CN110604312A - Marine biological product with effects of expelling toxin, beautifying, enriching blood and tonifying qi and preparation method thereof - Google Patents
Marine biological product with effects of expelling toxin, beautifying, enriching blood and tonifying qi and preparation method thereof Download PDFInfo
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- CN110604312A CN110604312A CN201910888301.5A CN201910888301A CN110604312A CN 110604312 A CN110604312 A CN 110604312A CN 201910888301 A CN201910888301 A CN 201910888301A CN 110604312 A CN110604312 A CN 110604312A
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Classifications
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- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/04—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from fish or other sea animals
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention provides a marine organism product with effects of expelling toxin, beautifying, enriching blood and benefiting qi and a preparation method thereof, relating to the field of health-care functional drinks, and comprising 30-50 parts of fish collagen, 5-10 parts of sea cucumber, 5-10 parts of medlar, 20-40 parts of cranberry, 40-60 parts of lemon, 30-50 parts of xylitol and 1-2 parts of xylooligosaccharide by weight; the method completely extracts and retains the nutrient substances in the sea cucumber by the extraction methods of wall breaking, ultrasonic treatment and enzymolysis, and effectively removes the harmful substances such as heavy metal and the like in the sea cucumber by centrifugation, ultrafiltration and chitosan addition; the fish collagen can delay skin aging and can not cause fatness; xylo-oligosaccharide can selectively promote the proliferation activity of intestinal bifidobacteria; the inherent fishy smell of the fish collagen is effectively covered by the lemon and the cranberry; the marine organism drink prepared by the preparation method is clear and has faint scent, and has the effects of beautifying and expelling toxin.
Description
Technical Field
The invention relates to the field of health-care functional drinks, in particular to a marine biological product with the effects of expelling toxin, beautifying, nourishing blood and tonifying qi and a preparation method thereof.
Background
The health-care functional drink contains a certain amount of functional components, can regulate the functions of human bodies, has a specific effect, is suitable for specific people, is gradually accepted by the masses in the current society, and the health-care food industry researches raw materials of health-care food, health-care food formulas and products for beautifying and aging all the time at present.
Chinese patent with publication number CN102860549B proposes a functional beverage with effects of caring skin and removing toxic substances and its preparation method. The functional beverage is prepared by adopting rose, medlar, honey, glucose, ganoderma lucidum spore powder, anthocyanin, soybean isoflavone, citric acid and rose natural essence as main raw materials, is sour, sweet and delicious, and has the functional components of beautifying and detoxifying. By using modern processing means such as enzymolysis, ultrafiltration separation and the like, the product is kept to a greater extent to contain more nutrient and functional components.
The sea cucumber is a marine organism and has a plurality of nutrient substances which can not be absorbed by land organisms, the sea cucumber has a plurality of tonifying and health-preserving functions which are specially designated by Chinese medical science, researches on more than 40 chemical components of the sea cucumber by scholars at home and abroad show that the sea cucumber is rich in more than 50 nutrient components which are needed by human bodies, such as amino acid, vitamin, chemical elements and the like, and also contains a plurality of bioactive substances, such as acid mucopolysaccharide, saponin, collagen and the like, and the pharmacological activity of the active substances of the sea cucumber is very wide, so that the sea cucumber is commonly applied to the field of food health care at present.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a marine organism beverage with the effects of beautifying and expelling toxin.
In order to achieve the first object of the present invention, the present invention provides the following technical solutions: the marine biological product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi comprises the following components in parts by weight:
more preferably, the addition ratio of the lemon to the fish collagen is greater than or equal to 1: 1.
More preferably, the composition comprises the following components in parts by weight:
the second invention aims to provide a preparation method of a marine organism product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi, and in order to realize the second invention aim, the invention provides the following technical scheme: a preparation method of a marine organism product with effects of expelling toxin, beautifying, enriching blood and benefiting qi comprises the following steps:
A. raw material pretreatment of sea cucumber, medlar, cranberry and lemon;
B. preparing a sea cucumber and medlar raw material extracting solution I;
C. preparing cranberry and lemon raw material extracting solution II;
D. preparing a fish collagen solution;
E. and mixing the raw material extracting solution I, the raw material extracting solution II and the fish collagen solution to obtain the marine biological product.
