CN110651980A - Peony pollen buccal tablet and preparation process thereof - Google Patents
Peony pollen buccal tablet and preparation process thereof Download PDFInfo
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- CN110651980A CN110651980A CN201910950084.8A CN201910950084A CN110651980A CN 110651980 A CN110651980 A CN 110651980A CN 201910950084 A CN201910950084 A CN 201910950084A CN 110651980 A CN110651980 A CN 110651980A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
- Medicinal Preparation (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention belongs to the technical field of health-care food, and particularly relates to a peony pollen buccal tablet and a preparation process thereof. The preparation process comprises the following steps: crushing and sieving the peony pollen, rape pollen and mint leaf raw medicinal materials, mixing, adding auxiliary materials into the mixed powder to prepare a soft material, preparing granules, drying and sieving the obtained granules, and finally tabletting to obtain the peony pollen buccal tablet. The buccal tablet prepared by the invention has moderate sweet and sour taste, sharp drug fragrance, uniform color and simple process, can supplement nutrition required by human body, has prostate health care effect, can meet market demand, and has wide market prospect.
Description
Technical Field
The invention belongs to the technical field of health-care food, and particularly relates to a peony pollen buccal tablet and a preparation process thereof.
Background
Paeonia suffruticosa Andr is deciduous shrub of Paeonia of Paeoniaceae. It is listed as the "Shen nong Ben Cao Jing" as the "Zhong Pin". The peony has high ornamental value, medicinal value and economic value. Cortex moutan is dried root bark of Paeonia suffruticosa Andr. Bitter and pungent in property, slightly cold in nature. It enters heart, liver and kidney meridians. Has antibacterial, antiinflammatory, hemostatic, analgesic, and antitumor effects, and can promote phagocytosis of monocyte, improve specific immunity, clear heat and cool blood, and cool blood without stasis, and promote blood circulation without loss of blood. Peony pollen contains abundant amino acids and proteins; contains various nutrients, vitamins and minerals; contains a large amount of natural active substances, such as enzyme, flavonoid, organic acid, hormone, nucleic acid, etc., and can promote health and enhance defense capability of organism.
Rape (Brassica campestris) is a plant of the genus Rutaceae, Ruta, and is an annual or biennial herb. The rape pollen is nearly spherical, and the appearance of the polar surface is a three-split round shape. The rape has large cultivation area, wide distribution area, multiple varieties, high yield and easy collection. Rape is an important oil crop in China, and is widely developed and utilized in China, and according to research, rape pollen has the effects of inhibiting prostatic hyperplasia, regulating the smooth muscle tension of the urinary system and inhibiting the growth of prostate cells in vitro.
Peppermint (Mentha haplocalyx Briq.) is the dried aerial parts of Mentha haplocalyx of Labiatae. It is pungent in flavor and cool in nature. It enters lung and liver meridians. Has effects of dispelling heat, clearing head and eyes, relieving sore throat, promoting eruption, dispersing stagnated liver qi, and activating qi-flowing.
Buccal tablets are pressed tablets which are slowly dissolved in oral cavity, and are convenient to carry and use, good in taste and wide in application range. As a health food, pollen is popular and important, and as early as two thousand years ago, the application of the pollen in China has been recorded in many ways. Peony resources are rich and various in China, but people have less research on peony pollen products, and a large amount of peony pollen is wasted. In order to improve the utilization rate of peony flower resources and facilitate the consumption of consumers, it is necessary to develop a buccal tablet using peony flower powder as a main raw material.
Disclosure of Invention
The invention provides a peony pollen buccal tablet and a preparation process thereof, which improve the utilization rate of peony resources and are convenient for consumers to eat.
The first purpose of the invention is to provide a peony pollen buccal tablet which is prepared from the following raw materials in parts by weight: 30-55 parts of peony pollen, 0-25 parts of rape pollen, 3-8 parts of mint leaves, 0.8-1.8 parts of citric acid, 40 parts of mannitol, 1-6 parts of sodium carboxymethyl starch and 10-30 parts of starch slurry.
Preferably, the peony pollen buccal tablet is prepared from the following raw materials in parts by weight: 35 parts of peony pollen, 13 parts of rape pollen, 6 parts of mint leaf, 1 part of citric acid, 40 parts of mannitol, 5 parts of sodium carboxymethyl starch and 20 parts of starch slurry.
Preferably, the mass concentration of the starch slurry in the peony pollen buccal tablet is 8-15 g/100 ml.
