CN110511092A - A kind of fertilizer synergistic auxiliary agent and preparation method thereof containing chlorogenic acid - Google Patents
A kind of fertilizer synergistic auxiliary agent and preparation method thereof containing chlorogenic acid Download PDFInfo
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- CN110511092A CN110511092A CN201910932681.8A CN201910932681A CN110511092A CN 110511092 A CN110511092 A CN 110511092A CN 201910932681 A CN201910932681 A CN 201910932681A CN 110511092 A CN110511092 A CN 110511092A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
- A01N37/46—N-acyl derivatives
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/26—Phosphorus; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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Abstract
The invention discloses a kind of fertilizer synergistic auxiliary agent and preparation method thereof containing chlorogenic acid, more particularly to agricultural technology field, used raw material (according to parts by weight) includes 10-20 parts of honeysuckle, 10-15 parts of folium isatidis, 10-15 parts of dandelion, 10-20 parts of polyglutamic acid, 10-20 parts of ammonium humate, 10-20 parts of potassium humate, 8-14 parts of potassium dihydrogen phosphate, 8-14 parts of ammonium phosphate and 5-10 parts of kaolin, and the auxiliary material includes 80-160 parts and distilled water 300-450 parts of ethyl alcohol according to parts by weight.The present invention is by increasing the extraction concentrate by honeysuckle, folium isatidis and dandelion, so that for when applying fertilizer after fertilizer synergistic auxiliary agent prepared by the present invention and fertilizer ratio, the bacterium in soil and in environment can effectively be inhibited, effectively reduce the damage to crops, be conducive to the normal growth of crops, and using plant as raw material, green and healthy, safety and environmental protection.
Description
Technical field
The present invention relates to agricultural technology fields, it is more particularly related to which a kind of fertilizer synergistic containing chlorogenic acid helps
Agent and preparation method thereof.
Background technique
Fertilizer refers to nutrient necessary to the one or more kinds of crops of offer, improves soil property, improves soil
One substance of fertility level, is one of material base of agricultural production, mainly water-soluble including ammonium phosphate fertilizers, a great number of elements
Property fertilizer, secondary nutrients, bio-feritlizer, organic fertilizer, multidimensional field energy concentrated organic fertilizer etc., organic fertilizer includes organic nitrogen
Fertilizer, synthetic organic nitrogen fertilizer etc..China's someone's Animal fecal pollution accustomed to using, barnyard manure, compost, is made compost with biogas manure etc. at green manure, is had
Machine inorganic fertilizer, that is, semi-organic fertilizer is that organic fertilizer and inorganic fertilizer pass through fertilizer made of mechanical mixture or chemical reaction.
Fertilizer synergist refers to a kind of active material for the purpose of increasing nutrient availability, by difficult in fixing nitrogen and activating soil
It is played a role in adjusting crops physiological function with the phosphorus, the potassium element that utilize to increase the supply to crop nutrition content,
It is usually to add it in common fertilizer, can suitably reduces rate of fertilizer, improves the utilization rate of fertilizer.
Existing fertilizer synergistic auxiliary agent cannot inhibit the bacterium in soil, so that the bacterium in soil and in environment
It is easy to damage crops, has seriously affected the normal growth of crops.
Summary of the invention
In order to overcome the drawbacks described above of the prior art, the embodiment of the present invention provides a kind of fertilizer synergistic containing chlorogenic acid and helps
Agent and preparation method thereof, by increasing the extraction concentrate by honeysuckle, folium isatidis and dandelion, so that fertilizer prepared by the present invention
For can effectively inhibit the bacterium in soil and in environment when applying fertilizer after material builder and fertilizer ratio, effectively reduce pair
The damage of crops is conducive to the normal growth of crops, and using plant as raw material, green and healthy, safety and environmental protection.