Preferably, the step A raw material treatment comprises the following steps:
(a1) the method comprises the following steps Cutting open fresh sea cucumber along abdomen, removing viscera, and washing with purified water for 1-5 times;
(b1) the method comprises the following steps Washing, airing and crushing the medlar to 80-100 meshes for later use;
(c1) the method comprises the following steps Washing, airing and crushing cranberries to 80-100 meshes for later use;
(d1) the method comprises the following steps Dipping lemons in water, rubbing the surface of the lemons with edible salt, removing dirt on the surface of the lemons, washing the lemons with water, and slicing the lemons;
(e1) the method comprises the following steps The fish collagen is prepared by taking cod skin and/or tilapia phosphorus as raw materials and performing extraction, enzymolysis and atomization drying on the raw materials.
Preferably, the average molecular weight of the fish collagen is 1000-3000 Da. The collagen is macromolecular fibrous scleroprotein, the relative molecular weight is as high as 30 ten thousand daltons, the collagen can not be directly absorbed by a human body after being eaten, and the collagen can be absorbed by the human body after being digested and decomposed into small molecular polypeptides or free amino acids, so that the effect is exerted, the absorption rate is very low, relatively speaking, the collagen peptide with the smaller molecular weight is easier to be absorbed by the human body, generally, when the molecular weight of the collagen peptide reaches about 2000 daltons, the absorption rate can reach 90% or more, and when the molecular weight is too small, the structure of the collagen peptide is damaged, the function is relatively influenced, the taste is changed, for example, the taste is bitter, therefore, the fish collagen with the molecular weight in the range of 1000-.
Preferably, the preparation of the raw material extracting solution I in the step B comprises the following steps:
(a2) the method comprises the following steps Weighing the sea cucumber according to the parts by weight of the sea cucumber powder in the claim 1, and homogenizing;
(b2) the method comprises the following steps Adding the crushed medlar according to the weight portion of claim 1;
(c2) the method comprises the following steps Adding purified water which is 10-25 times of the total amount of the mixture obtained in the step (a2) and the step (b 2);
(d2) the method comprises the following steps Adding papain with the weight of 0.1-0.5% of the total weight of the sea cucumber;
(e2) the method comprises the following steps Uniformly mixing, and then carrying out ultrasonic extraction for 1.5-3 hours at the temperature of 50-60 ℃;
(f2) the method comprises the following steps Heating to 100 ℃, keeping for 3-5 min, and cooling to room temperature;
(g2) the method comprises the following steps Centrifuging for the first time at the rotating speed of 3500-6000 rpm;
(h2) the method comprises the following steps Ultrafiltering the supernatant obtained by the first centrifugation by ultrafiltration equipment to obtain a concentrated solution and a filtrate;
(i2) the method comprises the following steps Adding chitosan with the weight of 0.1-0.6% of the filtrate into the filtrate, stirring at the rotating speed of 300-450 rpm, reacting for 1-2 hours, and standing for 30-60 min;
(j2) the method comprises the following steps And centrifuging the reacted filtrate for the second time, taking supernate and mixing the supernate with the concentrated solution to obtain a raw material extracting solution I.
Preferably, the preparation of the raw material extracting solution II in the step C comprises the following steps:
(a3) the method comprises the following steps Weighing the crushed cranberries and the sliced lemons according to the parts by weight in the claim 1;
(b3) the method comprises the following steps Adding purified water which is 5-10 times of the total amount of the mixture in the step (a 3);
(c3) the method comprises the following steps Adding pectinase accounting for 0.01-0.05% of the total amount of the cranberries and the lemons;
(d3) the method comprises the following steps Performing ultrasonic extraction on the mixture at 40-50 ℃ for 1-2 hours;
(e3) the method comprises the following steps Heating to 90 ℃, keeping for 3-5 minutes, and cooling to room temperature;
(f3) the method comprises the following steps Filtering with 400 mesh filter screen to obtain filtrate as raw material extractive solution II.
Preferably, the enzyme activity of the pectinase is 5000-20000U, and preferably, the enzyme activity of the pectinase is 10000U.
