette |
| CN109363230A (en) * | 2018-10-31 | 2019-02-22 | 云南恒罡科技有限公司 | It is a kind of to heat cigarette smoker particles inside material and preparation method thereof of not burning |
-
2019
- 2019-11-18 CN CN201911126843.5A patent/CN110742301A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101940361A (en) * | 2010-10-11 | 2011-01-12 | 广东中烟工业有限责任公司 | Processing method of waste tobacco |
| EP2881002A1 (en) * | 2013-12-06 | 2015-06-10 | Philip Morris Products S.A. | Methods, uses and apparatus for increasing the filling power of tobacco |
| CN103989246A (en) * | 2014-05-28 | 2014-08-20 | 广州市澳键丰泽生物科技有限公司 | Aroma-enhancing puffed tobacco stem particles and preparation method and application thereof |
| CN107927890A (en) * | 2017-11-23 | 2018-04-20 | 重庆中烟工业有限责任公司 | One kind heats the reconstituted tobacoo and preparation method thereof that do not burn |
| CN108142979A (en) * | 2017-11-27 | 2018-06-12 | 深圳瑞宏邦科技有限公司 | Low temperature cigarette and preparation method thereof |
| CN108713788A (en) * | 2018-06-08 | 2018-10-30 | 湖北中烟工业有限责任公司 | The reconstituted tobacoo and production technology of a kind of high porosity applied to low temperature cigarette |
| CN109363230A (en) * | 2018-10-31 | 2019-02-22 | 云南恒罡科技有限公司 | It is a kind of to heat cigarette smoker particles inside material and preparation method thereof of not burning |
Non-Patent Citations (1)
| Title |
|---|
| 高向阳: "《食品酶学》", 30 June 2016, 中国轻工业出版社 * |
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