CN110651980B - Peony pollen buccal tablet and preparation process thereof - Google Patents
Peony pollen buccal tablet and preparation process thereof Download PDFInfo
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- CN110651980B CN110651980B CN201910950084.8A CN201910950084A CN110651980B CN 110651980 B CN110651980 B CN 110651980B CN 201910950084 A CN201910950084 A CN 201910950084A CN 110651980 B CN110651980 B CN 110651980B
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
- A23P10/28—Tabletting; Making food bars by compression of a dry powdered mixture
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
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- Medicines Containing Plant Substances (AREA)
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Abstract
The invention belongs to the technical field of health-care foods, and in particular relates to a peony pollen buccal tablet and a preparation process thereof. The preparation process comprises the following steps: pulverizing flos moutan pollen, flos Brassicae campestris pollen, and folium Menthae, sieving, mixing, adding adjuvants, making soft mass, granulating, drying, sieving, and tabletting. The buccal tablet prepared by the invention has moderate sour and sweet taste, strong medicinal fragrance, uniform color and luster and simple process, can supplement nutrition required by human body, has the health care effect of the prostate, can adapt to market demands, and has wide market prospect.
Description
Technical Field
The invention belongs to the technical field of health-care foods, and particularly relates to a peony pollen buccal tablet and a preparation process thereof.
Background
The Paeonia suffruticosa (Paeonia suffruticosa Andr.) is a deciduous shrub of Paeoniaceae, paeonia. It is listed as a middle-grade product in Shen nong Ben Cao Jing. The peony has high ornamental value, and has high medicinal value and economic value. Cortex moutan is dry root bark of Paeonia suffruticosa of Ranunculaceae. Bitter and pungent properties and slight cold. It enters heart, liver and kidney meridians. Has antibacterial, antiinflammatory, hemostatic, analgesic, and antitumor effects, and can promote phagocytosis of monocyte and improve specific immunity, and is a heat clearing and blood cooling medicine with the advantages of cooling blood without blood stasis, promoting blood circulation, and preventing blood movement. The peony pollen contains rich amino acids and proteins; contains various nutrients, vitamins and minerals; contains a large amount of natural active substances such as enzymes, flavonoids, organic acids, hormones, nucleic acids, etc., and can promote health and enhance body defenses.
Rape (Brassica campestrie) is a cruciferous, rutaceae, ruta plant, annual or biennial herb. The rape pollen is nearly spherical and has a three-split round shape. The rape has large cultivation area, wide distribution area, multiple varieties, large yield and easy adoption. Rape is an important oil crop in China, has been widely developed and utilized in China, and has the effect of inhibiting prostatic hyperplasia according to research, regulating smooth muscle tension of the urinary system and inhibiting in-vitro prostatic cell growth.
Peppermint (Mentha haplocalyx briq.) is the dry aerial part of the Labiatae plant peppermint. It is pungent in flavor and cool in nature. It enters lung and liver meridians. Has effects of dispelling heat, clearing head and eyes, relieving sore throat, promoting eruption, dispersing stagnated liver qi, and activating qi-flowing.
The buccal tablet is a pressed tablet which is slowly dissolved in the oral cavity, is convenient to carry and use, has good taste and wide application range. As a health food, pollen is popular and important, and as early as two thousands of years ago, china has various records on pollen application. The peony flower in China is rich in resources and various in varieties, but people have less research on the peony pollen products, and a large amount of peony pollen is wasted. In order to improve the utilization rate of peony resources and facilitate eating by consumers, it is necessary to develop a buccal tablet using peony pollen as a main raw material.
Disclosure of Invention
The invention provides the peony pollen buccal tablet and the preparation process thereof, which improve the utilization rate of peony resources and are convenient for consumers to eat.
The invention provides a peony pollen buccal tablet which is prepared from the following raw materials in parts by weight: 30-55 parts of peony pollen, 0-25 parts of rape pollen, 3-8 parts of mint leaves, 0.8-1.8 parts of citric acid, 40 parts of mannitol, 1-6 parts of sodium carboxymethyl starch and 10-30 parts of starch slurry.
Preferably, the peony pollen buccal tablet is prepared from the following raw materials in parts by weight: 35 parts of peony pollen, 13 parts of rape pollen, 6 parts of mint leaves, 1 part of citric acid, 40 parts of mannitol, 5 parts of sodium carboxymethyl starch and 20 parts of starch slurry.