To achieve the above object, the invention provides the following technical scheme: a kind of fertilizer synergistic auxiliary agent containing chlorogenic acid, is made
It include 10-20 parts of honeysuckle, 10-15 parts of folium isatidis, 10-15 parts of dandelion, polyglutamic acid 10- with raw material (according to parts by weight)
20 parts, 10-20 parts of ammonium humate, 10-20 parts of potassium humate, 8-14 parts of potassium dihydrogen phosphate, 8-14 parts of ammonium phosphate and kaolin 5-
10 parts, the auxiliary material includes 80-160 parts and distilled water 300-450 parts of ethyl alcohol according to parts by weight.
In a preferred embodiment, the used raw material (according to parts by weight) include 10 parts of honeysuckle, it is big
10 parts of leafiness, 10 parts of dandelion, 10 parts of polyglutamic acid, 10 parts of ammonium humate, 10 parts of potassium humate, 8 parts of potassium dihydrogen phosphate, phosphoric acid
8 parts and 5 parts of kaolin of ammonium, the auxiliary material includes 80 parts and 300 parts of distilled water of ethyl alcohol according to parts by weight.
In a preferred embodiment, the used raw material (according to parts by weight) include 15 parts of honeysuckle, it is big
12.5 parts of leafiness, 12.5 parts of dandelion, 15 parts of polyglutamic acid, 15 parts of ammonium humate, 15 parts of potassium humate, potassium dihydrogen phosphate 11
Part, 11 parts of ammonium phosphate and 7.5 parts of kaolin, the auxiliary material include 120 parts and 375 parts of distilled water of ethyl alcohol according to parts by weight.
In a preferred embodiment, the used raw material (according to parts by weight) include 20 parts of honeysuckle, it is big
15 parts of leafiness, 15 parts of dandelion, 20 parts of polyglutamic acid, 20 parts of ammonium humate, 20 parts of potassium humate, 14 parts of potassium dihydrogen phosphate, phosphorus
14 parts and 10 parts of kaolin of sour ammonium, the auxiliary material includes 160 parts and 450 parts of distilled water of ethyl alcohol according to parts by weight.
The invention also includes the preparation methods of fertilizer synergistic auxiliary agent, and specific preparation process is as follows:
The preparation of S1, chlorogenic acid concentrate:
S1.1, honeysuckle is cleaned using clear water and is cleaned, then dried；
S1.2, dry honeysuckle is ground using tissue grinder instrument, is then wrapped the honeysuckle of grinding using filter paper,
It is then placed in Soxhlet extractor；
S1.3, ethyl alcohol is added in Soxhlet extractor to equal with siphon pipe, the honeysuckle of grinding is impregnated, then water again
It is heated to reflux on bath, then siphon 3-5 times；
S1.4, it carries out the phegma to pour into cucurbit and is evaporated under reduced pressure, distillate is then put into ultrasonic wave dissolution instrument
Ultrasonic dissolution is carried out, is then filtered using filter membrane, so that chlorogenic acid concentrate be made；
S2, preparation folium isatidis extract concentrate；
S3, preparation dandelion extract concentrate；
S4, mixing: the addition of polyglutamic acid, ammonium humate, potassium humate, potassium dihydrogen phosphate, ammonium phosphate and kaolin is ground
It is ground in grinding machine, blender mixing is added after grinding, the chlorogenic acid concentrate of preparation is then added into blender, folium isatidis mentions
It takes concentrate and dandelion to extract concentrate, continues to stir；
S5, granulation: being put into granulator and pelletize after stirring, so that fertilizer synergistic auxiliary agent be prepared.
In a preferred embodiment, soaking time is 1-3h in step S1.3, and being heated to reflux temperature is 65-75
℃。
In a preferred embodiment, grinder rotating speed is 1000-2000r/min, milling time in step s 4
For 10-15min, mixing time is 20-30min twice.
In a preferred embodiment, folium isatidis extraction concentrate preparation step is as follows in step s 2:
S2.1, folium isatidis is cleaned using clear water and is cleaned, then dried；
S2.2, dry folium isatidis is shredded, is then ground using tissue grinder instrument, by 1/6th distilled water and ground
Folium isatidis be mixed, be then placed in ultrasonic wave dissolution instrument in carry out ultrasonic dissolution, be then filtered；
/ 6th distilled water are added in S2.3, the filter residue filtered out, are then placed again into ultrasonic dissolution instrument and carry out ultrasound
It is filtered after dissolution；
S2.4, repeat the above steps, then mix filtered filtrate, mixed liquor be put into inside centrifuge from
The heart, centrifuge speed 1000-3000r/min, centrifugation time 10-20min stand 20-30min, Aspirate supernatant afterwards；
S2.5, supernatant heating under reduced pressure is concentrated, so that obtaining folium isatidis extracts concentrate.