Preferably, the preparation of the fish collagen solution in the step D comprises the following steps:
(a4) the method comprises the following steps Weighing fish collagen, xylitol and xylo-oligosaccharide according to the parts by weight in the claim 1;
(b4) the method comprises the following steps Adding purified water which is 3-6 times of the total amount of the mixture in the step (a4), wherein the temperature of the purified water is 45-55 ℃;
(c4) the method comprises the following steps And stirring the fish collagen solution in purified water at the temperature of 45-55 ℃ until no obvious undissolved substances are observed by visual inspection, and thus obtaining the fish collagen solution.
In summary, compared with the prior art, the invention has the following beneficial effects:
(1) the sea cucumber has a plurality of tonifying and health preserving functions specially designated by traditional Chinese medicine, the sea cucumber body not only contains more than 50 nutrient components required by human bodies such as amino acid, vitamin and chemical element, but also contains active substances such as acid mucopolysaccharide, saponin and collagen, the sea cucumber body is rich in macroelements and microelements necessary for human bodies, wherein the contents of iron and zinc in the microelements are obviously higher than those of other elements. Iron and zinc are trace elements with the most quantity required by human body, iron is a main component participating in forming hemoglobin, zinc is more than 200 components of zinc-containing enzyme, and plays an important role in nucleic acid and protein metabolism, and has a close relation with brain and intelligence development particularly; although the collagen extracted from pigs and cattle can also achieve the effect of supplementing the collagen of human bodies, the collagen contains a large amount of fat, and the collagen is easy to become fat after being orally taken; xylo-oligosaccharide can selectively promote the proliferation activity of intestinal bifidobacteria, does not influence the blood sugar concentration, does not increase the insulin level in blood sugar, and can be used by diabetics, obese patients and hypoglycemia patients;
(2) by centrifuging, ultrafiltering, adding chitosan and centrifuging during preparation of the raw material extracting solution I, harmful substances such as heavy metals in the sea cucumber are effectively removed through the adsorption effect of chitosan on metal ions, cholesterol, triglyceride, cholic acid, organic mercury and the like; the clarity of the raw material extracting solution II is improved by adding pectinase;
(3) the medlar is a traditional tonifying product, contains various trace elements, participates in the metabolic process together with enzymes, hormones, vitamins and the like in a human body, and protects the immunity of the human body. Many studies have shown that lycium barbarum polysaccharide, a characteristic component of lycium barbarum, has the effects of promoting immunity, resisting aging, resisting fatigue, resisting radiation, protecting liver and the like; collagen is a constituent material of human dermis, hard bone, fibrous cartilage and organ capsule, and the collagen contains abundant hydroxyproline which is a key substance for skin formation, so that the proper supplement of the hydroxyproline can effectively help the reconstruction of the collagen in vivo and the regeneration and the renewal of elastin; the collagen is macromolecular fibrous scleroprotein, the relative molecular weight is up to 30 ten thousand daltons, it is difficult to absorb directly after eating, the absorptivity is very low, and the collagen structure with too small molecular weight is destroyed, its function is relatively influenced, the mouthfeel will be bitter, etc., the invention prefers the collagen with suitable molecular weight, make the marine biological products suitable for the human body to absorb and improve its mouthfeel;
(4) the inherent fishy smell of the fish collagen is effectively covered by adding the lemon and the cranberry, and the lemon is rich in vitamin C and can promote the absorption of the fish collagen; the cranberry contains procyanidin, ellagic acid, phenolic acid, resveratrol and other substances, has antibacterial and antioxidant effects, has a good maintenance effect on female reproductive system, and can play a role in maintaining from inside to outside; flavonol and procyanidin have effects of preventing atherosclerosis, inhibiting oxidation of low density lipoprotein-cholesterol, reducing triglyceride level in blood, and promoting cardiovascular health;
(5) through experiments, when the mass ratio of the fish collagen to the lemon is more than or equal to 1:1, the inherent fishy smell of the fish collagen can be well covered, and the taste of the beverage can be enriched.
Detailed Description
The following examples will assist those skilled in the art in further understanding the invention, but are not intended to limit the invention in any way. It will be apparent to those skilled in the art that various changes and modifications may be made without departing from the spirit and scope of the invention. All falling within the scope of the present invention.
