CN110485148A - The aftertreatment technology of embroidery embroidery - Google Patents
The aftertreatment technology of embroidery embroidery Download PDFInfo
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- CN110485148A CN110485148A CN201910787687.0A CN201910787687A CN110485148A CN 110485148 A CN110485148 A CN 110485148A CN 201910787687 A CN201910787687 A CN 201910787687A CN 110485148 A CN110485148 A CN 110485148A
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- CN
- China
- Prior art keywords
- embroidery
- parts
- protective film
- aftertreatment technology
- polyvinyl alcohol
- Prior art date
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- 238000005516 engineering process Methods 0.000 title claims abstract description 22
- 230000001681 protective effect Effects 0.000 claims abstract description 35
- 239000003223 protective agent Substances 0.000 claims abstract description 34
- 238000009956 embroidering Methods 0.000 claims abstract description 20
- 238000012545 processing Methods 0.000 claims abstract description 20
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims abstract description 14
- 235000011613 Pinus brutia Nutrition 0.000 claims abstract description 14
- 241000018646 Pinus brutia Species 0.000 claims abstract description 14
- 239000000839 emulsion Substances 0.000 claims description 42
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 40
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 40
- 238000000576 coating method Methods 0.000 claims description 31
- 238000003756 stirring Methods 0.000 claims description 30
- 239000011248 coating agent Substances 0.000 claims description 22
- 229920001577 copolymer Polymers 0.000 claims description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 229920001451 polypropylene glycol Polymers 0.000 claims description 21
- IDQBJILTOGBZCR-UHFFFAOYSA-N 1-butoxypropan-1-ol Chemical compound CCCCOC(O)CC IDQBJILTOGBZCR-UHFFFAOYSA-N 0.000 claims description 20
- 235000014643 Orbignya martiana Nutrition 0.000 claims description 19
- 244000021150 Orbignya martiana Species 0.000 claims description 19
- AOBIOSPNXBMOAT-UHFFFAOYSA-N 2-[2-(oxiran-2-ylmethoxy)ethoxymethyl]oxirane Chemical compound C1OC1COCCOCC1CO1 AOBIOSPNXBMOAT-UHFFFAOYSA-N 0.000 claims description 17
- 239000000835 fiber Substances 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 10
- 238000006116 polymerization reaction Methods 0.000 claims description 10
- 238000002360 preparation method Methods 0.000 claims description 10
- 238000007761 roller coating Methods 0.000 claims description 10
- 238000007711 solidification Methods 0.000 claims description 10
- 230000008023 solidification Effects 0.000 claims description 10
- 238000007259 addition reaction Methods 0.000 claims description 9
- 125000005456 glyceride group Chemical group 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 2
- -1 glycidyl ester Chemical class 0.000 claims description 2
- RWNUSVWFHDHRCJ-UHFFFAOYSA-N 1-butoxypropan-2-ol Chemical compound CCCCOCC(C)O RWNUSVWFHDHRCJ-UHFFFAOYSA-N 0.000 claims 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims 1
- 150000002085 enols Chemical class 0.000 claims 1
- 241000894006 Bacteria Species 0.000 abstract description 22
- 244000005700 microbiome Species 0.000 abstract description 13
- 239000001993 wax Substances 0.000 description 17
- VOZRXNHHFUQHIL-UHFFFAOYSA-N glycidyl methacrylate Chemical compound CC(=C)C(=O)OCC1CO1 VOZRXNHHFUQHIL-UHFFFAOYSA-N 0.000 description 16
- 238000001035 drying Methods 0.000 description 9
- 238000004321 preservation Methods 0.000 description 8
- 235000009508 confectionery Nutrition 0.000 description 7
- 239000004519 grease Substances 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 230000004888 barrier function Effects 0.000 description 2
- 238000005034 decoration Methods 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- CTKINSOISVBQLD-UHFFFAOYSA-N Glycidol Chemical compound OCC1CO1 CTKINSOISVBQLD-UHFFFAOYSA-N 0.000 description 1
- HSRJKNPTNIJEKV-UHFFFAOYSA-N Guaifenesin Chemical compound COC1=CC=CC=C1OCC(O)CO HSRJKNPTNIJEKV-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004203 carnauba wax Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical compound C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000010417 needlework Methods 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/001—Treatment with visible light, infrared or ultraviolet, X-rays
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/15—Proteins or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
- D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
Abstract
The invention discloses a kind of aftertreatment technologies of embroidery of embroidering, comprising the following steps: (1) embroidery is placed under ultraviolet lamp and is irradiated;(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing.The present invention is by embroidery uv light irradiation; kill the microorganisms such as most of bacterium, mould; then the front and back sides of embroidery uniformly coat protective agent again; form protective film; pine branch sootiness is finally utilized, so that embroidery is dry and kills remaining bacterium and mould etc., inherently improves the surface nature of embroidery; requirement to Conservation environment substantially reduces, and can save in general room environment.
