CN110330842A - A kind of water dyeing mortar and preparation method thereof - Google Patents

A kind of water dyeing mortar and preparation method thereof Download PDF

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Publication number
CN110330842A
CN110330842A CN201910532784.5A CN201910532784A CN110330842A CN 110330842 A CN110330842 A CN 110330842A CN 201910532784 A CN201910532784 A CN 201910532784A CN 110330842 A CN110330842 A CN 110330842A
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CN
China
Prior art keywords
parts
water
stirring
mortar
dispersed
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CN201910532784.5A
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Chinese (zh)
Inventor
李蒙
陈明
张森
石峰
李生贵
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Zhengzhou Kuwaike Building Materials Co Ltd
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Zhengzhou Kuwaike Building Materials Co Ltd
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Priority to CN201910532784.5A priority Critical patent/CN110330842A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04Homopolymers or copolymers of esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses a kind of water dyeing mortars of technical field of paint preparation and preparation method thereof, component including following parts by weight: 60-80 parts of lotion, 0.2-0.5 parts of dispersion moisture agent, 5-10 parts of coalescing agent, 2-5 parts of other auxiliary agents, 1-1.5 parts of PH regulator, 1-1.5 parts of toner, 10-20 parts of deionized water, there is excellent color fastness, mechanical strength, the performances such as water-fast, resistance to boiling water, acid and alkali-resistance, solvent resistant, resistance to natural aging, artificial ageing resistance are prominent;Environmentally protective, Diamond Search does not generate three industrial wastes, is not limited, can arbitrarily be mixed colours by color, facilitates production, toning process simple, not high to equipment requirement, and low cost takes water as a solvent, raw material cost is low, and naturally dry does not consume energy;It can be used for building inside and outside wall coating, water-permeable brick, artificial stone, integrated board, artifacts production.