Examples 1 to 7, comparative examples 1 to 6
Example 1:
the marine biological product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi has the following components in the dosage shown in table 1, and the preparation method comprises the following steps:
step A, raw material treatment. Cutting open fresh sea cucumber along abdomen, removing viscera, and cleaning with purified water; cleaning fructus Lycii and cranberry, air drying, and pulverizing to 80 mesh; rubbing the surface of the lemon with edible salt after the lemon is dipped in water, washing the lemon with water after dirt on the surface is removed, and slicing the lemon; the cod skin is used as a raw material, and fish collagen is prepared by extraction, enzymolysis, atomization and drying, and the molecular weight of the fish collagen is 1000Da-3000 Da.
B, preparing a raw material extracting solution I, weighing the processed sea cucumbers according to the formula in the table 1, homogenizing, adding crushed medlar, adding purified water 15 times of the total amount and papain 0.1% of the total weight of the sea cucumbers, uniformly mixing, performing ultrasonic extraction at 50 ℃ for 1.5 hours, heating to 100 ℃, keeping for 3 minutes, cooling to room temperature, centrifuging at 3500rpm, filtering supernate by using ultrafiltration equipment, respectively collecting concentrated solution and filtrate, adding chitosan 0.1% of the weight of the filtrate into the filtrate, stirring at 300rpm for reaction for 1 hour, standing for 30 minutes, centrifuging again, effectively removing heavy metals in the process, collecting the centrifuged supernate again, and mixing the centrifuged supernate with the concentrated solution to obtain the raw material extracting solution I.
And step C, preparing a raw material extracting solution II. Weighing the processed cranberries and lemons according to the formula, adding purified water with 5 times of the total amount, adding pectinase (with the enzyme activity of 5000U) accounting for 0.01 percent of the total amount of the cranberries and the lemons, carrying out ultrasonic extraction for 1 hour at 40 ℃, heating to 90 ℃, keeping for 3 minutes, cooling to room temperature, filtering by a 400-mesh filter screen, and collecting filtrate to obtain a raw material extracting solution II.
And D, preparing a fish collagen solution. Weighing fish collagen, xylitol and xylo-oligosaccharide according to the formula, adding into purified water of 45 ℃ which is 3 times of the total amount, and stirring until the mixture is completely dissolved to obtain the fish collagen liquid.
And E, completely and uniformly mixing the raw material extracting solution I, the raw material extracting solution II and the fish collagen solution, adding xylo-oligosaccharide and xylitol according to the formula amount, and stirring until the xylo-oligosaccharide and the xylitol are completely dissolved to obtain the marine organism beverage.
Examples 2 to 5:
the marine organism product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi is different from the marine organism product in the embodiment 1 in that the addition amount of each component in the formula is different, and the preparation method is the same as the embodiment 1 as shown in the table 1.
TABLE 1 EXAMPLES 1-4 Components and amounts
| Raw materials | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 |
| Fish collagen | 50 | 40 | 30 | 50 | 50 |
| Sea cucumber | 5 | 8 | 10 | 8 | 5 |
| Chinese wolfberry | 5 | 8 | 10 | 8 | 5 |
| Cranberry | 40 | 30 | 20 | 35 | 40 |
| Lemon | 50 | 40 | 60 | 50 | 30 |
| Xylitol, its preparation method and use | 50 | 30 | 40 | 40 | 50 |
| Xylo-oligosaccharide | 1 | 1.5 | 2 | 1 | 1 |
Example 6:
the marine biological product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi is different from the marine biological product in the embodiment 1 in the preparation method conditions;
step A, raw material treatment. Cutting open fresh sea cucumber along abdomen, removing viscera, and cleaning with purified water; cleaning fructus Lycii and cranberry, air drying, and pulverizing to 100 mesh; rubbing the surface of the lemon with edible salt after the lemon is dipped in water, washing the lemon with water after dirt on the surface is removed, and slicing the lemon; tilapia scales are used as raw materials, and fish collagen is prepared through extraction, enzymolysis, atomization and drying, and the molecular weight of the fish collagen is 1000Da-3000 Da.