Description
Technical field
The present invention relates to a kind of aftertreatment technologies of embroidery of embroidering.Belong to embroidery technique field.
Background technique
The history that embroidery has at least 1,000 years in China, is one of folks of china traditional handicraft, is existed by needlework
The general name of embroidered various decorative patterns on fabric.The purposes of embroidery mainly includes life and artistic decoration, such as: on clothes, bed
Articles, the tablecloth, stage and artwork decoration etc..Either it is applied to which kind of field, have one to the preservation service life of embroidery embroidery
Provisioning request.
But the preservation for embroidery of embroidering is difficult, over time, embroidery embroidery will appear different degrees of face
Color falls off, change colour or even embroider line is rotted, and loses preservation value.More especially with the embroidery embroidery of reserve value, if not
Special protection is carried out, it often can not long-term preservation.
General embroidery embroidery keeps in dark place, is afraid of high temperature, is afraid of wet and is afraid of excessively to dry, and requires harshness to Conservation environment, slightly not
The careful destruction that just will receive external environment is corroded, and preservation difficulty is big, only fundamentally changes the property of embroidery embroidery, Fang Keyi
Lao Yongyi.
Summary of the invention
The purpose of the present invention is to overcome above-mentioned the deficiencies in the prior art, provide a kind of aftertreatment technology of embroidery of embroidering.
To achieve the above object, the present invention adopts the following technical solutions:
A kind of aftertreatment technology for embroidery of embroidering, comprising the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 20~30 minutes, kill the microorganisms such as most of bacterium, mould;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following
Made of the component of parts by weight: 30~40 parts of acrylate copolymer emulsion, 20~30 parts of babassu wax emulsion, metering system
10~18 parts of acid glycidyl ester, 12~15 parts of polypropylene glycol diglycidyl ether, 5~8 parts of polyvinyl alcohol, propandiol butyl ether 3
~4 parts, 1~2 part of pearl fiber, 1000 parts of water;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing, facilitate embroidery drying and kill residual
Bacterium and mould etc..
One of as a preferred technical scheme, the irradiation intensity of ultraviolet lamp is 220 μ W/cm2 in step (1).
One of as a preferred technical scheme, it is protectant the preparation method is as follows: water and polyvinyl alcohol are added in step (2)
Enter in reaction kettle, be heated with stirring to 80~90 DEG C, after polyvinyl alcohol is completely dissolved, be added acrylate copolymer emulsion, bar
Western palm wax emulsion, glycidyl methacrylate and polypropylene glycol diglycidyl ether stir 5~6 hours, are cooled to 40
~50 DEG C, continuously add propandiol butyl ether and pearl fiber, stir 2~3 hours to get.
One of as a preferred technical scheme, the polyvinyl alcohol in step (2), average degree of polymerization is 1700~1800, phase
It is 74800~79200 to molecular mass.