Preferably, the peony pollen buccal tablet is prepared from the starch slurry according to the following method: suspending 8-15 g of corn starch in 5-10 ml of normal-temperature water, adding boiling water to make up for 100ml, stirring while adding boiling water until gelatinization is achieved, and thus obtaining starch slurry.
The second purpose of the invention is to provide a preparation method of the peony pollen buccal tablet, which comprises the following steps:
weighing 30-55 parts of peony pollen, 0-25 parts of rape pollen, 3-8 parts of mint leaves, 0.8-1.8 parts of citric acid, 40 parts of mannitol, 1-6 parts of sodium carboxymethyl starch and 10-30 parts of starch slurry;
respectively crushing peony pollen, rape pollen and mint leaves, sieving with a sieve of 80-100 meshes to respectively obtain peony powder, rape flower powder and mint leaf powder, and storing at low temperature for later use;
uniformly mixing peony flower powder, rape flower powder, mint leaf powder, citric acid, mannitol and sodium carboxymethyl starch to obtain mixed powder;
adding the starch slurry into the mixed powder, and uniformly mixing to obtain a soft material;
and pouring the soft material into a granulation machine to prepare granules, drying the obtained granules, taking the granules with 24-100 meshes, and tabletting to obtain the peony pollen buccal tablet.
Preferably, the preparation method of the peony pollen buccal tablet comprises the following steps of uniformly mixing peony powder, rape flower powder, mint leaf powder, citric acid, mannitol and sodium carboxymethyl starch by an equivalent incremental method and a priming chromatography method, wherein the specific steps are as follows:
step 1, using the inner surface of a container used when mannitol saturated materials are mixed;
step 2, adding citric acid into the container, adding mint powder with the same mass as the citric acid, and uniformly mixing to obtain a mixture; adding herba Menthae powder with equal mass to the obtained mixture, mixing, and adding herba Menthae powder until the herba Menthae powder is completely added;
step 3, adding rape pollen with the quality equal to that of the mixture obtained in the last step in the step 2, and uniformly mixing; continuously adding rape pollen powder, wherein the adding amount of the rape pollen is equal to the total mass of the mixture obtained at the last time each time until the rape pollen is added;
and 3, adding peony pollen, uniformly mixing, and finally adding the rest mannitol, and uniformly mixing to obtain mixed powder.
Preferably, in the preparation method of the peony pollen buccal tablet, the concentration of the starch slurry is 10g/100ml, and the added amount of the starch slurry is 1g of starch slurry added to every 5g of mixed powder.
Compared with the prior art, the peony pollen buccal tablet and the preparation process thereof provided by the invention at least have the following beneficial effects:
the peony pollen buccal tablet is prepared by taking peony pollen as a main drug, rape pollen and mint leaf as auxiliary drugs, adding citric acid, sodium carboxymethyl starch, mannitol and starch slurry as auxiliary materials and adopting a wet granulation tabletting method. The developed peony pollen buccal tablet can fully utilize peony pollen, and simultaneously combines the pollen with the buccal tablet, so that the pollen is slowly dissolved in the oral cavity, the effective components in the pollen can be slowly released, the stimulation to the gastrointestinal tract is reduced, the nutritional and medicinal effects can be conveniently and quickly exerted, and the peony pollen buccal tablet is easy to store, convenient to carry and use and has more advantages than other dosage forms. It can not only supplement nutrients necessary for human body, but also has prostate health promotion effect. The peony pollen buccal tablet obtained by the test has moderate sweet and sour taste, strong medicinal fragrance, moderate hardness, can meet the market demand and has wide market prospect.
Drawings
FIG. 1 is an appearance diagram of the peony pollen buccal tablet prepared in example 1;
FIG. 2 is an appearance diagram of the peony pollen buccal tablet prepared in example 2;
FIG. 3 is an appearance diagram of the peony pollen buccal tablet prepared in example 3;
FIG. 4 is an appearance diagram of the peony pollen buccal tablet prepared in example 4;
fig. 5 is an appearance diagram of the peony pollen buccal tablet prepared in the comparative example 1.
Detailed Description
In order that those skilled in the art will better understand the technical solutions of the present invention to be implemented, the present invention will be further described with reference to the following specific embodiments and accompanying drawings. The following examples, as well as test methods not specifically identified in the summary of the invention, were conducted according to methods and conditions conventional in the art.
The experimental methods and the detection methods described in the following examples are all conventional methods unless otherwise specified; the reagents and materials are commercially available, unless otherwise specified. In the following examples: peony pollen from Fenhe peony group Co., Ltd, rape pollen from Taobao Mengda bee industry, and mint leaf from Shanxi Taigu kernel and big pharmacy.
