CN110663698A - Medicament for preventing and controlling cockroach - Google Patents
Medicament for preventing and controlling cockroach Download PDFInfo
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- CN110663698A CN110663698A CN201910955913.1A CN201910955913A CN110663698A CN 110663698 A CN110663698 A CN 110663698A CN 201910955913 A CN201910955913 A CN 201910955913A CN 110663698 A CN110663698 A CN 110663698A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/002—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits
- A01N25/006—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits insecticidal
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/08—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
- A01N25/10—Macromolecular compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/04—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aldehyde or keto groups, or thio analogues thereof, directly attached to an aromatic ring system, e.g. acetophenone; Derivatives thereof, e.g. acetals
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- A—HUMAN NECESSITIES
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
- A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
- A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
- A01N43/38—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
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- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
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Abstract
The invention relates to the technical field of cockroach control, and provides a medicament for controlling cockroaches, aiming at the problem that animal grease is easy to deteriorate, the technical scheme is as follows: the paint comprises the following components in parts by mass: 11-15 parts of fatty glyceride; 16-20 parts of beeswax; 10-30 parts of casein; 0.002-0.01 part of fipronil; 60-100 parts of saccharides; 0.001-0.03 part of vanillin; and 1-5 parts of propyl gallate. By adding the propyl gallate and utilizing the better antioxidant effect of the propyl gallate, the water, oxygen, microorganisms and the like are not easy to contact the fatty glyceride, the fatty glyceride is not easy to generate microorganisms such as bacteria and the like, and the medicament for preventing and treating the cockroaches is not easy to deteriorate.
Description
Technical Field
The invention relates to the technical field of cockroach control, in particular to a medicament for controlling cockroaches.
Background
Cockroach, broadly, refers to an insect belonging to the order "blattaria" (academic name), belongs to the phylum arthropoda, class insecta, order blattaria, commonly known as cockroach, and is a common medical insect. Cockroaches are omnivorous insects, and the food types are very wide, including bread, rice, cakes, meat and vegetable cooked foods, melons and fruits, beverages and the like, particularly flour foods which like to eat fragrance, sweetness and oil, and the cockroaches have the habit of being addicted to grease, so the cockroaches are called as oil stealing cocktails in some places.
Fipronil is a synthetic insecticide with high efficiency, broad spectrum, low toxicity and biological degradation, and has strong contact poisoning effect on insects, and the action mechanism is to disturb the normal physiology of insect nerves, so that the insects die from excitation, spasm to paralysis. The fipronil is safe to human and livestock and has little pollution to environment due to small dosage and low use concentration.
The fipronil is used as a contact insecticide to kill cockroaches, the fipronil and food which is loved to be eaten by the cockroaches are required to be mixed to prepare a medicament, the food is eaten by the induced cockroaches or the medicament is contacted with the body surfaces of the cockroaches, the fipronil can enter the bodies of the cockroaches to cause poisoning, the cockroaches have habits of being loved by animal oil, but in summer, the animal oil is more easily deteriorated when being placed in a higher-temperature environment for a long time, the living environment of people is influenced, and therefore the space for improvement is provided.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a medicament for preventing and treating cockroaches, which has the advantage that animal oil is not easy to deteriorate.
In order to achieve the purpose, the invention provides the following technical scheme:
11-15 parts of fatty glyceride;
16-20 parts of beeswax;
10-30 parts of casein;
0.002-0.01 part of fipronil;
60-100 parts of saccharides;
0.001-0.03 part of vanillin;
and 1-5 parts of propyl gallate.
The invention is further configured to: the paint comprises the following components in parts by mass:
11-13 parts of fatty glyceride;
16-18 parts of beeswax;
15-25 parts of casein;
0.002-0.008 parts of fipronil;
70-90 parts of saccharides;
0.001-0.02 parts of vanillin;
and 2-4 parts of propyl gallate.
