CN110467968A - A kind of quick-fried pearl grape essence and preparation method thereof, quick-fried pearl and cigarette - Google Patents
A kind of quick-fried pearl grape essence and preparation method thereof, quick-fried pearl and cigarette Download PDFInfo
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- CN110467968A CN110467968A CN201910615645.9A CN201910615645A CN110467968A CN 110467968 A CN110467968 A CN 110467968A CN 201910615645 A CN201910615645 A CN 201910615645A CN 110467968 A CN110467968 A CN 110467968A
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- Prior art keywords
- parts
- quick
- ethyl
- fried pearl
- methyl
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- 235000009754 Vitis X bourquina Nutrition 0.000 title claims abstract description 107
- 235000012333 Vitis X labruscana Nutrition 0.000 title claims abstract description 107
- 235000014787 Vitis vinifera Nutrition 0.000 title claims abstract description 107
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 240000006365 Vitis vinifera Species 0.000 title 1
- 241000219095 Vitis Species 0.000 claims abstract description 106
- 239000002994 raw material Substances 0.000 claims abstract description 13
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 66
- 150000002148 esters Chemical class 0.000 claims description 32
- -1 2-Methyl Butyric Acid -3- methylbutyl butenoates Chemical class 0.000 claims description 26
- XIRNKXNNONJFQO-UHFFFAOYSA-N ethyl hexadecanoate Chemical compound CCCCCCCCCCCCCCCC(=O)OCC XIRNKXNNONJFQO-UHFFFAOYSA-N 0.000 claims description 20
- SHZIWNPUGXLXDT-UHFFFAOYSA-N ethyl hexanoate Chemical compound CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 claims description 20
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims description 20
- RUVINXPYWBROJD-ONEGZZNKSA-N trans-anethole Chemical compound COC1=CC=C(\C=C\C)C=C1 RUVINXPYWBROJD-ONEGZZNKSA-N 0.000 claims description 20
- MTZQAGJQAFMTAQ-UHFFFAOYSA-N ethyl benzoate Chemical compound CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 claims description 19
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 claims description 18
- UAHWPYUMFXYFJY-UHFFFAOYSA-N beta-myrcene Chemical compound CC(C)=CCCC(=C)C=C UAHWPYUMFXYFJY-UHFFFAOYSA-N 0.000 claims description 17
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- HCRBXQFHJMCTLF-ZCFIWIBFSA-N ethyl (2r)-2-methylbutanoate Chemical compound CCOC(=O)[C@H](C)CC HCRBXQFHJMCTLF-ZCFIWIBFSA-N 0.000 claims description 16
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- OBNCKNCVKJNDBV-UHFFFAOYSA-N ethyl butyrate Chemical class CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 11
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- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 125000001820 oxy group Chemical group [*:1]O[*:2] 0.000 description 1
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 1
- RGSFGYAAUTVSQA-UHFFFAOYSA-N pentamethylene Natural products C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- UAXOELSVPTZZQG-UHFFFAOYSA-N tiglic acid Natural products CC(C)=C(C)C(O)=O UAXOELSVPTZZQG-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 235000012141 vanillin Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
- C11B9/0046—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings
- C11B9/0049—Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings the condensed rings sharing two common C atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of quick-fried pearl grape essence and preparation method thereof, quick-fried pearl and cigarette.The quick-fried pearl of the disclosure can get the fragrance of grape essence with grape essence by the collocation of various raw materials, due to not having using raw material of the essential oil as essence, therefore the quick-fried pearl of the disclosure is fixed with grape essence chemical component and content, it is not influenced by external factor such as working condition, storage condition, manufacturers, advantageously ensures that the quick-fried pearl stability of grape essence quality.And, the fragrance of the quick-fried pearl grape essence of the disclosure is abundant, harmony is good, can improve and modify fragrance well, increase sweet sense, cover miscellaneous gas, reduce irritation, improve fragrance quality and quantity, coordinate cigarette perfume, increase sense organ comfort level, improving and inhale taste and pleasant impression.
Description
Technical field
The present invention relates to cigarette field, more particularly, to a kind of quick-fried pearl grape essence and preparation method thereof, quick-fried pearl and
Cigarette.
Background technique
In recent years, with the rapid raising of the development of social economy and living standards of the people, various New-type cigarettes are obtained
Quickly development.Quick-fried pearl cigarette can pinch brokenly as a kind of emerging cigarette product, consumer during aspirating quick-fried pearl cigarette
Quick-fried pearl in filter tip discharges flavor component, has the function that mend fragrant, increase feature perfume, improves the suction experience of smoker.
Quick-fried pearl flavoring is very different with traditional tobacco perfuming, and quick-fried pearl is not involved in burning with fragrance, based on former fragrant transfer,
The fragrance generated after traditional pipe tobacco flavoring and casing burning is avoided to change.The quick-fried pearl cigarette of grape be higher quick-fried pearl cigarette product it
One.Moreover, quick-fried pearl grape essence has the characteristics that fragrant in taste, and promotes the production of body fluid and help digestion, relieves fatigue, enriching the blood and tonifying qi and other effects, In
It pinches brokenly quick-fried pearl front and back and provides two kinds of entirely different suctions impressions to consumer, considerably increase the pleasant feeling and entertaining of smoker
Property.
Existing quick-fried pearl is mostly the mixture of grape (taste) essential oil, other natural essential oils and some additives with grape essence.
Essential oil is influenced as plant extracts by factors such as plant growth environment temperature, moisture, soil, illumination, cause different year,
The quick-fried pearl of batch and producer is big with grape essence quality fluctuation, and stability is poor, affects quick-fried pearl grape perfume to a certain extent
Application of the essence in cigarette.Moreover, that there is also astringent tastes is overweight for the existing quick-fried pearl essence of grape, when suction, stimulated oral cavity and nasal cavity
The problems such as big.
Therefore, a kind of quality stabilization how is provided, harmony and the suction that can effectively improve essence and cigarette smoke are comfortable
Property quick-fried pearl with grape essence become this field urgent need to resolve technical problem.
