CN110354190A - A kind of concocting method of fresh tuber of pinellia integration processing pinellia - Google Patents
A kind of concocting method of fresh tuber of pinellia integration processing pinellia Download PDFInfo
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- CN110354190A CN110354190A CN201910752672.0A CN201910752672A CN110354190A CN 110354190 A CN110354190 A CN 110354190A CN 201910752672 A CN201910752672 A CN 201910752672A CN 110354190 A CN110354190 A CN 110354190A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/888—Araceae (Arum family), e.g. caladium, calla lily or skunk cabbage
- A61K36/8888—Pinellia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/906—Zingiberaceae (Ginger family)
- A61K36/9068—Zingiber, e.g. garden ginger
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Abstract
The present invention relates to technical field of traditional Chinese medicines, provide a kind of concocting method of fresh tuber of pinellia integration processing pinellia, comprising the following steps: (1) mix ginger, alum and water and decoct, obtain the first decoction liquor and the first filter residue；(2) the first filter residue and water that the step (1) obtains are mixed and is decocted, obtain the second decoction liquor and the second filter residue；(3) the first decoction liquor that the step (1) obtains and the second decoction liquor that step (2) obtains are mixed, obtains mixed liquor；(4) it will remove the peel after the fresh tuber of pinellia is mixed with the mixed liquor of the step (3) and impregnated, filtered, the tuber of pinellia after being impregnated；(5) tuber of pinellia after impregnating the step (4) is steamed, is sliced, is dried, and pinellia is obtained.Using concocting method of the invention, the hazard residue of fresh tuber of pinellia preliminary working sulfur fumigation is avoided, the content of obtained pinellia extract is much higher than States Pharmacopoeia specifications, has more retained drug effective active matter.
Description
Technical field
The present invention relates to Chinese medicine preparation technical fields, and in particular to a kind of processing side of fresh tuber of pinellia integration processing pinellia
Method.
Background technique
The stem tuber of the Pinellia Tenore aroid tuber of pinellia is the important medicinal material of one of Chinese medicine treasure-house.The tuber of pinellia is plant figure
The poisonous plant that modal data library is included, toxicity are that complete stool is toxic, and stem tuber is more toxic, and are eaten raw during 0.1~1.8g can cause
Poison.Intense stimulus can be caused to oral cavity, larynx, gastrointestinal mucosal；Clothes can make dispute numb on a small quantity, volume then Burning Pain swelling,
Sounding, salivation, vomiting, total numbness, oligopnea are unable to without whole, spasm, expiratory dyspnea.
Pinellia is the processed product of the tuber of pinellia, has the function of middle benefit gas resolving sputum, stopping nausea and vomiting by lowering the adverse flow of QI, is used for phlematic vomiting, gastral cavilty ruffian
Full effect.Using the dry tuber of pinellia raw material of market tradition preliminary working, sulfur dioxide residual quantity when pinellia processes in the prior art
Harmful substance is more, and effective active matter reduces, and influences quality of medicinal material, and is not easy to produce and process into qualified pinellia finished product.
Summary of the invention
In view of this, the purpose of the present invention is to provide a kind of concocting methods of fresh tuber of pinellia integration processing pinellia.This
The concocting method for inventing the pinellia provided eliminates the dry link of sulphuring, avoids harmful substance sulfur dioxide in medicinal material
Residual, reduce the cost of production and processing, taken precautions against material quality risk, effectively retained the effective active of pinellia
Substance.
In order to achieve the above-mentioned object of the invention, the present invention the following technical schemes are provided:
The present invention provides a kind of concocting methods of fresh tuber of pinellia integration processing pinellia, comprising the following steps:
(1) ginger, alum and water are mixed and is decocted, obtain the first decoction liquor and the first filter residue；The ginger, alum
Mass ratio with water is 20~22:8~10:80~120；
(2) the first filter residue and water that the step (1) obtains are mixed and is decocted, obtain the second decoction liquor and the second filter
Slag；The dosage of the water is the 80%~120% of the quality of the first decoction liquor；
(3) the first decoction liquor that the step (1) obtains and the second decoction liquor that step (2) obtains are mixed, is mixed
Close liquid；
(4) it will remove the peel after the fresh tuber of pinellia is mixed with the mixed liquor of the step (3) and impregnated, filtered, after being impregnated
The tuber of pinellia；The mass ratio of the peeling tuber of pinellia and mixed liquor is 1:1.8~2.2；
(5) tuber of pinellia after impregnating the step (4) is steamed, is sliced, is dried, and pinellia is obtained.
Preferably, the time of the decoction is 1~2h.