Description

A kind of water dyeing mortar and preparation method thereof
Technical field
The present invention relates to technical field of paint preparation, specially a kind of water dyeing mortar and preparation method thereof.
Background technique
Currently, external wall largely uses lacquer as ornament materials, the main raw material(s) of exterior wall true stone paint first is that Natural colour sand.And natural colour sand belongs to non-renewable mineral resources, under environment-protecting high-pressure situation in recent years, more and more mines are prohibited It only exploits, the color sand of part colours is caused often to run out of goods.There are two types of existing dye sand technologies: high temperature sintering and oiliness contaminate sand: high temperature Sand burning energy consumption is high, and product batches are unstable;Oiliness contaminates sand and largely uses oil-based solvent in process of production, generates a large amount of Energy-saving requirement is not achieved in VOCs, both the above method.
Based on this, the present invention devises a kind of water dyeing mortar and preparation method thereof, to solve mentioned above ask Topic.
Summary of the invention
The purpose of the present invention is to provide a kind of water dyeing mortars and preparation method thereof, to solve above-mentioned background technique The problem of middle proposition.
To achieve the above object, the invention provides the following technical scheme: a kind of water dyeing mortar, including following weight The component of number: 60-80 parts of lotion, 0.2-0.5 parts of dispersion moisture agent, 5-10 parts of coalescing agent, 2-5 parts of other auxiliary agents, PH tune Agent 1-1.5 parts, 1-1.5 parts of toner, 10-20 parts of deionized water of section.
Preferably, other described auxiliary agents include the component of following parts by weight: 0.6-2.5 parts of thickener, defoaming agent 1-1.5 Part, 0.3-0.4 parts of antifreeze, 0.1-0.4 parts of fungicide.
Preferably, the lotion uses pure-acrylic emulsion.
Preferably, the dispersion moisture agent is selected from Sodium Polyacrylate, tertiary sodium phosphate, silicate, alkyl phenol polyoxyethylene ether One or more of with sodium alklyarylsulfonate.
Preferably, the coalescing agent is selected from one or both of polyesterols, polyvinyl alcohol, sodium alginate and xanthan gum More than.
A kind of preparation method of water dyeing mortar, comprising the following steps:
S1: first by the deionized water in formula, dispersion moisture agent, thickener, defoaming agent, antifreeze and fungicide are in 2000- It is dispersed with stirring 5-30min under the conditions of 4000r/min and obtains mixed liquor, for use;
S2: coalescing agent is dispersed with stirring 5-20min under the conditions of 1000- 2500r/min, the step S1 is added thereto In mixed liquor, continue to be dispersed with stirring 5-20min under the conditions of 1000-2500r/ min, continuously add PH regulator stirring 5- 10min is ground to no particle, obtains aqueous slurry;
S3: 2-10 part aqueous slurry in selecting step S2 in parts by weight puts into lotion and mill base into the slurry of selection, It is dispersed with stirring 10-15min under the conditions of 500-600r/ min, obtains the water dyeing mortar of required color after mixing evenly.
Preferably, the device being dispersed with stirring in described step S1, S2, S3 uses high speed disperser.
Compared with prior art, the beneficial effects of the present invention are: (1) have excellent color fastness, mechanical strength, it is water-fast, The performances such as resistance to boiling water, acid and alkali-resistance, solvent resistant, resistance to natural aging, artificial ageing resistance are prominent;(2) environmentally protective, Diamond Search does not generate Three industrial wastes are not limited by color, can arbitrarily be mixed colours, facilitate production, toning process simple, not high to equipment requirement, low cost, It takes water as a solvent, at low cost, naturally dry does not consume energy;(3) it can be used for building inside and outside wall coating, water-permeable brick, artificial stone, one Body plate, artifacts production.
Specific embodiment
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on this Embodiment in invention, all other reality obtained by those of ordinary skill in the art without making creative efforts Example is applied, shall fall within the protection scope of the present invention.
Embodiment one
A kind of water dyeing mortar, the component including following parts by weight: 60 parts of lotion, 0.2 part of dispersion moisture agent, film forming helps 5 parts of agent, 0.6 part of thickener, 1 part of defoaming agent, 0.3 part of antifreeze, 0.1 part of fungicide, 1 part of PH regulator, 1 part of toner, go from 10 parts of sub- water.
A kind of preparation method of water dyeing mortar, comprising the following steps:
S1: first by the deionized water in formula, dispersion moisture agent, thickener, defoaming agent, antifreeze and fungicide are in 2000r/ It is dispersed with stirring 5min under the conditions of min and obtains mixed liquor, for use;
S2: being dispersed with stirring 5min for coalescing agent under the conditions of 1000r/min, and the mixing in the step S1 is added thereto Liquid continues to be dispersed with stirring 5min under the conditions of 1000r/ min, continuously adds PH regulator stirring 5min, is ground to no particle, Obtain aqueous slurry;
S3: 2 parts of aqueous slurries in selecting step S2 in parts by weight put into lotion and mill base into the slurry of selection, It is dispersed with stirring 10min under the conditions of 500r/ min, obtains water dyeing mortar after mixing evenly.
Embodiment two
A kind of water dyeing mortar, the component including following parts by weight: 65 parts of lotion, 0.3 part of dispersion moisture agent, film forming helps 6 parts of agent, 0.6 part of thickener, 1 part of defoaming agent, 0.3 part of antifreeze, 0.1 part of fungicide, 1 part of PH regulator, 1 part of toner, go from 13 parts of sub- water.