Summary of the invention
It is an object of the present invention to provide a kind of new solutions of quick-fried pearl grape essence.
According to the first aspect of the invention, a kind of quick-fried pearl grape essence is provided.
The quick-fried pearl includes 0.800-1.200 parts of methyl anthranilates, 0.600- with grape essence by weight
0.800 part of ethylmaltol, 0.400-0.600 parts of apple esters, 0.200-0.300 parts of 3- methyl butanols, 0.150-0.250 parts of 2-
Methylbutanoic acid ethyl ester, 0.100-0.150 part 1- (1- ethoxy ethoxy) pentane, 0.050-0.150 parts of ethyl acetate, 0.050-
0.100 part of ethyl hexanoate, 0.050-0.100 parts of 2- methyl-1-propyl alcohol, 0.050-0.100 parts of benzyl carbinols, 0.050-0.100 parts
2-Methyl Butyric Acid -3- methylbutyl butenoate, 0.050-0.100 parts of ethyl propionates, 0.050-0.080 parts of ethyl benzoates, 0.050-
0.080 part of acetic acid -3- methylbutyl butenoate, 0.040-0.080 parts of 2- methyl butanols, 0.040-0.060 parts of 1- (1- ethoxy ethoxies
Base) butane, 0.040-0.060 parts of acetals, 0.030-0.050 parts of acetic acid, 0.020-0.040 parts of ligustrazines, 0.020-0.040
It is part alpha, beta-lonone, 0.020-0.040 parts of n-butyl alcohols, 0.010-0.030 parts of β-furturals, 0.010-0.030 parts strange thin
Lotus alcohol, 0.010-0.020 part leaf-alcohol, 0.010-0.020 parts of nerolidols, 0.010-0.020 parts of butyl acetates, 0.010-
0.020 part of ethyl palmitate, 0.010-0.020 parts of melonals, 0.005-0.015 parts of α-farnesenes, 0.005-0.015 part penta
Acetoacetic ester, 0.005-0.015 parts of Z-3- methylbutanoic acid -3- hexene esters, 0.005-0.015 parts of ethyl butyrates, 0.005-0.010 parts
2-Methyl Butyric Acid -2- methylbutyl butenoate, 0.003-0.006 parts of 2- methyl-2-pentenal servings, 0.003-0.006 parts of isoamyl hexanoates,
0.003-0.006 parts of beta-myrcenes, 0.002-0.005 parts of 3- methyl-1-isopropyl cyclopentenes, 0.001-0.003 parts of australenes,
0.001-0.003 parts of 3- isopropyl phenylpiperidines, 0.001-0.003 parts of caproic acids, 0.005-0.010 parts of 3- carenes, 0.350-0.550 parts
Anethole, 0.200-0.300 part d-limonen, 0.100-0.200 parts of damascenones, 0.050-0.100 parts of vanillic aldehydes, 0.005-
0.010 part of isomenthone, 0.002-0.005 parts of ethyl acetoacetates, 0.040-0.070 parts of menthols, 0.050-0.100 part two
Hydrogen actinidia lactone, 0.040-0.070 parts of cis--limonene oxides and 0.005-0.010 parts of Ethyl vanillins.
Optionally, the methyl anthranilate, ethylmaltol, apple ester, 3- methyl butanol, 2-Methyl Butyric Acid second
Ester, 1- (1- ethoxy ethoxy) pentane, ethyl acetate, ethyl hexanoate, 2- methyl-1-propyl alcohol, benzyl carbinol, 2-Methyl Butyric Acid-
3- methylbutyl butenoate, ethyl propionate, ethyl benzoate, acetic acid -3- methylbutyl butenoate, 2- methyl butanol, 1- (1- ethoxy ethoxy)
Butane, acetal, acetic acid, ligustrazine, alpha, beta-lonone, n-butyl alcohol, β-furtural, neoisomenthol, leaf-alcohol, flores aurantii uncle
Alcohol, butyl acetate, ethyl palmitate, melonal, α-farnesene, ethyl valerate, Z-3- methylbutanoic acid -3- hexene ester, butyric acid
Ethyl ester, 2-Methyl Butyric Acid-2- methylbutyl butenoate, 2- methyl-2-pentenal serving, isoamyl hexanoate, beta-myrcene, 3- methyl-1-isopropyl
It is cyclopentene, australene, 3- isopropyl phenylpiperidines, caproic acid, 3- carene, anethole, d-limonen, damascenone, vanillic aldehyde, different thin
Lotus ketone, ethyl acetoacetate, menthol, dihydroactinidiolide, cis--limonene oxide and Ethyl vanillin mass ratio be
(0.800-1.200):(0.600-0.800):(0.400-0.600):(0.200-0.300):(0.150-0.250):(0.100-
0.150):(0.050-0.150):(0.050-0.100):(0.050-0.100):(0.050-0.100):(0.050-0.100):
(0.050-0.100):(0.050-0.080):(0.050-0.080):(0.040-0.080):(0.040-0.060):(0.040-
0.060):(0.030-0.050):(0.020-0.040):(0.020-0.040):(0.020-0.040):(0.010-0.030):
(0.010-0.030):(0.010-0.020):(0.010-0.020):(0.010-0.020):(0.010-0.020):(0.010-
0.020):(0.005-0.015):(0.005-0.015):(0.005-0.015):(0.005-0.015):(0.005-0.010):
(0.003-0.006):(0.003-0.006):(0.003-0.006):(0.002-0.005):(0.001-0.003):(0.001-
0.003):(0.001-0.003):(0.005-0.010):(0.350-0.550):(0.200-0.300):(0.100-0.200):
(0.050-0.100):(0.005-0.010):(0.002-0.005):(0.040-0.070):(0.050-0.100):(0.040-
0.070):(0.005-0.010)。
Optionally, the quick-fried pearl grape essence does not include ethyl caprilate, ethyl caprate, 1- (1- ethoxy ethoxy) third
Alkane, 4- ethyl -2- metoxyphenol, octanoic acid, acetic acid -2- methylbutyl butenoate, octanoic acid -3- methylbutyl butenoate, 1,3- dioxane, 1,1-
Diethoxy -3- methybutane, pentadecanoic acid -3- methylbutyl butenoate, 4- methyl -2- amyl -1,3- dioxane, 2- hydroxyl -4- first
Oxygroup benzaldehyde, sad isobutyl ester, 2- tert-butyl -3- methyl oxirane, acetic acid -2- [2- [2- [2- (2- butoxy ethoxy
Base) ethyoxyl] ethyoxyl] ethyoxyl] ethyl ester, ethylidene cyclobutane, 2- acetaminobenzoic acid phenethyl ester and cyclohexene.