In a preferred embodiment, dandelion extracts concentrate preparation step in step s3 and folium isatidis is extracted
Concentrate preparation step is identical.
Technical effect and advantage of the invention:
1, the present invention passes through chlorogenic acid concentrate, the folium isatidis that increase is extracted respectively by honeysuckle, folium isatidis and dandelion
It extracts concentrate and dandelion extracts concentrate, since chlorogenic acid has antibacterial bacteriostatic and antiviral functions, folium isatidis is extracted dense
Contracting liquid has resisting pathogenic microbes and anti-endotoxin effect, and dandelion extracts the objects such as the sterols having in concentrate and volatile oil
Confrontation bacterium and germ are with there is inhibiting effect to have effect, so that fertilizer synergistic auxiliary agent prepared by the present invention and fertilizer ratio
Afterwards for can effectively inhibit the bacterium in soil and in environment, effectively reduce the damage to crops, be conducive to agriculture when applying fertilizer
The normal growth of crop, and using plant as raw material, so that the fertilizer synergistic auxiliary agent of preparation is green and healthy, while entire system
Standby process will not generate the pollutant for being unfavorable for environment, energy-saving and emission-reduction, safety and environmental protection；
2, the present invention can effectively facilitate effect of the crops to mineral absorption by adding polyglutamic acid, pass through addition
Ammonium humate, potassium humate, potassium dihydrogen phosphate and ammonium phosphate can be effectively improved soil, improve soil combination fertility, while right
Crop root system is stimulated, promote crop root system development, be conducive to crop growth, effectively improve the disease-resistant of crops and
Drought-resistant ability；
3, for the present invention by addition kaolin, kaolin has the excellent characteristics such as surface area is larger and absorption property is good, energy
The pollutants such as the heavy metal in enough effectively absorption soil, effectively improve the quality of soil, further ensure the normal production of plant,
And kaolin rich reserves, source is wide, at low cost, is easily obtained.
Specific embodiment
Below in conjunction with the embodiment in the present invention, technical solution in the embodiment of the present invention is carried out clearly and completely
Description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on this hair
Embodiment in bright, every other implementation obtained by those of ordinary skill in the art without making creative efforts
Example, shall fall within the protection scope of the present invention.
Embodiment 1:
The present invention provides a kind of fertilizer synergistic auxiliary agent containing chlorogenic acid, used raw material (according to parts by weight) include gold
10-20 parts of honeysuckle flower, 10-15 parts of folium isatidis, 10-15 parts of dandelion, 10-20 parts of polyglutamic acid, 10-20 parts of ammonium humate, humic
Sour potassium 10-20 parts, 8-14 parts of potassium dihydrogen phosphate, 8-14 parts of ammonium phosphate and 5-10 parts of kaolin, the auxiliary material is according to parts by weight
Including 80-160 parts and distilled water 300-450 parts of ethyl alcohol.
And specific in the present embodiment: the used raw material (according to parts by weight) includes 10 parts of honeysuckle, folium isatidis
10 parts, 10 parts of dandelion, 10 parts of polyglutamic acid, 10 parts of ammonium humate, 10 parts of potassium humate, 8 parts of potassium dihydrogen phosphate, ammonium phosphate 8
Part and 5 parts of kaolin, the auxiliary material includes 80 parts of ethyl alcohol and 300 parts of distilled water according to parts by weight.