B, preparing a raw material extracting solution I, weighing the processed sea cucumbers according to the formula in the table 1, homogenizing, adding crushed medlar, adding purified water accounting for 25 times of the total amount and papain accounting for 0.5 percent of the total weight of the sea cucumbers, uniformly mixing, performing ultrasonic extraction at 60 ℃ for 3 hours, heating to 100 ℃, keeping the temperature for 5 minutes, cooling to room temperature, centrifuging at the rotating speed of 6000rpm, filtering supernate by using ultrafiltration equipment, respectively collecting concentrated solution and filtrate, adding chitosan accounting for 0.6 percent of the weight of the filtrate into the filtrate, stirring at the rotating speed of 450rpm for reaction for 2 hours, standing for 60 minutes, re-centrifuging, effectively removing heavy metals in the process, collecting the re-centrifuged supernate and mixing the concentrated solution to obtain the raw material extracting solution I.
And step C, preparing a raw material extracting solution II. Weighing the processed cranberries and lemons according to the formula, adding purified water with the amount of 10 times of the total amount of the cranberries and the lemons, adding pectinase (with the enzyme activity of 20000U) accounting for 0.05 percent of the total amount of the cranberries and the lemons, performing ultrasonic extraction for 2 hours at 50 ℃, heating to 90 ℃, keeping for 5 minutes, cooling to room temperature, filtering by a 400-mesh filter screen, and collecting filtrate to obtain a raw material extracting solution II.
And D, preparing a fish collagen solution. Weighing fish collagen, xylitol and xylo-oligosaccharide according to the formula, adding into purified water with the temperature of 55 ℃ which is 6 times of the total amount, and stirring until the mixture is completely dissolved to obtain the fish collagen liquid.
And E, completely and uniformly mixing the raw material extracting solution I, the raw material extracting solution II and the fish collagen solution, adding xylo-oligosaccharide and xylitol according to the formula amount, and stirring until the xylo-oligosaccharide and the xylitol are completely dissolved to obtain the marine organism beverage.
Example 7:
the marine biological product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi is different from the marine biological product in the embodiment 1 in the preparation method conditions;
step A, raw material treatment. Cutting open fresh sea cucumber along abdomen, removing viscera, and cleaning with purified water; cleaning fructus Lycii and cranberry, air drying, and pulverizing to 90 mesh; rubbing the surface of the lemon with edible salt after the lemon is dipped in water, washing the lemon with water after dirt on the surface is removed, and slicing the lemon; cod skin and tilapia mossambica scale are used as raw materials, and fish collagen is prepared through extraction, enzymolysis, atomization and drying, and the molecular weight of the fish collagen is 1000Da-3000 Da.
B, preparing a raw material extracting solution I, weighing the processed sea cucumbers according to the formula in the table 1, homogenizing, adding crushed medlar, adding 10 times of purified water and 0.2% of papain of the total weight of the sea cucumbers, uniformly mixing, performing ultrasonic extraction at 55 ℃ for 2.5 hours, heating to 100 ℃, keeping the temperature for 4 minutes, cooling to room temperature, centrifuging at the rotating speed of 4500rpm, filtering supernate by using ultrafiltration equipment, respectively collecting concentrated solution and filtrate, adding chitosan of which the weight is 0.5% of the weight of the filtrate into the filtrate, stirring at the rotating speed of 400rpm, reacting for 1.5 hours, standing for 45 minutes, centrifuging again, effectively removing heavy metals in the process, collecting the centrifuged supernate again, and mixing the centrifuged supernate with the concentrated solution to obtain the raw material extracting solution I.
And step C, preparing a raw material extracting solution II. Weighing the processed cranberries and lemons according to the formula, adding purified water 7 times the total amount of the cranberries and the lemons, adding pectinase (with the enzyme activity of 10000U) 0.02 percent of the total amount of the cranberries and the lemons, performing ultrasonic extraction for 1.5 hours at 45 ℃, heating to 90 ℃, keeping for 4 minutes, cooling to room temperature, filtering by a 400-mesh filter screen, and collecting filtrate to obtain a raw material extracting solution II.
And D, preparing a fish collagen solution. Weighing fish collagen, xylitol and xylo-oligosaccharide according to the formula, adding into purified water of 50 ℃ which is 5 times of the total amount, and stirring until the mixture is completely dissolved to obtain the fish collagen liquid.
And E, completely and uniformly mixing the raw material extracting solution I, the raw material extracting solution II and the fish collagen solution, adding xylo-oligosaccharide and xylitol according to the formula amount, and stirring until the xylo-oligosaccharide and the xylitol are completely dissolved to obtain the marine organism beverage.