By adopting the technical scheme, the propyl gallate is added, and the better antioxidation effect of the propyl gallate is utilized, so that moisture, oxygen, microorganisms and the like are not easy to contact with the fatty glyceride, the fatty glyceride is not easy to generate microorganisms such as bacteria and the like, and further the medicament for preventing and controlling the cockroach is not easy to deteriorate, the effect of placing the medicament in corners for trapping and killing the cockroach is better, the use time is longer, and the living environment of people is not easily influenced;
by adding vanillin as a stabilizer, the stability of the propyl gallate is improved, the propyl gallate is high-temperature resistant, the propyl gallate is not easy to decompose in the heating process of the fatty glyceride, the propyl gallate is stable, the propyl gallate is further ensured to generate a better oxidation resistance effect on the fatty glyceride, the fatty glyceride is further prevented from generating bacteria and other microorganisms, and the medicament for preventing and treating the cockroaches is further prevented from going bad;
by adding the fatty glyceride and the saccharides, the cockroaches can easily find the corners where the medicament for preventing and controlling the cockroaches is placed, and the trapping and killing capacity of the medicament is improved;
by adding beeswax, the cockroach attractant has excellent effect on cockroach feeding, is dissolved when being heated, has better fluidity by mixing fatty glyceride with beeswax, is easier to keep the shape of the cockroach control agent after the beeswax is solidified, and is easy to process;
by adding casein as an adhesive, fatty glyceride, fipronil, saccharide, vanillin and propyl gallate are adhered together, so that various raw materials are uniformly mixed together to form a solid compound in the cooling process of the cockroach-controlling medicament, and the cockroach-controlling medicament is easy to divide and then is convenient to disperse in corners.
The invention is further configured to: the saccharide comprises one or more of glucose, brown sugar and maltose.
Through adopting above-mentioned technical scheme, include one or more in glucose, brown sugar, the maltose through the sugar for the medicament of prevention and cure cockroach attracts the cockroach more easily, makes the medicament trap and kill the effect and rises, and then increases the mortality of cockroach.
The invention is further configured to: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
5-10 parts of tannin.
Through adopting above-mentioned technical scheme, through adding the tannin, lure the cockroach to get to eat and make the cockroach contact the medicament of prevention and cure cockroach for the cockroach is easily touched and killed, improves the effect of trapping and killing the cockroach.
The invention is further configured to: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
5-9 parts of polyamide resin.
Through adopting above-mentioned technical scheme, through adding polyamide resin, have good heat conductivity for the heat in each big raw materials in the medicament of prevention and cure cockroach is derived fast, makes the medicament of prevention and cure cockroach cool off fast, and after the medicament of prevention and cure cockroach cooled off, the medicament that has increased the prevention and cure cockroach is solid state's stability, makes the shape of the medicament of prevention and cure cockroach comparatively stable.
The invention is further configured to: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
2-4 parts of hemicellulose.
By adopting the technical scheme, the hemicellulose and the polyamide resin form a reticular aggregate by adding the hemicellulose, so that the stability of the medicament for preventing and treating the cockroaches is improved, and the solid medicament for preventing and treating the cockroaches is convenient to cut.
The invention is further configured to: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
1-3 parts of vaseline.
By adopting the technical scheme, the medicament for preventing and treating the cockroach has better anti-rot effect by adding the vaseline, and the breeding of bacteria and the like in the medicament for preventing and treating the cockroach is reduced.
The invention is further configured to: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
5-7 parts of catecholamine.
Through adopting above-mentioned technical scheme, through adding catecholamine for the effect that the medicament of prevention and cure cockroach lured the food is better, makes the cockroach changeing through getting the food and contact the medicament of prevention and cure cockroach, makes the cockroach easier to be touched out, improves the effect of trapping and killing the cockroach.
The invention is further configured to: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
2-4 parts of xanthan gum.
Through adopting above-mentioned technical scheme, through adding xanthan gum, the medicament of prevention and cure cockroach when initial heating melts, forms the protection film on fatty glyceride's surface, promotes propyl gallate and utilizes the oxidation resistance for oxygen, the difficult inside that gets into the medicament of prevention and cure cockroach of water, make difficult production bacterium in the medicament of prevention and cure cockroach, xanthan gum has stronger emulsion stabilization simultaneously as the thickener, and chemical property is comparatively stable when making fatty glyceride cool off to solidify.
