CN110432291A - A kind of peracetic acid disinfectant and its preparation process that corrosivity is low - Google Patents
A kind of peracetic acid disinfectant and its preparation process that corrosivity is low Download PDFInfo
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- CN110432291A CN110432291A CN201910781023.3A CN201910781023A CN110432291A CN 110432291 A CN110432291 A CN 110432291A CN 201910781023 A CN201910781023 A CN 201910781023A CN 110432291 A CN110432291 A CN 110432291A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
Abstract
The invention discloses a kind of peracetic acid disinfectants and its preparation process that corrosivity is low to be made of by mass percentage component A 78%-85% and B component 15%-22%；Wherein, the raw material composition of component A: Peracetic acid, emulsifier, citric acid, dibutyl phthalate, deionized water；The raw material of B component forms: folium artemisiae argyi, kuh-seng, Artemisia capillaris, big maple leaf, tea polyphenols；The present invention is made based on traditional disinfection formula of liquid, and using modern advanced medical pharmaceutical technology, substantially improves the unstable labile problem of traditional Peracetic acid, while effectively reducing Peracetic acid itself corrosivity；It is strong with sterilizing ability, work fast, the good remarkable advantage of stability, and thimerosal of the present invention uses simplicity, it is directly diluted with water and can carry out disinfection to body surface, use cost is low, and inventive formulation design is reasonable, Disinfection Effect is good, can promote and apply in the fields such as medical treatment, agricultural, aquatic products, public health.
Description
Technical field
The invention belongs to thimerosal technical field, it is related to a kind of peracetic acid disinfectant that corrosivity is low and its preparation work
Skill.
Background technique
The principle active component of peracetic acid disinfectant is Peracetic acid, which has very strong sterilizing ability, energy
Bacterial propagule, mycobacteria, bacterial spore, fungi, algae and virus are killed, bacteriotoxin can also be destroyed, answered extensively
Disinfection and sterilizing for general body surface, food processing equipment etc..
Currently, common peracetic acid disinfectant on the market often comes with some shortcomings a little: 1. performances are not sufficiently stable, and are easily divided
Solution；2. the metals such as pair copper steel, brass, aluminium have stronger corrosiveness, the use of peracetic acid disinfectant is limited.For this purpose,
It is necessary to prepare a kind of peracetic acid disinfectant, to solve the above technical problems.
Summary of the invention
In view of the deficiencies of the prior art, the object of the present invention is to provide a kind of peracetic acid disinfectant that corrosivity is low and its
Preparation process substantially improves the unstable labile problem of traditional Peracetic acid, while effectively reducing Peracetic acid certainly
Body corrosivity；The present invention also provides its preparation process, rationally, simple process is easy to industrialized production for design.
To achieve the goals above, the present invention adopts the following technical scheme:
The low peracetic acid disinfectant of corrosivity is by mass percentage by component A 78%-85% and B component
15%-22% composition；Wherein, component A is made of the raw material of following mass percent: Peracetic acid 7.5%-9.0%, emulsifier
2.5%-5.3%, citric acid 2.0%-3.0%, dibutyl phthalate 1.2%-1.5%, deionized water surplus；B component
Be made of the raw material of following parts by weight: 10 parts -15 parts of folium artemisiae argyi, 2 parts -4 parts of kuh-seng, 5 parts -8 parts of Artemisia capillaris, 1 part -4 parts of big maple leaf,
2 parts -3 parts of tea polyphenols.
The low peracetic acid disinfectant of corrosivity is by mass percentage by component A 78%-80% and B component
20%-22% composition.
It is the emulsifier polyglycerol aliphatic ester, petroleum sodium sulfonate, one or two kinds of in neopelex.