Comparative examples 1 to 3:
the marine biological product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi is different from the marine biological product in the embodiment 1 in that the addition amount of each component in the formula is different, and the preparation method is the same as the embodiment 1 as shown in table 2 specifically;
TABLE 2 comparative examples 1-3 compositions and amounts
| Raw materials | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Fish collagen | 0 | 50 | 50 |
| Sea cucumber | 5 | 5 | 5 |
| Chinese wolfberry | 5 | 5 | 5 |
| Cranberry | 40 | 40 | 40 |
| Lemon | 50 | 0 | 50 |
| Xylitol, its preparation method and use | 50 | 50 | 0 |
| Xylo-oligosaccharide | 1 | 1 | 1 |
Comparative example 4:
the marine biological product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi is different from the marine biological product in the embodiment 4 in that chitosan is not added in the step B for removing heavy metals, and the rest preparation method is the same as the embodiment 4.
Comparative example 5:
the marine organism product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi is different from the marine organism product in the embodiment 3 in that pectinase is not added in the step C, and the rest preparation method is the same as the embodiment 3.
Comparative example 6:
the marine biological product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi is different from the marine biological product in the embodiment 7 in that the papain is not added in the step B, and the other preparation methods are the same as the embodiment 7.
Second, test standard
1. The quality standards are shown in Table 3
TABLE 3 quality standards
2. The sensory and mouthfeel testing method comprises the following steps:
randomly selecting 20 workers aiming at the user experience (sense and mouthfeel) of the embodiment to test the sample of the embodiment; wherein the passing state of the sense organ is from uniform to uniform, the precipitation amount is graded from more to less into 1-5 points, and the taste is graded from low to high into 1-5 points through the comprehensive taste.
Third, test results
1. The sensory and taste test results are shown in Table 4
Table 4 sensory and mouthfeel results of examples 1-6, comparative examples 1-6
| Sample (I) | Sense organ | Taste of the product |
| Example 1 | 5 | 5 |
| Example 2 | 5 | 4 |
| Example 3 | 5 | 5 |
| Example 4 | 5 | 5 |
| Example 5 | 4 | 4 |
| Example 6 | 4 | 5 |
| Example 7 | 5 | 5 |
| Comparative example 1 | 5 | 3 |
| Comparative example 2 | 5 | 1 |
| Comparative example 3 | 5 | 2 |
| Comparative example 4 | 5 | 4 |
| Comparative example 5 | 3 | 3 |
| Comparative example 6 | 4 | 4 |
2. The results of the quality tests are shown in Table 5
The results of tests on nutrients (amino acids, hydroxyproline) and microorganisms were performed on samples with a sensory and mouthfeel of more than 3 points in the comparative example are shown in table 5:
TABLE 5 nutrient (amino acids, hydroxyproline) and microbiological test results
The influence of the use or non-use of chitosan on the lead index of the product is shown in the table 6:
TABLE 6 lead test results
According to the detection result, the detection value of heavy metal lead can be lower than the detection limit by using chitosan, while the detection value of lead is 0.22mg/L without adding chitosan, and the detection result shows that the detection values of heavy metal can be lower than the detection limit by using chitosan.
The foregoing description of specific embodiments of the present invention has been presented. It is to be understood that the present invention is not limited to the specific embodiments described above, and that various changes or modifications may be made by one skilled in the art within the scope of the appended claims without departing from the spirit of the invention. The embodiments and features of the embodiments of the present application may be combined with each other arbitrarily without conflict.
Claims (8)
1. The marine biological product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi is characterized by comprising the following components in parts by weight:
2. the preparation method of the marine organism product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi according to claim 1 is characterized by comprising the following steps of:
A. raw material pretreatment of sea cucumber, medlar, cranberry and lemon;
B. preparing a sea cucumber and medlar raw material extracting solution I;
C. preparing cranberry and lemon raw material extracting solution II;
D. preparing a fish collagen solution;
E. and mixing the raw material extracting solution I, the raw material extracting solution II and the fish collagen solution to obtain the marine biological product.