One of as a preferred technical scheme, the coating method in step (2) is: using blade coating or rubber cylinder hand by hand
Work roller coating.
One of as a preferred technical scheme, it is heated to be formed by curing protective film in step (2) after coating protective agent.
As further preferred one of technical solution, the process conditions being heating and curing are: 150~160 DEG C of solidification temperature,
Curing time is 5~6 minutes.
One of as a preferred technical scheme, the protective film with a thickness of 0.03~0.05mm.
One of as a preferred technical scheme, in step (3), the sootiness processing time is 1~2 hour.
Beneficial effects of the present invention:
1, embroidery uv light irradiation is killed the microorganisms such as most of bacterium, mould by the present invention, and then embroidery is being just again
Reverse side uniformly coats protective agent, forms protective film, finally utilizes pine branch sootiness so that embroidery it is dry and kill remaining bacterium and
Mould etc. inherently improves the surface nature of embroidery, and the requirement to Conservation environment substantially reduces, can be in general room environment
Middle preservation.
2, the time of uv light irradiation was advisable with 20~30 minutes, too short that the effect for killing most of microorganism is not achieved,
The microorganism put aside inside embroidery cannot be completely removed by subsequent pine branch sootiness, long-term preservation may further breed micro-
Biology leads to mildew etc.;It is too long fabric and embroider line to be damaged, so that it is become fragile and be easily damaged, will affect embroidery instead
Save the service life.
3, protective agent of the invention is played anti-well based on acrylate copolymer emulsion and babassu wax emulsion
Water effect, is aided with glycidyl methacrylate and polypropylene glycol diglycidyl ether, further increases barrier air, moisture
The effects of, the addition of polyvinyl alcohol and propandiol butyl ether facilitates the evenly dispersed of each ingredient, and the present invention is also added into a small amount of treasure
Pearl fiber avoids the flexibility and comfortable sense of touch that embroidery itself is influenced after forming protective film.In addition, the protection that the present invention is formed
The thickness of film is colorless and transparent also than relatively thin, will not influence the flexibility and original color of embroidery, while also can guarantee barrier property
Energy.
Specific embodiment
Below with reference to embodiment, the present invention will be further elaborated, it should explanation, following the description merely to
It explains the present invention, its content is not defined.
Acrylate copolymer emulsion of the present invention is purchased from Shenzhen Xian Zhi Chemical Industry Science Co., Ltd (SF-1);
Babassu wax emulsion is purchased from Fushun text Aixin Technology Co., Ltd..
Embodiment 1:
A kind of aftertreatment technology for embroidery of embroidering, comprising the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 20 minutes, kill the microorganisms such as most of bacterium, mould;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following
Made of the component of parts by weight: 30 parts of acrylate copolymer emulsion, 20 parts of babassu wax emulsion, Glycidyl methacrylate is sweet
10 parts of grease, 12 parts of polypropylene glycol diglycidyl ether, 5 parts of polyvinyl alcohol, 3 parts of propandiol butyl ether, 1 part of pearl fiber, water
1000 parts;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing, facilitate embroidery drying and kill residual
Bacterium and mould etc..
Wherein, the irradiation intensity of ultraviolet lamp is 220 μ W/cm2 in step (1).
It is protectant the preparation method is as follows: being heated with stirring to 80 in water and polyvinyl alcohol addition reaction kettle in step (2)
DEG C, after polyvinyl alcohol is completely dissolved, acrylate copolymer emulsion, babassu wax emulsion, Glycidyl methacrylate is added
Glyceride and polypropylene glycol diglycidyl ether stir 5 hours, are cooled to 40 DEG C, continuously add propandiol butyl ether and pearl is fine
Dimension, stir 2 hours to get.
Polyvinyl alcohol in step (2), average degree of polymerization 1700, relative molecular mass 74800.
Coating method in step (2) is: using blade coating or rubber cylinder craft roller coating by hand.