Preferably, the diameter of the peeling tuber of pinellia is 1.2cm or more.
Preferably, the time impregnated in the step (4) is 5~6d.
Preferably, the mass ratio of the peeling tuber of pinellia and mixed liquor is 1:2.0 in the step (4).
Preferably, the pressure steamed in the step (5) is 0.1~0.2Mpa, and the temperature steamed is 100~120 DEG C.
Preferably, the time steamed is 5~6h.
Preferably, the pinellia after described steam is cut into the sheet with a thickness of 0.3~0.5cm.
Preferably, temperature dry in the step (5) is 60~70 DEG C, and the dry time is 6~7h.
It hands over the concocting method of pinellia the present invention provides a kind of fresh tuber of pinellia integration, method provided by the invention is saved
The step of sulfur smoking processing, residual of the harmful substance sulfur dioxide in medicinal material is avoided, production and processing cost is reduced, prevented
Model material quality risk, has effectively retained the effective active matter of pinellia.The present invention is more existing using the process steamed
There is the process cooked in technology to not only avoid the residual of harmful substance sulfur dioxide, reduce the loss of effective active matter,
And the production and processing time is shortened, save energy consumption.
Specific embodiment
The present invention provides a kind of concocting methods of fresh tuber of pinellia integration processing pinellia, comprising the following steps:
(1) ginger, alum and water are mixed and is decocted, obtain the first decoction liquor and the first filter residue；The ginger, alum
Mass ratio with water is 20~22:8~10:80~120；
(2) the first filter residue and water that the step (1) obtains are mixed and is decocted, obtain the second decoction liquor and the second filter
Slag；The dosage of the water is the 80%~120% of the quality of the first decoction liquor；
(3) the first decoction liquor that the step (1) obtains and the second decoction liquor that step (2) obtains are mixed, is mixed
Close liquid；
(4) it impregnated, filtered after the fresh hide tuber of pinellia being gone to mix with the mixed liquor of the step (3), after being impregnated
The tuber of pinellia；The fresh tuber of pinellia and the mass ratio of mixed liquor removed the peel is 1:1.8~2.2；
(5) tuber of pinellia after impregnating the step (4) is steamed, is sliced, is dried, and pinellia is obtained.
Ginger, alum and water are mixed and are decocted by the present invention, obtain the first decoction liquor and the first filter residue；The ginger,
The mass ratio of alum and water is 20~22:8~10:80~120.The dosage of ginger of the present invention is the 20% of fresh tuber of pinellia weight
~22%, preferably 21%；The dosage of the alum is the 8%~10% of fresh tuber of pinellia weight, preferably 9%；The use of the water
Amount is the 160%~240% of fresh tuber of pinellia weight, preferably 200%.The present invention is not particularly limited the mixed mode,
Using conventional mixing method.In the present invention, it is preferred to which ginger is cleaned, decocted again with alum and water after slice, institute
The diameter for stating ginger slice is preferably 0.2~0.4cm, more preferably 0.3cm.
In the present invention, the temperature of the decoction is preferably 90~110 DEG C, and more preferably 100 DEG C；The time of decoction is preferred
For 1~2h, more preferably 1.5h.
The first obtained filter residue and water are mixed and are decocted by the present invention, obtain the second decoction liquor and the second filter residue；
The dosage of the water is the 80%~120% of the first decoction liquor, preferably 100%.
The present invention mixes the first obtained decoction liquor and the second obtained decoction liquor, obtains mixed liquor.The present invention
The mixed method is not particularly limited, using the method routinely mixed.
The present invention is impregnated after mixing the fresh tuber of pinellia of peeling with mixed liquor, is filtered, the tuber of pinellia after being impregnated；Institute
Stating and removing the peel the mass ratio of the fresh tuber of pinellia and mixed liquor is 1:1.8~2.2, preferably 1:2.In the present invention, the fresh tuber of pinellia of peeling
Mass ratio with the first decoction liquor is preferably 1:1~1.2.In the present invention, the time of the immersion is preferably 5~6d.This hair
The bright method to the filtration is not particularly limited, using conventional filter method.
The fresh tuber of pinellia of peeling of the present invention preferably elutes fresh tuber of pinellia crust, obtains the fresh tuber of pinellia of peeling.This
Invention is not particularly limited the method for the elution, using the method for conventional fresh tuber of pinellia elution.
In the present invention, it is preferred to which the fresh tuber of pinellia size stepping of the obtained peeling is obtained diameter in 1.2cm or more
The fresh tuber of pinellia.The present invention is not particularly limited the method for the tuber of pinellia size stepping, using the method for conventional stepping.?