Preferably, the mass concentration of the peony pollen buccal tablet and the starch slurry is 8-15 g/100ml.
Preferably, the peony pollen buccal tablet is prepared from the following starch slurry by the following method: 8-15 g of corn starch is suspended in 5-10 ml of warm water, and then 100ml of boiling water is added for supplementing, and the mixture is stirred while adding the boiling water until gelatinization, so as to obtain starch slurry.
The second object of the present invention is to provide a preparation method of the peony pollen buccal tablet, comprising the following steps:
weighing 30-55 parts of peony pollen, 0-25 parts of rape pollen, 3-8 parts of mint leaves, 0.8-1.8 parts of citric acid, 40 parts of mannitol, 1-6 parts of sodium carboxymethyl starch and 10-30 parts of starch slurry;
pulverizing peony pollen, rape pollen and mint leaves respectively, sieving with 80-100 mesh sieve to obtain peony powder, rape powder and mint leaf powder respectively, and storing at low temperature for later use;
uniformly mixing peony flower powder, rape flower powder, mint leaf powder, citric acid, mannitol and sodium carboxymethyl starch to obtain mixed powder;
adding starch slurry into the mixed powder, and uniformly mixing to obtain a soft material;
and (3) pouring the soft material into a granulator to prepare granules, drying the obtained granules, taking 24-100 meshes of granules, and tabletting to obtain the peony pollen buccal tablets.
Preferably, the preparation method of the peony pollen buccal tablet comprises the following steps of uniformly mixing peony powder, rape flower powder, mint leaf powder, citric acid, mannitol and sodium carboxymethyl starch by an equivalent incremental method and a bottoming and color-coating method:
step 1, using mannitol to saturate the inner surface of a container used in the mixing process of materials;
step 2, adding citric acid into the container, adding mint powder with the same mass as the citric acid, and uniformly mixing to obtain a mixture; adding the mint powder with the same mass as the obtained mixture, and continuing to add the mint powder, wherein the adding amount of the mint powder each time is equal to the total mass of the mixture obtained last time until the mint powder is added;
step 3, adding rape pollen with the same quality as the mixture obtained in the step 2 for the last time, and uniformly mixing; continuously adding rape pollen, wherein the adding amount of rape pollen is equal to the total mass of the mixture obtained last time, until the rape pollen is added;
referring to the method in the step 3, peony pollen is added and mixed uniformly, and finally the rest mannitol is added and mixed uniformly to obtain mixed powder.
Preferably, in the preparation method of the peony pollen buccal tablet, the concentration of the starch slurry is 10g/100ml, and the amount of the starch slurry added is 1g of starch slurry added to 5g of mixed powder.
Compared with the prior art, the peony pollen buccal tablet and the preparation process thereof provided by the invention have at least the following beneficial effects:
the peony pollen buccal tablet is prepared by taking peony pollen as a main medicine, taking rape pollen and mint leaves as auxiliary medicines, adding citric acid, sodium carboxymethyl starch, mannitol and starch slurry as auxiliary materials, and adopting a wet granulating and tabletting method. The developed peony pollen buccal tablet can fully utilize peony pollen, combines pollen with buccal tablets, ensures that pollen is contained in an oral cavity to be slowly dissolved, can ensure that active ingredients in the pollen are slowly released, reduces stimulation to gastrointestinal tracts, can conveniently and rapidly exert the effects of nutrition and medicine, is easy to store, convenient to carry and convenient to use, and has more advantages than other dosage forms. It not only can supplement nutrition required by human body, but also has the health-care function of prostate. The peony pollen buccal tablet obtained by the test has moderate sour and sweet taste, strong medicinal fragrance and moderate hardness, can meet market demands, and has wide market prospect.
Drawings
FIG. 1 is an appearance diagram of peony pollen buccal tablets prepared in example 1;
FIG. 2 is an external view of a peony pollen buccal tablet prepared in example 2;
FIG. 3 is an appearance of peony pollen buccal tablet prepared in example 3;
FIG. 4 is an appearance of peony pollen buccal tablet prepared in example 4;
FIG. 5 is an external view of a peony pollen buccal tablet prepared in comparative example 1.