The preparation process of the low peracetic acid disinfectant of corrosivity, specifically includes the following contents:
(1) preparation of component A: each raw material is weighed by constitutive material mass percent, deionized water is first poured into reaction kettle
In, then Peracetic acid, emulsifier, are mixed, and mixing speed is 60-80 revs/min, and whipping temp is 30 DEG C -35 DEG C,
Mixing time be 10-15 minute, stirring after the completion of again thereto be added citric acid, dibutyl phthalate and carry out mix stir
It mixes, mixing speed is 70-80 revs/min, and whipping temp is 35 DEG C -40 DEG C, and mixing time is 10-15 minutes, obtains group after the completion
Divide A；
(2) preparation of component B: weighing each raw material by constitutive material parts by weight, first by folium artemisiae argyi, kuh-seng, Artemisia capillaris, big maple leaf
Decontamination is cleaned, and is placed in container, after the 8-10 times of deionized water measured immersion being added 4-6 hours, is boiled 3-4 hours, is extracted；Again
Distilled water is measured in secondary 5-7 times of addition, is boiled 2-3 hours, is extracted；Merge extracting solution twice, it is spare to obtain filtrate for filtering；Then to it
Middle addition tea polyphenols stir and evenly mix to obtain component B；
(3) said components A and component B are compounded according to mass percent, stirs and evenly mixs to obtain the low mistake of corrosivity
Fluoroacetic acid thimerosal.
Heating stirring mode uses heating water bath in the step (1).
The extract of described step (2) the component B obtains fine powder by spray drying, and the spray drying temperature is
105℃-110℃。
The low peracetic acid disinfectant of the corrosivity and water carry out mixing sprinkling according to 1:30-40 ratio.
Beneficial effects of the present invention:
Compared with prior art, the present invention is made based on traditional disinfection formula of liquid, and using modern advanced medicine
Medicine technology is made, and substantially improves the unstable labile problem of traditional Peracetic acid, while effectively reducing Peracetic acid
Itself corrosivity；It is strong with sterilizing ability, work fast, the good remarkable advantage of stability, and also the present invention disappears
Venom is using simplicity, and being directly diluted with water can carry out disinfection to body surface, and use cost is low, and inventive formulation design is closed
Reason, Disinfection Effect is good, can promote and apply in the fields such as medical treatment, agricultural, aquatic products, public health.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without creative efforts belongs to the model that the present invention protects
It encloses.
Embodiment 1: the low peracetic acid disinfectant of corrosivity is formed by 80 jin and 20 jin of B component of component A；Wherein, A group
Divide and be made of the raw material of following mass percent: Peracetic acid 8.0%, polyglyceryl fatty acid ester 4.0%, citric acid 2.5%, neighbour
Dibatyl phithalate 1.3%, deionized water surplus；B component is made of the raw material of following parts by weight: 10 parts of folium artemisiae argyi, kuh-seng 3
Part, 6 parts of Artemisia capillaris, 3 parts of big maple leaf, 2 parts of tea polyphenols.
The preparation process of the low peracetic acid disinfectant of corrosivity, specifically includes the following contents:
(1) preparation of component A: each raw material is weighed by constitutive material mass percent, deionized water is first poured into reaction kettle
In, then Peracetic acid, emulsifier, heating water bath are mixed, and mixing speed is 70 revs/min, and whipping temp is 30 DEG C,
Mixing time is 12 minutes, and citric acid, dibutyl phthalate is added after the completion of stirring thereto again and is mixed,
Mixing speed is 75 revs/min, and whipping temp is 35 DEG C, and mixing time is 15 minutes, obtains component A after the completion；
(2) preparation of component B: weighing each raw material by constitutive material parts by weight, first by folium artemisiae argyi, kuh-seng, Artemisia capillaris, big maple leaf
Decontamination is cleaned, and is placed in container, after being added deionized water immersion 5 hours of 10 times of amounts, is boiled 3 hours, is extracted；It is added again
5 times of amount distilled water, boil 2 hours, extract；Merge extracting solution twice, it is spare to obtain filtrate for filtering；Then it is more that tea is added thereto
Phenol stirs and evenly mixs to obtain component B, obtains fine powder through 110 DEG C of spray drying；
(3) said components A and component B are compounded according to mass percent, stirs and evenly mixs to obtain the low mistake of corrosivity
Fluoroacetic acid thimerosal.
Embodiment 2: the low peracetic acid disinfectant of corrosivity is formed by 78 jin and 22 jin of B component of component A；Wherein, A group
Divide and be made of the raw material of following mass percent: Peracetic acid 9.0%, polyglyceryl fatty acid ester 2.5%, petroleum sodium sulfonate
2.5%, citric acid 3.0%, dibutyl phthalate 1.5%, deionized water surplus；B component by following parts by weight raw material
Composition: 15 parts of folium artemisiae argyi, 2 parts of kuh-seng, 7 parts of Artemisia capillaris, 2 parts of big maple leaf, 3 parts of tea polyphenols.