Specific step is as follows for the preparation method of fertilizer synergistic auxiliary agent:
The preparation of S1, chlorogenic acid concentrate:
S1.1, honeysuckle is cleaned using clear water and is cleaned, then dried；
S1.2, dry honeysuckle is ground using tissue grinder instrument, is then wrapped the honeysuckle of grinding using filter paper,
It is then placed in Soxhlet extractor；
S1.3, ethyl alcohol is added in Soxhlet extractor to equal with siphon pipe, 1-3h is impregnated to the honeysuckle of grinding, then
It is heated to reflux on water-bath again, temperature is 65 DEG C, then siphon 3 times；
S1.4, it carries out the phegma to pour into cucurbit and is evaporated under reduced pressure, distillate is then put into ultrasonic wave dissolution instrument
Ultrasonic dissolution is carried out, is then filtered using filter membrane, so that chlorogenic acid concentrate be made；
S2, preparation folium isatidis extract concentrate, and specific preparation process is as follows:
S2.1, folium isatidis is cleaned using clear water and is cleaned, then dried；
S2.2, dry folium isatidis is shredded, is then ground using tissue grinder instrument, by 1/6th distilled water and ground
Folium isatidis be mixed, be then placed in ultrasonic wave dissolution instrument in carry out ultrasonic dissolution, be then filtered；
/ 6th distilled water are added in S2.3, the filter residue filtered out, are then placed again into ultrasonic dissolution instrument and carry out ultrasound
It is filtered after dissolution；
S2.4, repeat the above steps, then mix filtered filtrate, mixed liquor be put into inside centrifuge from
The heart, centrifuge speed 1000r/min, centrifugation time 10min stand 20min, Aspirate supernatant afterwards；
S2.5, supernatant heating under reduced pressure is concentrated, so that obtaining folium isatidis extracts concentrate；
S3, preparation dandelion extract concentrate: dandelion extracts concentrate preparation step and folium isatidis extracts concentrate system
Standby step is identical；
S4, mixing: the addition of polyglutamic acid, ammonium humate, potassium humate, potassium dihydrogen phosphate, ammonium phosphate and kaolin is ground
It is ground in grinding machine, grinder rotating speed 1000r/min, milling time 10min, blender mixing 20min is added after grinding, so
The chlorogenic acid concentrate of preparation is added in backward blender, folium isatidis extracts concentrate and dandelion extracts concentrate, continue into
Row stirring 20min；
S5, granulation: being put into granulator and pelletize after stirring, so that fertilizer synergistic auxiliary agent be prepared.
Embodiment 2:
The present invention provides a kind of fertilizer synergistic auxiliary agent containing chlorogenic acid, used raw material (according to parts by weight) include gold
10-20 parts of honeysuckle flower, 10-15 parts of folium isatidis, 10-15 parts of dandelion, 10-20 parts of polyglutamic acid, 10-20 parts of ammonium humate, humic
Sour potassium 10-20 parts, 8-14 parts of potassium dihydrogen phosphate, 8-14 parts of ammonium phosphate and 5-10 parts of kaolin, the auxiliary material is according to parts by weight
Including 80-160 parts and distilled water 300-450 parts of ethyl alcohol.
And specific in the present embodiment: the used raw material (according to parts by weight) includes 15 parts of honeysuckle, folium isatidis
12.5 parts, 12.5 parts of dandelion, 15 parts of polyglutamic acid, 15 parts of ammonium humate, 15 parts of potassium humate, 11 parts of potassium dihydrogen phosphate, phosphorus
11 parts and 7.5 parts of kaolin of sour ammonium, the auxiliary material includes 120 parts and 375 parts of distilled water of ethyl alcohol according to parts by weight.