Detailed Description
In order that those skilled in the art will better understand the technical scheme of the present invention, the present invention will be further described with reference to specific embodiments and drawings. The following examples, as well as the experimental procedures not identified in the above summary, were carried out in accordance with methods and conditions conventional in the art.
The experimental methods and the detection methods described in the following examples are all conventional methods unless otherwise specified; the reagents and materials are commercially available unless otherwise specified. In the following examples: peony pollen provided by Fenhe peony group Co., ltd., rape pollen purchased from Taobaomeng to the Royal, peppermint leaf purchased from Shanxi Taigu bene and big pharmacy.
The invention provides a peony pollen buccal tablet which is prepared from the following raw materials in parts by weight: 30-55 parts of peony pollen, 0-25 parts of rape pollen, 3-8 parts of mint leaves, 0.8-1.8 parts of citric acid, 40 parts of mannitol, 1-6 parts of sodium carboxymethyl starch and 10-30 parts of starch slurry. Wherein, the adding amount of the starch slurry is 8-15% of the total mass of other materials; if less than 8%, the tackiness is too small to form particles; if the content is more than 15%, the formed particles are long-strip-shaped or noodle-shaped, and are not suitable for tabletting.
In the invention, peony pollen contains abundant amino acids and proteins; contains a large amount of natural active substances, etc., and can promote health and enhance body defenses.
Rape pollen can inhibit prostatic hyperplasia and regulate smooth muscle tension of urinary system.
Bo He is pungent and cool in nature. It enters lung and liver meridians. Has effects of dispelling heat, relieving sore throat, promoting eruption, refreshing brain, dispersing stagnated liver qi, and activating qi-flowing.
Mannitol is white crystal or crystalline powder, odorless, sweet, and often used as filler and sweetener. Is easily dissolved in water, absorbs heat when dissolved, and has cool feeling. In the food sector, mannitol can be used as a low calorie, low sugar sweetener.
Citric acid has a refreshing sour taste and is used as a sour agent.
Sodium carboxymethyl starch (CMS-Na) is white or white-like powder, odorless, highly swellable, and is an excellent swelling agent for use as a disintegrant.
Starch slurry is a common adhesive, and the preparation method mainly comprises a slurry flushing method and a slurry boiling method. The embodiment of the invention is prepared by adopting a slurry flushing method. The mass concentration of the starch slurry is 8-15 g/100ml, and the preparation method is as follows: 8-15 g of corn starch is suspended in 5-10 ml of warm water, and then 100ml of boiling water is added for supplementing, and the mixture is stirred while adding the boiling water until gelatinization, so as to obtain starch slurry.
Example 1
A peony pollen buccal tablet is prepared from the following raw materials in parts by weight: 30g of peony pollen, 20.2g of rape pollen, 6g of mint leaves, 0.8g of citric acid, 40g of mannitol, 3g of sodium carboxymethyl starch and 20g of starch slurry.
The preparation process of the peony pollen buccal tablet comprises the following steps:
weighing 30g of peony pollen, 20.2g of rape pollen, 6g of mint leaves, 0.8g of citric acid, 40g of mannitol, 3g of sodium carboxymethyl starch and 20g of starch slurry;
pulverizing flos moutan pollen, rape pollen and folium Menthae respectively, sieving with 80 mesh sieve to obtain flos moutan powder, flos Brassicae campestris powder and folium Menthae powder respectively, and storing at 4deg.C for use;
uniformly mixing peony flower powder, rape flower powder, mint leaf powder, citric acid, mannitol and sodium carboxymethyl starch by adopting an equivalent incremental method and a priming color method to obtain mixed powder;
adding 10g/100ml starch slurry into the mixed powder, and mixing to obtain soft material;
the soft material is poured into a small-sized granulator (YK-60, electric technology Co., ltd.) to prepare granules, the obtained granules are dried and sieved by a 100-mesh sieve to be granulated, and then the granules are pressed by a manual tablet pressing machine (a mould of a manual tablet pressing machine, auspicious pharmaceutical machinery Co., ltd.) to obtain a peony pollen buccal tablet, and the appearance diagram of the peony pollen buccal tablet is shown in figure 1.