According to the second aspect of the invention, a kind of preparation method of quick-fried pearl grape essence of the invention is provided.
The preparation method of the quick-fried pearl grape essence include by each raw material under conditions of 15 DEG C -35 DEG C with 50r/min-
The revolving speed of 70r/min stirs the step of 20min-40min.
Optionally, include the steps that each raw material stirring 30min under conditions of 25 DEG C with the revolving speed of 60r/min.
According to the third aspect of the invention we, a kind of quick-fried pearl is provided.
The quick-fried pearl includes shell and grape pastil, and the grape pastil includes solvent and quick-fried pearl of the invention grape perfume
The mass ratio of essence, the solvent and the quick-fried pearl grape essence is (93833-96184): (3816-6167).
Optionally, the solvent is Glycerin, mixed triester with caprylic acid capric acid.
Optionally, the content of the grape pastil in the quick-fried pearl is 15-25 μ L/.
Optionally, the outer diameter of the quick-fried pearl is 3.3mm-3.6mm.
According to the fourth aspect of the invention, a kind of cigarette is provided.
The cigarette includes quick-fried pearl of the invention.
The quick-fried pearl of the disclosure can get the fragrance of grape essence with grape essence by the collocation of various raw materials, due to not having
Raw material using essential oil as essence, therefore the quick-fried pearl of the disclosure is fixed with grape essence chemical component and content, is not produced
The influence of the external factor such as condition, storage condition, manufacturer advantageously ensures that the quick-fried pearl stability of grape essence quality.
Moreover, the fragrance of the quick-fried pearl grape essence of the disclosure is abundant, harmony is good, can improve and modify fragrance well, increase
It is sweet sense, cover miscellaneous gas, reduce irritation, improve fragrance quality and quantity, coordinate cigarette perfume, increase sense organ comfort level, improve inhale taste and
Pleasant impression.
Specific embodiment
It will be described in various exemplary embodiments of the invention now.It should also be noted that unless specifically stated otherwise, otherwise
The component and the positioned opposite of step, numerical expression and numerical value illustrated in these embodiments does not limit the scope of the invention.
Be to the description only actually of at least one exemplary embodiment below it is illustrative, never as to the present invention
And its application or any restrictions used.
Technology, method and apparatus known to person of ordinary skill in the relevant may be not discussed in detail, but suitable
In the case of, the technology, method and apparatus should be considered as part of specification.
It is shown here and discuss all examples in, any occurrence should be construed as merely illustratively, without
It is as limitation.Therefore, other examples of exemplary embodiment can have different values.
The quick-fried pearl of the disclosure include by weight with grape essence 0.800-1.200 parts of methyl anthranilates,
0.600-0.800 parts of ethylmaltols, 0.400-0.600 parts of apple esters, 0.200-0.300 parts of 3- methyl butanols, 0.150-
0.250 part of ethyl 2-methylbutyrate, 0.100-0.150 parts of 1- (1- ethoxy ethoxy) pentanes, 0.050-0.150 parts of acetic acid second
Ester, 0.050-0.100 part ethyl hexanoate, 0.050-0.100 parts of 2- methyl-1-propyl alcohol, 0.050-0.100 parts of benzyl carbinols,
0.050-0.100 parts of 2-Methyl Butyric Acid -3- methylbutyl butenoates, 0.050-0.100 parts of ethyl propionates, 0.050-0.080 parts of benzoic acid
Ethyl ester, 0.050-0.080 parts of acetic acid -3- methylbutyl butenoates, 0.040-0.080 parts of 2- methyl butanols, 0.040-0.060 parts of 1- (1-
Ethoxy ethoxy) butane, 0.040-0.060 parts of acetals, 0.030-0.050 parts of acetic acid, 0.020-0.040 parts of ligustrazines,
0.020-0.040 parts of alpha, beta-lonones, 0.020-0.040 parts of n-butyl alcohols, 0.010-0.030 parts of β-furturals, 0.010-
0.030 part of neoisomenthol, 0.010-0.020 parts of leaf-alcohols, 0.010-0.020 parts of nerolidols, 0.010-0.020 parts of acetic acid fourths
Ester, 0.010-0.020 part ethyl palmitate, 0.010-0.020 parts of melonals, 0.005-0.015 parts of α-farnesenes, 0.005-
0.015 part of ethyl valerate, 0.005-0.015 parts of Z-3- methylbutanoic acid -3- hexene esters, 0.005-0.015 parts of ethyl butyrates,
0.005-0.010 parts of 2-Methyl Butyric Acid -2- methylbutyl butenoates, 0.003-0.006 parts of 2- methyl-2-pentenal servings, 0.003-0.006 parts
Isoamyl hexanoate, 0.003-0.006 part beta-myrcene, 0.002-0.005 parts of 3- methyl-1-isopropyl cyclopentenes, 0.001-
0.003 part of australene, 0.001-0.003 parts of 3- isopropyl phenylpiperidines, 0.001-0.003 parts of caproic acids, 0.005-0.010 parts of 3- caranes
Alkene, 0.350-0.550 part anethole, 0.200-0.300 parts of d-limonens, 0.100-0.200 parts of damascenones, 0.050-
It is 0.100 part of vanillic aldehyde, 0.005-0.010 parts of isomenthones, 0.002-0.005 parts of ethyl acetoacetates, 0.040-0.070 parts thin
Lotus brain, 0.050-0.100 part dihydroactinidiolide, 0.040-0.070 parts of cis--limonene oxides and 0.005-0.010 parts
Ethyl vanillin.