Specific step is as follows for the preparation method of fertilizer synergistic auxiliary agent:
The preparation of S1, chlorogenic acid concentrate:
S1.1, honeysuckle is cleaned using clear water and is cleaned, then dried；
S1.2, dry honeysuckle is ground using tissue grinder instrument, is then wrapped the honeysuckle of grinding using filter paper,
It is then placed in Soxhlet extractor；
S1.3, ethyl alcohol is added in Soxhlet extractor to equal with siphon pipe, 1-3h is impregnated to the honeysuckle of grinding, then
It is heated to reflux on water-bath again, temperature is 70 DEG C, then siphon 4 times；
S1.4, it carries out the phegma to pour into cucurbit and is evaporated under reduced pressure, distillate is then put into ultrasonic wave dissolution instrument
Ultrasonic dissolution is carried out, is then filtered using filter membrane, so that chlorogenic acid concentrate be made；
S2, preparation folium isatidis extract concentrate, and specific preparation process is as follows:
S2.1, folium isatidis is cleaned using clear water and is cleaned, then dried；
S2.2, dry folium isatidis is shredded, is then ground using tissue grinder instrument, by 1/6th distilled water and ground
Folium isatidis be mixed, be then placed in ultrasonic wave dissolution instrument in carry out ultrasonic dissolution, be then filtered；
/ 6th distilled water are added in S2.3, the filter residue filtered out, are then placed again into ultrasonic dissolution instrument and carry out ultrasound
It is filtered after dissolution；
S2.4, repeat the above steps, then mix filtered filtrate, mixed liquor be put into inside centrifuge from
The heart, centrifuge speed 2000r/min, centrifugation time 15min stand 25min, Aspirate supernatant afterwards；
S2.5, supernatant heating under reduced pressure is concentrated, so that obtaining folium isatidis extracts concentrate；
S3, preparation dandelion extract concentrate: dandelion extracts concentrate preparation step and folium isatidis extracts concentrate system
Standby step is identical；
S4, mixing: the addition of polyglutamic acid, ammonium humate, potassium humate, potassium dihydrogen phosphate, ammonium phosphate and kaolin is ground
It is ground in grinding machine, grinder rotating speed 1500r/min, milling time 12.5min, blender mixing 25min is added after grinding,
Then the chlorogenic acid concentrate of preparation is added into blender, folium isatidis extracts concentrate and dandelion extracts concentrate, continuation
It is stirred 25min；
S5, granulation: being put into granulator and pelletize after stirring, so that fertilizer synergistic auxiliary agent be prepared.
Embodiment 3:
The present invention provides a kind of fertilizer synergistic auxiliary agent containing chlorogenic acid, used raw material (according to parts by weight) include gold
10-20 parts of honeysuckle flower, 10-15 parts of folium isatidis, 10-15 parts of dandelion, 10-20 parts of polyglutamic acid, 10-20 parts of ammonium humate, humic
Sour potassium 10-20 parts, 8-14 parts of potassium dihydrogen phosphate, 8-14 parts of ammonium phosphate and 5-10 parts of kaolin, the auxiliary material is according to parts by weight
Including 80-160 parts and distilled water 300-450 parts of ethyl alcohol.
And specific in the present embodiment: the used raw material (according to parts by weight) includes 20 parts of honeysuckle, folium isatidis
15 parts, 15 parts of dandelion, 20 parts of polyglutamic acid, 20 parts of ammonium humate, 20 parts of potassium humate, 14 parts of potassium dihydrogen phosphate, ammonium phosphate
14 parts and 10 parts of kaolin, the auxiliary material includes 160 parts and 450 parts of distilled water of ethyl alcohol according to parts by weight.