The preparation process of the low peracetic acid disinfectant of corrosivity, specifically includes the following contents:
(1) preparation of component A: each raw material is weighed by constitutive material mass percent, deionized water is first poured into reaction kettle
In, then Peracetic acid, emulsifier, heating water bath are mixed, and mixing speed is 80 revs/min, and whipping temp is 35 DEG C,
Mixing time is 10 minutes, and citric acid, dibutyl phthalate is added after the completion of stirring thereto again and is mixed,
Mixing speed is 70 revs/min, and whipping temp is 40 DEG C, and mixing time is 15 minutes, obtains component A after the completion；
(2) preparation of component B: weighing each raw material by constitutive material parts by weight, first by folium artemisiae argyi, kuh-seng, Artemisia capillaris, big maple leaf
Decontamination is cleaned, and is placed in container, after being added deionized water immersion 5 hours of 10 times of amounts, is boiled 3-4 hours, is extracted；Again plus
Enter 6 times of amount distilled water, boil 2 hours, extracts；Merge extracting solution twice, it is spare to obtain filtrate for filtering；Then tea is added thereto
Polyphenol stirs and evenly mixs to obtain component B, obtains fine powder through 110 DEG C of spray drying；
(3) said components A and component B are compounded according to mass percent, stirs and evenly mixs to obtain the low mistake of corrosivity
Fluoroacetic acid thimerosal.
Embodiment 3: the low peracetic acid disinfectant of corrosivity is formed by 85 jin and 15 jin of B component of component A；Wherein, A group
Point be made of the raw material of following mass percent: Peracetic acid 8.5%, neopelex 3.0%, citric acid 2.5%,
Dibutyl phthalate 1.3%, deionized water surplus；B component is made of the raw material of following parts by weight: 12 parts of folium artemisiae argyi, kuh-seng 3
Part, 5 parts of Artemisia capillaris, 2 parts of big maple leaf, 2.5 parts of tea polyphenols.
The preparation process of the low peracetic acid disinfectant of corrosivity, specifically includes the following contents:
(1) preparation of component A: each raw material is weighed by constitutive material mass percent, deionized water is first poured into reaction kettle
In, then Peracetic acid, emulsifier, heating water bath are mixed, and mixing speed is 60 revs/min, and whipping temp is 30 DEG C,
Mixing time is 10 minutes, and citric acid, dibutyl phthalate is added after the completion of stirring thereto again and is mixed,
Mixing speed is 75 revs/min, and whipping temp is 35 DEG C, and mixing time is 15 minutes, obtains component A after the completion；
(2) preparation of component B: weighing each raw material by constitutive material parts by weight, first by folium artemisiae argyi, kuh-seng, Artemisia capillaris, big maple leaf
Decontamination is cleaned, and is placed in container, after being added deionized water immersion 4 hours of 10 times of amounts, is boiled 3 hours, is extracted；It is added again
6 times of amount distilled water, boil 2 hours, extract；Merge extracting solution twice, it is spare to obtain filtrate for filtering；Then it is more that tea is added thereto
Phenol stirs and evenly mixs to obtain component B, obtains fine powder through 110 DEG C of spray drying；
(3) said components A and component B are compounded according to mass percent, stirs and evenly mixs to obtain the low mistake of corrosivity
Fluoroacetic acid thimerosal.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (7)
1. a kind of peracetic acid disinfectant that corrosivity is low, which is characterized in that be by component A 78%- by mass percentage
85% and B component 15%-22% composition；Wherein, component A is made of the raw material of following mass percent: Peracetic acid 7.5%-
9.0%, emulsifier 2.5%-5.3%, citric acid 2.0%-3.0%, dibutyl phthalate 1.2%-1.5%, deionization
Water surplus；B component is made of the raw material of following parts by weight: 10 parts -15 parts of folium artemisiae argyi, 2 parts -4 parts of kuh-seng, 5 parts -8 parts of Artemisia capillaris, big
1 part -4 parts of maple leaf, 2 parts -3 parts of tea polyphenols.