In the present invention, preferably by diameter in 1.2cm or more.
The tuber of pinellia after the immersion is steamed, be sliced, dried by the present invention, obtains pinellia.The present invention is to the steaming
The method of system is not particularly limited, it is preferred to use steam box is steamed.In the present invention, the pressure steamed is preferably 0.1
~0.2Mpa, the temperature steamed are preferably 100~120 DEG C, and the time steamed is preferably 5~6h.The present invention is to the drying
Method is not particularly limited, it is preferred to use oven drying.In the present invention, the temperature of the drying is preferably 60~70 DEG C, more
Preferably 65 DEG C；The time of the drying is preferably 6~7h.In the present invention, the thickness of the material being dried is preferred
It is preferably stirred per hour 1 time in the drying process for < 30cm.In the present invention, after the drying pinellia moisture content
Preferably < 13%.
Below in conjunction with the embodiment in the present invention, the technical solution in the present invention is clearly and completely described.It is aobvious
So, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1
The concocting method of pinellia:
(1) fresh tuber of pinellia 300kg crust is eluted, obtains the fresh tuber of pinellia of peeling；
(2) by the fresh tuber of pinellia size stepping of obtained peeling, diameter is obtained in the fresh tuber of pinellia of 1.2cm or more,
(3) ginger 60kg is cleaned, is cut into 0.3cm piece, alum 30kg and water 300kg mixing, 100 DEG C carry out first and decoct
1h obtains the first decoction liquor and the first filter residue；
(4) obtained the first filter residue and water are mixed and carries out the second decoction, obtain the second decoction liquor and the second filter residue；
(5) the first obtained decoction liquor and the second obtained decoction liquor are mixed, obtains mixed liquor；
(6) the fresh tuber of pinellia is mixed with mixed liquor and impregnates 5d, filtration, the tuber of pinellia after being impregnated；
(7) tuber of pinellia after immersion is steamed into normal pressure steamer 6h, the tuber of pinellia steamed is sliced in 60 DEG C of oven drying 6h,
Obtain pinellia.
It is detected using 2015 editions " Chinese Pharmacopoeia " first pinellia detection methods, alum limitation is 5.3%, total ash
It is divided into 2.3%, the content of extract is 30.40%, sulfur dioxide residual quantity 0ppm, utilizes concocting method big gun of the embodiment of the present invention
The pinellia of system meets the regulation of 2015 editions " Chinese Pharmacopoeia ".
Comparative example 1
It takes the commercially available net tuber of pinellia to be soaked in water to interior without the dry heart, takes out；The ginger of tuber of pinellia weight 25% is taken, cleaned, be sliced and decoct
Soup adds 12.5% alum of tuber of pinellia weight and the tuber of pinellia of the saturating heart of immersion well-done altogether, boils 5h；It takes out the tuber of pinellia to dry, obtains pinellia.It adopts
It is detected with detection method same as Example 1, alum limitation is 4.5%, total ash 2.6%, the content of extract
It is 20.20%, sulfur dioxide residual quantity 145ppm.
Embodiment 2
The concocting method of pinellia:
(1) fresh tuber of pinellia 500kg crust is eluted, obtains the fresh tuber of pinellia of peeling；
(2) by the fresh tuber of pinellia size stepping of obtained peeling, diameter is obtained in the fresh tuber of pinellia of 1.2cm or more；
(3) ginger 100kg is cleaned, is cut into 0.4cm piece, alum 50kg and water 500kg mixing, 100 DEG C carry out first and decoct
1h is boiled, the first decoction liquor and the first filter residue are obtained；
(4) obtained the first filter residue and water are mixed and carries out the second decoction, obtain the second decoction liquor and the second filter residue；It is described
The dosage of water is the 100% of the first decoction liquor；
(5) the first obtained decoction liquor and the second obtained decoction liquor are mixed, obtains mixed liquor；
(6) the fresh tuber of pinellia is mixed with mixed liquor and impregnates 5d, filtration, the tuber of pinellia after being impregnated；The tuber of pinellia and mixed liquor
Mass ratio be 1:2；
(7) tuber of pinellia after immersion is steamed into normal pressure steamer 6h, the tuber of pinellia steamed is cut into 0.3cm sheet in 60 DEG C
Oven drying 6h, obtains pinellia.
It is detected using 2015 editions " Chinese Pharmacopoeia " first pinellia detection methods, alum limitation is 4.9%, total ash
It is divided into 2.1%, the content of extract is 28.8%, sulfur dioxide residual quantity 0mpp, utilizes concocting method big gun of the embodiment of the present invention
The pinellia of system meets the regulation of 2015 editions " Chinese Pharmacopoeia ".