Specific step is as follows for the preparation method of fertilizer synergistic auxiliary agent:
The preparation of S1, chlorogenic acid concentrate:
S1.1, honeysuckle is cleaned using clear water and is cleaned, then dried；
S1.2, dry honeysuckle is ground using tissue grinder instrument, is then wrapped the honeysuckle of grinding using filter paper,
It is then placed in Soxhlet extractor；
S1.3, ethyl alcohol is added in Soxhlet extractor to equal with siphon pipe, 1-3h is impregnated to the honeysuckle of grinding, then
It is heated to reflux on water-bath again, temperature is 75 DEG C, then siphon 5 times；
S1.4, it carries out the phegma to pour into cucurbit and is evaporated under reduced pressure, distillate is then put into ultrasonic wave dissolution instrument
Ultrasonic dissolution is carried out, is then filtered using filter membrane, so that chlorogenic acid concentrate be made；
S2, preparation folium isatidis extract concentrate, and specific preparation process is as follows:
S2.1, folium isatidis is cleaned using clear water and is cleaned, then dried；
S2.2, dry folium isatidis is shredded, is then ground using tissue grinder instrument, by 1/6th distilled water and ground
Folium isatidis be mixed, be then placed in ultrasonic wave dissolution instrument in carry out ultrasonic dissolution, be then filtered；
/ 6th distilled water are added in S2.3, the filter residue filtered out, are then placed again into ultrasonic dissolution instrument and carry out ultrasound
It is filtered after dissolution；
S2.4, repeat the above steps, then mix filtered filtrate, mixed liquor be put into inside centrifuge from
The heart, centrifuge speed 3000r/min, centrifugation time 20min stand 30min, Aspirate supernatant afterwards；
S2.5, supernatant heating under reduced pressure is concentrated, so that obtaining folium isatidis extracts concentrate；
S3, preparation dandelion extract concentrate: dandelion extracts concentrate preparation step and folium isatidis extracts concentrate system
Standby step is identical；
S4, mixing: the addition of polyglutamic acid, ammonium humate, potassium humate, potassium dihydrogen phosphate, ammonium phosphate and kaolin is ground
It is ground in grinding machine, grinder rotating speed 2000r/min, milling time 15min, blender mixing 30min is added after grinding, so
The chlorogenic acid concentrate of preparation is added in backward blender, folium isatidis extracts concentrate and dandelion extracts concentrate, continue into
Row stirring 30min；
S5, granulation: being put into granulator and pelletize after stirring, so that fertilizer synergistic auxiliary agent be prepared.
Embodiment 4:
Fertilizer synergistic auxiliary agent obtained by above-described embodiment 1-3 is taken to be mixed with the fertilizer of same dose respectively, then
Being given at 90 respectively, there is crop planting region of the same area to apply fertilizer, and be one group at every 30, divide three groups to try out three respectively
The fertilizer synergistic auxiliary agent prepared in a embodiment obtains following data after fertilising 1 month:
As seen from the above table, raw material mixing ratio is moderate in embodiment 2, and the fertilizer synergistic auxiliary agent mixed fertilizer of preparation is to farming
Object applies fertilizer, and can be effectively improved soil, improves the quality of soil, inhibits the bacterium in soil and in environment, is conducive to agriculture
The growth of crop, green and healthy, safety and environmental protection.
Last: the foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, all in the present invention
Spirit and principle within, any modification, equivalent replacement, improvement and so on, should be included in protection scope of the present invention it
It is interior.
Claims (9)
1. a kind of fertilizer synergistic auxiliary agent containing chlorogenic acid, it is characterised in that: used raw material (according to parts by weight) includes gold and silver
Flower 10-20 parts, 10-15 parts of folium isatidis, 10-15 parts of dandelion, 10-20 parts of polyglutamic acid, 10-20 parts of ammonium humate, humic acid
10-20 parts of potassium, 8-14 parts of potassium dihydrogen phosphate, 8-14 parts of ammonium phosphate and 5-10 parts of kaolin, the auxiliary material wraps according to parts by weight
Include 80-160 parts and distilled water 300-450 parts of ethyl alcohol.
2. a kind of fertilizer synergistic auxiliary agent containing chlorogenic acid according to claim 1, it is characterised in that: the used raw material
(according to parts by weight) include 10 parts of honeysuckle, 10 parts of folium isatidis, 10 parts of dandelion, 10 parts of polyglutamic acid, 10 parts of ammonium humate,
10 parts of potassium humate, 8 parts of potassium dihydrogen phosphate, 8 parts of ammonium phosphate and 5 parts of kaolin, the auxiliary material includes ethyl alcohol according to parts by weight
80 parts and 300 parts of distilled water.
3. a kind of fertilizer synergistic auxiliary agent containing chlorogenic acid according to claim 1, it is characterised in that: the used raw material
It (according to parts by weight) include 15 parts of honeysuckle, 12.5 parts of folium isatidis, 12.5 parts of dandelion, 15 parts of polyglutamic acid, ammonium humate
15 parts, 15 parts of potassium humate, 11 parts of potassium dihydrogen phosphate, 11 parts of ammonium phosphate and 7.5 parts of kaolin, the auxiliary material is according to parts by weight
Including 120 parts and 375 parts of distilled water of ethyl alcohol.