The invention provides a peony pollen buccal tablet which is prepared from the following raw materials in parts by weight: 30-55 parts of peony pollen, 0-25 parts of rape pollen, 3-8 parts of mint leaves, 0.8-1.8 parts of citric acid, 40 parts of mannitol, 1-6 parts of sodium carboxymethyl starch and 10-30 parts of starch slurry. Wherein the addition amount of the starch slurry is 8-15% of the total mass of other materials; if less than 8%, the viscosity is too low to form particles; if the content is more than 15%, the formed granules are long strips or noodles, and are not suitable for tabletting.
In the invention, the peony pollen contains abundant amino acid and protein; contains a large amount of natural active substances, and can promote health and enhance body defense ability.
Rape pollen can inhibit prostatic hyperplasia and regulate urinary system smooth muscle tension.
Mint is pungent in flavor and cool in nature. It enters lung and liver meridians. Has effects of dispelling heat, relieving sore throat, promoting eruption, clearing head and eyes, dispersing stagnated liver qi, and activating qi-flowing.
Mannitol is a white crystalline or crystalline powder, odorless, sweet in taste, and is often used as a bulking agent and sweetener. It is easily dissolved in water, and has heat absorption and refreshing feeling. In the food sector, mannitol is used as a low-calorie, low-sugar sweetener.
Citric acid has a refreshing sour taste and is used as a sour agent.
Sodium carboxymethyl starch (CMS-Na) is white or quasi-white powder, odorless, highly swellable, and used as disintegrant.
Starch slurry is a common adhesive, and the preparation method mainly comprises a slurry punching method and a slurry cooking method. The embodiment of the invention is prepared by adopting a slurry method. The mass concentration of the starch slurry is 8-15 g/100ml, and the preparation method comprises the following steps: suspending 8-15 g of corn starch in 5-10 ml of normal-temperature water, adding boiling water to make up for 100ml, stirring while adding boiling water until gelatinization is achieved, and thus obtaining starch slurry.
Example 1
The peony pollen buccal tablet is prepared from the following raw materials in parts by weight: 30g of peony pollen, 20.2g of rape pollen, 6g of mint leaf, 0.8g of citric acid, 40g of mannitol, 3g of sodium carboxymethyl starch and 20g of starch slurry.
The preparation process of the peony pollen buccal tablet comprises the following steps:
weighing 30g of peony pollen, 20.2g of rape pollen, 6g of mint leaves, 0.8g of citric acid, 40g of mannitol, 3g of sodium carboxymethyl starch and 20g of starch slurry;
respectively crushing peony pollen, rape pollen and mint leaves, respectively sieving with a 80-mesh sieve to respectively obtain peony flower powder, rape flower powder and mint leaf powder, and storing at low temperature of 4 ℃ for later use;
uniformly mixing peony flower powder, rape flower powder, mint leaf powder, citric acid, mannitol and sodium carboxymethyl starch by an equivalent incremental method and a priming chromatography method to obtain mixed powder;
adding 10g/100ml starch slurry into the mixed powder, and mixing to obtain soft material;
pouring the soft material into a small-sized granulator (YK-60, Changsha Corning electronic technology Co., Ltd.) to prepare granules, drying the obtained granules, sieving with a 100-mesh sieve to obtain granules, and tabletting with a manual tabletting machine (auspicious pharmaceutical machinery Co., Ltd., manual tabletting machine die) to obtain the peony pollen buccal tablet, wherein the appearance diagram of the peony pollen buccal tablet is shown in figure 1.
Wherein, the equal quantity increases progressively the method and gives a bottom to the chromatography and mixes, the concrete step is as follows:
step 1, using the inner surface of a container used when mannitol saturated materials are mixed;
step 2, adding citric acid into the container, adding mint powder with the same mass as the citric acid, and uniformly mixing to obtain a mixture; adding herba Menthae powder with equal mass to the obtained mixture, mixing, and adding herba Menthae powder until the herba Menthae powder is completely added;
step 3, adding rape pollen with the quality equal to that of the mixture obtained in the last step in the step 2, and uniformly mixing; continuously adding rape pollen powder, wherein the adding amount of the rape pollen is equal to the total mass of the mixture obtained at the last time each time until the rape pollen is added;
and 3, adding peony pollen, uniformly mixing, and finally adding the rest mannitol, and uniformly mixing to obtain mixed powder.