The invention is further configured to: the preparation method of the medicament for preventing and treating the cockroaches comprises the following steps:
s1, heating beeswax at a high temperature until the beeswax is completely melted, and adding fatty glyceride to form a molten solution;
s2, adding casein, fipronil, saccharides, vanillin and propyl gallate into the molten solution to form a medicament premix;
s3, injecting the medicament premix into a stainless steel mold to be cooled, solidified and molded so as to form the medicament for preventing and controlling the cockroaches.
Through adopting above-mentioned technical scheme, pour into to stainless steel mould in through the premix, the mould provides the space, the shape when making the medicament of prevention and cure cockroach cool off and solidify is comparatively stable, easily process into a plurality of shapes, because the cockroach is omnivorous insect, the accessible mould cuts into many copies with the medicament of prevention and cure cockroach, make the medicament of prevention and cure cockroach disperse in each corner, make the medicament suitability of prevention and cure cockroach wider, can place kitchen, room etc., make the medicament of prevention and cure cockroach touch and kill the cockroach effect more showing.
In conclusion, the invention has the following beneficial effects:
1. by adding the propyl gallate and utilizing the good antioxidant effect of the propyl gallate, moisture, oxygen, microorganisms and the like are not easy to contact with the fatty glyceride, the fatty glyceride is not easy to generate microorganisms such as bacteria and the like, and further the medicament for preventing and controlling the cockroaches is not easy to deteriorate, so that the medicament has good effect when being placed in corners for trapping and killing the cockroaches, has long service time and does not influence the living environment of people;
2. the preparation method comprises the following steps of adding casein as an adhesive, adhering fatty glyceride, fipronil, saccharides, vanillin and propyl gallate together, and enabling various raw materials to be uniformly mixed together to form a solid compound in the cooling process of the cockroach control agent, so that the cockroach control agent is easily divided and then dispersed in corners;
3. the sugar comprises one or more of glucose, brown sugar and maltose, so that the cockroach control agent can attract the cockroaches more easily, the trapping and killing effect of the cockroach control agent is improved, and the death rate of the cockroaches is increased.
Drawings
FIG. 1 is a schematic flow chart of the preparation method of the cockroach-controlling agent of the present invention.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings and examples.
In the following examples, the fatty acid glyceride used was a fatty acid glyceride sold by Cianhua Ruizhii food ingredients Co.
In the following examples, the beeswax was anhydrous beeswax sold by Guangdong gold ant chemical products Co.
In the following examples, casein is sold by Fuxi Zhen Fang food ingredient Co.
In the following examples, fipronil sold by the Canjiekang sanitary insecticide Ministry of drumbeat, Fuzhou is used.
In the following examples, edible glucose sold by Zhengzhou Dengyuan chemical products Co., Ltd was used as the glucose.
In the following examples, brown sugar is sold by bioscience, Inc., Yunan Peng.
In the following examples, the maltose is a maltose sold by chemical technology ltd of Jinanlin.
In the following examples, vanillin sold by Wuhana white pharmaceutical chemical Co., Ltd was used.
In the following examples, propyl gallate sold by Hakka zetta Biotechnology Co., Ltd is used.
In the following examples, tannins sold by Jinan Jiyang Biotech Co., Ltd are used.
In the following examples, PA66, which is a polyamide resin sold by Guanguan general Plastic materials Co., Ltd, was used as the polyamide resin.
In the following examples, hemicellulose is a hemicellulose sold by Anhui Biotech Co., Ltd.
In the following examples, white petrolatum sold by morning chemical industry Co., Ltd, Guangzhou city was used as the petrolatum.
In the following examples, catecholamines sold by Suzhou Tianke trade company, Inc. were used.
In the following examples, xanthan gum sold by yunxin biotechnology limited of quanzhou is used.