4. a kind of fertilizer synergistic auxiliary agent containing chlorogenic acid according to claim 1, it is characterised in that: the used raw material
(according to parts by weight) include 20 parts of honeysuckle, 15 parts of folium isatidis, 15 parts of dandelion, 20 parts of polyglutamic acid, 20 parts of ammonium humate,
20 parts of potassium humate, 14 parts of potassium dihydrogen phosphate, 14 parts of ammonium phosphate and 10 parts of kaolin, the auxiliary material includes second according to parts by weight
160 parts and 450 parts of distilled water of alcohol.
5. a kind of fertilizer synergistic auxiliary agent containing chlorogenic acid according to any one of claims 1-4, it is characterised in that: also wrap
The preparation method of fertilizer synergistic auxiliary agent is included, specific preparation process is as follows:
The preparation of S1, chlorogenic acid concentrate:
S1.1, honeysuckle is cleaned using clear water and is cleaned, then dried；
S1.2, dry honeysuckle is ground using tissue grinder instrument, is then wrapped the honeysuckle of grinding using filter paper, then
It is put into Soxhlet extractor；
S1.3, ethyl alcohol is added in Soxhlet extractor to equal with siphon pipe, the honeysuckle of grinding is impregnated, then water-bath again
On be heated to reflux, then siphon 3-5 times；
S1.4, it carries out the phegma to pour into cucurbit and is evaporated under reduced pressure, distillate is then put into ultrasonic wave dissolution instrument and is carried out
Then ultrasonic dissolution is filtered using filter membrane, so that chlorogenic acid concentrate be made；
S2, preparation folium isatidis extract concentrate；
S3, preparation dandelion extract concentrate；
S4, mixing: grinder is added in polyglutamic acid, ammonium humate, potassium humate, potassium dihydrogen phosphate, ammonium phosphate and kaolin
Blender mixing is added in middle grinding after grinding, chlorogenic acid concentrate, the folium isatidis extraction that preparation is then added into blender are dense
Contracting liquid and dandelion extract concentrate, continue to stir；
S5, granulation: being put into granulator and pelletize after stirring, so that fertilizer synergistic auxiliary agent be prepared.
6. a kind of preparation method of fertilizer synergistic auxiliary agent containing chlorogenic acid according to claim 5, it is characterised in that: in step
Soaking time is 1-3h in rapid S1.3, and being heated to reflux temperature is 65-75 DEG C.
7. a kind of preparation method of fertilizer synergistic auxiliary agent containing chlorogenic acid according to claim 5, it is characterised in that: in step
Grinder rotating speed is 1000-2000r/min in rapid S4, and milling time 10-15min, mixing time is 20-30min twice.
8. a kind of preparation method of fertilizer synergistic auxiliary agent containing chlorogenic acid according to claim 5, it is characterised in that: in step
It is as follows to extract concentrate preparation step for folium isatidis in rapid S2:
S2.1, folium isatidis is cleaned using clear water and is cleaned, then dried；
S2.2, dry folium isatidis is shredded, is then ground using tissue grinder instrument, by the big of 1/6th distilled water and grinding
Leafiness is mixed, and is then placed in ultrasonic wave dissolution instrument and carries out ultrasonic dissolution, is then filtered；
/ 6th distilled water are added in S2.3, the filter residue filtered out, are then placed again into ultrasonic dissolution instrument and carry out ultrasonic dissolution
After filter；
S2.4, it repeating the above steps, then mixes filtered filtrate, mixed liquor is put into centrifugation inside centrifuge, from
Scheming revolving speed is 1000-3000r/min, and centrifugation time 10-20min stands 20-30min, Aspirate supernatant afterwards；
S2.5, supernatant heating under reduced pressure is concentrated, so that obtaining folium isatidis extracts concentrate.
9. a kind of preparation method of fertilizer synergistic auxiliary agent containing chlorogenic acid according to claim 8, it is characterised in that: in step
It is identical as folium isatidis extraction concentrate preparation step to extract concentrate preparation step for dandelion in rapid S3.
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