It is heated to be formed by curing protective film in step (2) after coating protective agent.The process conditions being heating and curing are: solidification
150 DEG C of temperature, curing time is 5 minutes.
Protective film with a thickness of 0.03mm.
In step (3), the sootiness processing time is 1 hour.
Embodiment 2:
A kind of aftertreatment technology for embroidery of embroidering, comprising the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 30 minutes, kill the microorganisms such as most of bacterium, mould;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following
Made of the component of parts by weight: 40 parts of acrylate copolymer emulsion, 30 parts of babassu wax emulsion, Glycidyl methacrylate is sweet
18 parts of grease, 15 parts of polypropylene glycol diglycidyl ether, 8 parts of polyvinyl alcohol, 4 parts of propandiol butyl ether, 2 parts of pearl fiber, water
1000 parts;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing, facilitate embroidery drying and kill residual
Bacterium and mould etc..
Wherein, the irradiation intensity of ultraviolet lamp is 220 μ W/cm2 in step (1).
It is protectant the preparation method is as follows: being heated with stirring to 90 in water and polyvinyl alcohol addition reaction kettle in step (2)
DEG C, after polyvinyl alcohol is completely dissolved, acrylate copolymer emulsion, babassu wax emulsion, Glycidyl methacrylate is added
Glyceride and polypropylene glycol diglycidyl ether stir 6 hours, are cooled to 50 DEG C, continuously add propandiol butyl ether and pearl is fine
Dimension, stir 3 hours to get.
Polyvinyl alcohol in step (2), average degree of polymerization 1800, relative molecular mass 79200.
Coating method in step (2) is: using blade coating or rubber cylinder craft roller coating by hand.
It is heated to be formed by curing protective film in step (2) after coating protective agent.The process conditions being heating and curing are: solidification
160 DEG C of temperature, curing time is 6 minutes.
Protective film with a thickness of 0.05mm.
In step (3), the sootiness processing time is 2 hours.
Embodiment 3:
A kind of aftertreatment technology for embroidery of embroidering, comprising the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 20 minutes, kill the microorganisms such as most of bacterium, mould;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following
Made of the component of parts by weight: 40 parts of acrylate copolymer emulsion, 20 parts of babassu wax emulsion, Glycidyl methacrylate is sweet
18 parts of grease, 12 parts of polypropylene glycol diglycidyl ether, 8 parts of polyvinyl alcohol, 3 parts of propandiol butyl ether, 2 parts of pearl fiber, water
1000 parts;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing, facilitate embroidery drying and kill residual
Bacterium and mould etc..
Wherein, the irradiation intensity of ultraviolet lamp is 220 μ W/cm2 in step (1).
It is protectant the preparation method is as follows: being heated with stirring to 80 in water and polyvinyl alcohol addition reaction kettle in step (2)
DEG C, after polyvinyl alcohol is completely dissolved, acrylate copolymer emulsion, babassu wax emulsion, Glycidyl methacrylate is added
Glyceride and polypropylene glycol diglycidyl ether stir 6 hours, are cooled to 40 DEG C, continuously add propandiol butyl ether and pearl is fine
Dimension, stir 3 hours to get.
Polyvinyl alcohol in step (2), average degree of polymerization 1700, relative molecular mass 74800.
Coating method in step (2) is: using blade coating or rubber cylinder craft roller coating by hand.
It is heated to be formed by curing protective film in step (2) after coating protective agent.The process conditions being heating and curing are: solidification
150 DEG C of temperature, curing time is 6 minutes.
Protective film with a thickness of 0.03mm.
In step (3), the sootiness processing time is 2 hours.