The quick-fried pearl of the disclosure can get the fragrance of grape essence with grape essence by the collocation of various raw materials.Due to not having
Raw material using essential oil as essence, therefore the quick-fried pearl of the disclosure is fixed with grape essence chemical component and content, is not produced
The influence of the external factor such as condition, storage condition, manufacturer advantageously ensures that the quick-fried pearl stability of grape essence quality.
Moreover, the fragrance of the quick-fried pearl grape essence of the disclosure is abundant, harmony is good, can improve and modify perfume well
Gas increases sweet sense, covers miscellaneous gas, reduce irritation, improve fragrance quality and quantity, coordinate cigarette perfume, increase sense organ comfort level, improve
Inhale taste and pleasant impression.
In a kind of embodiment of the quick-fried pearl grape essence of the disclosure, methyl anthranilate, ethylmaltol,
Apple ester, 3- methyl butanol, ethyl 2-methylbutyrate, 1- (1- ethoxy ethoxy) pentane, ethyl acetate, ethyl hexanoate, 2-
Methyl-1-propyl alcohol, benzyl carbinol, 2-Methyl Butyric Acid-3- methylbutyl butenoate, ethyl propionate, ethyl benzoate, acetic acid-3- methylbutyl butenoate,
2- methyl butanol, 1- (1- ethoxy ethoxy) butane, acetal, acetic acid, ligustrazine, alpha, beta-lonone, n-butyl alcohol, β-furans
Formaldehyde, neoisomenthol, leaf-alcohol, nerolidol, butyl acetate, ethyl palmitate, melonal, α-farnesene, ethyl valerate,
Z-3- methylbutanoic acid -3- hexene ester, ethyl butyrate, 2-Methyl Butyric Acid -2- methylbutyl butenoate, 2- methyl-2-pentenal serving, caproic acid isoamyl
Ester, beta-myrcene, 3- methyl-1-isopropyl cyclopentene, australene, 3- isopropyl phenylpiperidines, caproic acid, 3- carene, anethole, dextrorotation
Limonene, damascenone, vanillic aldehyde, isomenthone, ethyl acetoacetate, menthol, dihydroactinidiolide, cis--oxidation lemon
The mass ratio of lemon alkene and Ethyl vanillin is (0.800-1.200): (0.600-0.800): (0.400-0.600): (0.200-
0.300):(0.150-0.250):(0.100-0.150):(0.050-0.150):(0.050-0.100):(0.050-0.100):
(0.050-0.100):(0.050-0.100):(0.050-0.100):(0.050-0.080):(0.050-0.080):(0.040-
0.080):(0.040-0.060):(0.040-0.060):(0.030-0.050):(0.020-0.040):(0.020-0.040):
(0.020-0.040):(0.010-0.030):(0.010-0.030):(0.010-0.020):(0.010-0.020):(0.010-
0.020):(0.010-0.020):(0.010-0.020):(0.005-0.015):(0.005-0.015):(0.005-0.015):
(0.005-0.015):(0.005-0.010):(0.003-0.006):(0.003-0.006):(0.003-0.006):(0.002-
0.005):(0.001-0.003):(0.001-0.003):(0.001-0.003):(0.005-0.010):(0.350-0.550):
(0.200-0.300):(0.100-0.200):(0.050-0.100):(0.005-0.010):(0.002-0.005):(0.040-
0.070):(0.050-0.100):(0.040-0.070):(0.005-0.010)。
It is suitably matched by each ingredient, can further improve the harmony of quick-fried pearl grape essence, and effectively avoid perfume (or spice)
Gas is flat, generates the problems such as miscellaneous gas.
In a kind of embodiment of the quick-fried pearl grape essence of the disclosure, quick-fried pearl does not include sad second with grape essence
Ester, ethyl caprate, 1- (1- ethoxy ethoxy) propane, 4- ethyl -2- metoxyphenol, octanoic acid, acetic acid -2- methylbutyl butenoate,
Octanoic acid -3- methylbutyl butenoate, 1,3- dioxane, 1,1- diethoxy -3- methybutane, pentadecanoic acid -3- methylbutyl butenoate, 4- first
Base -2- amyl -1,3- dioxane, 2- hydroxyl -4-methoxybenzaldehyde, sad isobutyl ester, 2- tert-butyl -3- methyl epoxy second
Alkane, acetic acid -2- [2- [2- [2- (2- Butoxyethoxy) ethyoxyl] ethyoxyl] ethyoxyl] ethyl ester, ethylidene cyclobutane, 2-
Acetaminobenzoic acid phenethyl ester and cyclohexene.
In this embodiment, it will unfavorable compound is generated to flue gas and the ingredient that conflicts with cigarette style characteristic from
Quick-fried pearl is rejected in grape essence, can avoid fractions bring adverse effect.
The disclosure additionally provides a kind of preparation method of quick-fried pearl grape essence.
Quick-fried pearl grape essence of the preparation method based on the disclosure, by each raw material under conditions of 15 DEG C -35 DEG C with
The revolving speed of 50r/min-70r/min stirs 20min-40min.
By selecting suitable preparation process condition, each volatility of raw material can effectively avoid, and effectively avoid because high temperature is fast
The problem that quick-fried pearl caused by fast long agitation is gone bad with grape essence.
Item in a kind of embodiment of the preparation method of the quick-fried pearl grape essence of the disclosure, by each raw material at 25 DEG C
30min is stirred with the revolving speed of 60r/min under part.Quick-fried pearl made from the process conditions is stablized with grape essence quality, and suction is coordinated
Property is good.
The disclosure additionally provides a kind of quick-fried pearl.
The quick-fried pearl includes shell and grape pastil.Shell may be, for example, gelatin.Grape pastil includes solvent and the disclosure
Quick-fried pearl grape essence.Solvent commonly used in the art, such as Glycerin, mixed triester with caprylic acid capric acid etc. can be used in solvent.Solvent and quick-fried pearl grape
The mass ratio of essence is (93833-96184): (3816-6167).