A kind of preparation method of water dyeing mortar, comprising the following steps:
S1: first by the deionized water in formula, dispersion moisture agent, thickener, defoaming agent, antifreeze and fungicide are in 2500r/ It is dispersed with stirring 10min under the conditions of min and obtains mixed liquor, for use;
S2: being dispersed with stirring 10min for coalescing agent under the conditions of 1500r/min, and the mixing in the step S1 is added thereto Liquid continues to be dispersed with stirring 10min under the conditions of 1500r/ min, continuously adds PH regulator stirring 5min, is ground to no particle, Obtain aqueous slurry;
S3: 4 parts of aqueous slurries in selecting step S2 in parts by weight put into lotion and mill base into the slurry of selection, It is dispersed with stirring 10min under the conditions of 500r/ min, obtains water dyeing mortar after mixing evenly.
Embodiment three
A kind of water dyeing mortar, the component including following parts by weight: 70 parts of lotion, 0.3 part of dispersion moisture agent, film forming helps It 8 parts of agent, 1.5 parts of thickener, 1.2 parts of defoaming agent, 0.3 part of antifreeze, 0.1 part of fungicide, 1 part of PH regulator, 1 part of toner, goes 15 parts of ionized water.
A kind of preparation method of water dyeing mortar, comprising the following steps:
S1: first by the deionized water in formula, dispersion moisture agent, thickener, defoaming agent, antifreeze and fungicide are in 3000r/ It is dispersed with stirring 15min under the conditions of min and obtains mixed liquor, for use;
S2: being dispersed with stirring 15min for coalescing agent under the conditions of 1800r/min, and the mixing in the step S1 is added thereto Liquid continues to be dispersed with stirring 15min under the conditions of 1800r/ min, continuously adds PH regulator stirring 7min, is ground to no particle, Obtain aqueous slurry;
S3: 6 parts of aqueous slurries in selecting step S2 in parts by weight put into lotion and mill base into the slurry of selection, It is dispersed with stirring 12min under the conditions of 550r/ min, obtains water dyeing mortar after mixing evenly.
Example IV
A kind of water dyeing mortar, the component including following parts by weight: 75 parts of lotion, 0.4 part of dispersion moisture agent, film forming helps 9 parts of agent, 2 parts of thickener, 1.3 parts of defoaming agent, 0.4 part of antifreeze, 0.4 part of fungicide, 1.5 parts of PH regulator, 1.5 parts of toner, 18 parts of deionized water.
S1: first the deionized water in formula, dispersion moisture agent, thickener, defoaming agent, antifreeze and fungicide are existed It is dispersed with stirring 25min under the conditions of 3500r/min and obtains mixed liquor, for use;
S2: being dispersed with stirring 15min for coalescing agent under the conditions of 2000r/min, and the mixing in the step S1 is added thereto Liquid continues to be dispersed with stirring 15min under the conditions of 2000r/ min, continuously adds PH regulator stirring 8min, is ground to no particle, Obtain aqueous slurry;
S3: 8 parts of aqueous slurries in selecting step S2 in parts by weight put into lotion and mill base into the slurry of selection, It is dispersed with stirring 14min under the conditions of 580r/ min, obtains water dyeing mortar after mixing evenly.
Embodiment five
A kind of water dyeing mortar, the component including following parts by weight: 80 parts of lotion, 0.5 part of dispersion moisture agent, film forming helps 10 parts of agent, 2.5 parts of thickener, 1.5 parts of defoaming agent, 0.4 part of antifreeze, 0.4 part of fungicide, 1.5 parts of PH regulator, toner 1.5 Part, 20 parts of deionized water.
S1: first the deionized water in formula, dispersion moisture agent, thickener, defoaming agent, antifreeze and fungicide are existed It is dispersed with stirring 30min under the conditions of 4000r/min and obtains mixed liquor, for use;
S2: being dispersed with stirring 20min for coalescing agent under the conditions of 2500r/min, and the mixing in the step S1 is added thereto Liquid continues to be dispersed with stirring 20min under the conditions of 2500r/ min, continuously adds PH regulator stirring 10min, is ground to nothing Grain, obtains aqueous slurry;
S3: 10 parts of aqueous slurries in selecting step S2 in parts by weight put into lotion and mill base into the slurry of selection, It is dispersed with stirring 15min under the conditions of 600r/ min, obtains water dyeing mortar after mixing evenly.
The water dyeing mortar prepared through embodiment one, embodiment two, embodiment three, example IV and embodiment five Material experiment is it is found that the properties of finished product prepared by preparation method of the invention are significantly excellent in common production in the prior art Product, and the preferred preparation method in the embodiment of the present invention three, obtained end properties are the most excellent.
In the description of this specification, the description of reference term " one embodiment ", " example ", " specific example " etc. means Particular features, structures, materials, or characteristics described in conjunction with this embodiment or example are contained at least one implementation of the invention In example or example.In the present specification, schematic expression of the above terms may not refer to the same embodiment or example. Moreover, particular features, structures, materials, or characteristics described can be in any one or more of the embodiments or examples to close Suitable mode combines.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification, It can make many modifications and variations.These embodiments are chosen and specifically described to this specification, is in order to better explain the present invention Principle and practical application, so that skilled artisan be enable to better understand and utilize the present invention.The present invention is only It is limited by claims and its full scope and equivalent.