2. the low peracetic acid disinfectant of corrosivity according to claim 1, it is characterised in that: by mass percentage,
It is made of component A 78%-80% and B component 20%-22%.
3. the low peracetic acid disinfectant of corrosivity according to claim 1, it is characterised in that: the emulsifier gathers sweet
It is oil and fat acid esters, petroleum sodium sulfonate, one or two kinds of in neopelex.
4. a kind of preparation process for the peracetic acid disinfectant that corrosivity as described in claim 1 is low, which is characterized in that specific
Including the following contents:
(1) preparation of component A: each raw material is weighed by constitutive material mass percent, is first poured into deionized water in reaction kettle, so
Peracetic acid, emulsifier afterwards, are mixed, and mixing speed is 60-80 revs/min, and whipping temp is 30 DEG C -35 DEG C, stirring
Time is 10-15 minutes, and citric acid, dibutyl phthalate is added after the completion of stirring thereto again and is mixed,
Mixing speed is 70-80 revs/min, and whipping temp is 35 DEG C -40 DEG C, and mixing time is 10-15 minutes, obtains component A after the completion；
(2) preparation of component B: weighing each raw material by constitutive material parts by weight, first by folium artemisiae argyi, kuh-seng, Artemisia capillaris, big maple leaf impurity elimination
Matter is cleaned, and is placed in container, after the 8-10 times of deionized water measured immersion being added 4-6 hours, is boiled 3-4 hours, is extracted；Again plus
Enter 5-7 times and measure distilled water, boil 2-3 hours, extracts；Merge extracting solution twice, it is spare to obtain filtrate for filtering；Then add thereto
Enter tea polyphenols, stirs and evenly mixs to obtain component B；
(3) said components A and component B are compounded according to mass percent, stirs and evenly mixs to obtain the low peroxide second of corrosivity
Cinic acid liquid.
5. the preparation process of the low peracetic acid disinfectant of corrosivity according to claim 4, which is characterized in that described
Heating stirring mode uses heating water bath in step (1).
6. the preparation process of the low peracetic acid disinfectant of corrosivity according to claim 4, which is characterized in that described
The extract of step (2) component B obtains fine powder by spray drying, and the spray drying temperature is 105 DEG C -110 DEG C.
7. the low peracetic acid disinfectant of corrosivity according to claim 1, which is characterized in that the corrosivity is low
Peracetic acid disinfectant and water carry out mixing sprinkling according to 1:30-40 ratio.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910781023.3A CN110432291A (en) | 2019-08-22 | 2019-08-22 | A kind of peracetic acid disinfectant and its preparation process that corrosivity is low |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910781023.3A CN110432291A (en) | 2019-08-22 | 2019-08-22 | A kind of peracetic acid disinfectant and its preparation process that corrosivity is low |
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| CN110432291A true CN110432291A (en) | 2019-11-12 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110917196A (en) * | 2020-02-05 | 2020-03-27 | 广州康健医学科技有限公司 | Chloroquine antibacterial disinfectant and application thereof |
| CN113615712A (en) * | 2021-09-01 | 2021-11-09 | 华能南京燃机发电有限公司 | Bactericide for power plant and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104430575A (en) * | 2014-09-01 | 2015-03-25 | 李晔 | Disinfectant for disinfecting wards and preparation method of disinfectant for disinfecting wards |
-
2019
- 2019-08-22 CN CN201910781023.3A patent/CN110432291A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104430575A (en) * | 2014-09-01 | 2015-03-25 | 李晔 | Disinfectant for disinfecting wards and preparation method of disinfectant for disinfecting wards |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110917196A (en) * | 2020-02-05 | 2020-03-27 | 广州康健医学科技有限公司 | Chloroquine antibacterial disinfectant and application thereof |
| CN110917196B (en) * | 2020-02-05 | 2020-06-05 | 广州康健医学科技有限公司 | Chloroquine antibacterial disinfectant and application thereof |
| CN113615712A (en) * | 2021-09-01 | 2021-11-09 | 华能南京燃机发电有限公司 | Bactericide for power plant and preparation method thereof |
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Application publication date: 20191112 |