The quick-fried pearl of the disclosure can coordinate with cigarette smoke, improves and modify well fragrance, improve aroma quality, improves fragrance
It measures, covers miscellaneous gas, increase sweet sense, coordinate cigarette perfume, improve flue gas concentration, increase sense organ comfort level, reduce irritation, improving and inhale
Taste and pleasant impression.Moreover, the quick-fried pearl of the disclosure can also effectively reduce the problems such as stagnant mouthfeel of the quick-fried pearl bring of existing grape and miscellaneous gas.
In a kind of embodiment of the quick-fried pearl of the disclosure, solvent is Glycerin, mixed triester with caprylic acid capric acid.
It is overweight in order to more effectively solve astringent taste in a kind of embodiment of the quick-fried pearl of the disclosure, to oral cavity when suction
It is stimulated the problems such as excessive with nasal cavity, the content of the grape pastil in quick-fried pearl is 15-25 μ L/.
It is overweight in order to more effectively solve astringent taste in a kind of embodiment of the quick-fried pearl of the disclosure, to oral cavity when suction
The problems such as excessive with nasal cavity stimulation, the outer diameter of quick-fried pearl is 3.3mm-3.6mm.
The disclosure additionally provides a kind of cigarette.
This includes the quick-fried pearl of the disclosure.When it is implemented, a quick-fried pearl can be added in the filter stick of cigarette, the position of quick-fried pearl away from
At 12.5mm from the free end of filter stick, to provide preferably suction experience.
Experimental method used in following embodiments is conventional method unless otherwise specified, used material and
Reagent is commercially available unless otherwise specified, and equipment used in experiment is this field unless otherwise specified
Equipment known to technical staff.
Embodiment 1
By weight, by 1.087 parts of methyl anthranilate, 0.617 part of ethylmaltol, 0.493 part of apple ester,
0.269 part of 3- methyl butanol, 0.202 part of ethyl 2-methylbutyrate, 0.103 part of 1- (1- ethoxy ethoxy) pentane, acetic acid second
0.097 part of ester, 0.085 part of ethyl hexanoate, 2- methyl-1-0.074 part of propyl alcohol, 0.088 part of benzyl carbinol, 2-Methyl Butyric Acid-3- first
0.06 part of base butyl ester, 0.059 part of ethyl propionate, 0.068 part of ethyl benzoate, 0.05 part of acetic acid -3- methylbutyl butenoate, 2- methyl fourth
0.046 part of alcohol, 0.041 part of 1- (1- ethoxy ethoxy) butane, 0.049 part of acetal, 0.044 part of acetic acid, ligustrazine 0.028
Part, 0.026 part of alpha, beta-lonone, 0.026 part of n-butyl alcohol, 0.016 part of β-furtural, 0.021 part of neoisomenthol, leaf-alcohol
0.014 part, 0.014 part of nerolidol, 0.013 part of butyl acetate, 0.016 part of ethyl palmitate, 0.013 part of melonal, α-gold
0.009 part of silk tree alkene, 0.011 part of ethyl valerate, 0.01 part of Z-3- methylbutanoic acid -3- hexene ester, 0.009 part of ethyl butyrate, 2-
0.006 part of methylbutanoic acid -2- methylbutyl butenoate, 0.005 part of 2- methyl-2-pentenal serving, 0.005 part of isoamyl hexanoate, beta-myrcene
0.004 part, 3- methyl-1-0.003 part of isopropyl cyclopentene, 0.002 part of australene, 0.002 part of 3- isopropyl phenylpiperidines, caproic acid
0.002 part, 0.009 part of 3- carene, 0.464 part of anethole, 0.214 part of d-limonen, 0.133 part of damascenone, vanillic aldehyde
0.064 part, 0.005 part of isomenthone, 0.003 part of ethyl acetoacetate, 0.049 part of menthol, dihydroactinidiolide 0.074
Part, cis- -0.048 part of limonene oxide and 0.008 part of Ethyl vanillin are stirred under conditions of 25 DEG C with the revolving speed of 60r/min
30min to get arrive quick-fried pearl grape essence S1.
Quick-fried pearl after 4858:95142 is mixed in mass ratio, is obtained into grape perfume with grape essence S1 and Glycerin, mixed triester with caprylic acid capric acid
Agent.Then the quick-fried pearl D1 of grape is made in grape pastil.The content of grape pastil is 20 μ L/ in the quick-fried pearl D1 of grape, and outer diameter is
3.5mm.The quick-fried pearl D1 of grape is placed in cigarette filter rod again, obtains the quick-fried pearl cigarette L1 of grape after connecing cigarette sample.
Embodiment 2
By weight, by 1.162 parts of methyl anthranilate, 0.708 part of ethylmaltol, 0.542 part of apple ester,
0.251 part of 3- methyl butanol, 0.239 part of ethyl 2-methylbutyrate, 0.145 part of 1- (1- ethoxy ethoxy) pentane, acetic acid second
0.119 part of ester, 0.091 part of ethyl hexanoate, 2- methyl-1-0.092 part of propyl alcohol, 0.075 part of benzyl carbinol, 2-Methyl Butyric Acid-3- first
0.067 part of base butyl ester, 0.056 part of ethyl propionate, 0.052 part of ethyl benzoate, 0.062 part of acetic acid -3- methylbutyl butenoate, 2- methyl
0.055 part of butanol, 0.046 part of 1- (1- ethoxy ethoxy) butane, 0.047 part of acetal, 0.04 part of acetic acid, ligustrazine
0.026 part, 0.026 part of alpha, beta-lonone, 0.027 part of n-butyl alcohol, 0.023 part of β-furtural, 0.02 part of neoisomenthol, leaf
0.018 part of alcohol, 0.018 part of nerolidol, 0.015 part of butyl acetate, 0.011 part of ethyl palmitate, 0.011 part of melonal, α-
0.011 part of farnesene, 0.008 part of ethyl valerate, 0.009 part of Z-3- methylbutanoic acid -3- hexene ester, 0.009 part of ethyl butyrate,
0.005 part of 2-Methyl Butyric Acid -2- methylbutyl butenoate, 0.004 part of 2- methyl-2-pentenal serving, 0.005 part of isoamyl hexanoate, β-laurel
0.003 part of alkene, 3- methyl-1-0.003 part of isopropyl cyclopentene, 0.002 part of australene, 0.002 part of 3- isopropyl phenylpiperidines, caproic acid
0.002 part, 0.007 part of 3- carene, 0.481 part of anethole, 0.238 part of d-limonen, 0.138 part of damascenone, vanillic aldehyde
0.055 part, 0.006 part of isomenthone, 0.003 part of ethyl acetoacetate, 0.057 part of menthol, dihydroactinidiolide 0.053
Part, cis- -0.044 part of limonene oxide and 0.009 part of Ethyl vanillin are stirred under conditions of 25 DEG C with the revolving speed of 60r/min
30min to get arrive quick-fried pearl grape essence S2.