Example 1
The preparation method of the cockroach-controlling agent comprises the following steps:
a. heating 16kg of beeswax to be completely melted in a stirring kettle, and then adding 11kg of fatty glyceride to form a molten solution;
b. adding 10kg of casein, 0.002kg of fipronil, 10kg of glucose, 20kg of brown sugar, 30kg of maltose, 0.001kg of vanillin and 1kg of propyl gallate into a stirring kettle, and stirring for 10min at the rotating speed of 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Example 2
The preparation method of the cockroach-controlling agent comprises the following steps:
a. heating 17kg of beeswax to be completely melted in a stirring kettle, and then adding 12kg of fatty glyceride to form a molten solution;
b. adding 15kg of casein, 0.004kg of fipronil, 20kg of glucose, 20kg of brown sugar, 30kg of maltose, 0.002kg of vanillin and 2kg of propyl gallate into a stirring kettle, and stirring for 10min at the rotating speed of 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Example 3
The preparation method of the cockroach-controlling agent comprises the following steps:
a. heating 18kg of beeswax to be completely melted in a stirring kettle, and then adding 13kg of fatty glyceride to form a molten solution;
b. adding casein 20kg, fipronil 0.006kg, glucose 20kg, brown sugar 30kg, maltose 30kg, vanillin 0.01kg and propyl gallate 3kg into a stirring kettle, stirring for 10min at 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Example 4
The preparation method of the cockroach-controlling agent comprises the following steps:
a. heating 19kg of beeswax to be completely melted in a stirring kettle, and then adding 14kg of fatty glyceride to form a molten solution;
b. adding 25kg of casein, 0.008kg of fipronil, 20kg of glucose, 30kg of brown sugar, 40kg of maltose, 0.02kg of vanillin and 4kg of propyl gallate into a stirring kettle, and stirring for 10min at the rotating speed of 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Example 5
The preparation method of the cockroach-controlling agent comprises the following steps:
a. in a stirring kettle, firstly heating 20kg of beeswax to be completely molten, and then adding 15kg of fatty glyceride to form a molten solution;
b. adding 30kg of casein, 0.01kg of fipronil, 20kg of glucose, 35kg of brown sugar, 45kg of maltose, 0.03kg of vanillin and 5kg of propyl gallate into a stirring kettle, and stirring for 10min at the rotating speed of 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Example 6
The preparation method of the cockroach-controlling agent comprises the following steps:
a. heating 18kg of beeswax to be completely melted in a stirring kettle, and then adding 12kg of fatty glyceride to form a molten solution;
b. adding 22kg of casein, 0.005kg of fipronil, 22kg of glucose, 30kg of brown sugar, 43kg of maltose, 0.02kg of vanillin and 3kg of propyl gallate into a stirring kettle, and stirring for 10min at the rotating speed of 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Example 7
The preparation method of the cockroach-controlling agent comprises the following steps:
a. heating 18kg of beeswax to be completely melted in a stirring kettle, and then adding 12kg of fatty glyceride to form a molten solution;
b. adding 22kg of casein, 0.005kg of fipronil, 22kg of glucose, 30kg of brown sugar, 43kg of maltose, 0.02kg of vanillin, 3kg of propyl gallate, 5kg of tannin, 5kg of polyamide resin, 2kg of hemicellulose, 1kg of vaseline, 5kg of catecholamine and 2kg of xanthan gum into a stirring kettle, and stirring for 10min at the rotating speed of 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Example 8
The preparation method of the cockroach-controlling agent comprises the following steps:
a. heating 18kg of beeswax to be completely melted in a stirring kettle, and then adding 12kg of fatty glyceride to form a molten solution;
b. adding 22kg of casein, 0.005kg of fipronil, 22kg of glucose, 30kg of brown sugar, 43kg of maltose, 0.02kg of vanillin, 3kg of propyl gallate, 7.5kg of tannin, 7kg of polyamide resin, 3kg of hemicellulose, 2kg of vaseline, 6kg of catecholamine and 3kg of xanthan gum into a stirring kettle, and stirring for 10min at the rotating speed of 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Example 9
The preparation method of the cockroach-controlling agent comprises the following steps:
a. heating 18kg of beeswax to be completely melted in a stirring kettle, and then adding 12kg of fatty glyceride to form a molten solution;
b. adding 22kg of casein, 0.005kg of fipronil, 22kg of glucose, 30kg of brown sugar, 43kg of maltose, 0.02kg of vanillin, 3kg of propyl gallate, 10kg of tannin, 9kg of polyamide resin, 4kg of hemicellulose, 3kg of vaseline, 7kg of catecholamine and 4kg of xanthan gum into a stirring kettle, and stirring for 10min at the rotating speed of 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Example 10
The preparation method of the cockroach-controlling agent comprises the following steps:
a. heating 18kg of beeswax to be completely melted in a stirring kettle, and then adding 12kg of fatty glyceride to form a molten solution;
b. adding 22kg of casein, 0.005kg of fipronil, 22kg of glucose, 30kg of brown sugar, 43kg of maltose, 0.02kg of vanillin, 3kg of propyl gallate, 8kg of tannin, 9kg of polyamide resin, 3.7kg of hemicellulose, 2kg of vaseline, 5kg of catecholamine and 3.5kg of xanthan gum into a stirring kettle, and stirring for 10min at the rotating speed of 70r/min to form a medicament premix;
c. injecting the medicament premix into a stainless steel mold, pressing the medicament premix under the pressure of 3MPa, cooling and molding the medicament premix to form the medicament for preventing and treating the cockroaches, and then cutting the medicament for preventing and treating the cockroaches into a plurality of pieces.