Embodiment 3
The concocting method of pinellia:
(1) fresh tuber of pinellia 1000kg crust is eluted, obtains the fresh tuber of pinellia of peeling；
(2) by the fresh tuber of pinellia size stepping of obtained peeling, diameter is obtained in the fresh tuber of pinellia of 1.2cm or more；
(3) ginger 100kg is cleaned, is cut into 0.3cm piece, alum 100kg and water 1000kg mixing, 100 DEG C carry out first
1h is decocted, the first decoction liquor and the first filter residue are obtained；
(4) obtained the first filter residue and water are mixed and carries out the second decoction, obtain the second decoction liquor and the second filter residue；It is described
The dosage of water is the 100% of the first decoction liquor；
(5) the first obtained decoction liquor and the second obtained decoction liquor are mixed, obtains mixed liquor；
(6) the fresh tuber of pinellia is mixed with mixed liquor and impregnates 5d, filtration, the tuber of pinellia after being impregnated；The tuber of pinellia and mixed liquor
Mass ratio be 1:2；
(7) tuber of pinellia after immersion is steamed into normal pressure steamer 6h, the sheet that the tuber of pinellia steamed cuts 0.3cm is dried in 60 DEG C
Case dries 6h, obtains pinellia.
It is detected using 2015 editions " Chinese Pharmacopoeia " first pinellia detection methods, alum limitation is 5.1%, total ash
It is divided into 2.2%, the content of extract is 29.2%, sulfur dioxide residual quantity 0PPm, utilizes concocting method big gun of the embodiment of the present invention
The pinellia of system meets the regulation of 2015 editions " Chinese Pharmacopoeia ".
By above embodiments and comparative example it is found that using concocting method of the invention, obtained pinellia effective active object
The content of matter extract increases about 1.5 times compared with comparative example, and without sulfur dioxide residue.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (9)
1. a kind of concocting method of fresh tuber of pinellia integration processing pinellia, which comprises the following steps:
(1) ginger, alum and water are mixed and is decocted, obtain the first decoction liquor and the first filter residue；The ginger, alum and water
Mass ratio be 20~22:8~10:80~120；
(2) the first filter residue and water that the step (1) obtains are mixed and is decocted, obtain the second decoction liquor and the second filter residue；
The dosage of the water is the 80%~120% of the quality of the first decoction liquor；
(3) the first decoction liquor that the step (1) obtains and the second decoction liquor that step (2) obtains are mixed, obtains mixed liquor；
(4) it will remove the peel after the fresh tuber of pinellia is mixed with the mixed liquor of the step (3) and impregnated, filtered, the tuber of pinellia after being impregnated；
The fresh tuber of pinellia and the mass ratio of mixed liquor removed the peel is 1:1.8~2.2；
(5) the fresh tuber of pinellia after impregnating the step (4) is steamed, is sliced, is dried, and pinellia is obtained.
2. concocting method according to claim 1, which is characterized in that the time of the decoction is 1~2h.
3. concocting method according to claim 1 or 2, which is characterized in that the diameter of the fresh tuber of pinellia of the peeling be 1.2cm with
On.
4. concocting method according to claim 1, which is characterized in that the time impregnated in the step (4) is 5~6d.
5. concocting method according to claim 1, which is characterized in that the fresh tuber of pinellia of peeling and mixed liquor in the step (4)
Mass ratio be 1:2.0.
6. concocting method according to claim 1, which is characterized in that the pressure steamed in the step (5) be 0.1~
0.2Mpa, the temperature steamed are 100~120 DEG C.
7. concocting method according to claim 1 or 6, which is characterized in that the time steamed is 5~6h.
8. concocting method according to claim 1, which is characterized in that by the pinellia after described steam be cut into a thickness of
The sheet of 0.3~0.5cm.
9. concocting method according to claim 1, which is characterized in that dry temperature is 60~70 in the step (5)
DEG C, the dry time is 6~7h.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910752672.0A CN110354190A (en) | 2019-08-15 | 2019-08-15 | A kind of concocting method of fresh tuber of pinellia integration processing pinellia |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910752672.0A CN110354190A (en) | 2019-08-15 | 2019-08-15 | A kind of concocting method of fresh tuber of pinellia integration processing pinellia |
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| CN110354190A true CN110354190A (en) | 2019-10-22 |
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| CN201910752672.0A Withdrawn CN110354190A (en) | 2019-08-15 | 2019-08-15 | A kind of concocting method of fresh tuber of pinellia integration processing pinellia |
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