Wherein, the equal increment method and the bottoming chromatography are evenly mixed, and the specific steps are as follows:
step 1, using mannitol to saturate the inner surface of a container used in the mixing process of materials;
step 2, adding citric acid into the container, adding mint powder with the same mass as the citric acid, and uniformly mixing to obtain a mixture; adding the mint powder with the same mass as the obtained mixture, and continuing to add the mint powder, wherein the adding amount of the mint powder each time is equal to the total mass of the mixture obtained last time until the mint powder is added;
step 3, adding rape pollen with the same quality as the mixture obtained in the step 2 for the last time, and uniformly mixing; continuously adding rape pollen, wherein the adding amount of rape pollen is equal to the total mass of the mixture obtained last time, until the rape pollen is added;
referring to the method in the step 3, peony pollen is added and mixed uniformly, and finally the rest mannitol is added and mixed uniformly to obtain mixed powder.
Example 2
A peony pollen buccal tablet is prepared from the following raw materials in parts by weight: 35g of peony pollen, 13.8g of rape pollen, 7g of mint leaves, 1.2g of citric acid, 40g of mannitol, 3g of sodium carboxymethyl starch and 20g of starch slurry. The preparation method of the peony pollen buccal tablet is basically the same as that of the example 1, and the difference is that: and pouring the soft material into a granulator to prepare granules, drying the obtained granules, and taking 24-mesh granules. Example 2 peony pollen buccal tablet the appearance is shown in figure 2.
Example 3
A peony pollen buccal tablet is prepared from the following raw materials in parts by weight: 35g of peony pollen, 13g of rape pollen, 6g of mint leaves, 1g of citric acid, 40g of mannitol, 5g of sodium carboxymethyl starch and 20g of starch slurry. The preparation method of the peony pollen buccal tablet is basically the same as that of the example 1, and the difference is that: and pouring the soft material into a granulator to prepare granules, drying the obtained granules, and taking 80-mesh granules. Example 3 peony pollen buccal tablet the appearance of which is shown in figure 3.
Example 4
A peony pollen buccal tablet is prepared from the following raw materials in parts by weight; the raw materials comprise 40g of peony pollen, 8.8g of rape pollen, 6g of mint leaves, 1.2g of citric acid, 40g of mannitol, 4g of sodium carboxymethyl starch and 20g of starch slurry. The preparation method of the peony pollen buccal tablet is the same as in example 1. Example 4 peony pollen buccal tablet the appearance is shown in figure 4.
Example 5
A peony pollen buccal tablet is prepared from the following raw materials in parts by weight; the raw materials comprise 55g of peony pollen, 3g of mint leaves, 0.8g of citric acid, 40g of mannitol, 1g of sodium carboxymethyl starch and 10g of starch slurry. The preparation method of the peony pollen buccal tablet is basically the same as that of the embodiment 1, and the difference is that: pulverizing flos moutan powder, rape pollen and folium Menthae respectively, sieving with 100 mesh sieve respectively to obtain flos moutan powder, rape flower powder and folium Menthae powder respectively, and storing at 10deg.C; the concentration of the starch slurry was 15g/100ml.
Example 6
A peony pollen buccal tablet is prepared from the following raw materials in parts by weight; the raw materials comprise 30g of peony pollen, 25g of rape pollen, 8g of mint leaves, 1.8g of citric acid, 40g of mannitol, 6g of sodium carboxymethyl starch and 30g of starch slurry. The preparation method of the peony pollen buccal tablet is basically the same as that of the embodiment 1, and the difference is that: pulverizing flos moutan pollen, rape pollen and folium Menthae respectively, sieving with 100 mesh sieve respectively to obtain flos moutan powder, flos Brassicae campestris powder and folium Menthae powder respectively, and storing at 5deg.C; the concentration of the starch slurry was 8g/100ml.
Comparative example 1
A peony pollen buccal tablet is prepared from the following raw materials in parts by weight; the raw materials comprise 30g of peony pollen, 25g of rape pollen, 8g of mint leaves, 1.8g of citric acid, 40g of mannitol, 6g of sodium carboxymethyl starch and 7g of starch slurry, and the preparation method is the same as that of the example 1. The results showed that the buccal tablet prepared in comparative example 1 had a spot, was close to a split and had poor appearance. Comparative example 1 peony pollen buccal tablet the appearance is shown in figure 5.
Subsequently, to verify the mouthfeel of the present invention, a sensory panel was evaluated by 10 persons of the composition, and the sensory evaluation criteria are shown in table 1.