Comparative example 1
The difference from example 10 is that:
in step b, propyl gallate is not added.
Comparative example 2
The difference from example 10 is that:
in step b, vanillin is removed.
Comparative example 3
The difference from example 10 is that:
in step b, the addition of tannin is eliminated.
Comparative example 4
The difference from example 10 is that:
in step b, the addition of hemicellulose is eliminated.
Comparative example 5
The difference from example 10 is that:
in step b, the addition of catecholamines is eliminated.
Comparative example 6
The difference from example 10 is that:
in step b, xanthan gum is not added.
Test 1
The method comprises the following steps:
1. selecting a constant temperature box, placing a plastic basin in the constant temperature box, and scattering a layer of bread crumbs in the plastic basin, wherein the thickness of the bread crumbs is about 2-3 mm.
2. Distilled water was sprayed on the bread crumbs, and during the experiment, a warm and humid environment was kept in an incubator, 2g of the cockroach control agent of each example and each comparative example was placed in a paper cup (diameter 50mm, height 40mm), the opening of the paper cup was faced upward, the width of the opening was 10mm, 3 repeating groups were provided for each example and comparative example, 51 paper cups in a plastic pot were randomly arranged and numbered.
3. 1000 Blattella germanica were placed in the center of a plastic pot and tested in an indoor incubator (28 + -2 deg.C, 86 + -4% RH) in the dark.
4. Every morning 7: 00 and night 12: 00 observing once respectively, observing and recording the number of the cockroaches in each paper cup, observing for 7d totally, calculating the times of the cockroaches appearing in the paper cups, calculating the relative reaction rate of the cockroaches to the cockroach control medicaments of each embodiment and comparative example according to the following formula, and setting the relative reaction rate of the cockroach control medicament accumulating the maximum number of the cockroaches to be 100%; the "relative reaction rate" reflects the degree of preference of the cockroach against the cockroach-controlling agent, and the larger the numerical value is, the stronger the intention of the cockroach to take the cockroach-controlling agent is, and the deterioration of each example and each comparative example was observed simultaneously during the test period.
Test 2
The method comprises the following steps:
1. selecting a constant temperature box, placing a plastic basin in the constant temperature box, and scattering a layer of bread crumbs in the plastic basin, wherein the thickness of the bread crumbs is about 2-3 mm.
2. Some distilled water was sprayed on the breading and during the experiment, a warm and moist environment was maintained in the incubator.
3. 1000 Blatta germanica were placed in the center of a plastic pot, and 2g of the cockroach control agents of examples and comparative examples were placed in a cockroach group, and the cockroach control agents were tested in an indoor incubator (28. + -. 2 ℃ C., 86. + -. 4% RH) in the dark, and the death results of 7d Blatta Seu Periplaneta were observed.
TABLE 1
Relative reaction rate% | Degree of deterioration | The mortality rate is% | |
Example 1 | 92 | No deterioration | 92 |
Example 2 | 93 | No deterioration | 93 |
Example 3 | 94 | No deterioration | 94 |
Example 4 | 93 | No deterioration | 93 |
Example 5 | 94 | No deterioration | 94 |
Example 6 | 95 | No deterioration | 95 |
Example 7 | 98 | No deterioration | 98 |
Example 8 | 98 | No deterioration | 98 |
Example 9 | 99 | No deterioration | 99 |
Example 10 | 100 | No deterioration | 100 |
Comparative example 1 | 85 | Deterioration of the quality | 85 |
Comparative example 2 | 99 | No deterioration | 99 |
Comparative example 3 | 93 | No deterioration | 93 |
Comparative example 4 | 95 | No deterioration | 95 |
Comparative example 5 | 96 | No deterioration | 96 |
According to table 1, it is known that the propyl gallate makes the cockroach controlling chemical not easy to deteriorate, makes the chemical better placed in the corners where cockroaches are trapped and killed, has a longer service time, and does not affect the living environment of people by comparing example 10 with comparative example 1.