Example 2
The peony pollen buccal tablet is prepared from the following raw materials in parts by weight: 35g of peony pollen, 13.8g of rape pollen, 7g of mint leaf, 1.2g of citric acid, 40g of mannitol, 3g of sodium carboxymethyl starch and 20g of starch slurry. The preparation method of the peony pollen buccal tablet is basically the same as that of the embodiment 1, and the differences are that: and (3) pouring the soft material into a granulation machine to prepare granules, drying the obtained granules, and taking the granules with 24 meshes. Example 2 the appearance of the peony pollen buccal tablet is shown in figure 2.
Example 3
The peony pollen buccal tablet is prepared from the following raw materials in parts by weight: 35g of peony pollen, 13g of rape pollen, 6g of mint leaf, 1g of citric acid, 40g of mannitol, 5g of sodium carboxymethyl starch and 20g of starch slurry. The preparation method of the peony pollen buccal tablet is basically the same as that of the embodiment 1, and the differences are that: and (3) pouring the soft material into a granulation machine to prepare granules, drying the obtained granules, and taking 80-mesh granules. Example 3 the appearance of the peony pollen buccal tablet is shown in figure 3.
Example 4
A buccal tablet of peony pollen is prepared from the following raw materials in parts by weight; the raw materials comprise 40g of peony pollen, 8.8g of rape pollen, 6g of mint leaves, 1.2g of citric acid, 40g of mannitol, 4g of sodium carboxymethyl starch and 20g of starch slurry. The preparation method of the peony pollen buccal tablet is the same as that of the embodiment 1. Example 4 the appearance of the peony pollen buccal tablet is shown in figure 4.
Example 5
A buccal tablet of peony pollen is prepared from the following raw materials in parts by weight; the raw materials comprise 55g of peony pollen, 3g of mint leaves, 0.8g of citric acid, 40g of mannitol, 1g of sodium carboxymethyl starch and 10g of starch slurry. The preparation method of the peony pollen buccal tablet is basically the same as that of the embodiment 1, and the differences are that: respectively crushing peony pollen, rape pollen and mint leaves, respectively sieving with a 100-mesh sieve to respectively obtain peony powder, rape flower powder and mint leaf powder, and storing at a low temperature of 10 ℃; the concentration of the starch slurry was 15g/100 ml.
Example 6
A buccal tablet of peony pollen is prepared from the following raw materials in parts by weight; the raw materials comprise 30g of peony pollen, 25g of rape pollen, 8g of mint leaf, 1.8g of citric acid, 40g of mannitol, 6g of sodium carboxymethyl starch and 30g of starch slurry. The preparation method of the peony pollen buccal tablet is basically the same as that of the embodiment 1, and the differences are that: respectively crushing peony pollen, rape pollen and mint leaves, respectively sieving with a 100-mesh sieve to respectively obtain peony powder, rape flower powder and mint leaf powder, and storing at a low temperature of 5 ℃; the concentration of the starch slurry was 8g/100 ml.
Comparative example 1
A buccal tablet of peony pollen is prepared from the following raw materials in parts by weight; the raw materials comprise 30g of peony pollen, 25g of rape pollen, 8g of mint leaf, 1.8g of citric acid, 40g of mannitol, 6g of sodium carboxymethyl starch and 7g of starch slurry, and the preparation method is the same as that of example 1. The results show that the buccal tablet prepared in the comparative example 1 has mottle, is close to a split tablet and has poor appearance effect. Comparative example 1 the appearance of the peony pollen buccal tablet is shown in fig. 5.
Subsequently, in order to verify the mouthfeel of the present invention, sensory evaluations were performed by a 10-person panelist, and the sensory evaluation criteria are shown in table 1.
TABLE 1 sensory Scoring criteria
The sensory evaluation was performed on examples 1 to 6 and comparative example 1 in accordance with table 1, and the results are shown in tables 2 to 3, including an average score of 87 points for example 1, an average score of 89 points for example 2, an average score of 90 points for example 3, an average score of 83 points for example 4, an average score of 80 points for example 5, an average score of 85 points for example 6, and an average score of 66 points for comparative example 1.
TABLE 2 sensory scores for examples 1-3 and comparative examples
Table 3 examples 4-6 sensory scores
The physicochemical evaluation criteria were carried out in accordance with the pharmacopoeia of the people's republic of China (2015 edition), and the test results are shown in Table 4.