Embodiment 4:
A kind of aftertreatment technology for embroidery of embroidering, comprising the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 30 minutes, kill the microorganisms such as most of bacterium, mould;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following
Made of the component of parts by weight: 30 parts of acrylate copolymer emulsion, 30 parts of babassu wax emulsion, Glycidyl methacrylate is sweet
10 parts of grease, 15 parts of polypropylene glycol diglycidyl ether, 5 parts of polyvinyl alcohol, 4 parts of propandiol butyl ether, 1 part of pearl fiber, water
1000 parts;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing, facilitate embroidery drying and kill residual
Bacterium and mould etc..
Wherein, the irradiation intensity of ultraviolet lamp is 220 μ W/cm2 in step (1).
It is protectant the preparation method is as follows: being heated with stirring to 90 in water and polyvinyl alcohol addition reaction kettle in step (2)
DEG C, after polyvinyl alcohol is completely dissolved, acrylate copolymer emulsion, babassu wax emulsion, Glycidyl methacrylate is added
Glyceride and polypropylene glycol diglycidyl ether stir 5 hours, are cooled to 50 DEG C, continuously add propandiol butyl ether and pearl is fine
Dimension, stir 2 hours to get.
Polyvinyl alcohol in step (2), average degree of polymerization 1800, relative molecular mass 79200.
Coating method in step (2) is: using blade coating or rubber cylinder craft roller coating by hand.
It is heated to be formed by curing protective film in step (2) after coating protective agent.The process conditions being heating and curing are: solidification
160 DEG C of temperature, curing time is 5 minutes.
Protective film with a thickness of 0.05mm.
In step (3), the sootiness processing time is 1 hour.
Embodiment 5:
A kind of aftertreatment technology for embroidery of embroidering, comprising the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 25 minutes, kill the microorganisms such as most of bacterium, mould;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following
Made of the component of parts by weight: 35 parts of acrylate copolymer emulsion, 25 parts of babassu wax emulsion, Glycidyl methacrylate is sweet
15 parts of grease, 13 parts of polypropylene glycol diglycidyl ether, 6 parts of polyvinyl alcohol, 3.5 parts of propandiol butyl ether, 1.5 parts of pearl fiber,
1000 parts of water;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing, facilitate embroidery drying and kill residual
Bacterium and mould etc..
Wherein, the irradiation intensity of ultraviolet lamp is 220 μ W/cm2 in step (1).
It is protectant the preparation method is as follows: being heated with stirring to 85 in water and polyvinyl alcohol addition reaction kettle in step (2)
DEG C, after polyvinyl alcohol is completely dissolved, acrylate copolymer emulsion, babassu wax emulsion, Glycidyl methacrylate is added
Glyceride and polypropylene glycol diglycidyl ether stir 5.5 hours, are cooled to 45 DEG C, continuously add propandiol butyl ether and pearl
Fiber, stir 2.5 hours to get.
Polyvinyl alcohol in step (2), average degree of polymerization 1800, relative molecular mass 79200.
Coating method in step (2) is: using blade coating or rubber cylinder craft roller coating by hand.
It is heated to be formed by curing protective film in step (2) after coating protective agent.The process conditions being heating and curing are: solidification
155 DEG C of temperature, curing time is 5.5 minutes.
Protective film with a thickness of 0.04mm.
In step (3), the sootiness processing time is 1.5 hours.
Comparative example 1
A kind of aftertreatment technology for embroidery of embroidering, comprising the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 25 minutes, kill the microorganisms such as most of bacterium, mould;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following
Made of the component of parts by weight: 35 parts of acrylate copolymer emulsion, 25 parts of babassu wax emulsion, Glycidyl methacrylate is sweet
15 parts of grease, 13 parts of polypropylene glycol diglycidyl ether, 6 parts of polyvinyl alcohol, 3.5 parts of propandiol butyl ether, 1000 parts of water;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing, facilitate embroidery drying and kill residual
Bacterium and mould etc..
Wherein, the irradiation intensity of ultraviolet lamp is 220 μ W/cm2 in step (1).