The relative reaction rate of the cockroaches can be effectively improved by adding the tannin and the catecholamine, the cockroaches are induced to eat so that the cockroaches contact with the medicament for preventing and controlling the cockroaches, the cockroaches are easy to be killed by touch, and the death rate of the trapped cockroaches is improved.
The embodiments of the present invention are preferred embodiments of the present invention, and the scope of the present invention is not limited by these embodiments, so: all equivalent changes made according to the structure, shape and principle of the invention are covered by the protection scope of the invention.
Claims (10)
1. The cockroach control agent is characterized in that: the paint comprises the following components in parts by mass:
11-15 parts of fatty glyceride;
16-20 parts of beeswax;
10-30 parts of casein;
0.002-0.01 part of fipronil;
60-100 parts of saccharides;
0.001-0.03 part of vanillin;
and 1-5 parts of propyl gallate.
2. The agent for controlling cockroach according to claim 1, which comprises: the paint comprises the following components in parts by mass:
11-13 parts of fatty glyceride;
16-18 parts of beeswax;
15-25 parts of casein;
0.002-0.008 parts of fipronil;
70-90 parts of saccharides;
0.001-0.02 parts of vanillin;
and 2-4 parts of propyl gallate.
3. The agent for controlling cockroach according to claim 2, which comprises: the saccharide comprises one or more of glucose, brown sugar and maltose.
4. The agent for controlling cockroach according to claim 3, which comprises: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
5-10 parts of tannin.
5. The agent for controlling cockroach according to claim 4, which comprises: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
5-9 parts of polyamide resin.
6. The agent for controlling cockroach according to claim 1, which comprises: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
2-4 parts of hemicellulose.
7. The agent for controlling cockroach according to claim 1, which comprises: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
1-3 parts of vaseline.
8. The agent for controlling cockroach according to claim 1, which comprises: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
5-7 parts of catecholamine.
9. The agent for controlling cockroach according to claim 1, which comprises: the medicament for preventing and treating the cockroach further comprises the following components in parts by mass:
2-4 parts of xanthan gum.
10. The agent for controlling cockroach according to claim 1, which comprises: the preparation method of the medicament for preventing and treating the cockroaches comprises the following steps:
s1, heating beeswax at a high temperature until the beeswax is completely melted, and adding fatty glyceride to form a molten solution;
s2, adding casein, fipronil, saccharides, vanillin and propyl gallate into the molten solution to form a medicament premix;
s3, injecting the medicament premix into a stainless steel mold to be cooled, solidified and molded so as to form the medicament for preventing and controlling the cockroaches.
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CN102845466A (en) * | 2012-08-13 | 2013-01-02 | 北京绿叶世纪日化用品有限公司 | High-efficiency cockroach-killing bait and preparation method thereof |
CN106305803A (en) * | 2015-07-10 | 2017-01-11 | 王忠良 | Method for preparing tung oil pesticide |
CN107047608A (en) * | 2017-05-26 | 2017-08-18 | 东至县珊瑚生态农业发展有限公司 | A kind of preparation method for trapping and killing cockroach high-efficiency environment friendly medicament |
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2019
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CN102845466A (en) * | 2012-08-13 | 2013-01-02 | 北京绿叶世纪日化用品有限公司 | High-efficiency cockroach-killing bait and preparation method thereof |
CN106305803A (en) * | 2015-07-10 | 2017-01-11 | 王忠良 | Method for preparing tung oil pesticide |
CN107047608A (en) * | 2017-05-26 | 2017-08-18 | 东至县珊瑚生态农业发展有限公司 | A kind of preparation method for trapping and killing cockroach high-efficiency environment friendly medicament |
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