TABLE 1 perception scoring criteria
Sensory evaluation was performed on examples 1 to 6 and comparative example 1 according to table 1, and the results are shown in tables 2 to 3, with the average score of example 1 being 87, the average score of example 2 being 89, the average score of example 3 being 90, the average score of example 4 being 83, the average score of example 5 being 80, the average score of example 6 being 85, and the average score of comparative example 1 being 66.
Table 2 examples 1-3 and comparative examples sensory scores
Table 3 examples 4-6 sensory scores
The physical and chemical evaluation criteria were carried out according to the pharmacopoeia of the people's republic of China (2015 edition), and the test results are shown in Table 4.
Table 4 sensory scores for different examples and comparative examples
The buccal tablet prepared by the invention has moderate sour and sweet taste, strong medicinal fragrance, uniform color and luster and simple process. The research and development of the peony pollen buccal tablet can fully utilize peony pollen, combines the pollen with the buccal tablet, ensures that the pollen is contained in the oral cavity to be slowly dissolved, can ensure that the active ingredients in the pollen are slowly released, reduces the stimulation to the gastrointestinal tract, can conveniently and rapidly exert the nutrition and medicinal effects, can supplement nutrition required by human bodies, and has the prostate health care effect. Can meet the market demand and has wide market prospect.
It should be noted that, when numerical ranges are referred to in the present invention, it is understood that two endpoints of each numerical range and any numerical value between the two endpoints are optional, and the preferred embodiments are described in order to prevent redundancy, but other variations and modifications can be made to the embodiments by those skilled in the art once they learn of the basic inventive concepts. It is therefore intended that the following claims be interpreted as including the preferred embodiments and all such alterations and modifications as fall within the scope of the invention. It will be apparent to those skilled in the art that various modifications and variations can be made to the present invention without departing from the spirit or scope of the invention. Thus, it is intended that the present invention also include such modifications and alterations insofar as they come within the scope of the appended claims or the equivalents thereof.
Claims (1)
1. The preparation method of the peony pollen buccal tablet is characterized by comprising the following raw materials in parts by weight: 35 parts of peony pollen, 13 parts of rape pollen, 6 parts of mint leaves, 1 part of citric acid, 40 parts of mannitol, 5 parts of sodium carboxymethyl starch and 20 parts of starch slurry; the concentration of the starch slurry is 10g/100ml, and the amount of the starch slurry added is 1g of starch slurry added to 5g of mixed powder;
the preparation method of the peony pollen buccal tablet comprises the following steps:
weighing 35 parts of peony pollen, 13 parts of rape pollen, 6 parts of mint leaves, 1 part of citric acid, 40 parts of mannitol, 5 parts of sodium carboxymethyl starch and 20 parts of starch slurry;
pulverizing peony pollen, rape pollen and mint leaves respectively, sieving with 80-100 mesh sieve to obtain peony powder, rape powder and mint leaf powder respectively, and storing at low temperature for later use;
uniformly mixing peony flower powder, rape flower powder, mint leaf powder, citric acid, mannitol and sodium carboxymethyl starch by adopting an equivalent incremental method and a priming and color-coating method, and specifically comprising the following steps of:
step 1, saturating the inner surface of a container with mannitol;
step 2, adding citric acid into the container, adding mint leaf powder with the same mass as the citric acid, and uniformly mixing to obtain a mixture; adding the mint leaf powder with the same mass as the obtained mixture, and continuing to add the mint leaf powder, wherein the adding amount of the mint leaf powder each time is equal to the total mass of the mixture obtained last time until the mint leaf powder is added;
step 3, adding rape pollen with the same quality as the mixture obtained in the step 2 for the last time, and uniformly mixing; continuously adding rape pollen, wherein the adding amount of rape pollen is equal to the total mass of the mixture obtained last time, until the rape pollen is added;
referring to the method in the step 3, adding peony pollen, uniformly mixing, and finally adding the rest mannitol, uniformly mixing to obtain mixed powder;
adding starch slurry into the mixed powder, and uniformly mixing to obtain a soft material;
the starch slurry is prepared according to the following method: suspending 10g of corn starch in 5-10 ml of warm water, adding boiling water to complement 100ml, and stirring while adding boiling water until gelatinization to obtain starch slurry;
and (3) pouring the soft material into a granulator to prepare granules, drying the obtained granules, taking 24-100 meshes of granules, and tabletting to obtain the peony pollen buccal tablets.
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