Claims (7)

1. a kind of water dyeing mortar, which is characterized in that the component including following parts by weight: 60-80 parts of lotion, dispersion profit 0.2-0.5 parts of humectant, 5-10 parts of coalescing agent, 2-5 parts of other auxiliary agents, 1-1.5 parts of PH regulator, 1-1.5 parts of mill base, deionization 10-20 parts of water.
2. a kind of water dyeing mortar according to claim 1, it is characterised in that: other described auxiliary agents include following weight The component of amount number: 0.6-2.5 parts of thickener, 1-1.5 parts of defoaming agent, 0.3-0.4 parts of antifreeze, 0.1-0.4 parts of fungicide.
3. a kind of water dyeing mortar according to claim 1, it is characterised in that: the lotion uses pure-acrylic emulsion.
4. a kind of water dyeing mortar according to claim 1, it is characterised in that: the dispersion moisture agent is selected from poly- third One or more of olefin(e) acid sodium, tertiary sodium phosphate, silicate, alkyl phenol polyoxyethylene ether and sodium alklyarylsulfonate.
5. a kind of water dyeing mortar according to claim 1, it is characterised in that: the coalescing agent is selected from polyester One or more of alcohol, polyvinyl alcohol, sodium alginate and xanthan gum.
6. a kind of preparation method of water dyeing mortar, it is characterised in that: the following steps are included:
S1: first by the deionized water in formula, dispersion moisture agent, thickener, defoaming agent, antifreeze and fungicide are in 2000- It is dispersed with stirring 5-30min under the conditions of 4000r/min and obtains mixed liquor, for use;
S2: coalescing agent is dispersed with stirring 5-20min under the conditions of 1000- 2500r/min, the step S1 is added thereto In mixed liquor, continue to be dispersed with stirring 5-20min under the conditions of 1000-2500r/ min, continuously add PH regulator stirring 5- 10min is ground to no particle, obtains aqueous slurry;
S3: 2-10 part aqueous slurry in selecting step S2 in parts by weight puts into lotion and mill base into the slurry of selection, It is dispersed with stirring 10-15min under the conditions of 500-600r/ min, obtains the water dyeing mortar of required color after mixing evenly.
7. a kind of preparation method of water dyeing mortar according to claim 6, it is characterised in that: the step S1, The device being dispersed with stirring in S2, S3 uses high speed disperser.
CN201910532784.5A 2019-06-19 2019-06-19 A kind of water dyeing mortar and preparation method thereof Pending CN110330842A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113004757A (en) * 2021-04-06 2021-06-22 陈素平 Dyed sand slurry, artificial colored sand and preparation method
CN114350219A (en) * 2022-03-09 2022-04-15 富思特新材料科技发展股份有限公司 Water-based reflective heat-insulation dyed mortar material, preparation method and application thereof, and preparation method of dyed sand

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JPS5855356A (en) * 1981-09-28 1983-04-01 日本鋼管株式会社 Manufacture of colored polymer cement mortar
CN101074168A (en) * 2007-06-20 2007-11-21 深圳市明远氟涂料有限公司 Composition for adjusting concrete color
CN102234186A (en) * 2010-04-29 2011-11-09 陈轶 Natural color sand decorative mortar
CN108219562A (en) * 2018-02-06 2018-06-29 漳州三德利油漆涂料有限公司 Colorful environmental protection coating material of sunlight heat reflecting heat insulation water burnt-in sand and preparation method thereof

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Publication number Priority date Publication date Assignee Title
JPS5855356A (en) * 1981-09-28 1983-04-01 日本鋼管株式会社 Manufacture of colored polymer cement mortar
CN101074168A (en) * 2007-06-20 2007-11-21 深圳市明远氟涂料有限公司 Composition for adjusting concrete color
CN102234186A (en) * 2010-04-29 2011-11-09 陈轶 Natural color sand decorative mortar
CN108219562A (en) * 2018-02-06 2018-06-29 漳州三德利油漆涂料有限公司 Colorful environmental protection coating material of sunlight heat reflecting heat insulation water burnt-in sand and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113004757A (en) * 2021-04-06 2021-06-22 陈素平 Dyed sand slurry, artificial colored sand and preparation method
CN114350219A (en) * 2022-03-09 2022-04-15 富思特新材料科技发展股份有限公司 Water-based reflective heat-insulation dyed mortar material, preparation method and application thereof, and preparation method of dyed sand

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