Quick-fried pearl after 5198:94802 is mixed in mass ratio, is obtained into grape perfume with grape essence S2 and Glycerin, mixed triester with caprylic acid capric acid
Agent.Then the quick-fried pearl D2 of grape is made in grape pastil.The content of grape pastil is 20 μ L/ in the quick-fried pearl D2 of grape, and outer diameter is
3.5mm.The quick-fried pearl D2 of grape is placed in cigarette filter rod again, obtains the quick-fried pearl cigarette L2 of grape after connecing cigarette sample.
Embodiment 3
By weight, by 0.824 part of methyl anthranilate, 0.747 part of ethylmaltol, 0.562 part of apple ester,
0.243 part of 3- methyl butanol, 0.199 part of ethyl 2-methylbutyrate, 0.125 part of 1- (1- ethoxy ethoxy) pentane, acetic acid second
0.089 part of ester, 0.089 part of ethyl hexanoate, 2- methyl-1-0.068 part of propyl alcohol, 0.076 part of benzyl carbinol, 2-Methyl Butyric Acid-3- first
0.08 part of base butyl ester, 0.054 part of ethyl propionate, 0.061 part of ethyl benzoate, 0.051 part of acetic acid -3- methylbutyl butenoate, 2- methyl
0.045 part of butanol, 0.045 part of 1- (1- ethoxy ethoxy) butane, 0.051 part of acetal, 0.042 part of acetic acid, ligustrazine
0.037 part, 0.022 part of alpha, beta-lonone, 0.024 part of n-butyl alcohol, 0.021 part of β-furtural, 0.02 part of neoisomenthol, leaf
0.017 part of alcohol, 0.013 part of nerolidol, 0.015 part of butyl acetate, 0.012 part of ethyl palmitate, 0.01 part of melonal, α-gold
0.011 part of silk tree alkene, 0.008 part of ethyl valerate, 0.011 part of Z-3- methylbutanoic acid -3- hexene ester, 0.009 part of ethyl butyrate, 2-
0.006 part of methylbutanoic acid -2- methylbutyl butenoate, 0.004 part of 2- methyl-2-pentenal serving, 0.005 part of isoamyl hexanoate, beta-myrcene
0.003 part, 3- methyl-1-0.003 part of isopropyl cyclopentene, 0.002 part of australene, 0.002 part of 3- isopropyl phenylpiperidines, caproic acid
0.002 part, 0.008 part of 3- carene, 0.501 part of anethole, 0.254 part of d-limonen, 0.139 part of damascenone, vanillic aldehyde
0.063 part, 0.005 part of isomenthone, 0.003 part of ethyl acetoacetate, 0.055 part of menthol, dihydroactinidiolide 0.064
Part, cis- -0.048 part of limonene oxide and 0.007 part of Ethyl vanillin are stirred under conditions of 25 DEG C with the revolving speed of 60r/min
30min to get arrive quick-fried pearl grape essence S3.
Quick-fried pearl after 4855:95145 is mixed in mass ratio, is obtained into grape perfume with grape essence S3 and Glycerin, mixed triester with caprylic acid capric acid
Agent.Then the quick-fried pearl D3 of grape is made in grape pastil.The content of grape pastil is 30 μ L/ in the quick-fried pearl D3 of grape, and outer diameter is
3.5mm.The quick-fried pearl D3 of grape is placed in cigarette filter rod again, obtains the quick-fried pearl cigarette L3 of grape after connecing cigarette sample.
Embodiment 4
By weight, by 0.931 part of methyl anthranilate, 0.77 part of ethylmaltol, 0.551 part of apple ester,
0.276 part of 3- methyl butanol, 0.244 part of ethyl 2-methylbutyrate, 0.104 part of 1- (1- ethoxy ethoxy) pentane, acetic acid second
0.108 part of ester, 0.094 part of ethyl hexanoate, 2- methyl-1-0.084 part of propyl alcohol, 0.072 part of benzyl carbinol, 2-Methyl Butyric Acid-3- first
0.074 part of base butyl ester, 0.06 part of ethyl propionate, 0.05 part of ethyl benzoate, 0.052 part of acetic acid -3- methylbutyl butenoate, 2- methyl fourth
0.059 part of alcohol, 0.048 part of 1- (1- ethoxy ethoxy) butane, 0.059 part of acetal, 0.035 part of acetic acid, ligustrazine 0.025
Part, 0.028 part of alpha, beta-lonone, 0.021 part of n-butyl alcohol, 0.022 part of β-furtural, 0.018 part of neoisomenthol, leaf-alcohol
0.018 part, 0.016 part of nerolidol, 0.014 part of butyl acetate, 0.014 part of ethyl palmitate, 0.012 part of melonal, α-gold
0.008 part of silk tree alkene, 0.008 part of ethyl valerate, 0.01 part of Z-3- methylbutanoic acid -3- hexene ester, 0.009 part of ethyl butyrate, 2-
0.006 part of methylbutanoic acid -2- methylbutyl butenoate, 0.005 part of 2- methyl-2-pentenal serving, 0.004 part of isoamyl hexanoate, beta-myrcene
0.004 part, 3- methyl-1-0.003 part of isopropyl cyclopentene, 0.002 part of australene, 0.002 part of 3- isopropyl phenylpiperidines, caproic acid
0.002 part, 0.008 part of 3- carene, 0.391 part of anethole, 0.274 part of d-limonen, 0.114 part of damascenone, vanillic aldehyde
0.062 part, 0.005 part of isomenthone, 0.003 part of ethyl acetoacetate, 0.063 part of menthol, dihydroactinidiolide 0.057
Part, cis- -0.049 part of limonene oxide and 0.007 part of Ethyl vanillin are stirred under conditions of 25 DEG C with the revolving speed of 60r/min
30min to get arrive quick-fried pearl grape essence S4.