3. The preparation method of the marine biological product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi according to claim 2, wherein the step A raw material treatment comprises the following steps:
(a1) the method comprises the following steps Cutting open fresh sea cucumber along abdomen, removing viscera, and washing with purified water for 1-5 times;
(b1) the method comprises the following steps Washing, airing and crushing the medlar to 80-100 meshes for later use;
(c1) the method comprises the following steps Washing, airing and crushing cranberries to 80-100 meshes for later use;
(d1) the method comprises the following steps Dipping lemons in water, rubbing the surface of the lemons with edible salt, removing dirt on the surface of the lemons, washing the lemons with water, and slicing the lemons;
(e1) the method comprises the following steps The fish collagen is prepared by taking cod skin and/or tilapia phosphorus as raw materials and performing extraction, enzymolysis and atomization drying on the raw materials.
4. The method for preparing a marine organism product with effects of expelling toxin, beautifying skin, enriching blood and benefiting qi as claimed in claim 3, wherein the average molecular weight of the fish collagen is 1000-3000 Da.
5. The method for preparing a marine organism product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi according to claim 3, wherein the preparation of the raw material extracting solution I in the step B comprises the following steps:
(a2) the method comprises the following steps Weighing the sea cucumber according to the parts by weight of the sea cucumber powder in the claim 1, and homogenizing;
(b2) the method comprises the following steps Adding the crushed medlar according to the weight portion of claim 1;
(c2) the method comprises the following steps Adding purified water which is 10-25 times of the total amount of the mixture obtained in the step (a2) and the step (b 2);
(d2) the method comprises the following steps Adding papain with the weight of 0.1-0.5% of the total weight of the sea cucumber;
(e2) the method comprises the following steps Uniformly mixing, and then carrying out ultrasonic extraction for 1.5-3 hours at the temperature of 50-60 ℃;
(f2) the method comprises the following steps Heating to 100 ℃, keeping for 3-5 min, and cooling to room temperature;
(g2) the method comprises the following steps Centrifuging for the first time at the rotating speed of 3500-6000 rpm;
(h2) the method comprises the following steps Ultrafiltering the supernatant obtained by the first centrifugation by ultrafiltration equipment to obtain a concentrated solution and a filtrate;
(i2) the method comprises the following steps Adding chitosan with the weight of 0.1-0.6% of the filtrate into the filtrate, stirring at the rotating speed of 300-450 rpm, reacting for 1-2 hours, and standing for 30-60 min;
(j2) the method comprises the following steps And centrifuging the reacted filtrate for the second time, taking supernate and mixing the supernate with the concentrated solution to obtain a raw material extracting solution I.
6. The method for preparing a marine organism product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi according to claim 3, wherein the preparation of the raw material extracting solution II in the step C comprises the following steps:
(a3) the method comprises the following steps Weighing the crushed cranberries and the sliced lemons according to the parts by weight in the claim 1;
(b3) the method comprises the following steps Adding purified water which is 5-10 times of the total amount of the mixture in the step (a 3);
(c3) the method comprises the following steps Adding pectinase accounting for 0.01-0.05% of the total amount of the cranberries and the lemons;
(d3) the method comprises the following steps Performing ultrasonic extraction on the mixture at 40-50 ℃ for 1-2 hours;
(e3) the method comprises the following steps Heating to 90 ℃, keeping for 3-5 minutes, and cooling to room temperature;
(f3) the method comprises the following steps Filtering with 400 mesh filter screen to obtain filtrate as raw material extractive solution II.
7. The preparation method of the marine organism product with the effects of expelling toxin, beautifying, enriching the blood and tonifying qi according to claim 6, wherein the enzyme activity of the pectinase is 5000-20000U.
8. The method for preparing a marine organism product with the effects of expelling toxin, beautifying the face, replenishing the blood and tonifying qi according to claim 3, wherein the step D of preparing the fish collagen solution comprises the following steps:
(a4) the method comprises the following steps Weighing fish collagen, xylitol and xylo-oligosaccharide according to the parts by weight in the claim 1;
(b4) the method comprises the following steps Adding purified water which is 3-6 times of the total amount of the mixture in the step (a4), wherein the temperature of the purified water is 45-55 ℃;
(c4) the method comprises the following steps And stirring the fish collagen solution in purified water at the temperature of 45-55 ℃ until no obvious undissolved substances are observed by visual inspection, and thus obtaining the fish collagen solution.
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Application publication date: 20191224 |