It is protectant the preparation method is as follows: being heated with stirring to 85 in water and polyvinyl alcohol addition reaction kettle in step (2)
DEG C, after polyvinyl alcohol is completely dissolved, acrylate copolymer emulsion, babassu wax emulsion, Glycidyl methacrylate is added
Glyceride and polypropylene glycol diglycidyl ether stir 5.5 hours, are cooled to 45 DEG C, continuously add propandiol butyl ether, stir
2.5 hours to get.
Polyvinyl alcohol in step (2), average degree of polymerization 1800, relative molecular mass 79200.
Coating method in step (2) is: using blade coating or rubber cylinder craft roller coating by hand.
It is heated to be formed by curing protective film in step (2) after coating protective agent.The process conditions being heating and curing are: solidification
155 DEG C of temperature, curing time is 5.5 minutes.
Protective film with a thickness of 0.04mm.
In step (3), the sootiness processing time is 1.5 hours.
Comparative example 2
A kind of aftertreatment technology for embroidery of embroidering, comprising the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 25 minutes, kill the microorganisms such as most of bacterium, mould;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following
Made of the component of parts by weight: 35 parts of acrylate copolymer emulsion, 15 parts of glycidyl methacrylate, polypropylene glycol two
13 parts of glycidol ether, 6 parts of polyvinyl alcohol, 3.5 parts of propandiol butyl ether, 1.5 parts of pearl fiber, 1000 parts of water;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing, facilitate embroidery drying and kill residual
Bacterium and mould etc..
Wherein, the irradiation intensity of ultraviolet lamp is 220 μ W/cm2 in step (1).
It is protectant the preparation method is as follows: being heated with stirring to 85 in water and polyvinyl alcohol addition reaction kettle in step (2)
DEG C, after polyvinyl alcohol is completely dissolved, acrylate copolymer emulsion, glycidyl methacrylate and polypropylene glycol is added
Diglycidyl ether stirs 5.5 hours, is cooled to 45 DEG C, continuously adds propandiol butyl ether and pearl fiber, stirs 2.5 hours,
To obtain the final product.
Polyvinyl alcohol in step (2), average degree of polymerization 1800, relative molecular mass 79200.
Coating method in step (2) is: using blade coating or rubber cylinder craft roller coating by hand.
It is heated to be formed by curing protective film in step (2) after coating protective agent.The process conditions being heating and curing are: solidification
155 DEG C of temperature, curing time is 5.5 minutes.
Protective film with a thickness of 0.04mm.
In step (3), the sootiness processing time is 1.5 hours.
Comparative example 3
A kind of aftertreatment technology for embroidery of embroidering, comprising the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 25 minutes, kill the microorganisms such as most of bacterium, mould;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following
Made of the component of parts by weight: 35 parts of acrylate copolymer emulsion, 25 parts of babassu wax emulsion, polypropylene glycol two shrinks sweet
13 parts of oily ether, 6 parts of polyvinyl alcohol, 3.5 parts of propandiol butyl ether, 1.5 parts of pearl fiber, 1000 parts of water;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing, facilitate embroidery drying and kill residual
Bacterium and mould etc..
Wherein, the irradiation intensity of ultraviolet lamp is 220 μ W/cm2 in step (1).
It is protectant the preparation method is as follows: being heated with stirring to 85 in water and polyvinyl alcohol addition reaction kettle in step (2)
DEG C, after polyvinyl alcohol is completely dissolved, acrylate copolymer emulsion, babassu wax emulsion and polypropylene glycol two is added and shrinks
Glycerin ether stirs 5.5 hours, is cooled to 45 DEG C, continuously adds propandiol butyl ether and pearl fiber, stir 2.5 hours to get.
Polyvinyl alcohol in step (2), average degree of polymerization 1800, relative molecular mass 79200.
Coating method in step (2) is: using blade coating or rubber cylinder craft roller coating by hand.