Quick-fried pearl after 4955:95045 is mixed in mass ratio, is obtained into grape perfume with grape essence S4 and Glycerin, mixed triester with caprylic acid capric acid
Agent.Then the quick-fried pearl D4 of grape is made in grape pastil.The content of grape pastil is 40 μ L/ in the quick-fried pearl D4 of grape, and outer diameter is
4.5mm.The quick-fried pearl D4 of grape is placed in cigarette filter rod again, obtains the quick-fried pearl cigarette L4 of grape after connecing cigarette sample.
Pearl cigarette L1-L4 quick-fried to grape, be placed in the quick-fried pearl of blank blank cigarette sample (the quick-fried pearl of blank refers to not comprising essence
Quick-fried pearl) and be placed in the quick-fried pearl of existing grape cigarette sample carry out suction evaluation, be as a result detailed in following table.
By the above smoking result it can be seen that being placed in the quick-fried pearl cigarette of existing grape compared with blank cigarette, items refer to
Mark is whole to become better, but miscellaneous gas and irritation increase problem occurs.The quick-fried pearl cigarette L1-L4 mass of the grape of the disclosure is stablized, not only
The problems such as having well solved irritation existing for the quick-fried pearl cigarette of existing grape and miscellaneous gas, and keep cigarette flavor matter further
It is promoted, perfume quantity further increases, and the sweet sense of flue gas and saturating hair property further increase, and flue gas is finer and smoother, and pleasant impression is more comfortable.
Grape similarity degree, significance degree and smoker's fancy grade also have very high promotion simultaneously, have important practical value.
Although some specific embodiments of the invention are described in detail by example, the skill of this field
Art personnel it should be understood that example above merely to being illustrated, the range being not intended to be limiting of the invention.The skill of this field
Art personnel are it should be understood that can without departing from the scope and spirit of the present invention modify to above embodiments.This hair
Bright range is defined by the following claims.
Claims (10)
1. a kind of quick-fried pearl grape essence, which is characterized in that by weight include 0.800-1.200 parts of ortho-aminobenzoic acid first
Ester, 0.600-0.800 part ethylmaltol, 0.400-0.600 parts of apple esters, 0.200-0.300 parts of 3- methyl butanols, 0.150-
0.250 part of ethyl 2-methylbutyrate, 0.100-0.150 parts of 1- (1- ethoxy ethoxy) pentanes, 0.050-0.150 parts of acetic acid second
Ester, 0.050-0.100 part ethyl hexanoate, 0.050-0.100 parts of 2- methyl-1-propyl alcohol, 0.050-0.100 parts of benzyl carbinols,
0.050-0.100 parts of 2-Methyl Butyric Acid -3- methylbutyl butenoates, 0.050-0.100 parts of ethyl propionates, 0.050-0.080 parts of benzoic acid
Ethyl ester, 0.050-0.080 parts of acetic acid -3- methylbutyl butenoates, 0.040-0.080 parts of 2- methyl butanols, 0.040-0.060 parts of 1- (1-
Ethoxy ethoxy) butane, 0.040-0.060 parts of acetals, 0.030-0.050 parts of acetic acid, 0.020-0.040 parts of ligustrazines,
0.020-0.040 parts of alpha, beta-lonones, 0.020-0.040 parts of n-butyl alcohols, 0.010-0.030 parts of β-furturals, 0.010-
0.030 part of neoisomenthol, 0.010-0.020 parts of leaf-alcohols, 0.010-0.020 parts of nerolidols, 0.010-0.020 parts of acetic acid fourths
Ester, 0.010-0.020 part ethyl palmitate, 0.010-0.020 parts of melonals, 0.005-0.015 parts of α-farnesenes, 0.005-
0.015 part of ethyl valerate, 0.005-0.015 parts of Z-3- methylbutanoic acid -3- hexene esters, 0.005-0.015 parts of ethyl butyrates,
0.005-0.010 parts of 2-Methyl Butyric Acid -2- methylbutyl butenoates, 0.003-0.006 parts of 2- methyl-2-pentenal servings, 0.003-0.006 parts
Isoamyl hexanoate, 0.003-0.006 part beta-myrcene, 0.002-0.005 parts of 3- methyl-1-isopropyl cyclopentenes, 0.001-
0.003 part of australene, 0.001-0.003 parts of 3- isopropyl phenylpiperidines, 0.001-0.003 parts of caproic acids, 0.005-0.010 parts of 3- caranes
Alkene, 0.350-0.550 part anethole, 0.200-0.300 parts of d-limonens, 0.100-0.200 parts of damascenones, 0.050-
It is 0.100 part of vanillic aldehyde, 0.005-0.010 parts of isomenthones, 0.002-0.005 parts of ethyl acetoacetates, 0.040-0.070 parts thin
Lotus brain, 0.050-0.100 part dihydroactinidiolide, 0.040-0.070 parts of cis--limonene oxides and 0.005-0.010 parts
Ethyl vanillin.