TABLE 4 sensory scores for various examples and comparative examples
The buccal tablet prepared by the invention has moderate sweet and sour taste, fragrant medicine fragrance, uniform color and luster and simple process. The peony pollen buccal tablet researched and developed by the invention can fully utilize peony pollen, and simultaneously combine pollen with the buccal tablet, so that the pollen is contained in the oral cavity and slowly dissolved, the active ingredients in the pollen can be slowly released, the stimulation to the gastrointestinal tract is reduced, the nutritional and medicinal effects can be conveniently and quickly exerted, the nutrition required by a human body can be supplemented, and the prostate health-care effect is achieved. Can meet the market demand and has wide market prospect.
It should be noted that, when referring to numerical ranges in the present invention, it should be understood that both endpoints of each numerical range and any number between the two endpoints can be selected, and in order to prevent redundant description, the present invention describes the preferred embodiment, but those skilled in the art can make other changes and modifications to the embodiment once they learn the basic inventive concept. Therefore, it is intended that the appended claims be interpreted as including preferred embodiments and all such alterations and modifications as fall within the scope of the invention. It will be apparent to those skilled in the art that various changes and modifications may be made in the present invention without departing from the spirit and scope of the invention. Thus, if such modifications and variations of the present invention fall within the scope of the claims of the present invention and their equivalents, the present invention is also intended to include such modifications and variations.
Claims (7)
1. The peony pollen buccal tablet is characterized by being prepared from the following raw materials in parts by weight: 30-55 parts of peony pollen, 0-25 parts of rape pollen, 3-8 parts of mint leaves, 0.8-1.8 parts of citric acid, 40 parts of mannitol, 1-6 parts of sodium carboxymethyl starch and 10-30 parts of starch slurry.
2. The peony pollen buccal tablet according to claim 1, which is prepared from the following raw materials in parts by weight: 35 parts of peony pollen, 13 parts of rape pollen, 6 parts of mint leaf, 1 part of citric acid, 40 parts of mannitol, 5 parts of sodium carboxymethyl starch and 20 parts of starch slurry.
3. The peony pollen buccal tablet as claimed in claim 1, wherein the mass concentration of the starch slurry is 8-15 g/100 ml.
4. The peony pollen buccal tablet according to claim 3, wherein the starch slurry is prepared by the following method: suspending 8-15 g of corn starch in 5-10 ml of normal-temperature water, adding boiling water to make up for 100ml, stirring while adding boiling water until gelatinization is achieved, and thus obtaining starch slurry.
5. The preparation method of the peony pollen buccal tablet according to claim 1, which is characterized by comprising the following steps:
weighing 30-55 parts of peony pollen, 0-25 parts of rape pollen, 3-8 parts of mint leaves, 0.8-1.8 parts of citric acid, 40 parts of mannitol, 1-6 parts of sodium carboxymethyl starch and 10-30 parts of starch slurry;
respectively crushing peony pollen, rape pollen and mint leaves, sieving with a sieve of 80-100 meshes to respectively obtain peony powder, rape flower powder and mint leaf powder, and storing at low temperature for later use;
uniformly mixing peony flower powder, rape flower powder, mint leaf powder, citric acid, mannitol and sodium carboxymethyl starch to obtain mixed powder;
adding the starch slurry into the mixed powder, and uniformly mixing to obtain a soft material;
and pouring the soft material into a granulation machine to prepare granules, drying the obtained granules, taking the granules with 24-100 meshes, and tabletting to obtain the peony pollen buccal tablet.
6. The preparation method of the peony pollen buccal tablet according to claim 5, wherein the peony flower powder, the rape flower powder, the mint leaf powder, the citric acid, the mannitol and the sodium carboxymethyl starch are mixed uniformly by an equivalent incremental method and a priming chromatography method, and the specific steps are as follows:
step 1, using the inner surface of a container used when mannitol saturated materials are mixed;
step 2, adding citric acid into the container, adding mint powder with the same mass as the citric acid, and uniformly mixing to obtain a mixture; adding herba Menthae powder with equal mass to the obtained mixture, mixing, and adding herba Menthae powder until the herba Menthae powder is completely added;
step 3, adding rape pollen with the quality equal to that of the mixture obtained in the last step in the step 2, and uniformly mixing; continuously adding rape pollen powder, wherein the adding amount of the rape pollen is equal to the total mass of the mixture obtained at the last time each time until the rape pollen is added;
and 3, adding peony pollen, uniformly mixing, and finally adding the rest mannitol, and uniformly mixing to obtain mixed powder.
7. The method for preparing peony pollen buccal tablet according to claim 5, wherein the concentration of starch slurry is 10g/100ml, and the amount of starch slurry added is 1g per 5g of mixed powder.
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