It is heated to be formed by curing protective film in step (2) after coating protective agent.The process conditions being heating and curing are: solidification
155 DEG C of temperature, curing time is 5.5 minutes.
Protective film with a thickness of 0.04mm.
In step (3), the sootiness processing time is 1.5 hours.
Test example
According to the aftertreatment technology of Examples 1 to 5 or comparative example 1~3 respectively to identical (specification, fabric and embroider line
Material, embroidery pattern etc.) embroidery handled, do not do other any protection (such as glass), investigate coating front and back embroidery
After variation, and indoor (25 DEG C, 45%RH) preservations 12 months the case where embroidery, measured according further to GB/T9995-1997 whole
The regain of body embroidery, the results are shown in Table 1.
The comparison of 1. embroidery disposition of table
As shown in Table 1, the embroidery of the technique post-processing of Examples 1 to 5, regain is low, and interior does not do any protection
I.e. can be reserved at least 12 months, the protective film that the present invention is formed will not color, sense of touch etc. to embroidery impact, far superior to
Comparative example 1~3.
Above-mentioned, although specific embodiments of the present invention have been described, not to the limit of the scope of the present invention
System, based on the technical solutions of the present invention, those skilled in the art do not need to make the creative labor can make it is each
Kind modification or deformation are still within protection scope of the present invention.
Claims (7)
1. a kind of aftertreatment technology for embroidery of embroidering, which comprises the following steps:
(1) embroidery is placed under ultraviolet lamp and is irradiated 25 minutes;
(2) after taking out embroidery, protective agent is uniformly coated in its front and back sides, forms protective film;The protective agent is by following weight
Made of the component of part: 30~40 parts of acrylate copolymer emulsion, 20~30 parts of babassu wax emulsion, methacrylic acid contracting
10~18 parts of water glyceride, 12~15 parts of polypropylene glycol diglycidyl ether, 5~8 parts of polyvinyl alcohol, propandiol butyl ether 3~4
Part, 1~2 part of pearl fiber, 1000 parts of water;
(3) embroidery is transferred in Fumigator, lights pine branch sootiness processing;The irradiation intensity of ultraviolet lamp is in step (1)
220μW/cm2;It is protectant the preparation method is as follows: being heated with stirring in water and polyvinyl alcohol addition reaction kettle in step (2)
80~90 DEG C, after polyvinyl alcohol is completely dissolved, acrylate copolymer emulsion, babassu wax emulsion, metering system is added
Acid glycidyl ester and polypropylene glycol diglycidyl ether stir 5~6 hours, are cooled to 40~50 DEG C, continuously add propylene glycol
Butyl ether and pearl fiber, stir 2~3 hours to get.
2. a kind of aftertreatment technology of embroidery of embroidering according to claim 1, which is characterized in that the poly- second in step (2)
Enol, average degree of polymerization are 1700~1800, and relative molecular mass is 74800~79200.
3. a kind of aftertreatment technology of embroidery of embroidering according to claim 1, which is characterized in that the coating in step (2)
Method is: using blade coating or rubber cylinder craft roller coating by hand.
4. a kind of aftertreatment technology of embroidery of embroidering according to claim 1, which is characterized in that coating is protected in step (2)
It is heated to be formed by curing protective film after protecting agent.
5. a kind of aftertreatment technology of embroidery of embroidering according to claim 1, which is characterized in that the technique item being heating and curing
Part is: 150~160 DEG C of solidification temperature, curing time is 5~6 minutes.
6. a kind of aftertreatment technology of embroidery of embroidering according to claim 1, which is characterized in that the thickness of the protective film
For 0.03~0.05mm.
7. a kind of aftertreatment technology of embroidery of embroidering according to claim 1, which is characterized in that in step (3), at sootiness
Managing the time is 1~2 hour.
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CN103233367B (en) * | 2013-04-17 | 2015-08-05 | 梁雪芳 | A kind of embroidered painting surfacecti proteon processing method |
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