2. quick-fried pearl grape essence according to claim 1, which is characterized in that the methyl anthranilate, ethyl
Maltol, apple ester, 3- methyl butanol, ethyl 2-methylbutyrate, 1- (1- ethoxy ethoxy) pentane, ethyl acetate, caproic acid
Ethyl ester, 2- methyl-1-propyl alcohol, benzyl carbinol, 2-Methyl Butyric Acid-3- methylbutyl butenoate, ethyl propionate, ethyl benzoate, acetic acid-3- first
Base butyl ester, 2- methyl butanol, 1- (1- ethoxy ethoxy) butane, acetal, acetic acid, ligustrazine, alpha, beta-lonone, 1- fourth
Alcohol, β-furtural, neoisomenthol, leaf-alcohol, nerolidol, butyl acetate, ethyl palmitate, melonal, α-farnesene,
Ethyl valerate, Z-3- methylbutanoic acid -3- hexene ester, ethyl butyrate, 2-Methyl Butyric Acid -2- methylbutyl butenoate, 2- methyl -2- amylene
Aldehyde, isoamyl hexanoate, beta-myrcene, 3- methyl-1-isopropyl cyclopentene, australene, 3- isopropyl phenylpiperidines, caproic acid, 3- carene,
Anethole, d-limonen, damascenone, vanillic aldehyde, isomenthone, ethyl acetoacetate, menthol, dihydroactinidiolide,
The mass ratio of cis--limonene oxide and Ethyl vanillin is (0.800-1.200): (0.600-0.800): (0.400-
0.600):(0.200-0.300):(0.150-0.250):(0.100-0.150):(0.050-0.150):(0.050-0.100):
(0.050-0.100):(0.050-0.100):(0.050-0.100):(0.050-0.100):(0.050-0.080):(0.050-
0.080):(0.040-0.080):(0.040-0.060):(0.040-0.060):(0.030-0.050):(0.020-0.040):
(0.020-0.040):(0.020-0.040):(0.010-0.030):(0.010-0.030):(0.010-0.020):(0.010-
0.020):(0.010-0.020):(0.010-0.020):(0.010-0.020):(0.005-0.015):(0.005-0.015):
(0.005-0.015):(0.005-0.015):(0.005-0.010):(0.003-0.006):(0.003-0.006):(0.003-
0.006):(0.002-0.005):(0.001-0.003):(0.001-0.003):(0.001-0.003):(0.005-0.010):
(0.350-0.550):(0.200-0.300):(0.100-0.200):(0.050-0.100):(0.005-0.010):(0.002-
0.005):(0.040-0.070):(0.050-0.100):(0.040-0.070):(0.005-0.010)。
3. quick-fried pearl grape essence according to claim 1 or 2, which is characterized in that the quick-fried pearl is not wrapped with grape essence
Include ethyl caprilate, ethyl caprate, 1- (1- ethoxy ethoxy) propane, 4- ethyl -2- metoxyphenol, octanoic acid, acetic acid -2- first
Base butyl ester, octanoic acid -3- methylbutyl butenoate, 1,3- dioxane, 1,1- diethoxy -3- methybutane, pentadecanoic acid -3- methyl fourth
Ester, 4- methyl -2- amyl -1,3- dioxane, 2- hydroxyl -4-methoxybenzaldehyde, sad isobutyl ester, 2- tert-butyl -3- first
Hexadecyl ethylene oxide, acetic acid -2- [2- [2- [2- (2- Butoxyethoxy) ethyoxyl] ethyoxyl] ethyoxyl] ethyl ester, ethylidene ring
Butane, 2- acetaminobenzoic acid phenethyl ester and cyclohexene.
4. the preparation method of quick-fried pearl grape essence described in a kind of any one of claims 1 to 3, which is characterized in that including
The step of each raw material is stirred into 20min-40min under conditions of 15 DEG C -35 DEG C with the revolving speed of 50r/min-70r/min.
5. the preparation method according to claim 4, which is characterized in that including by each raw material under conditions of 25 DEG C with 60r/
The revolving speed of min stirs the step of 30min.
6. a kind of quick-fried pearl, which is characterized in that including shell and grape pastil, the grape pastil includes solvent and claim 1
To quick-fried pearl grape essence described in any one of 3, the mass ratio of the solvent and the quick-fried pearl grape essence is (93833-
96184):(3816-6167)。
7. quick-fried pearl according to claim 6, which is characterized in that the solvent is Glycerin, mixed triester with caprylic acid capric acid.
8. quick-fried pearl according to claim 6, which is characterized in that the content of the grape pastil in the quick-fried pearl is 15-25 μ L/
Grain.
9. quick-fried pearl according to claim 6, which is characterized in that the outer diameter of the quick-fried pearl is 3.3mm-3.6mm.
10. a kind of cigarette, which is characterized in that including quick-fried pearl described in any one of claim 6 to 9.
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| CN201910615645.9A CN110467968A (en) | 2019-07-09 | 2019-07-09 | A kind of quick-fried pearl grape essence and preparation method thereof, quick-fried pearl and cigarette |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112574819A (en) * | 2020-11-18 | 2021-03-30 | 云南中烟工业有限责任公司 | Kyoho grape essence and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107034017A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl savory essence of dried orange peel and its application in cigarette |
| CN107164093A (en) * | 2017-07-05 | 2017-09-15 | 湖北民族学院 | A kind of compound method of grape flavor flavouring essence for tobacco |
-
2019
- 2019-07-09 CN CN201910615645.9A patent/CN110467968A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107034017A (en) * | 2017-04-27 | 2017-08-11 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl savory essence of dried orange peel and its application in cigarette |
| CN107164093A (en) * | 2017-07-05 | 2017-09-15 | 湖北民族学院 | A kind of compound method of grape flavor flavouring essence for tobacco |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112574819A (en) * | 2020-11-18 | 2021-03-30 | 云南中烟工业有限责任公司 | Kyoho grape essence and preparation method and application thereof |
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Inventor after: Xi Gaolei Inventor after: Chu Wenjuan Inventor after: Cui Ting Inventor after: Gu Liang Inventor after: Wang Hongwei Inventor after: Xu Kejing Inventor after: Du Jia Inventor after: Yang Jinchu Inventor after: Chen Zhifei Inventor after: Cai Lili Inventor after: Wang Pengfei Inventor before: Xi Gaolei Inventor before: Chu Wenjuan Inventor before: Cui Yan Inventor before: Gu Liang Inventor before: Wang Hongwei Inventor before: Xu Kejing Inventor before: Du Jia Inventor before: Yang Jinchu Inventor before: Chen Zhifei Inventor before: Cai Lili Inventor before: Wang Pengfei |
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Application publication date: 20191119 |
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| RJ01 | Rejection of invention patent application after publication |